Test Procedures Manual 2015
Test Procedures Manual 2015
Test Procedures Manual 2015
for Materials
Springfield, Illinois
The Manual of Test Procedures for Materials will be reviewed by the Engineer of Concrete and Soils for adequacy annually and
updated annually to reflect current test methods. Hard copies prior to January 1, 2015 are controlled. Archives are available from
Policy Distribution. The Illinois Modifications for ASTM and AASHTO test methods and standards are available online. Please see
Copyright Notice herein for additional information.
Revisions to the documents listed below are denoted within by a vertical line in the left margin. Effective dates are as indicated on
the individual documents and within the tables of contents.
1. POLICY
It is the policy of the Department of Transportation to publish and maintain a manual that
provides test procedures for quality control, quality assurance, and acceptance testing of
aggregates, hot mix asphalt and Portland cement concrete and soils. Illinois test
procedures for other materials may be included.
2. PERSONS AFFECTED
3. PURPOSE
The purpose of this policy is to provide for the publication of a manual to ensure
consistent test procedures in the production and acceptance of materials.
A. The manual will provide test procedures currently used by the department.
B. The test procedures are applicable to quality control, quality assurance, and
acceptance testing required by construction contracts. The procedures are
applicable to testing performed by the contractor, the department, or consultants
retained by either.
C. Department training classes shall utilize the current edition of this manual for all
applicable test procedures.
5. RESPONSIBILITIES
A. The Bureau of Materials and Physical Research (BMPR) is responsible for the
issuance and maintenance of this policy.
Departmental Policy MAT-13: Manual of Test Procedures for Materials March 6, 2015
B. The DOH regions/districts are responsible for ensuring compliance with this
policy.
6. REVISION HISTORY
CLOSING NOTICE
Page 2 of 2
SEQUENTIAL TABLE OF CONTENTS
(continued)
MANUAL OF TEST PROCEDURES
FOR MATERIALS
Illinois Test Procedure 11 Materials Finer Than 75-m (No. 200) Sieve in
(formerly AASHTO T 11) Mineral Aggregates by Washing ............................... 11
(Effective 01/01/15)
Illinois Test Procedure 27 Sieve Analysis of Fine and Coarse Aggregates ....... 29
(formerly AASHTO T 27)
(Effective 01/01/15)
Illinois Test Procedure 302 Aggregate Specific Gravity and Moisture Content
(Effective 02/01/14) by Dunagan Method ................................................. 71
Illinois Test Procedure 502 Static Cone Penetration (SCP) ................................. 103
(formerly 402)
(Effective 04/01/10)
Illinois Test Procedure 4791 Flat Particles, Elongated Particles, or Flat and
(formerly ASTM D 4791) Elongated Particles in Coarse Aggregate ................. 107
(Effective 06/01/12)
ASTM D 1188-07 Standard Test Method for Bulk Specific Gravity and
(Illinois Modified 01/01/15) Density of Compacted Bituminous Mixtures Using
Coated Samples ....................................................... 131
AASHTO T 121M/T 121-12 Weight per Cubic Foot, Yield, and Air Content
(Illinois Modified 02/01/14) (Gravimetric) of Concrete ......................................... 153
AASHTO T 309M/T 309 See ASTM C 1064/C 1064 M (Illinois Modified) .... 211
AASHTO R 30-02 (2010) Mixture Conditioning of Hot-Mix Asphalt (HMA) ....... 243
(formerly PP 2-99)
(Illinois Modified 01/01/15)
AASHTO R 39-07 (2012) Making and Curing Concrete Test Specimens in the
(formerly T 126) Laboratory ................................................................ 253
(Illinois Modified 02/01/14)
AASHTO R 46-08 (2012) Designing Stone Matrix Asphalt (SMA) .................... 255
(formerly PP 41-01)
(Illinois Modified 01/01/15)
Illinois Test Procedure SCC-1 Sampling, Determining Yield and Air Content, and
(Effective 03/01/13) Making and Curing Strength Test Specimens of
Self-Consolidating Concrete ................................... 259
AAggregate
Appendix B18 Ignition Oven Aggregate Mass Loss Procedure ....... B91
(Effective 05/01/05)
(Revised 05/01/07)
Appendix E4 PFP Hot Mix Asphalt Random Jobsite Sampling ..... E25
(Effective 04/01/11)
(Revised 01/01/13)
Appendix E7 Best Practices for PFP and QCP Implementation .... E47
(Effective 04/01/12)
AGGREGATE
Illinois Test Procedure 11 Materials Finer Than 75-m (No. 200) Sieve in
(formerly AASHTO T 11) Mineral Aggregates by Washing ............................... 11
(Effective 01/01/15)
Illinois Test Procedure 27 Sieve Analysis of Fine and Coarse Aggregates ....... 29
(formerly AASHTO T 27)
(Effective 01/01/15)
Illinois Test Procedure 4791 Flat Particles, Elongated Particles, or Flat and
(formerly ASTM D 4791) Elongated Particles in Coarse Aggregate ................. 107
(Effective 06/01/12)
AASHTO R 30-02 (2010) Mixture Conditioning of Hot-Mix Asphalt (HMA) ...... 243
(formerly PP 2-99)
(Illinois Modified 01/01/15)
Appendix B18 Ignition Oven Aggregate Mass Loss Procedure ...... B91
(Effective 05/01/05)
(Revised 05/01/07)
Appendix E4 PFP Hot Mix Asphalt Random Jobsite Sampling ..... E25
(Effective 04/01/11)
(Revised 01/01/13)
Appendix E5 PFP Dispute Resolution Instructions ....................... E37
(Effective 04/01/10)
Appendix E6 QCP Pay Calculation ............................................... E39
(Effective 01/01/12)
(Revised 01/01/15)
Appendix E7 Best Practices for PFP and QCP Implementation ... E47
(Effective 04/01/12)
Illinois Test Procedure 302 Aggregate Specific Gravity and Moisture Content
(Effective 02/01/14) by Dunagan Method................................................. 71
AASHTO T 121M/T 121-12 Weight per Cubic Foot, Yield, and Air Content
(Illinois Modified 02/01/14) (Gravimetric) of Concrete ..................................... 153
AASHTO T 309M/T 309 See ASTM C 1064/C 1064M (Illinois Modified) ..... 211
Illinois Test Procedure SCC-1 Sampling, Determining Yield and Air Content, and
(Effective 03/01/13) Making and Curing Strength Test Specimens of
Self-Consolidating Concrete ..................................... 259
SOILS
Illinois Test Procedure 502 Static Cone Penetration (SCP) ................................ 103
(formerly 402)
(Effective 04/01/10)
GENERAL
This Manual includes Illinois Modified Test Procedures to be used in conjunction with
and according to the noted ASTM and AASHTO test methods. ASTM and AASHTO test
methods cannot be reproduced in this manual due to copyright. Individual ASTM and
AASHTO standards may be requested from the respective addresses below:
ASTM AASHTO
100 Barr Harbor Drive 444 North Capitol Street, N. W.
West Conshohocken, PA 19428-2959 Suite 249
(610) 832-9500 Washington, D.C. 20001
www.astm.org (202) 624-5800
www.transportation.org
Contact:
Mark Axelman
ASTM International
Email: maxelman@astm.org
Notes below apply to Fine and Coarse Aggregate Gradation Tables Only
X = Required Gradation Specification Sieves
XC = Required Cutter Sieves
MB = Master Band Sieves for Category I & II Coarse Aggregate for PCC and HMA Mixes; Bituminous use only for fine aggregate.
MN = Maximum Nominal Sieve for Crushed Gravels Maximum Nominal Size is defined as the first specification sieve in the product
gradation on which material may be retained.
