Nabl 122 02 PDF

NABL 122-02
NATIONAL ACCREDITATION BOARD FOR

TESTING AND CALIBRATION
LABORATORIES
SPECIFIC CRITERIA
for CALIBRATION LABORATORIES
IN MECHANICAL DISCIPLINE :
MASS (Weights)
MASTER COPY
Reviewed by
Approved by
Quality Officer
Director, NABL
ISSUE No.
: 05
ISSUE DATE: 12.08.2014
AMENDMENT No.
: 00
AMENDMENT DATE:
AMENDMENT SHEET
Sl
no
Page
No.
Clause
No.
Date of
Amendment
Amendment
made
Reasons
Signature
QO
Signature
Director
10
National Accreditation Board for Testing and Calibration Laboratories

Doc. No: NABL 122-02
Issue No: 05
Specific Criteria for Calibration Laboratories in Mechanical Discipline Mass (Weights)

Issue Date: 12.08.2014
Amend No: 00
Amend Date: Page No: 1 of 22
Sl. No.
Contents
Page No.
1
1.1
General Requirements
Scope
1.2
Calibration Measurement Capability(CMC)
1.3
Personnel, Qualification and Training
3-4
1.4
Accommodation and Environmental Conditions
4-5
1.5
Special Requirements of Laboratory
1.6
Safety Precautions
1.7
Other Important Points
1.8
Proficiency Testing
5
5-6
Specific Requirements - Calibration of Weights
2.1
Scope
2.2
National/ International Standards, References and Guidelines
2.3
Metrological Requirements
7-8
2.4
Terms & Definitions
8-9
2.5
Selection of Reference Weights
2.6
Selection of Comparator/ Balance
2.7
Calibration Interval
10
2.8
Legal Aspects
11
2.9
Environmental Conditions
2.10
Calibration Methods
2.11
2.13
Determination of Air Density and its Uncertainty

Equations for Determination of Conventional Mass, True Mass
and their Uncertainties
Measurement Uncertainty
2.14
Reporting of Results
19
2.15
Evaluation of CMC
19-20
2.16
Sample Scope
20
2.17
Minimum Requirement for Accreditation
20
2.18
Maximum Permissible Error & Uncertainty Chart

Calibration of Newton Weights, Pressure Balance Weights and NonMetric Weights
Key Points
21
2.12
2.19
2.20
9
9-10
11-12
13
13-15
15-18
19
22
22

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1 General Requirement:
The purpose of this document is to specify requirements with which a laboratory has to operate and
demonstrate its competency to carry out calibration in accordance with ISO/IEC 17025:2005.
To achieve uniformity between the laboratories, assessors and assessment process in terms of
maximum permissible error, CMC, measurement uncertainty etc in line with National/International
standards.
To achieve uniformity in selection of equipments, calibration methods, maintaining required
environmental conditions, personnel with relevant qualification and experience.
1.1 Scope
This specific criteria lays down the specific requirements in calibration of weights under mechanical
discipline. This part of the document thus amplifies the specific requirements for calibration of weights
and supplements the requirements of ISO/IEC 17025:2005.
1.2 Calibration and Measurement Capability (CMC)
1.2.1
CMC is one of the parameters that is used by NABL to define the scope of an accredited
calibration laboratory, the others being parameter/quantity measured, standard/master used,
calibration method used and measurement range. The CMC is expressed as the smallest
uncertainty that a laboratory can achieve when calibrating the best existing device. It is an
expanded uncertainty estimated at a confidence level of approximately 95% corresponding to a
coverage factor k=2.
1.2.2
For evaluation of CMC laboratories should follow NABL 143 - Policy on Calibration and
Measurement Capability (CMC) and Uncertainty in Calibration.
1.3 Personnel, Qualification and Training

1.3.1 Technical Personnel:
1.3.1.1 Qualification required for carrying out calibration activity:
The following are the specific requirements. However, qualification and experience
will not be the only criteria for the required activity. They have to prove their skill,
knowledge and competency in their specific field of calibration activity.
1.3.1.2
a)
B.E / B.Tech or M.Sc. (having Physics as one of the subject) degree with 3
months experience in Basics of Mass Metrology.
b)
B.Sc (with Physics as one of the subject) or Diploma with 6 months experience in
Basics of Mass Metrology.
c)
ITI with 1 year of experience in Basics of Mass Metrology.
Training and experience required:

a)
Training may be external/ internal depending on the expertise available in the

field.
b)
Training in Mass Metrology and in Uncertainty Measurements, CMC including

statistical analysis for Technical Manager.

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1.3.2
c)
Experience and competence in Basics of Mass Metrology.
d)
Sufficient knowledge about handling of reference equipment, maintenance,

traceability, calibration procedure and effect of environmental conditions on the
results of calibration.
e)
During training calibration activity should be done under supervision.
Authorised Signatory:
1.3.2.1 Qualification required for interpretation of results and signing the calibration
certificates:
The following are only guidelines. However, qualification and experience will not be
the only criteria for the required activity. They have to prove their skill, knowledge
and competency in analysis and interpretation of calibration results.
1.3.2.2
a)
B.E / B.Tech or M.Sc. (with having Physics as one of the subject) degree with 6
months experience in Mass Metrology.
b)
B.Sc. (with Physics as one of the subject) or Diploma with 1 year experience in
Mass Metrology.
Training and experience required:

a)
Training may be external/ internal depending on the expertise available in the

field
b)
Training, Experience and Competence in Mass Metrology and Training in

Uncertainty Measurements, CMC including statistical analysis for Technical
Manager.
c)
Sufficient knowledge and competence in effective implementation of ISO/IEC

17025, specific criteria and NABL guidelines.
d)
Competency in reviewing of results, giving opinion and interpretations.
e)
During training the relevant activity has to be done under supervision
1.4 Accommodation and Environmental Conditions

Accommodation and environmental conditions adversely affect the results of calibration and
measurement accuracy unless they are controlled and monitored. Hence, they play a very important role.
The influencing parameters may be one or more of the following i. e. temperature, relative humidity,
atmospheric pressure, vibration, acoustic noise, dust, air currents/draft, illumination (wherever
applicable), voltage fluctuations, electrical earthing and direct sunlight etc., depending on the nature of
calibration services provided. The variables described above can play a major factor on calibration
results.
The laboratories are advised to follow the requirement of accommodation and environment depending
on the types of services provided as recommended
By the manufacturers of the reference equipment.
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By the manufacturers of the Unit under calibration.

