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    SOP Soil Loss On Ignition

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    hui143
    This document outlines the loss on ignition (LOI) reference method for determining soil organic matter content. The method involves drying a soil sample, heating it to 550°C to burn off organic matter, and calculating the mass lost. Specifically, it (1) sieves and dries the soil, (2) heats empty crucibles as a reference, (3) weighs the dried soil and crucible, (4) ignites the soil at 550°C for 2-4 hours, (5) reweighs the crucible and ignited soil, and (6) calculates LOI as the percentage mass lost from ignition.

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    SOP Soil Loss On Ignition

    Uploaded by

    hui143
    306 views2 pages
    This document outlines the loss on ignition (LOI) reference method for determining soil organic matter content. The method involves drying a soil sample, heating it to 550°C to burn off organic matter, and calculating the mass lost. Specifically, it (1) sieves and dries the soil, (2) heats empty crucibles as a reference, (3) weighs the dried soil and crucible, (4) ignites the soil at 550°C for 2-4 hours, (5) reweighs the crucible and ignited soil, and (6) calculates LOI as the percentage mass lost from ignition.

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    SOP Soil Loss on Ignition

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    This document outlines the loss on ignition (LOI) reference method for determining soil organic matter content. The method involves drying a soil sample, heating it to 550°C to burn off organic matter, and calculating the mass lost. Specifically, it (1) sieves and dries the soil, (2) heats empty crucibles as a reference, (3) weighs the dried soil and crucible, (4) ignites the soil at 550°C for 2-4 hours, (5) reweighs the crucible and ignited soil, and (6) calculates LOI as the percentage mass lost from ignition.

    Copyright:

    Attribution Non-Commercial (BY-NC)
    Download as DOC, PDF, TXT or read online from Scribd
    Download as doc, pdf, or txt
    306 views2 pages

    SOP Soil Loss On Ignition

    Uploaded by

    hui143
    This document outlines the loss on ignition (LOI) reference method for determining soil organic matter content. The method involves drying a soil sample, heating it to 550°C to burn off organic matter, and calculating the mass lost. Specifically, it (1) sieves and dries the soil, (2) heats empty crucibles as a reference, (3) weighs the dried soil and crucible, (4) ignites the soil at 550°C for 2-4 hours, (5) reweighs the crucible and ignited soil, and (6) calculates LOI as the percentage mass lost from ignition.

    Copyright:

    Attribution Non-Commercial (BY-NC)
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    Soil and Water Conservation Laboratory Standard Operating Procedure

    Loss on Ignition (LOI) Reference Method: Wilke, Berndt-Michael,2005, Determination of Chemical and Physical Soil Properties, in Manual of Soil Analysis, Eds. Margensin, R. & F. Schinner, Springer, Germany, pp. 74 76. Purpose To determine the soil organic matter of the soil of interest. The loss on ignition method is based on based on ignition of a dried soil sample. The soil organic matter is calculated as the mass difference before and after ignition (550 25o C). Methods and Equipment 2-mm mesh sieve Drying oven, controlled at a fixed temperature of 105 5o C Muffle furnace, capable of maintaining a temperature of 550 25o C Analytical balance, accuracy 0.01g Porcelain crucibles or bowls Desiccator Gloves and thongs Protective eyewear Appropriate lab attire Procedure 1. Use field moist, sieved (< 5mm) soil or air-dried (< 2mm) soil. Prior to LOI prepare the soil sample by drying the soil to 105o C (refer to drying method as outlined in soil moisture content or bulk density). 2. Next heat crucibles/ bowls in the muffle furnace at 550 25o C for 20 minutes. Cool in the desiccator and weigh (mc) to 0.1g. 3. Weigh 5 20 g of soil and put in the crucibles (m1). Then place crucibles with soil in the cold muffle furnace. 4. Gradually heat the muffle furnace to 550 25o C for 2 -4 hours until a constant mass is reached. 5. Open muffle furnace door and cool to 100o C. 6. Remove crucibles and place in the desiccator and cool to room temperature (~ 1 hour). 7. Measure the mass of the crucible + ignited soil (m2) twice. The difference of the individual measurements from the mean should not exceed 5%. Calculation 1. Calculate the loss of mass after ignition at 550 o C (m; g): 2. Calculate the LOI which corresponds to the soil organic matter content:
    m = m1 m 2

    LOI (%) =

    m 100 md

    * Remember,

    md = m1 mc

    m: loss of mass of the soil after ignition at 550oC (g) mc: mass of crucible (g) m1: mass of the soil dried at 105o C (g) and crucible m2: mass of the soil ignited to 550o C (g) and crucible md: mass of the soil dried at 105o C (g) Example Calculation mc = 3.11 g m1 = 19.36 g m2 = 16.77 g 1. m = 19.36g 16.77g = 2.59 g 2. md = 19.36g 3.11g = 16.25 g LOI = 16 .25 g 100 = 15.94 %
    2.59 g

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