1 = CA = Coarse Aggregate; CM = Coarse Aggregate, Modified; FA = Fine Aggregate; FM = Fine Aggregate, Modified
2 = CM and FM gradations shall be sampled and tested the same as the corresponding CA and FA gradations.
3 = Slag should be adjusted accordingly due to its lighter or heavier mass.
4 = Will vary with the gradation of the material being used
5 = Control Charts Required
6 = Required Sieve for Control Charts
1 SCOPE
1.1 This procedure covers sampling of coarse and fine aggregates for the following
purposes.
Note 1 Sampling plans and acceptance and control tests vary with the type of
construction in which the material is used.
1.2 The text of this standard references notes which provide explanatory material. These
notes (excluding those in tables and figures) shall not be considered as requirements
of the procedure.
1.3 The values stated in either SI units or inch-pound units are to be regarded separately
as standard. The values stated in each system may not be exact equivalents;
therefore, each system shall be used independently of the other. Combining values
from the two systems may result in non-conformance with the procedure.
1.4 This standard does not purport to address all of the safety concerns, if any,
associated with its use. It is the responsibility of the user of this procedure to
establish appropriate safety and health practices and determine the applicability of
regulatory limitations prior to use.
Note 2 The quality of the results produced by this procedure are dependent on the
competence of the personnel performing the procedure and the capability, calibration,
and maintenance of the equipment used.
2 REFERENCED DOCUMENTS
3 TERMINOLOGY
3.1 Definitions:
3.1.3 nominal maximum aggregate size (of aggregate), nin specifications for, or
descriptions of aggregatesmallest sieve opening through which the entire amount of
the aggregate is permitted to pass.
3.1.4.1 DiscussionThese definitions in 3.1.2 and 3.1.4 apply to hot mix asphalt (HMA)
mixtures designed using the Superpave system only.
4.1 Sampling is equally as important as the testing, and the sampler shall use every
precaution to obtain samples that will show the nature and condition of the materials
which they represent.
5 APPARATUS
5.1 Template The template shall be designed with two end plates and shall be
adjustable. The distance between the end plates may therefore be changed to gather
more material from the belt for each increment. The end plates shall also be
machined or cut to the approximate belt size and shape.
A single template end plate may be used in the sampling procedure, if care is
exercised.
5.2 Sampling Device The sample device used to cut the flow stream from the end of the
belt or the bin discharge must be strong enough to handle the force of the flow
stream. The device must also be large and deep enough to cut the entire flow stream
and not overflow when passing through the stream. The device may be a bucket, a
pan, or a manufactured sampling container.
5.3 Shovel The shovel shall be square-nosed and of a size easily handled. It shall also
have built-up sides and back (approximately 1 [37.5mm]) to facilitate the retention
of material on the shovel when sampling.
6 SECURING SAMPLES
6.1 General Where practicable, samples to be tested for quality shall be obtained from
the finished product. Samples from the finished product to be tested for abrasion loss
shall not be subject to further crushing or manual reduction in particle size in
preparation for the abrasion test unless the size of the finished product is such that it
requires further reduction for the testing purposes.
6.2 Inspection The material shall be inspected to determine discernible variations. The
seller shall provide suitable equipment needed for proper inspection and sampling.
Belt-Stream Sampling The sample shall be taken by cutting the stream of aggregate
as it leaves the end of the production belt. A sampling device is passed uniformly
through the entire width and depth stream flow during normal production and belt
load. Each sampling pass (increment) is combined with others to make up the field
sample. A minimum of three increments shall be taken during a 10 to 15 minute
sampling period. Enough increments shall be taken and combined to provide the
correct field sample size.
Extreme care shall be taken to make sure the sampling device passes completely and
uniformly through the entire stream flow (from outside the stream on one side to
outside the stream on the other side) and to ensure the device does not overflow.
Before cutting the bin discharge stream, the bin must be emptied until such time that
the stream of material entering the bin is the stream of material exiting the bin.
Sampling may take place at that time.
Extreme care shall be taken to make sure the sampling device passes completely and
uniformly through the entire stream flow (from outside the stream on one side to
outside the stream on the other side) and to ensure the device does not overflow.
Samples shall be taken only during normal plant operation and when the bin is being
fed under normal load.
Samples shall be taken only during normal plant operation and when the belt is under
normal load.
Truck-Dump Sampling The sample shall be taken by placing one or two truck
dumps together. This may occur during the building of a stockpile or feeding of a
plant. The truck dump(s) shall be cut with an end loader and two or more bucket
loads extracted. The bucket loads shall be dumped on one another to form a small
pile. The small pile shall then be mixed from two directions perpendicular to each
other. To mix the pile, the end loader shall cut into the pile along its base until
approximately its midpoint. The loader bucket shall be lifted, the loader moved 1 to 2
feet forward, and the bucket dumped on the other half of the pile. Care shall be
exercised to avoid cutting below the base of the truck dumps or small pile and
contaminating the material to be sampled.
After mixing twice, the end loader shall drop the angle of its bucket downward on one
side of the pile and back drag the pile into a layer not less than 1 foot thick.
The layer shall be sampled using a required shovel to take increments in a random
X pattern over the layer. The shovel shall be forced vertically to its full depth when
sampling each increment except that care shall be used to not dig completely through
the layer. This would contaminate the sample being obtained. Care shall also be
exercised to retain as much material on the shovel as possible when taking
increments. Sufficient increments shall be taken to make up a correct field sample.
Stockpile Sampling The sample shall be taken from the working face of the
stockpile. The working face shall be parallel to the direction of flow used to build the
stockpile. Stockpiles having no working face shall have one established prior to
sampling. The working face shall have the interior of the pile exposed to permit
proper re-blending of the pile to eliminate segregated aggregate. If necessary,
material may be brought out of the main piles working face into the sub-stockpile for
sampling.
The stockpile sampling procedure shall follow the truck-dump sampling procedure
using an end loader. The end loader shall cut across the working face as detailed in
Truck-Dump Sampling. Any special mixing procedure used during loading shall be
used when taking any samples.
6.4.1 The number of field samples (obtained by one of the methods described in 5.3)
required depends on the criticality of, and variation in, the properties to be measured.
Designate each unit from which a field sample is be obtained prior to sampling. The
number of field samples from the production should be sufficient to give the desired
confidence in test results.
6.4.2 Field Sample Sizes The field sample size shall meet the minimum requirements as
detailed in the Illinois Specification 201.
7 Shipping Samples
7.2 Shipping containers for aggregate samples shall have a LM-5 envelope attached to
the container. Written on the outside of the LM-5 shall be the following information:
producer number, test id# (including suffix), material code, ledge description. The
required information to be written on the outside of the LM-5 shall also be written on
the outside of the sample container. Inside the LM-5 shall contain a fully completed
LM-6 form. The LM-6 form shall be the most recent version of the Bureau of
Materials and Physical Research online template (no other LM-6 forms will be
accepted).
8.1 The Bureau of Materials and Physical Research has established a procedure which
allows the producer the opportunity to delivering their quality samples directly to the
Springfield testing facility.
Your sample, taken by the district, will be sampled following the procedures outlined
in this test procedure. Upon completion of the sampling the District shall Red Tag
the sample containers. During the tagging process the District shall write the Red
Tag serial number on the LM-6 form. If the serial number is not indicated on the LM-
6 form the samples will not be accepted.
Once the sample containers are tagged and the documentation has been completed
the producer will then be allowed to deliver the samples to the Bureau.