As specified in the National/ International Standards or guidelines followed for the calibration.
The environmental monitoring equipments used should also meet the requirement of manufacturers
recommendations and specifications as per the relevant standards followed.
If, accommodation and environmental conditions are not specified either by manufacturer or by
National/International standards / guidelines, the laboratory shall follow the below recommendations.
1.4.1 Vibration
The calibration area shall be free from vibrations generated by central air-conditioning plants,
vehicular traffic and other sources to ensure consistent and uniform operational conditions. The
laboratory shall take all special/ protective precautions like mounting of sensitive apparatus on
vibration free tables and pillars etc., isolated from the floor, if necessary.
1.4.2 Acoustic Noise
Acoustic noise level in the laboratory shall be maintained to facilitate proper performance of
calibration work. Noise level shall be maintained less than 60 dBA, wherever it affects
adversely the required accuracy of measurement.
1.4.3 Illumination
The calibration area shall have adequate level of illumination. Where permissible, fluorescent
lighting is preferred to avoid localized heating and temperature drift. The recommended level
of illumination is 250-500 lux on the working table.
1.4.4
Environmental Conditions and Monitoring

The environmental conditions for the activity of the laboratory shall be such as not to adversely
affect the required accuracy of measurement. Facilities shall be provided whenever necessary
for recording temperature, pressure and humidity values prevailing during calibration. The
atmospheric conditions maintained in the laboratory during calibration shall be reported in the
calibration report/ certificate.
1.5 Special Requirements of Laboratory

1.5.1
The calibration laboratory shall make arrangements for regulated and uninterrupted power
supply of proper rating. The recommended voltage regulation level is 2% or better, and
Frequency variation 2.5Hz or better on the calibration bench.
1.5.2
The reference standards shall be maintained at temperatures specified for their maintenance on
order to ensure their conformance to the required level of operation.
1.5.3
The laboratory shall take adequate measures against dust and external air pressure.
1.6 Safety Precautions

1.6.1
Relevant fire extinguishing equipment for possible fire hazards, shall be available in the
corridors or convenient places in the laboratory. Adequate safety measures against electrical,
chemical fire hazards must be available at the work place. Laboratory rooms/ areas where

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Amend No: 00
highly inflammable materials are used/ stored shall be identified. Access to the relevant fire
equipment shall be assured near these rooms/ areas.
1.6.2
Specification SP 31- 1986, a special publication in the form of a wall chart, giving the method
of treatment in case of electric shock, should be followed. The chart shall be placed near the
power supply switchgear and at other prominent places as prescribed under Indian Electricity
Rules 1956.
1.6.3
Effective mains earthing shall be provided in accordance with relevant specification IS: 3043.
This shall be periodically checked to ensure proper contact with earth rod.
1.7 Other Important Points

1.7.1. Entry to the Calibration Area: As far as possible, only the staff engaged in the calibration
activity shall be permitted entry inside the calibration area.
1.7.2. Space in Calibration Area: The calibration Laboratory shall ensure adequate space for
calibration activity without adversely effecting the results.
1.8 Proficiency Testing
To give further assurance to the accuracy or Uncertainty of measurements, a laboratory will be required
to participate, from time to time, in Proficiency Testing Program. The laboratory shall remain prepared
to participate in the Proficiency Testing Program through inter-laboratory, inter-comparison schemes
wherever it is technically feasible. (Ref. NABL 162, 163 and 164 for further details)

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2. Specific Requirement Calibration of Weights

2.1 Scope: Calibration of Weights
Specific Requirements for calibration of weights with following details:
Sl.
No.
1
Description
Relevant
Standard
Permanent
facility
Onsite
calibration
Mobile
facility
Weights (E 1 , E 2 , F 1 ,
F 2, M 1, M 2, M 3 )
OIML-R 111-1
Note 1: Newton weights, non-metric weights can also be calibrated to accuracy class equivalent to
OIML R111 -1. However, the conventional mass values and its uncertainty should be given in
SI units.
Note 2: This technical requirement is based on the above mentioned guideline. Lab may
follow
any relevant standard, however care shall be taken to follow the
requirements in totality.
Note 3: ASTM standard weights can also be calibrated if the relevant standard is followed in total.
Note 4: Laboratory shall apply for calibration and not for verification of Weights. Verification may
require approval from Dept. of Legal Metrology, Regulatory Bodies, etc.
2.2 National/ International Standards, References and Guidelines
OIML R111-1-2004 Metrological and technical requirement of weights Classes E 1 , E 2 , F 1 , F 2 , M 1 ,
M2, M3.
OIML D28 2004: Conventional value of the result of weighing in air.
ASTM E617 - 13 Standard Specifications for Laboratory Weights and Precision Mass Standards.
OIML R 47 Edition 1079(E) - Standard weights for testing of high capacity weighing machines.
2.3 Metrological Requirements
2.3.1
For Each weight, the expanded uncertainty, U, for k=2, of the conventional mass, shall be less
than or equal to one third of the maximum permissible error.
2.3.2
For each weight, the conventional mass, m c (determined with an expanded uncertainty, U,
according to 5.2 of OIML R-111-1) shall not differ from the nominal value of the weights, m0
by more than the maximum permissible error, m minus the expanded uncertainty.
m 0 (m-U) m c m 0 + (m-U)
2.3.3
For class E 1 and E 2 weights, which are always accompanied by certificates giving the
appropriate data, the deviation from the nominal value, m c -m 0 , shall be taken into account by
the user.
2.3.4
Calibration certificate shall state, as a minimum: the conventional mass of each weight, mc an
indication of whether a weight has been adjusted prior to calibration, its expanded uncertainty
U and the values of the coverage factor k.

