This document discusses research into developing sensor-enabled geogrids (SEGs) coated with a carbon black-filled polymer for monitoring tensile strains in earthen structures. The research aims to determine how percentage strain relates to electrical resistance under isolated tensile testing and how axial stresses impact geocomposite performance. Prior research on carbon black-filled polymers is reviewed. The methodology involves tensile and direct shear testing of PVC/CB polymer and PVC/CB coated geogrid samples. This research could lead to a more cost-effective, accurate method of monitoring embankment and foundation performance without excavation.
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Sample Research Memorandum #2
This document discusses research into developing sensor-enabled geogrids (SEGs) coated with a carbon black-filled polymer for monitoring tensile strains in earthen structures. The research aims to determine how percentage strain relates to electrical resistance under isolated tensile testing and how axial stresses impact geocomposite performance. Prior research on carbon black-filled polymers is reviewed. The methodology involves tensile and direct shear testing of PVC/CB polymer and PVC/CB coated geogrid samples. This research could lead to a more cost-effective, accurate method of monitoring embankment and foundation performance without excavation.
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To: Alex Parry
From: Mary Smith, Kyle Smith, William Smith
Re: Tensoresistive Polymer Composites for Performance Monitoring of Earthen Structures Date: April 5, 2016 1. Summary Both academia and industry employ the use of geosynthetic and geosynthetic technology for slope stability and performance monitoring of earthen structures. Geogrids are geosynthetic materials placed between soil layers to maintain and increase soil stability. A new generation of geosynthetic material is being developed with the capability to self-measure tensile strains below ground surface. These sensor-enabled geogrids will be coated with a carbon black-infused polymer filled with electrically conducting particles, allowing the tensile strain of the geogrid to be measured in-situ. In this study, sensorenabled geogrid (SEG) materials will be coated with a carbon blackfilled polyvinyl chloride (PVC) polymer and the tensoresitive properties will be measured in order to predict field-level tensile strains of reinforced soil-based structures. In this study, purpose of analysis will be twofold: (1) determine the dependence of percentage strain on relative resistance in isolated tensoresistivity testing, and (2) investigate the influence of axial stresses on the performance of geocomposites. 2. Background 2.1. Importance of Health-Monitoring of Structures It is imperative in geotechnical engineering to understand the subsurface force structure and stratigraphy. This analysis will lead to correct bearing capacity for embankment or foundation construction, or will lead to the choice of a reinforcing structure, such as a geotextile. This will help prevent catastrophic failures such as landslides, slope failures, or dam and levee breaches (Basham, 2015). Traditionally, strain gauges and extensometers have been used to assess the stability of earthen structures. However, strain gauges and extensometers require complex and expensive data acquisition systems, are not accurate due to calibration factors measured in isolation, and protective assemblies inherent in the apparatus result in unknown local stiffening and interlocking effects with adjacent soil or aggregates, influencing the measurements (Hatami, 2009).
2.2. Carbon Black-Filled Polymers for Geosynthetics
Many different mixtures of carbon black-filled polymers have been used for strain monitoring of PVC composites subjected to tensile cyclic loading (Yazdani, 2015). Influence factors such as magnitude of strain, loading rate, and pre-straining on tensoresistivity performance of coating composite have been analyzed in order to quantify composite performance under cyclic loading. Carbon Black 1 (CB1) has been used in the past as a higher-structure with less deformation under loading (Basham, 2015). The use of Carbon Black 1 (CB1) was abandoned in favor of Carbon Black 2 (CB2) due to chemical composition and bonding behavior in polymer formulation, particularly to avoid branching of polymer chains. It was necessary to execute testing in a fine material in the absence of electrolytes (Basham, 2016). 3. Project Description 3.1. Benefits to Field Geotechnical and transportation engineers will be able to use this research to develop and mass-produce SEGs without the need of excavation. This material will also allow for a more cost-effective and accurate method of performance monitoring of earthen structures. 3.2. Methodology An evaluation of the influence of vertical and axial stresses on the resistivity of polyvinylchloride/carbon black (PVC/CB) coated sensor enabled geogrid (SEG) structures was conducted based on analysis of stresses as a function of deformation. Integrity of SEG samples will be determined through tensoresitivity testing and a twofold in-soil testing process: (1) PVC/CB polymer samples subjected to direct shear and (2) PVC/CB coated polyester reinforced samples subjected to combined tensoresistivity and direct shear testing. Samples will be prepared using a sonication probe as well as manual mixing to ensure optimal adherence of particles within the polymer. For in-soil shear testing, a fine, nonconductive material such as sawdust with fines less than 0.42 mm (passing the #40 sieve) will be used for in-soil shear testing in order to apply desired stresses as a simulation of geogrid performance on the laboratory scale. During in-soil testing, electrical resistivity will be simultaneously measured using (DC) high-resistance meter at voltage of 10mA. Experimentation was repeated until samples produced an in-air stress-strain response for strains greater than 10%. Finally, a predicable linear model with unique slope given as a function of applied normal stress will be determined from least-squares optimization of empirical laboratory data.
3.3. Difference from Prior Research
The use of CB2-filled SEGs will allow for a more accurate strain reading in-field. Since CB2 filling results in less molecular branching in the polymer, the coating of the geosynthetic grid will better transfer electric conductivity, allowing for more accuracy in tensoresistivity readings. References Basham, M., Hatami, K., Pfeiffer, T., McMullen, N., Sarfatis, C. (2015). Multiscale 3D Dispersion Characterization of Carbon Nanotube-filled Polymer Composites Using Microscopic Imaging and Data Mining. Carbon Nanotechnology. Vol. 32, Issue 5 (2015). pp. 1253-1260. DOI:10.1007/s10706014-9796-x. Basham, M., (2016). Tensoresisitive Polymer Composites for Performance Monitoring of Earthen Structures. Poster session presented at GeoEnvironmental Conference, Chicago, IL. Fathi A, Hatami K, Grady BP. Effect of Carbon Black Structure on LowStrain Conductivity of Polypropylene and Low-Density Polyethylene Composites. Polym Eng Sci 2012;52(3):54956. Hatami K, Grady BP, Ulmer MC. Sensor-enabled geosynthetics: use of conducting carbon networks as geosynthetic sensors. J Geotechn Geoenviron Eng 2009;135(7):86374. http://dx.doi.org/10.1061/ (ASCE)GT.1943- 5606.0000062. Yazdani, H., "Tensoresistive PVC Coating for Sensor-Enabled Geogrids", Ph.D., University of Oklahoma, 2015.
Interview with Dr. K. Hatami
Q: What is your area of expertise? A: I am a geotechnical engineer, and so I study slope stability and earthwork performance. I also delve into materials science, particularly concerning polymer composites. Q: What are unsolved problems in the your area of expertise? A: I am currently working with the NSF, ODOT, and the University of Oklahoma to develop sensor-enabled geogrids for performance monitoring. Q: What is the next step you will pursue with your research? A: I already have a patent on this research and development, and the research now is to get the polymer composites ready for mass production by industry. Q: What room for research and development exists with this project? A: It is quite extensive. Industry is very concerned with obtaining an inexpensive, less obtrusive method for strain monitoring of embankments and other earthen structures. Q: What work has already been completed on this topic? A: There was your project, I had a PhD student working on the materials science portion of polymerization, and Dr. Grady in the chemical engineering department has been working on this with me for the last 10 years. Q: Are there any grant or funding opportunities for this type of research? A: The NSF [National Science Foundation] funds a lot of this project. ODOT [Oklahoma Department of Transportation] also has shown interest, and industry which I cannot name at this point in time has provided extensive funding to SEGs.
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