9 Keywords
9.1 aggregates; exploration of potential sources; aggregates; number and sizes needed
to estimate character; aggregates; sampling
1 SCOPE
1.1 This test procedure covers the determination of the amount of material finer than a
No. 200 (75m) sieve in aggregate by washing. Clay particles and other aggregate
particles that are dispersed by the wash water, as well as water-soluble materials, will
be removed from the aggregate during the test.
1.3 This standard does not purport to address all of the safety concerns, if any,
associated with its use. It is the responsibility of the user of this procedure to
establish appropriate safety and health practices and determine the applicability of
regulatory limitations prior to use.
2 REFERENCED DOCUMENTS
3 SUMMARY OF METHOD
3.1 A sample of the aggregate is washed in a prescribed manner, using plain water . The
decanted wash water, containing suspended and dissolved material, is passed
through a No. 200 (75m) sieve. The loss in mass resulting from the wash treatment
is calculated as mass percent of the original sample and is reported as the
percentage of material finer than a No. 200 (75m) sieve by washing.
4.1 Material finer than the No. 200 (75m) sieve can be separated from larger particles
much more efficiently and completely by wet sieving than through the use of dry
sieving. Therefore, when accurate determinations of material finer than No. 200
(75m) in fine or coarse aggregate are desired, this test method is used on the
sample prior to dry sieving in accordance with ITP 27. The results of this test method
are included in the calculation in ITP 27, and the total amount of material finer than
the No. 200 (75m) by washing, plus that obtained by dry sieving the same sample, is
reported with the results of ITP 27. Usually the additional amount of material finer
than No. 200 (75m) obtained in the dry-sieving process is a small amount. If it is
large, the efficiency of the washing operation should be checked. A large amount of
material could also be an indication of degradation of the aggregate.
4.2
5 APPARATUS AND MATERIALS
5.1 Balance The balance shall have sufficient capacity, be readable to 0.1 percent of
the sample mass, or better, and conform to the requirements of M 231.
5.2 Sieves A nest of two sieves, the lower being a No. 200 (75m) sieve and the upper
being a sieve with openings in the range of No. 8 (2.36mm) to No. 16 (1.18mm) , both
conforming to the requirement of ASTM E 11.
5.3 Container A pan or vessel of a sufficient size to contain the sample covered with
water and to permit vigorous agitation without loss of any part of the sample or water.
Note 1 A mechanical device, such as a Ploog Washer, may be used for coarse
aggregate samples providing its results match the manual procedure. When using a
mechanical washing device, loss of fines from damage to the drum or dripping water
will not be allowed. Applying wax to the rim of the drum will help prevent water from
dripping down the outside of the drum.
6 SAMPLING
6.1 Field samples of aggregate shall be taken according to ITP 2. The field sample size
shall meet the minimum requirements in the Illinois Specification 201.
6.2 Field samples of aggregate shall be reduced to test sample size before testing
according to ITP 248.
Test sample size for gradation samples shall meet the minimum requirements found
in the Illinois Specification 201.
7 PROCEDURE
7.1 The test sample shall be dried back to constant mass in an oven specifically designed
for drying, set at and capable of maintaining a uniform temperature of 2309F
(1105C) . Constant mass is defined as the sample mass at which there has not
been more than a 0.5 gram mass loss during 1 hour of drying. This should be verified
occasionally.
The sample may also be dried to constant mass in a pan on an electric hot plate or
gas burner. The technician shall continually attend the sample when drying on the
electric hot plate or gas burner. The electric hot plate or gas burner should be
operated on a low-as-needed heat to prevent popping, crackling, and/or sizzling noise
from the aggregate during drying. If these noises occur, the heat must be turned
down and/or the sample must be constantly stirred during drying to prevent potential
aggregate particle breakdown.
After the test sample has been dried to constant mass and cooled down to room
temperature, the sample shall have its mass determined to the nearest 1 gram for
coarse aggregate and to the nearest 0.1 gram for fine aggregate. All balances or
scales shall be tared before being used to determination of mass required by this test
procedure. This procedure provides the Total Dry Mass, g (TDM) of the original test
sample.
7.2 After drying and determining the mass, place the test sample in the container and add
sufficient water to cover it. No detergent, dispersing agent, or other substance shall
be added to the water. Agitate the sample with sufficient vigor to result in complete
separation of all particles finer than the No. 200 (75m) sieve from the coarser
particles, and to bring the fine material into suspension. The use of a large spoon or
other similar tool shall be used to stir and agitate the aggregate in the wash water.
Once the wash water becomes clear pour the wash water containing the suspended
and dissolved solids over the nested sieves, arranged with the coarser sieve on top.
Take care to avoid, as much as feasible, the decantation of coarser particles of the
sample.
7.3 Add a second charge of water to the sample in the container, agitate, and decant as
before. Repeat this operation until the wash water is clear.
Note 3 A spray nozzle or a piece of rubber tubing attached to a water faucet may be
used to rinse any of the material that may have fallen onto the sieves. The velocity of
water, which may be increased by pinching the tubing or by use of a nozzle, should
not be sufficient to cause any splashing of the sample over the sides of the sieve.
7.4 Return all material retained on the nested sieves by flushing per note 4. Dry the
washed test sample to constant mass and determine the mass of the test sample in
the same manner as detailed in 8.1 herein. This procedure provides the Total Wash
Mass, g (TWM).
Note 4 Following the washing of the sample and flushing any material retained on
the No. 200 (75m) sieve back into the container by washing from the back of the
sieve. No water should be decanted from the container except through the No. 200
(75m) sieve, to avoid loss of material. Excess water from flushing should be
evaporated from the sample in the drying process.
8 CALCULATION
8.1 The Percent Minus 75m (No. 200) by Washing shall be determined by using the
following formula:
% - No. 200 (-75m) by Washing = 100
9 REPORT
9.1 The test results shall be rounded to the nearest 0.1 percent and recorded on the
Illinois Department of Transportation (IDOT) gradation form. All rounding shall be
according to ASTM E 29 (Illinois Modified)
1 SCOPE
1.1. This test procedure covers the determination of bulk density (unit weight) of
aggregate in a compacted or loose condition, and calculated voids between particles
in fine, coarse, or mixed aggregates based on the same determination. This test
method is applicable to aggregates not exceeding 125mm (5 in.) in nominal maximum
size.
Note 1 Unit weight is the traditional terminology used to describe the property
determined by this test method, which is weight per unit volume (more correctly, mass
per unit volume or density).
1.2. The values stated in either inch-pound units or acceptable metric units are to be
regarded separately as standard, as appropriate for a specification with which this test
method is used. An exception is with regard to sieve sizes and nominal size of
aggregate, in which the metric values are the standard as stated in ASTM E 11.
Within the text, inch-pound units are shown in brackets. The values stated in each
system in ASTM E 11. Within the text, inch-pound units are shown in brackets. The
values stated in each system may not be exact equivalents; therefore, each system
must be used independently of the other, without combining values in any way.
1.3. This standard does not purport to address all of the safety concerns, if any,
associated with its use. It is the responsibility of the user of this procedure to
establish appropriate safety and health practices and determine the applicability of
regulatory limitations prior to use.
2 REFERENCED DOCUMENTS
Illinois Specifications:
AASHTO Standards:
C 29/C 29M, Standard Test Method for Bulk Density (Unit Weight) and Voids
in Aggregate
C 125, Standard Terminology Relating to Concrete and Concrete Aggregates
C 670, Standard Practice for Preparing Precision and Bias Statements for
Test Methods for Construction Materials
D 123, Standard Terminology Relating to Textiles
E 11, Woven Wire Test Sieve Cloth and Test Sieves
E 29 (Illinois Modified), Standard Practice for Using Significant Digits in Test
Data to Determine Conformance with Specifications
3. TERMINOLOGY
3.1. Bulk density, n of aggregate, the mass of a unit volume of bulk aggregate material,
in which the volume includes the volume of the individual particles and the volume of
the voids between the particles. Expressed in lb/ft3 (kg/m3).