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2.3.5
The certificate for class E 1 weights shall state, as a minimum, the values of conventional mass,
m c , the expanded uncertainty, U, and the coverage factor k and density or volume for each
weight. In addition, the certificate shall state if the density or volume was measured or
estimated.
2.3.6
The certificate for class E 2 weights shall state, as a minimum, the value of conventional mass
m c, of each weight, the expanded uncertainty, U, and the coverage factor k.
2.3.7
Altitude and corresponding changes in air density can affect the measurement error when
using the conventional mass of weight; therefore, the buoyancy correction shall be used,
which requires the density of the weight to be known. If class E weights are to be used above
330 m, the density of the weights shall be provided along with their associated uncertainty for
Class F1 the same is true above 800 m. Otherwise, the manufacturer shall take the lowered
buoyancy affect at higher altitude in to consideration in specifying the weights class for the
standards of conventional mass.
2.4 Terms & Definitions

Accuracy Class
Class designation of a Weight or Weight set which meets certain metrological requirements intended
to maintain the mass values within the specified limit.
Buoyancy Correction
A buoyancy correction is the correction applied when Weights of different densities are compared
with each other during the calibration process, the buoyancy being a result of the upward force when
the weight is immersed in a fluid / air during the weighing process.
Conventional Mass (Conventional Value of the Mass)
Conventional value of the result of weighing in air, in accordance with OIML D-28 (conventional
value of the result of weighing in air) for a weight taken at a reference temperature of 20C, The
conventional mass of a body is the mass of a standard weight of density 8000 kg/m3 at 20C which
balances this body in air of density 1.2 kg/m3.
True Mass
The true mass of a body relates to the amount of material it contains. The prefix true is added to the
word mass where it is important to make it clear that a particular mass being considered is not a
conventional mass value and it is important to avoid potential ambiguity. The International prototype
kilogram, on which the International mass scale is realized, is defined as a true mass of exactly 1
kilogram. Most high accuracy comparisons are performed on a true mass basis, and converted to
conventional mass when quoted on a certificate.
The concept of true mass (mass in vacuum) might be appropriately described as a theoretical
comparison of a mass against a reference standard mass (with a known value) on a equal arm
balance inside a vacuum chamber. Although this scenario is impossible to achieve, one can easily
understand that such an arrangement, were it possible, would remove any influence on the weighing
process from the buoyant effect of air.
Discriminations / Sensitivity
Sensitivity is the smallest change in mass that can be detected by the weighing Instrument. For
practical purpose discrimination is synonymous with readability. Discrimination is also synonymous
with the sensitivity of an analog weighing Instrument.
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Readability
The smallest scale division or digital interval of the weighing Instrument. For same mechanical
weighing Instruments the scale marks may be sufficiently far apart for an estimation to be made of
the actual weighing instrument reading when the pointer lies between two scale marks. The
estimated readability may therefore be lower than the marked readability.
Resolution
The readability expressed as a portion of the capacity. For example a weighing Instrument with a
capacity of 3000g and a readability of 0.1g has a resolution of 1 part in 30000.
Scale Interval
The value expressed in units of Mass of in the case of analog indication, the difference between the
values that correspond to two scale marks. In the case of digital Indication, the difference between
two consecutively indicated values.
Weight
A material measure of mass, regulated in regard to its physical and metrological characteristics:
Shape, Mass, material, surface quality, nominal value and maximum permissible error.
2.5 Selection of Reference Weights
The reference weight shall generally be of a higher class of accuracy than the weight to be calibrated. In
the calibration of weights of class E 1 , the reference weight shall have similar or better metrological
characteristics (magnetic properties, surface roughness) than the weights to be calibrated [refer C.2.3 of
OIML R 111-1, 2004 for more details].
Class of Weights that can be Calibrated
Weight that can be
used as Reference
E1
E2
F1
F2
E1
E2
F1
F2
M1
M2
M3
Note: Standard weights of each class shall have the technical requirements such as shape,
construction, material, marking etc as per OIML R111. M1, M2, and M3 class weights are not
recommended to be used as a reference for the calibration of weights. However, M1 weights can
be used for above 20kg with coarser uncertainty.
2.6 Selection of Comparator/Balance
On the basis of the accuracy class, a mass comparator is to be selected in such a way that its uncertainty
component is balanced in proportion to the overall uncertainty of the weighing result. The most
important uncertainty component of a mass comparator is calculated from its standard deviation. The
specification of the manufacturer can be selected as a first approximation for the value of a standard
deviation. It must be taken into account. However, that this indication is decisive for the smallest
nominal value. It should therefore not exceed an amount of 30% of the combined standard uncertainty
u1 (k=2).

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Amend No: 00
2.6.1 Example:
Weight to be
Calibrated
Class
Permissible
Error as per
OIML R 111
Uncertainty required
(1/3 of the error)
with k=2
Standard Deviation of the

Comparator required =
1 mg
E2
0.006 mg
0.002 mg
(0.002)/3 mg
S 0.00067 mg
Note: It is not recommended to calibrate a higher accuracy class weight with a lower accuracy class of
reference weight and comparator/balance with coarser resolution without the consent of the
customer.
2.6.2
Selection of comparator balance for calibration of weights depending on class of accuracy:

Nominal Value
5000
2000
1000
500
200
100
50
20
10
5
2
1
500
200
100
50
20
10
5
2
1
500
200
100
50
20
10
5
2
1
kg
kg
kg
kg
kg
kg
kg
kg
kg
kg
kg
kg
g
g
g
g
g
g
g
g
g
mg
mg
mg
mg
mg
mg
mg
mg
mg
E1
2.78
1.11
0.56
0.28
0.11
0.056
0.028
0.011
0.006
0.0033
0.0028
0.0022
0.0018
0.0013
0.0011
0.0009
0.0007
0.0006
0.0004
0.0003
0.0003
0.0003
0.0003
0.0003
E2
F1
F2
M1
M2
Standard Deviation of Repeatability in mg
2778
8889
27778
88889
1111
3333
11111
33333
178
556
1778
5556
17778
89
278
889
2778
8889
33
111
333
1111
3333
17.8
56
178
556
1778
8.9
28
89
278
889
3.3
11
33
111
333
1.78
6
18
56
178
0.89
2.8
8.9
28
89
0.33
1.11
3.3
11.1
33
0.178
0.556
1.78
5.56
17.8
0.089
0.278
0.89
2.78
8.89
0.033
0.111
0.33
1.11
3.33
0.018
0.056
0.18
0.556
1.78
0.011
0.034
0.11
0.333
1.11
0.009
0.028
0.089
0.278
0.889
0.007
0.022
0.067
0.222
0.667
0.006
0.018
0.056
0.178
0.556
0.004
0.013
0.044
0.133
0.444
0.0034
0.011
0.033
0.111
0.333
0.0028
0.009
0.028
0.089
0.278
0.0022
0.007
0.022
0.067
0.222
0.0018
0.006
0.018
0.056
0.178
0.0013
0.004
0.013
0.044
0.0011
0.0034
0.011
0.034
0.0009
0.0028
0.009
0.028
0.0007
0.0022
0.006
0.022
0.0007
0.0022
0.006
0.022
0.0007
0.0022
0.006
0.022
M3
277778
111111
55556
27778
11111
5556
2778
1111
556
278
111
56
28
11.1
5.56
3.33
2.78
2.22
1.78
1.33
1.11
8.89
2.7 Calibration Interval

