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1 Preparing Benzoic Acid/caffeine STD.: Result and Data

The document describes preparing caffeine standards of varying concentrations from 20-100 ppm by calculating the volume of stock solution needed using the equation M1V1=M2V2. A table shows the retention times and peak areas of each standard. A figure graphs the peak area against concentration, showing a linear relationship. A soda sample was also tested with a retention time and peak area reported.

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18 views

1 Preparing Benzoic Acid/caffeine STD.: Result and Data

The document describes preparing caffeine standards of varying concentrations from 20-100 ppm by calculating the volume of stock solution needed using the equation M1V1=M2V2. A table shows the retention times and peak areas of each standard. A figure graphs the peak area against concentration, showing a linear relationship. A soda sample was also tested with a retention time and peak area reported.

Uploaded by

Maisarah
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOCX, PDF, TXT or read online on Scribd
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RESULT AND DATA

1 Preparing benzoic acid/caffeine std.

i 20ppm

M1V1 = M2V2

(1000) V1 = 20 (100mL)

V1= 2mL

ii 40ppm

M1V1 = M2V2

(1000) V1 = 40 (100mL)

V1 = 4mL

iii 60ppm

M1V1 = M2V2

(1000) V1 = 60 (100mL)

V1 = 6mL

iv 80ppm

(1000) V1 = 80 (100mL)

V1 = 8mL

v 100ppm

(1000) V1 = 100 (100mL)

V1 = 10mL
Table 1 below shows Retentation of Caffeine in Standard
Concentration (ppm) Retentation time (min) Peak area (v.s)
20 2.088 376333.10
40 2.097 662888.20
60 2.109 966511.40
80 2.075 1339400.10
100 2.081 1748956.80
Soda sample 2.045 979098.40

Figure 1 below shows the graph of Concentration vs Peak Area

Concentration vs Peak Area


2000000
1800000
1600000
1400000
1200000
1000000
Peak area, (v.s)
800000
600000
400000
200000
0
20 40 60 80 100

Concentration, (ppm)

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