3.1.1 Discussion units of mass are the pound (lb), the kilogram (kg), or units derived from
these. Mass may also be visualized as equivalent to inertia, or the resistance offered
by a body to change of motion (acceleration). Masses are compared by weighing the
bodies, which amounts to comparing the forces of gravitation acting on them. ASTM
D 123.
3.2 Unit weight, n - weight (mass) per unit volume. (Deprecated term - used preferred
term bulk density.)
3.2.1. Discussion the term weight means the force of gravity acting on the mass.
3.3 Weight, n the force exerted on a body by gravity. (See also mass.)
3.3.1 Discussion weight is equal to the mass of the body multiplied by the acceleration
due to gravity. Weight may be expressed in absolute units (poundals, newtons) or in
gravitational units (lbf, kgf), for example: on the surface of the earth, a body with a
mass of 1lb has a weight of 1 lbf (approximately 32.2 poundals or 4.45N), or a body
with a mass of 1kg has a weight of 1kgf (approximately 9.81N). . Since weight is
equal to mass times the acceleration due to gravity the weight of a body will vary with
the location where the weight is determined, while the mass of the body remains
constant. On the surface of the earth, the force of gravity imparts to a body that is
free to fall an acceleration of approximately 32.2 ft/s2 (9.81m/s2). ASTM D 123.
3.4 Voids, n in unit volume of aggregate, the space between particles in an aggregate
mass not occupied by solid mineral matter.
3.4.1 Discussion voids within particles, either permeable of impermeable, are not included
in voids as determined by 13.2, herein. .
4.1. This test method is often used to determine bulk density values that are necessary for
use for many methods of selecting proportions for concrete mixtures.
4.2. The bulk density also may be used for determining mass/volume relationships for
conversions in purchase agreements. However, the relationship between degree of
compaction of aggregates in a hauling unit or stockpile and that achieved in this
method is unknown. Further, aggregates in hauling units and stockpiles usually
contain absorbed and surface moisture (the latter affecting bulking), while this method
determines the bulk density on a dry basis.
4.3. A procedure is included for computing the percentage of voids between the aggregate
particles based on the bulk density determined by this method.
5. APPARATUS
5.1. Balance The balance shall have sufficient capacity, be readable to 0.1 percent of
the sample mass, or better, and conform to the requirements of AASHTO M 231.
5.2. Tamping Rod A round, straight steel rod, 5/8 (16mm) in diameter and a minimum
of 23 inches (584mm) long, having one end rounded to a hemispherical tip of the
same diameter as the rod.
5.3. Measure A cylindrical metal measure, preferably provided with handles. It shall be
watertight, with the top and bottom true and even, and sufficiently rigid to retain its
form under rough usage. The measure should have a height approximately equal to
the diameter, but in no case shall the height be less than 80 percent nor more than
150 percent of the diameter. The capacity of the measure shall conform to the limits
in Table 1 for the aggregate size to be tested. The thickness of metal in the measure
shall be as described in Table 2. The top rim shall be smooth and plane within 0.01
in. (0.25mm) and shall be parallel to the bottom within 0.5 (Note 2). The interior wall
of the measure shall be a smooth and continuous surface.
Note 2 The top rim is satisfactorily plane if a 0.01 in (0.25mm) feeler gauge cannot
be inserted between the rim and a piece of 6mm (1/4 in.) or thicker plate glass laid
over the measure. The top and bottom are satisfactorily parallel if the slope between
pieces of plate glass in contact with the top and bottom does not exceed 0.87 percent
in any direction.
5.3.1. If the measure also is to be used for testing for bulk density of freshly mixed concrete
according to AASHTO T 121M/T 121 (Illinois Modified), the measures shall be made
of steel or other suitable metal not readily subject to attack by cement. Reactive
materials, such as aluminum alloys are permitted, where as a consequence of an
initial reaction, a surface film is formed which protects the metal against further
corrosion.
5.3.2. Measures larger than nominal 1 ft3 (28L) capacity shall be made of steel for rigidity, or
the minimum thicknesses of metal listed in Table 2 should be suitably increased.
5.4. Shovel or Scoop A shovel or scoop of convenient size for filling the measure with
aggregate.
5.5.1. Plate Glass A piece of plate glass, preferably at least in (6mm) thick and at least
1in (25mm) larger than the diameter of the measure to be calibrated.
Note 3 Petrolatum, vacuum grease, water pump grease, or chassis grease are
examples of suitable material used to form a seal between the glass plate and
measure.
5.5.3. Thermometer A thermometer having a range of at least 50 to 90F (10 to 32C) and
that is readable to at least 1F (0.5C).
5.6 Source of Heat An oven of sufficient size, specifically built for drying, capable of
maintaining a uniform temperature of 2309F (1105C) shall be used for drying. In
addition, a gas burner or electric hot plate may be used. Microwave ovens are not
permitted for drying unit weight or voids test samples.
6. SAMPLING
6.1 Field samples of aggregate shall be taken according to ITP 2. Field sample size shall
conform to the minimum requirements in the Illinois Specification 201. Reduction of
field samples shall be according to ITP 248.
7. SAMPLE
7.1 The size of sample shall be approximately 125 to 200 percent of the quantity required
to fill the measure and shall be handled in a manner to avoid segregation. The test
sample shall be dried to constant mass in an oven, specifically built for drying, set at
and capable of maintaining a uniform temperature of 2309F (1105C). Constant
mass is defined as the sample mass at which there has not been more than a 0.5
gram loss during 1 hour of drying. This should be verified occasionally.
The sample may also be dried to constant mass in a pan on an electric hot plate or
gas burner. The technician shall continually attend the sample when drying on the
electric hot plate or gas burner. Microwave ovens are not permitted for drying unit
weight or voids test samples.
The electric hot plate or gas burner should be operated on a low-as-needed heat to
prevent popping, crackling, and/or sizzling noise from the aggregate during drying. If
these noises occur, the heat must be turned down and/or the sample must be
constantly stirred during drying to prevent potential aggregate particle breakdown.
Note 4 When testing Recycled Asphalt Pavement (RAP) samples shall be air dried
to a constant mass.
8. CALIBRATION OF MEASURE
8.1 Measures shall be recalibrated at least once a year or whenever there is reason to
question the accuracy of the calibration.
8.2 Place a thin layer of grease on the rim of the measure to prevent leakage of water
from the measure.
8.3 Determine the mass of the plate glass and measure to the nearest 0.1 lb (0.05kg).
8.4 Fill the measure with water that is at room temperature and cover with the plate glass
in such a way as to eliminate bubbles and excess water. Remove any water that may
have overflowed onto the measure or plate glass.
8.5 Determine the mass of the water, plate glass and measure to the nearest 0.1 lb (0.05kg).
8.6 Measure the temperature of the water to the nearest 1F (0.5C) and determine its
density from Table 3, interpolating if necessary.
8.7. Calculate the volume, V, of the measure. Alternatively, calculate the factor, F, for the
measure.
V= (1)
F= (2)
where:
Note 5 For the calculation of bulk density, the volume of the measure in acceptable
metric units should be expressed in cubic meters, or the factor as l/m3. However, for
convenience the size of the measure may be expressed in liters (equal to m3/1000).
9. SELECTION OF PROCEDURE
9.1 The compact bulk density shall be determined by the rodding procedure for
aggregates having a nominal maximum size of 1 1/2 in (37.5mm) or less, or by jigging
procedure for aggregates have a nominal maximum size greater than 1 1/2im
(37.5mm) and not exceeding 5in (125mm).