For the reference Weights and comparators used in calibration of Weights at permanent lab facility
Reference Equipment
Weights of E 1 and E 2 class
Weights of class F 1 to M 1
Comparator / Balance
Recommended Interval
3 years
2 years
1 year
Note: Based on the historical data validity of reference weights may be extended upto 5 years for E 1 .
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2.8 Legal Aspects

Calibration of weights done by any accredited laboratories is meant for scientific and industrial purpose
only. However, if used for commercial trading, additional recognition/ approval shall be complied as
required by Dept. of Legal metrology, Regulatory bodies, etc. This should be clearly mentioned in the
calibration certificate issued to the customer.
2.9 Environmental Conditions required for Calibration and Requirement of Environment
Monitoring System
2.9.1
2.9.2
Environmental Conditions
2.9.1.1
Laboratory is advised to follow Manufacturers recommendation for environmental

conditions, operation and maintenance of weights, weighing balance, comparator, etc.
2.9.1.2
Accuracy or reliability of weighing results is closely connected with the place where,
mass comparators are installed, and also with the weights used, with the measuring
room conditions and operator's skill. The place of installation (measuring room) for
mass comparators shall be designed in such a way that, the disturbances of the
environment do not affect the result. Manufacturers recommendation shall be
considered.
The calibration of weights shall be performed at suitable conditions under ambient atmospheric
pressure at temperatures closer to room temperature (1) Typical recommended values are given
below:
Weight
Class
E1
E2
F1
F2
M1
Temperature change during Calibration(2)
Range of Relative Humidity of the

Air(3)
0.3C per hour with a maximum of 0.5C per

12 hours
0.7C per hour with a maximum of 1C per 12
hours
1.5C per hour with a maximum of 2C per 12
hours
2C per hour with a maximum of 3.5C per 12
hours
3C per hour with a maximu m of 5C per 12
hours
40% to 60% with a maximum of

5% per 4 hours
10% per 4 hours
15% per 4 hours
Note (1): It is also important that the difference in temperature between the weights and the air
inside the mass comparator is as small as possible. Keeping the reference weight and
the test weight inside the mass comparator before and during the calibration to
reduce the temperature difference.
Note (2): This is the change in the temperature of the laboratory. Thermal stabilization of
balances and weights also requires an appropriate temperature stability of laboratory
for 24 hours before calibration.
Note (3): The upper limit is mainly important when storing the weight.For E1 and E2 class
weights, the temperature should be within
C 18
to 27C. The
environmental
conditions shall be within the specifications of the weighing instruments.
2.9.3
Recommended Environment Monitoring Equipments

Temperature with a resolution of 0.1C.

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Humidity with a resolution of 1% RH

Barometer with 1 mbar
However, laboratory shall evaluate the requirement of accuracy, resolution and uncertainty
depending on the CMC aimed at.
2.9.4
Thermal Stabilization Requirement for Test Weights

2.9.4.1 Thermal stabilization
Prior to performing any calibration, the weights need to be acclimated to the ambient
conditions of the laboratory. In particular, weights of classes E 1 , E 2 and F 1 shall be
close to the temperature in the weighing area.
The mandatory minimum times required for temperature stabilization (depending on
weight size, weight class and on the difference between the initial temperature of the
weights and the room temperature in the laboratory) are shown in Table below. As a
practical guideline, a waiting time of 24 hours is recommended.
2.9.4.2 Thermal stabilization in hours:
T*
20 C
5 C
2 C
0.5C
Nominal value
1 000, 2 000, 5 000 kg

100, 200, 500 kg
10, 20, 50 kg
1, 2, 5 kg
100, 200, 500 g
10, 20, 50 g
< 10 g
1 000, 2 000, 5 000 kg
100, 200, 500 kg
10, 20, 50 kg
1, 2, 5 kg
100, 200, 500g
10, 20, 50 g
< 10 g
1 000, 2 000, 5 000 kg
100, 200, 500 kg
10, 20, 50 kg
1, 2, 5 kg
100, 200, 500 g
< 100 g
1 000, 2 000, 5 000 kg
100, 200, 500 kg
10, 20, 50 kg
1, 2, 5 kg
100, 200, 500 g
< 100 g
Class E1
Class E2
Class F1
Class F2
45
18
8
2
70
27
12
5
2
79
33
12
6
3
1
5
4
3
2
1
1
40
18
8
4
1
1
2
4
3
2
1
1
1
1
1
0.5
0.5
1
1
1
1
1
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
1
36
15
6
2
0.5
0.5
27
12
5
2
11
7
3
1
16
10
5
3
1
1
1
1
0.5
0.5
0.5
1
0.5
T* = Initial difference between weight temperature and laboratory temperature.