10.1 Fill the measure one-third full and level the surface with the fingers. Rod the layer of
aggregate with 25 strokes of the tamping rod evenly distributed over the surface. Fill
the measure two-thirds full and again level and rod as above. Finally, fill the measure
to overflowing and rod again in the manner previously mentioned. Level the surface
of the aggregate with the fingers or a straightedge in such a way that any slight
projections of the larger pieces of the coarse aggregate approximately balance the
larger voids in the surface below the top of the measure. The tamping rod may be
used as a straightedge.
10.2 In rodding the first layer, do not allow the rod to strike the bottom of the measure
forcibly. In rodding the second and third layers, use vigorous effort, but not more
force than to cause the tamping rod to penetrate to the previous layer of aggregate.
Note 6 In rodding the larger sizes of coarse aggregate, it may not be possible to
penetrate the layer being consolidated, especially with angular aggregates. The
intent of the procedure will be accomplished if vigorous effort is used.
10.3 Determine the mass of the measure plus contents, and the mass of the measure
alone and record the values to the nearest 0.1lb (0.05kg).
11.1 Fill the measure in three approximately equal layers as described in Section 10.1,
compacting each layer by placing the measure on a firm base, such as a cement-
concrete floor, raising the opposite sides alternately about 2in (50mm), and allowing
the measure to drop in such a manner as to hit with a sharp, slapping blow. The
aggregate particles, by this procedure, will arrange themselves in a densely
compacted condition. Compact each layer by dropping the measure 50 times in the
manner described, 25 times on each side. Level the surface of the aggregate with the
fingers or a straightedge in such a way that any slight projections of the larger pieces
of the coarse aggregate approximately balance the larger voids in the surface below
the top of the measure.
11.2 Determine the mass of the measure plus contents, and the mass of the measure
alone, and record the values to the nearest 0.1lb (0.05kg).
12.1 Unit Weight Calculate the unit weight for the rodding or jigging procedure as follows:
M= (3)
or,
M= (4)
where:
M = bulk density of aggregate, lb/ft3 (kg/m3);
G = mass of aggregate plus the measure, lb (kg);
T = mass of the measure, lb (kg);
V = volume of measure, ft3 (m3); and
F = factor for measure, ft3 (m-3).
12.1.1. The bulk density determined by this method is for aggregate in an oven-dry condition.
If the bulk density in terms of saturated surface-dry (SSD) condition is desired, use
the exact procedure in this method, and then calculate the SSD bulk density by the
following formula:
M SSD = [1 + ] (5)
100
where:
12.2. Void Content Calculate the void content in the aggregate using the unit weight
determined by either the rodding or jigging procedures as follows:
where:
M = bulk density of aggregate, lb/ft3 (kg/m3);
12.3 When more than one size of coarse aggregate is used in IDOTs mortar-voids design
method for concrete mixtures, the void content is determined from a sample
consisting of the coarse aggregate combination. To perform the calculation in Section
13.2, the bulk specific gravity (dry basis) shall be a weighted average of the coarse
aggregate combination.
Example:
13. REPORT
13.1. Report the results for unit weight to the nearest 1 lb/ft (1 kg/m). All rounding shall be
according to ASTM E 29 (Illinois Modified).
13.2. Report the results for void content to the nearest one percent as follows:
14.1. The following estimates of precision for this method are based on results from the
AASHTO Materials Reference laboratory (AMRL) Proficiency Sample Program, with
testing conducted by this method and ASTM C 29. There are no significant
differences between the two methods. The data are based on the analyses of more
than 100 paired test results from 40 to 100 laboratories.
14.2.1. Single-Operator Precision The single-operator standard deviation has been found to
be (0.88 lb/ft3 (14 kg/m3) (1s). Therefore, results of two properly conducted tests by
the same operator on similar material should not differ by more than 2.50 lb/ft3 (40
kg/m3) (d2s).
14.2.2. Multilaboratory Precision The multilaboratory standard deviation has been found to
be 1.87 lb/ft3 (30 kb/m3) (1s). Therefore, results of two properly conducted tests from
two different laboratories on similar material should not differ by more than 5.3 lb/ft3
(85 kg/m3) (d2s).
14.3.1. Single-Operator Precision The single-operator standard deviation has been found to
be (0.88 lb/ft3 (14 kg/m3) (1s). Therefore, results of two properly conducted tests from
the same operator on similar material should not differ by more than 40 kg/m3
(2.5lb/ft3) (d2s
14.3.2. Multialaboratory Precision The multilaboratory standard deviation has been found to
be 2.76 lb/ft3 (44 kg/m3) (1s). Therefore, results of two properly conducted tests from
two different laboratories on similar material should not differ by more than 7.8 lb/ft3
(125 kg/m3) (d2s).
14.4 No precision data on void content are available. However as the void content in
aggregate is calculated from bulk density and bulk specific gravity, the precision of the
voids content reflects the precision of these measured parameters given in Sections
15.2 and 15.3 of this method and in ITP 84 and ITP 85.
14.5 Bias The procedure in this test method for measuring bulk density and void content
has no bias because the values for bulk density and void content can be defined only
in terms of a test method.
1. SCOPE
1.1 This procedure covers the determination of the particle size distribution of fine
and coarse aggregates by sieving.
1.2 Some specifications for aggregates, which reference this method, contain
grading requirements including both coarse and fine fractions. Instructions are
included for sieve analysis of such aggregates.
1.3 The values stated in SI units are to be regarded as the standard. The values
in parentheses are provided for information purposes only.
1.4 This standard does not purport to address all of the safety concerns, if any,
associated with its use. It is the responsibility of the user of this procedure to
establish appropriate safety and health practices and determine the
applicability of regulatory limitations prior to use.
2. REFERENCED DOCUMENTS
3 TERMINOLOGY
3.1 Definitions For definitions of terms used in this standard, refer to ASTM C
125.
4 SUMMARY OF METHOD
5.2 Accurate determination of material finer than the No. 200 (75m) sieve cannot
be achieved by used of this method alone. ITP 11 for material finer than the
No. 200 (75m) sieve by washing should be employed.
6 APPARATUS
6.1 Balance The balance shall have sufficient capacity, be readable to 0.1
percent of the sample mass, or better, and conform to the requirements of
AASHTO M 231.
6.2 Sieves The sieve cloth shall be mounted on substantial frames constructed
in a manner that will prevent loss of material during sieving. The sieve cloth
and standard sieve frames shall conform to the requirements of ASTM E 11.
Nonstandard sieve frames shall conform to requirements of ASTM E 11 as
applicable.
6.3 Mechanical Sieve Shaker A mechanical sieving device, shall create motion
of the sieves to cause the particles to bounce, tumble, or otherwise turn so as
the present different orientations to the sieving surface. The sieving action
shall be such that the criterion for adequacy of sieving described in Section
8.4 is met in a reasonable time period.
In addition, a gas burner or electric hot plate may be used. Microwave ovens
are not permitted for drying aggregate gradation samples.
7 SAMPLING
7.1 Field samples of aggregate shall be taken according to ITP 2. The field
sample size shall meet the minimum requirements in the Illinois Specification
201.
7.2 Field samples of aggregate shall be reduced to test sample size before testing
according to ITP 248.
Test sample size for gradation samples shall meet the minimum requirements
in the Illinois Specification 201.
7.3 In the event that the amount of material finer than No. 200 (75m) sieve is to
be determined by ITP 11, proceed as follows: use the procedure described in
Section 7.3.1 or 7.3.2, whichever is applicable.
7.3.1 Use the same test sample for testing by ITP 11 and by this method. First test
the sample according to ITP 11 through the final drying operation, and then
dry-sieve the sample as stipulated in Sections 8.2 through 8.6 of this method.
7.3.2 If the test sample is not to be tested by ITP 11, follow Section 8, Procedure.
8 PROCEDURE
8.1 If the test sample has not been subject to testing by ITP 11, the test sample
shall be dried back to constant mass in an oven specifically designed for
drying, set at and capable of maintaining a uniform temperature of 2309F
(1105C) . Constant mass is defined as the sample mass at which there has
not been more than a 0.5 gram mass loss during 1 hour of drying. This should
be verified occasionally.
The sample may also be dried to constant mass in a pan on an electric hot
plate or gas burner. The technician shall continually attend the sample when
drying on the electric hot plate or gas burner. Microwave ovens are not
permitted for drying gradation samples.
After the test sample has been dried to constant mass and cooled down to
room temperature, the sample shall have its mass determined to the nearest 1
gram for coarse aggregate and to the nearest 0.1 gram for fine aggregate. All
balances or scales shall be tared before being used for determination of mass
required by this test procedure. This procedure provides the Total Dry Mass,
g (TDM) of the original test sample. When testing Recycled Asphalt
Pavement (RAP) samples shall be air dried to a constant mass.
8.2 A nested set of sieves (8 inch [203mm] or 12 inch [305mm]) shall be gathered
and stacked. As the sieves are being stacked, they should be inspected for
cracks, breaks, or any other problem which would exclude their continued use.
The size of the sieves used shall conform to the gradation specifications of the
aggregate tested. The No. 200 (75m) sieve is required to be part of all
nested sets when running a gradation test. It is also required that 8 inch
(203mm) and 12 inch (305mm) round sieves use additional cutter sieves
beyond the specified gradation sieves for all coarse aggregate gradations.
Some cutter sieves may be required for fine aggregate gradations if
overloading of individual sieves occurs. Gradations CA/CM 7 and 11 require
the 5/8 inch (16.0mm), 3/8 inch (9.5mm), and 1/4 inch (6.3mm) sieves as
cutter sieves, while the gradations CA/CM 13, 14, and 16 require the 1/4 inch
(6.3mm) and the No. 8 (2.38mm) sieves. Cutter sieves for other gradations
can be found in Illinois Specification 201.
The sample shall then be introduced into the nested set of sieves and placed
in a mechanical shaker. The shaker shall impart a vertical, or lateral and
vertical, motion to the nested set. This causes the aggregate particles to
bounce and turn so as to present different particle orientations to the sieves.
This allows every chance for the particle to pass a certain sized sieve.
8.3 Extreme care shall be taken not to overload individual sieves or even
approach the overload limits. An overload is defined as several layers of
particles, one on top of the other, which do not permit the top layers of
particles access to the sieve openings. Sample results which show
overloading or a borderline situation are immediately suspect. If samples
continually overload a sieve or sieves, then future samples shall be run in the
appropriate number of portions to prevent overloading, or additional cutter
sieves shall be added to the nested set to correct the problem.
8.4 After mechanical shaking, all sieves shall be finished off by hand-shaking.
When hand-shaking, the largest sieve that contains material shall be removed
from the stack, visually inspected for overload, and inverted over an empty
pan. While inverted, all particles shall be cleaned from the sieve. The
material shall then be placed back on the same sieve and hand-shaken over
an empty pan. Any amount of material that is considered to be an overload or
to be approaching an overload shall be hand-shaken in a least two
increments. Any appreciable amount of particles passing a sieve may indicate
poor mechanical shaking or overloading. The finish hand-shaking described
in the following paragraph shall then be initiated.
Continue sieving for a sufficient period and in such manner that, after
completion, not more than 0.5 percent by mass of the total sample passes any
sieve during 1 minute of continuous hand sieving performed as follows: Hold
the individual sieve, provided with a snug-fitting pan and cover, in a slightly
inclined position in one hand. Strike the side of the sieve sharply and with an
upward motion against the heel of the other hand at a rate of about 150 times
per minute, turn the sieve about one-sixth of a revolution at intervals of about
25 strokes. In determining sufficiency of sieving for sizes larger than No. 4
(4.75mm) sieve, limit the material on the sieve to a single layer of particles. If
the size of the mounted testing sieves makes the described sieving motion
impractical, use 8 inch (203mm) diameter sieves to verify the sufficiency of
sieving.
8.5 After hand-shaking, material shall be removed from the sieve. Particles shall
not be forced through the sieves. The sieve shall be inverted and lightly
tapped on the sides to facilitate removal for weighing. A dowel rod or putty
knife may be used to gently remove wedged particles from all sieves down
through the No. 10 (2.00mm). A soft brass-wired brush shall be used on the
No. 16 (1.18mm) through the No. 40 (425m) sieve. A soft china brush shall
be used on the No. 50 (300m) through the No. 200 (75m) sieve. Any
material that passed the sieve during hand-shaking shall be placed on the
next smaller sieve. After use, all sieves shall be inspected for cracks, breaks,
or any other problem which would exclude their continued use.
Note: The dowel rod can be made of any material that will not deposit foreign
material into the test sample or cause damage to the sieves during the
removal of wedged particles.
8.6 After hand-shaking and cleaning, the material retained on each sieve shall
have its mass determined and the mass recorded. All determination of mass
shall start with the largest sieve in the nested set and proceed down to the
pan. Determination of mass shall be to the nearest 1 gram for coarse
aggregate and to the nearest 0.1 gram for fine aggregate. The total mass of
the material after sieving should check closely with original mass of samples
placed on the sieves. If the amounts differ by more than 0.3 percent, based
on the original dry sample mass, the results should not be used for
acceptance purposes.
9 CALCULATION
9.1 Calculation of test results shall follow the procedure described below:
Calculated the Cumulative Mass Retained for each sieve by adding its
Individual Mass Retained and the Individual Mass Retained for each larger
sieve in the nested set of sieves. Record the Cumulative Mass Retained.
Calculated the Cumulative Percent Retained for each sieve by using the
following formula and record it by rounding to the nearest 0.1 percent:
Cumulative % Retained = 100
Calculated the percent passing each sieve by using the following formula:
9.2 Calculate the fineness modulus, when required, by adding the total
percentages of material in the sample that is coarser than each of the
following sieves (cumulative percentages retained), and dividing the sum by
100; No. 100 (150m), No. 50 (300m), No. 30 (600m), No. 16 (1.18mm),
No. 8 (2.36mm), No. 4 (4.75mm), 3/8 in. (9.5mm), 3/4 in. (19.0mm), 1 1/2 in.
(37.5mm), and larger, increasing the ratio of 2 to 1.
10 REPORT
10.1 Depending upon the form of the specifications for used of the material under
test, the report shall include one of the following:
10.2 All percent passing results except the washed minus No. 200 (75m) and
minus No. 200 (75m) shall be reported on the gradation form as whole
numbers. The washed minus No. 200 (75m) and minus No. 200 (75m)
results shall be reported to the nearest 0.1 percent. Illinois Department of
Transportation (IDOT) gradation forms or forms approved by IDOT shall be
used. These forms shall be competed with all required information.
10.4 For all sieves that are considered overloaded and split in more than one
increment. An S next to the sieve must be notated on the worksheet.
11 COMPARISON PROCEDURE
11.1 All comparison testing shall be conducted in accordance with the most current
version of the Illinois Department of Transportation Manual of Test Procedures
for Materials (Appendix A7).