Note: Thermal stabilization hours before calibration should be clearly mentioned in
the certificate issued to the customer.
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2.10 Calibration Methods

There are two methods for determination of conventional mass of weights in a weight set.
2.10.1 Direct Comparison Method
Minimum Number of Weighing Cycles (as per OIML R-111-1)
Class
E1
E2
F1
F2
M 1, M 2 , M 3
Min. number of ABBA

Min. number of ABA
Min. number of AB 1 ...B n A
3
5
5
2
3
3
1
2
2
1
1
1
1
1
1
2.10.2 Sub -Division/Sub-Multiplication Method (Ref. C.3.2 of OIML)

Reference Weights
Reference Weights
5
5
2+1
2+1
2+1*
2+1*
2
2
2*
2*
Vs
Vs
Vs
Vs
Vs
Vs
Vs
Vs
Vs
Vs
Vs
Vs
5+2+2*+1
5+2+2*+1*
2+2*+1
2+2*+1*
2*+1*
2+1
2*+1
2*+1
1+1*
1+1*
1+1*
1+1*
Note: Method used for calibration should be clearly mentioned in the calibration certificate
issued to the customer.
2.11 Determination of Air Density and its Uncertainty
2.11.1 In 2008 CIPM recommended that the following equation be used to determine a the density
of Air
a = [3.483740+1.4446*(x co2 0.0004)]*10-3 *p/ZT*(1-0.378*x v )
Where, a : Density of air in kg/m3
x CO2 : The mole fraction of carbon diaoxide (assumed 400 ppm, if not measured)
p : pressure
Z : compressibility
x v : mole fraction of water vapor
T : Thermodynamic temperature using ITS-90
2.11.1.1
Mole fraction of water vapor, x v

The mole fraction of water vapor, xv that is a function of the relative humidity, rh
or dew-point temperature tr, an enhancement factor, f and the moist air saturation
vapor pressure, psv is given as follows:
x v = rhf(p,t)* p sv (t)/p = f(p,t r ) * p sv (t r )/p
Where, rh : relative humidity in fraction

Issue No: 05

Amend No: 00
p : pressure in mbar
t : temperature in C
psv(t) : saturation vapor pressure of moist air
tr : dew-point temperature
2.11.1.2
The moist air saturation vapor pressure, psv can be calculated using the following
equation:
Where A, B, C, D are the vapor pressure constant parameters at saturation. The

recommended values are as given in Table 2.
2.11.1.3
Enhancement Factor, f
The enhancement factor can be calculated using the following equation:
f = + p + t2
Where , , are constants of enhancement factor. The recommended values are as
given in Table below.
2.11.1.4
The compressibility factor, Z

The compressibility factor, Z, can be calculated using the following equation:
Where a 0 , a 1 , a 2 , b 0 ,b 1 , c 0 , c 1 , d, e are the compressibility factor constants. The

recommended values are as given in Table below.
2.11.1.5
Constant
A
B
C
D
Table: Recommended Values for Constants of Psv (A, B, C, D), f (, , ) and

Z (a 0 , a 1 , a 2 , b 0 , b 1 , c 0 , c 1 , d, e)
Psv
f
Z
1991
1991
1991
Recommended Unit Constant Recommended Unit Constant Recommended Unit
value
value
value
1.2378847 10-5 K-2
1.00062
a0
1.58123 10-6 KPa-1
-1.9121316 10-2 K-1
3.14 10-8 Pa-1

a1
-2.9331 10-8 Pa-1
-7
-2
33.93711047
5.60 10
K
a2
1.1043 10-10 K-1Pa-1
-6.3431645 103 K
b0
5.707 10-6 KPa-1
b1
-2.051 10-8 Pa-1
c0
1.9898 10-4 KPa-1
c1
-2.376 10-6 Pa-1
d
1.83 10-11 K2Pa-2
e
-7.65 10-8 K2Pa-2
2.11.2 Approximation Formula as per OIML R-111-1: 2004 (Page No. 76)
a =
0.34848p -0.009*h*exp(0.061*t)
273.15+t
(E-3.1 OIML)

Issue No: 05

Amend No: 00
Where, Pressure (p) in mbar, temperature (t) in C and humidity (h) in % Equation(E-3.1) has
a relative uncertainty of 2 X 10-4 in the range 900hPa < p<1100hPa, 10 C<t<30 C and
rh< 80%.
2.11.3 For class E1 weights, the density of air should always be determined based o corresponding
measurements. However, the following approximation equation is a way to estimate air
density at laboratories that have no means of determining the air density at the site. The height
above sea level is always known. Therefore, if the air density is not measured, it should be
calculated as a mean value for the laboratory site as follows:
0 * exp
a =
- 0
P0
*gh
Where p 0 = 101325 Pa
0 = 1.2 kg/m3
g = 9.81 m/s 2
h = height above sea level expressed in meter.
2.11.4 The Standard Uncertainty of Air Density is given by:
[From OIMLR111-1:2004(E),page 68,equation C.6.3-3 ]
u2 a =
u2 F +( a /p*u P )2+ ( a /T*u T )2+( a /rh*u rh )2
Where,
uF =
a/p =
a/ =
a/rh =
up =
uT =
u rh =
2.12
10-4 a , uncertainty of the formula used to calculate air density

10-5 a * Pa -1
(-3.4*10-3* a * K -1)
(-10-2 a )
uncertainty of pressure in mbar
uncertainty of temperature in C
uncertainty of relative humidity %RH
Equations for Determination of Conventional Mass, True mass and their uncertainties
2.12.1 Determination of Conventional Mass with reference to volume of the reference and test
Weights
2.12.1.1
Equation for Determination of Conventional Mass

m ct =[m cr + (V t - V r )( a - 0 )+ m w ]
Where,
V t = Volume of the test weight
V r = Volume of the reference weight
m ct = Conventional mass of test weight
m cr = Conventional mass of reference weight
a = Density of Air during calibration in kg/m3
0 = Density of Air (Conventional) 1.2 kg/m3
m w = difference in mass observed using ABBA weighing cycle.
Note: Vt and Vr can be calculated from density and the nominal mass of the
weights.

Issue No: 05

Amend No: 00
2.12.1.2
Equation for Air Buoyancy Correction

From the equation of the Clause 8.12.1.1, the term air buoyancy correction (B.C.)
is:
B.C. = (Vt Vr).(a 0 )
2.12.1.3
Equation for Determining the Uncertainty due to Air Buoyancy Correction

u'b2 = (V t - V r )2*u a 2+ (uv t 2 + uv r 2)*( a 0 )2
Note: If, the volume is determined from known density and mass values and
their uncertainties, uncertainty of volume (uV t ) can be calculated by the
relation uV t = u t / V t for test weight and similarly for the reference
weight.
2.12.2 Determination of Conventional Mass with reference to Density of the Reference and
Test Weights
2.12.2.1
Equation for Determination of Conventional Mass

m ct = m cr (1+C)+m w
Where,
m ct =
m cr =
C=
m w =
2.12.2.2
Conventional mass of test weight

Conventional mass of reference weight
Buoyancy correction factor
Difference in weight by ABBA method
Buoyancy Correction Factor for Conventional Mass

C = [( a - 0 ) (1/ t )-(1/ r )]
Where,
r =
t =
a =
0 =
2.12.2.3
Density of Reference Weight in kg/m3

Density of Test Weight in kg/m3
Density of Air during Calibration in kg/m3
Density of Air (Conventional) 1.2 kg/m3
Uncertainty in Air Buoyancy Correction

Formula for calculation of uncertainty in air Buoyancy correction in
Conventional Mass calculation to be verified:
u' b 2 =
{(m cr *( r - t )/ r * t ))*u a )}2)+{(m cr *( a - 0 ))2*[(u2 t /4)}+m2 cr *( a - 0 )*[( a - 0 )-2( a1 0 )]*(u2 r / r 4)}
Where,
u' b =
m cr =
r =
t =
Uncertainty of air buoyancy correction of conventional mass

Conventional mass of reference weight in kg
Density of reference weight in kg/m3
Density of test weight in kg/m3

Issue No: 05

Amend No: 00
a =
a1 =
u r =
u t =
u a =
0 =
Density of Air during calibration in kg/m3

Density of Air during earlier calibration of reference wt in kg/m3
Uncertainty in Density of reference weight in kg/m3
Uncertainty in Density of test weight in kg/m3
Uncertainty in Density of air in kg/m3
Density of air (conventional) 1.2 kg/m3
- In case where air buoyancy correction is estimated to be negligible i.e. if

C i 1/3*U/m 0.
- Even if the air buoyancy correction is negligible the uncertainty contribution
of the buoyancy effect may not be negligible and shall be taken into account if
u b u c /3.
- For classes M 1 , M 2 and M 3 the uncertainty due to air buoyancy correction is
negligible and can usually be omitted.
- If the air density is not measured and the average air density for the site is
used, than the uncertainty for the air density is to be estimated as:
u(pa)= 0.12/3.
- A lower value of uncertainty may be used if supporting data can be provided.
- At sea level the density of air shall be assumed to be 1.2.kg per m3.
- For class E weights, the density of air should be determined. Its uncertainty is
usually estimated from the uncertainties for temperature, pressure, and air
humidity. For class E 1 , the CIPM formula or an approximation can be used for
the calculation of air density.
Note: Where the air density is 1.2 kg/m3 within 10%, conventional mass value
shall be used in calculation and true mass shall be calculated from
conventional mass (OIML R- 111 C.2.1.2).
2.12.3 True Mass with reference to Volume of the Reference and Test Weights
2.12.3.1
Equation for Determination of Mass

m tt = [m cr + (V t -V r )( a )+ m]
2.12.3.2
Equation for Determining the Uncertainty due to Air Buoyancy Correction

ub2 = (V t - V r )2*u a 2+ (uv t 2- uv r 2) * a 2
Note:
If, the volume is determined from known density and mass values and
their uncertainties, uncertainty of volume (uV t ) can be calculated by
the relation uV t = u t / V t for test weight and similarly for the
reference weight.
2.12.4 True Mass with reference to Density of the Reference and Test Weights
2.12.4.1
Equation for Determination of Mass

M tt = m tr (1+B)+m w

Issue No: 05

Amend No: 00
Where,
M tt =
m tr =
B=
mw =
2.12.4.2
True mass of test weight

True mass of reference weight
Buoyancy correction factor for true mass
Difference in weight by ABBA method
Buoyancy Correction Factor for Calibration of Mass on True Mass basis

B = [( a )*(1/ t )-(1/ r )]
Where,
r =
t =
a =
2.12.4.3

Density of air in kg/m3
Equation for Calculation of Uncertainty in Buoyancy Correction in True Mass

ub2 =
{(m r *( r - t )/ r * t ))*u a )}
(u2 r / r 4)]}
{(m r
* a )
*[(u2 t / t 4)-
Where,
ub=
mr =
r =
t =
a =
u r =
u t =
u a =
Uncertainty in buoyancy correction in true mass

Mass of reference weight in kg
Density of air in kg/m3
Uncertainty in density of reference weight in kg/m3
Uncertainty in density of test weight in kg/m3
Uncertainty in density of air in kg/m3
Note 1: As per the standard if the air density deviates from 1.2 kg/m3 by more
than 10%, true mass values shall be used for calculations and the
conventional mass shall be calculated from the true mass.
Note 2: True mass is required for the realization of force, pressure and torque
etc by using dead weights.
Note 3: Calibration of weights in terms of Newton, bar, pascal etc (local "g"
value shall be known to be sufficient accuracy).
2.12.4.4
Conversion from Conventional Mass to True Mass

mt =
mc x
1- 0 / c
1- 0 /
Where,
mt =
mc=
0 =
c =
True mass
Conventional mass
Density of conventional Air (1.2) in kg/m3
Conventional density of Mass (8000) in kg/m3
Density of mass in kg/m3

Issue No: 05

Amend No: 00
2.13 Measurement Uncertainty

2.13.1
Contribution of Uncertainty in Calibration of Weights:

The estimation of the uncertainty measurement for the weight calibrated by a laboratory shall
consider at least the following contributions.
(a)
(b)
(c)
(d)
(e)
Repeatability-standard deviation of weighing result

The contribution of the reference standard weight.
The air buoyancy correction
The uncorrected drift of the reference standard weight
The resolution of the balance
2.13.2 Uncertainty Equation for Calibration Results

Type A Standard uncertainty,
Type B Standard uncertainty,
u c = (u 1 2+ u 2 2+ u 3 2+ u 4 2+ u 5 2)
Where,
u 1 = standard uncertainty associated with standard deviation of weighing
u 2 = Standard uncertainty associated with air buoyancy correction
u 3 = standard uncertainty associated with drift of the reference standard weight
u 4 = standard uncertainty associated with resolution of the comparator/balance
u 5 = Standard uncertainty associated with reference standard weight
Expanded uncertainty U = k x u c
Note:
For k value, students t table is to be referred.
2.14 Reporting of Results

The calibration certificates issued to the customer shall be in accordance with clause 5.10 of
ISO/IEC/17025:2005. Apart from that it shall also include the following:
a.
Thermal stabilization hours taken (as per 2.9.4.2) before calibration.
b.
Specific calibration method followed (as per 2.10).
c.
Density of Reference weight (whether assumed or measured).
d.
Density of Test weight (whether assumed or measured).
e.
Declaration that, the calibration certificate issued for weights/Mass used for scientific or
industrial purposes only.
2.15 Evaluation of CMC

2.15.1
Refer NABL 143 for CMC evaluation.
2.15.2
CMC value is not the same as expanded uncertainty reported in the calibration
Certificate/Report. CMC values exclude the uncertainties which are attributed to the DUC
(Device under calibration).