1 SCOPE
1.1 This procedure covers the determination of bulk and apparent specific gravity,
and absorption of fine aggregates
1.2 This method determines (after 15 to 19 hours in water) the bulk specific gravity
and the apparent specific gravity, the bulk specific gravity on the basis of mass
of saturated surface-dry aggregate, and the absorption.
1.3 The values stated are in SI units are to be regarded as the standard.
1.4 This standard does not purport to address all of the safety concerns, if any,
associated with its use. It is the responsibility of the user of this procedure to
establish appropriate safety and health practices and determine the
applicability of regulatory limitations prior to use.
2 REFERENCED DOCUMENTS
3 TERMINOLOGY
3.1 Definitions:
3.1.1 Absorption the increase in the mass of aggregate due to water in the pores
of the material, but not including water adhering to the outside surface of the
particles, expressed as a percentage of the dry mass. The aggregate is
considered dry when it has been maintained at a temperature of 2309F
(1105C) for sufficient time to remove all uncombined water by reaching a
constant mass.
3.1.2 Specific gravity the ratio of the mass (or weight in air) of a unit volume of a
material to the mass of the same volume of gas-free distilled water at stated
temperatures. Values are dimensionless.
3.1.2.1 Apparent specific gravity the ratio of the weight in air of a unit volume of the
impermeable portion of aggregate at a stated temperature to the weight in air
of an equal volume of gas-free distilled water at a stated temperature.
3.1.2.2 Bulk specific gravity the ratio of the weight in air of a unit volume of
aggregate (including the permeable and impermeable voids in the particles,
but not including the voids between particles) at a stated temperature to the
weight in air of an equal volume of gas-free distilled water at a stated
temperature.
3.1.2.3 Bulk specific gravity (SSD) the ratio of the mass in air of a unit volume of
aggregate, including the mass of water within the voids filled to the extent
achieved by submerging in water for approximately 15 to 19 hours (but not
including the voids between particles) at a stated temperature, compared to
the weight in air of an equal volume of gas-free distilled water at a stated
temperature.
4.1 Bulk specific gravity is the characteristic generally used for calculation of the
volume occupied by the aggregate in various mixtures containing aggregate
including portland cement concrete, bituminous concrete, and other mixtures
that are proportioned or analyzed on an absolute volume basis. Bulk specific
gravity is also used in the computation of voids in aggregate in ITP 19. Bulk
specific gravity determined on the saturated surface-dry basis is used if the
aggregate is wet, that is, if its absorption has been satisfied. Conversely, the
bulk specific gravity determined on the oven-dry basis is used for
computations when the aggregate is dry or assumed to be dry.
4.2 Apparent specific gravity pertains to the relative density of the solid material
making up the constituent particles not including the pore space within the
particles that is accessible to water. This value is not widely used in
construction aggregate technology.
4.3 Absorption values are used to calculate the change in the mass of an
aggregate due to water absorbed in the pore spaces within the constituent
particles, compared to the dry condition, when it is deemed that the aggregate
has been in contact with water long enough to satisfy most of the absorption
potential. The laboratory standard for absorption is that obtained after
submerging dry aggregate for approximately 15 hours in water. Aggregates
mined from below the water table may have a higher absorption when used, if
not allowed to dry. Conversely, some aggregates when used may contain an
amount of absorbed moisture less than the 15 to 19 hours soaked condition;
For an aggregate that has been in contact with water and that has free
moisture on the particle surfaces, the percentage of free moisture can be
determined by deducting the absorption from the total moisture content
determined by ITP 255 by drying.
5 APPARATUS
5.1 Balance The balance shall have sufficient capacity, be readable to 0.1
percent of the sample mass, or better, and conform to the requirements of
AASHTO M 231.
5.3 Mold A metal mold in the form of a frustum of a cone with dimensions as
follows: 1.570.12in. (403mm) inside diameter at the top 3.540.12in.
(903mm) inside diameter at the bottom, and 2.950.12in. (753mm) in
height, with the metal having a minimum thickness of 0.03in. (0.8mm).
5.4 Tamper A metal tamper having a mass of 34015g and having a flat circular
tamping face 0.980.12in. (253mm) in diameter.
5.5 Oven An oven of sufficient size, specifically built for drying, capable of
maintaining a uniform temperature of 2309F (1105C). No other heat
source for drying is permitted.
5.6 Water Tank A watertight tank into which the sample and container are
placed for complete immersion while suspended below the balance, equipped
with an overflow outlet for maintaining a constant water level.
6 SAMPLING
6.1 Field samples of fine aggregate shall be taken according to ITP 2. Field
sample size shall meet the minimum requirements in the Illinois Specification
201.
7.1 Obtain a test sample of approximately 4000 grams of fine aggregate from the
field sample by procedures described in ITP 248.
7.1.1 The sample shall not be dried. Cover the sample with water and permit to
stand 15 to 19 hours.
7.2 Decant excess water with care to avoid loss of fines, spread the sample on a
flat, nonabsorbent surface exposed to a gentle current (lowest setting if using
a fan) of warm air, and stir frequently to assure uniform drying. No mechanical
aids shall be used. Hand-stirring or diagonally lifting a nonabsorbent sheet
corner-to-corner may be used. Care shall be exercised not to lose any of the
test sample. As the material begins to dry sufficiently, it may be necessary to
work it with the hands in a rubbing motion to break up any conglomerations,
lumps, or balls of material that develop. Continue this operation until the test
specimen approaches a free-flowing condition. Follow the procedure in
Section 7.2.1 to determine whether or not surface moisture is present on the
fine aggregate particles. It is intended that the first trial of the cone test will be
made with some surface water in the specimen. Continue drying with
constant stirring, and if necessary, work the material with a hand-rubbing
motion, and test at frequent intervals until the test indicates that the specimen
has reached a surface-dry condition. If the first trial of the surface moisture
test indicates that moisture is not present on the surface, it has been dried
past the saturated surface-dry condition. In this case, thoroughly remoisten
the fine aggregate and permit the specimen to stand in a covered container for
30 minutes. Then resume the process of drying and testing at frequent
intervals for the onset of the surface-dry condition.
7.2.1 Place the mold firmly on a smooth, nonabsorbent surface with the large
diameter down. Place a portion of the partially dried fine aggregate loosely in
the mold by filling until overflow occurs. Hold the mold down tightly and
remove any loose fine aggregate from around the base of the mold. Lightly
tamp the fine aggregate into the mold with 25 light drops of the tamper. Each
drop should start about 0.2in. (5mm) above the top surface of the fine
aggregate. Permit the tamper to fall freely under gravitational attraction on
each drop. Adjust the starting height to the new surface elevation after each
drop and distribute the drops over the surface. Lift the mold vertically. If
surface moisture is still present, the fine aggregate will retain the molded
shape. For rounded and crushed natural sands, surface dry condition is
reached when all the material on the sides slumps off leaving a nickel-sized
plateau in the middle. For all other manufactured sands, surface dry condition
is reached when at least of a side of the molded cone shape slumps off.
8 PROCEDURE
8.2 Obtain two 1000.0 gram test samples from the saturated surface-dry fine
aggregate. This mass is the Wet Mass.
Immediately introduce one of the test samples into the sample container and
determine its mass in water at 73.43F (23.01.7C) using the specified
balance or scale. Take care to remove all entrapped air before weighing by
shaking and/or stirring the test sample. Let the fines settle out before
submerging. Discard sample after determining its mass in water. This
determination of mass establishes the Submerged Mass.