Issue No: 05

Amend No: 00
2.15.3
For the purpose of CMC evaluation the following components should be considered:
Repeatability-standard deviation of weighing result (for minimum 10 readings).
Uncertainty of the reference standard weight.
Drift in reference standard weight.
Uncertainty due to air buoyancy correction.
Uncertainty due to resolution of Balance.
2.16 Sample Scope

2.16.1
An illustrative example for right representation of scope

Laboratory: XYZ
Date(s) of Visit:
Discipline: Mechanical
Master
Parameter*/
Range(s) of Calibration and Measurement Capability **
Equipment
S.
Device
Measurement
Used
Claimed by Observed by Recommended
No
under
Assessor
by Assessor
Laboratory
calibration
1.
Mass
Weights.
F1 Class
Standard
Weights
and Mass
Comparator
(Readability
: 0.001mg)
1 mg
2 mg
5 mg
10 mg
20 mg
50 mg
100 mg
0.02 mg
0.02 mg
0.02 mg
0.027 mg
0.033 mg
0.04 mg
0.053 mg
0.02 mg
0.02 mg
0.02 mg
0.027 mg
0.033 mg
0.04 mg
0.053 mg
0.02 mg
0.02 mg
0.02 mg
0.027 mg
0.033 mg
0.04 mg
0.053 mg
Remarks+/
Method used
Calibration of
weights of Class
F2 accuracy and
coarser as per
OIML R-111
* Only for Electro-technical discipline; scope shall be recommended parameter wise (where applicable) and the
ranges may be mentioned frequency wise.
** NABL 143 shall be referred for the recommendation of CMC
+
Remarks shall also include whether the same scope is applicable for site calibration as well. NABL 130 shall be
referred while recommending the scope for site calibration.
Signature, Date
& Name of Lab
Representative
Signature, Date & Name of Assessor(s)
Signature, Date & Name of Lead Assessor
Note: CMC value shall be reported in absolute value i.e. in mg only.

2.17 Minimum Requirement for Accreditation
2.17.1
Laboratory shall have minimum F2 class of reference Weights for the calibration below 20
kg along with appropriate comparator / balance. However, M1 class reference weights may
be used for calibration above 20 kg.
2.17.2
Demonstration of any CMC values doesn't automatically qualify for granting accreditation
until the lab satisfies the stipulated requirement given above.

Issue No: 05

Amend No: 00
2.18 Maximum Permissible Error & Uncertainty Chart

2.18.1
Permissible error for classification weights as per OIML R-111-1, 2004.

Note: For each weight expanded uncertainty U, for k=2 the conventional mass, shall be as per the standard less than or equal to onethird of the maximum permissible error (U = 1/3 m)
Class
Nominal
Value
5000 kg
2000 kg
1000 kg
500 kg
200 kg
100 kg
50
kg
20
kg
10
kg
5
kg
2
kg
1
kg
500 g
200 g
100 g
50
g
20
g
10
g
5
g
2
g
1
g
500 g
200 g
100 mg
50
mg
20
mg
10
mg
5
mg
2
mg
1
mg
Error
mg
25
10
5.0
2.5
1.0
0.5
0.25
0.10
0.05
0.03
0.025
0.020
0.016
0.012
0.010
0.008
0.006
0.005
0.004
0.003
0.003
0.003
0.003
0.003
E1
Uncertainty
8.3
3.3
1.7
0.8
0.3
0.2
0.08
0.03
0.02
0.01
0.01
0.01
0.01
0.004
0.003
0.003
0.002
0.002
0.001
0.001
0.001
0.001
0.001
0.001
Error
mg
1600
800
300
160
80
30
16
8
3
1.6
0.8
0.3
0.16
0.10
0.08
0.06
0.05
0.04
0.03
0.025
0.020
0.016
0.012
0.010
0.008
0.006
0.006
0.006
E2
Uncertainty
533
267
100
53
27
10
5
3
1.0
0.5
0.3
0.10
0.05
0.03
0.03
0.02
0.02
0.01
0.01
0.008
0.007
0.005
0.004
0.003
0.003
0.002
0.002
0.002
Error
mg
25000
10000
5000
2500
1000
500
250
100
50
25
10
5
2.5
1.0
0.5
0.3
0.25
0.20
0.16
0.12
0.10
0.08
0.06
0.05
0.04
0.03
0.025
0.020
0.020
0.020
F1
Uncertainty
8333
3333
1667
833
333
167
83
33
17
8
3
2
1
0.3
0.2
0.1
0.1
0.1
0.1
0.04
0.03
0.03
0.02
0.02
0.01
0.01
0.01
0.01
0.01
0.01
Error
mg
80000
30000
16000
8000
3000
1600
800
300
160
80
30
16
8.0
3.0
1.6
1.0
0.8
0.6
0.5
0.4
0.3
0.25
0.20
0.16
0.12
0.10
0.08
0.06
0.06
0.06
F2
Uncertainty
26667
10000
5333
2667
1000
533
267
100
53
27
10
5
3
1
0.5
0.3
0.3
0.2
0.2
0.1
0.1
0.1
0.1
0.1
0.04
0.03
0.03
0.02
0.02
0.02
M1
M2
Error Uncertainty Error Uncertainty
mg
mg
250000
83333
800000
266667
100000
33333
300000
100000
50000
16667
160000
53333
25000
8333
80000
26667
10000
3333
30000
10000
5000
1667
16000
5333
2500
833
8000
2667
1000
333
3000
1000
500
167
1600
533
250
83
800
267
100
33
300
100
50
17
160
53
25
8
80
27
10
3
30
10
5
2
16
5
3
1
10
3
2.5
1
8
3
2
1
6
2
1.6
1
5
2
1.2
0.4
4
1
1.0
0.3
3
1
0.8
0.3
2.5
1
0.6
0.2
2.0
1
0.5
0.2
1.6
1
0.4
0.1
0.3
0.1
0.25
0.1
0.20
0.1
0.20
0.1
0.20
0.1
M3
Error Uncertainty
mg
2500000 833333
1000000 333333
500000
166667
250000
83333
100000
33333
50000
16667
25000
8333
10000
3333
5000
1667
2500
833
1000
333
500
167
250
83
100
33
50
17
30
10
25
8
20
7
16
5
12
4
10
3

Issue No: 05

Amend No: 00
Amend Date: -
Page No: 21 of 22
2.19 Calibration of Newton Weights, Pressure Balance Weights and Non-metric Weights
2.19.1
Weights used for realization of Pressure in Dead weight pressure balance or weights used for
realization of force in Newton are to be calibrated on true mass basis.
2.19.2
If, weights are calibrated on conventional mass basis equation for conversion from
conventional mass to true mass to be mentioned to enable the user to apply appropriate
buoyancy correction.
2.19.3
Newton or Force weights are typically of a slotted design or with a centre hole and are
typically marked with a nominal Force in Newton. Force is calculated with respect to Local
gravity g L during calibration using the formula given below:
F= m (1- a / m )*g LC
[2.19.3a]
Where
F = Force in Newton
m = True Mass in Kg
a = air density in kg/m3
m = density of weights in kg/m3
g L = Local gravity in m/sec2 (value of g at the customers site )
The force values can be converted either to the standard g value or to the customers g
value using the formula given below:
To convert Force to standard g value:
F= m (1- a / m )* g S /g LC
Where,
[2.19.3b]
g S = Standard gravity in m/sec2 (9.80665 m/sec2)

g LC = Local gravity in m/sec2 (value of g at the site of calibration).
To convert Force to g value at customers site:

F= m (1- a / m )*g L /g LC
Where,
[2.19.3c]
g L = Local gravity in m/sec2 (value of g at the customers site)
This conversion can be done if; the customer provides g value at his site.
2.19.4
When the customer requires the force weight with respect to his local g value he has to
provide the same with uncertainty. Then the force value shall be calculated using the local
g value and declare in the certificate in terms mass value along with the calculated value in
Newton. g value of the calibration laboratory shall also be known to sufficient accuracy.
2.19.5
The Laboratory may calibrate weights of non-metric units (e.g. Pound or Ounce etc.)
However, the results shall be reported in SI units like kg, g, mg, etc. along with the
calculated equivalent value in the non-metric unit or mention the conversion factor to be
used.
2.20 Key Points:

Demonstration of any CMC values doesn't automatically qualify for granting accreditation until the
lab satisfies the stipulated requirement given in this document.
Issue No: 05

Issue Date: 12.08.2014 Amend No: 00

NABL House
Plot No. 45, Sector- 44,
Gurgaon 122002, Haryana
Tel.: +91-124 4679700
Fax: +91-124 4679799
Website: www.nabl-india.org

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NABL 122-02

NATIONAL ACCREDITATION BOARD FOR

ISSUE DATE: 12.08.2014

National Accreditation Board for Testing and Calibration Laboratories

Specific Criteria for Calibration Laboratories in Mechanical Discipline Mass (Weights)

Calibration Measurement Capability(CMC)

Personnel, Qualification and Training

Accommodation and Environmental Conditions

Special Requirements of Laboratory

Other Important Points

Specific Requirements - Calibration of Weights

National/ International Standards, References and Guidelines

Terms & Definitions

Selection of Reference Weights

Selection of Comparator/ Balance

Determination of Air Density and its Uncertainty

Minimum Requirement for Accreditation

Maximum Permissible Error & Uncertainty Chart

National Accreditation Board for Testing and Calibration Laboratories

Specific Criteria for Calibration Laboratories in Mechanical Discipline Mass (Weights)

1.3 Personnel, Qualification and Training

ITI with 1 year of experience in Basics of Mass Metrology.

Training and experience required:

Training may be external/ internal depending on the expertise available in the

Training in Mass Metrology and in Uncertainty Measurements, CMC including

National Accreditation Board for Testing and Calibration Laboratories

Specific Criteria for Calibration Laboratories in Mechanical Discipline Mass (Weights)

Experience and competence in Basics of Mass Metrology.

Sufficient knowledge about handling of reference equipment, maintenance,

During training calibration activity should be done under supervision.

Training and experience required:

Training may be external/ internal depending on the expertise available in the

Training, Experience and Competence in Mass Metrology and Training in

Sufficient knowledge and competence in effective implementation of ISO/IEC

Competency in reviewing of results, giving opinion and interpretations.

During training the relevant activity has to be done under supervision

1.4 Accommodation and Environmental Conditions

Specific Criteria for Calibration Laboratories in Mechanical Discipline Mass (Weights)

By the manufacturers of the Unit under calibration.

Environmental Conditions and Monitoring

1.5 Special Requirements of Laboratory

1.6 Safety Precautions

National Accreditation Board for Testing and Calibration Laboratories

Specific Criteria for Calibration Laboratories in Mechanical Discipline Mass (Weights)

1.7 Other Important Points

National Accreditation Board for Testing and Calibration Laboratories

Specific Criteria for Calibration Laboratories in Mechanical Discipline Mass (Weights)

2. Specific Requirement Calibration of Weights

National Accreditation Board for Testing and Calibration Laboratories

Specific Criteria for Calibration Laboratories in Mechanical Discipline Mass (Weights)

2.4 Terms & Definitions

Specific Criteria for Calibration Laboratories in Mechanical Discipline Mass (Weights)

National Accreditation Board for Testing and Calibration Laboratories

Specific Criteria for Calibration Laboratories in Mechanical Discipline Mass (Weights)

Standard Deviation of the

Selection of comparator balance for calibration of weights depending on class of accuracy:

2.7 Calibration Interval

Specific Criteria for Calibration Laboratories in Mechanical Discipline Mass (Weights)

2.8 Legal Aspects

u2 F +( a /pu P )2+ ( a /Tu T )2+( a /rh*u rh )2

{(m cr ( r - t )/ r t ))u a )}2)+{(m cr ( a - 0 ))2[(u2 t /4)}+m2 cr ( a - 0 )[( a - 0 )-2( a1 0 )](u2 r / r 4)}