8.3 Dry the second 1000.0 gram sample immediately to constant mass in the
specified oven at 2309F (1105C). After the test sample has been dried to
constant mass and cooled to room temperature determine the mass to the
nearest 0.1 gram. Constant mass is defined as the sample mass at which
there has not been more the 0.5 gram mass loss during 1 hour of drying. This
should be verified occasionally. This determination of mass establishes the
Oven-Dry Mass.
A
=
BC
Calculate the bulk specific gravity, on the basis of weight of saturated surface-
dry aggregate as follows:
B
( ) =
BC
A
=
AC
12 ABSORPTION
12.1 ABSORPTION
, = 100
where A = oven-dry, g,
and B = wet mass, g.
13 REPORT
13.1 Report all specific gravity results to the nearest 0.001 and all absorption
results to the nearest 0.1 percent.
1 SCOPE
1.1 This procedure covers the determination of specific gravity and absorption of coarse
aggregate. The specific gravity may be expressed as bulk specific gravity, bulk
specific gravity (saturated-surface-dry (SSD)), or apparent specific gravity. The bulk
specific gravity (SSD) and absorption are based on aggregate after 15 to 19 hours
soaking in water. This method is not intended to be used with lightweight aggregates.
1.3 This standard does not purport to address all of the safety concerns, if any,
associated with its use. It is the responsibility of the user of this procedure to
establish appropriate safety and health practices and determine the applicability of
regulatory limitations prior to use.
2 REFERENCED DOCUMENTS
3 TERMINOLOGY
3.1 Definitions:
3.1.1 Absorption the increase in the mass of aggregate due to water in the pores of the
materials but not including water adhering to the outside surface of the particles,
expressed as a percentage of the dry mass. The aggregate is considered dry when
it has been maintained at a temperature of 2309F (110 5C) for sufficient time to
remove all uncombined water by reaching a constant mass.
3.1.2 Specify Gravity the ratio of the mass (or weight in air) of a unit volume of a material
to the mass of the same volume of gas-free distilled water at stated temperatures.
Values are dimensionless.
3.1.2.1 Apparent Specific Gravity the ratio of the weight in air of a unit volume of the
impermeable portion of aggregate at a stated temperature to the weight in air of an
equal volume of gas-free distilled water at a stated temperature.
3.1.2.2 Bulk Specific Gravity the ratio of the weight in air of a unit volume of aggregate
(including the permeable and impermeable voids in the particles, but not including the
voids between particles) at a stated temperature to the weight in air of an equal
volume of gas-free distilled water at a stated temperature.
3.1.2.3 Bulk Specific Gravity (SSD) the ratio of the mass in air of a unit volume of
aggregate, including the mass of water within the voids filed to the extent achieved by
submerging in water for approximately 15 to 19 hours (but not including the voids
between particles) at a stated temperature, compared to the weight in air of an equal
volume of gas-free distilled water at a stated temperature.
4.1 Bulk specific gravity is the characteristic generally used for calculation of the volume
occupied by the aggregate in various mixtures containing aggregate, including
portland cement concrete, bituminous concrete, and other mixtures that are
proportioned or analyzed on an absolute volume basis. Bulk specific gravity is also
used in the computation of voids in aggregate in ITP 19. Bulk specific gravity (SSD)
is used if the aggregate s wet, that is, if its absorption has been satisfied. Conversely,
the bulk specific gravity (oven-dry) is used for computations when the aggregate is
dry or assumed to be dry.
4.2 Apparent specific gravity pertains to the relative density of the solid material making
up the constituent particles not including the pore space within the particles which is
accessible to water.
4.3 Absorption values are used to calculate the change in the mass of an aggregate due
to water absorbed in the pore spaces within the constituent particles, compared to the
dry condition, when it is deemed that the aggregate has been in contact with water
long enough to satisfy most of the absorption potential. The laboratory standard for
absorption is that obtained after submerging dry aggregate for approximately 15 to 19
hours in water. Aggregates mined form below the water table may have a higher
absorption when used, if not allowed to dry. Conversely, some aggregates when
used may contain an amount of absorbed moisture less than the 15-hour soaked
condition. For an aggregate that has been in contact with water and that has free
moisture on the particle surfaces, the percentage of free moisture can be determined
by deducting the absorption form the total moisture content determined by ITP 255.
4.4 The general procedures described in this method are suitable for determining the
absorption of aggregates that have had conditioning other than the 15 to 19 hour
soak, such as boiling water or vacuum saturation. The values obtained for absorption
by other methods will be different than the values obtained by the prescribed 15 to 19
hour soak, as will the bulk specific gravity (SSD).
5 APPARATUS
5.1 Balance The balance shall have sufficient capacity, be readable to 0.1 percent of
the sample mass, or better, and conform to the requirements of AASHTO M 231. For
accurate SSD determination; a metal weigh pan should be utilized.
5.2 Sample Container A solid bucket of approximately equal breadth and height with a
capacity of approximately 366in3 (6000cm), or a wire mesh basket with No. 10
(2.0mm) mesh or smaller, may be used. The bucket/basket shall be constructed in a
way to prevent the trapping of air when the container is submerged. If using a bucket
when running Slag products the bucket shall be manufactured of copper.
5.3 Water Tank A watertight tank into which the sample and container are placed for
complete immersion while suspended below the balance equipped with an overflow
outlet for maintaining a constant water level.
5.4 Suspended Apparatus A nonabsorbent line of material (wire, fishing line, etc.) that
suspends the sample container such that the entire handle of the sample container is
below the surface of the water.
5.6 Oven An oven of sufficient size, specifically built for drying, capable of maintaining a
uniform temperature of 2309F (1105C). No other heat source for drying is
permitted.
6 SAMPLING
6.1 Field samples of coarse aggregate shall be taken according to ITP 2. Field sample
size shall meet the minimum requirements in the Illinois Specification 201.
6.2 Thoroughly mix the sample of aggregate and reduce it to the approximate quantity
needed using the applicable procedure in ITP 248. Reject all material passing a No.
8 (2.36mm) sieve by dry sieving. Steel and ACBF Slag shall be washed and dried
prior to testing.
6.3 The minimum mass of test sample to be used is given below. When testing
gradations that are two large to fit in the sample container, the sample may be split
into multiple samples. If multiple samples are tested the weights will be combined
prior to calculations.
7 PROCEDURE
7.1 When running slag products this method is further modified to require that all samples
be washed, dried, and weighed (for Original Weight) prior to testing using ITP 11.
Subsequently immerse the aggregate in water at room temperature for period of 15 to
19 hours.
7.2 Decant the water off the test sample. Thoroughly wash the sample in cool water to
remove dust or other coatings from the surface. Decant off excess water. Place
sample on large, absorbent cloth. Roll particles with a clean, dry towel until all visible
signs of water are removed. Take care to avoid evaporation of water from aggregate
pores during the operation of surface drying. Determine the mass of all test samples,
while in the saturated surface-dry condition, to the nearest 1 gram on a specified
balance or scale.
To check for an accurate surface dry condition, use the following method:
After obtaining the surface dry weight introduce the test sample into the sample
basket/bucket, do not immerse. Then immediately check the bottom of the weight
pan for the presence of water spots. If there are no spots present; the sample is too
dry and must be re-soaked for a minimum of 30 minutes. Then resume the process
of drying the test sample to surface dry condition.
If there is enough water present for the spots to run or streak the bottom of the weigh
pan, then the sample is too wet and must be spread back out on the absorbent cloth
and continue drying to obtain the surface dry condition.
7.3 After determining the mass, immediately place the saturated-surface-dry test sample
in the sample container and determine its mass in water at 733F (23.0 1.7C),
having a density of 620.1lb/ft3 (997 2 kg/m3). Take care to remove all entrapped air
before determining the mass by shaking the container while immersed.
7.4 Dry the test sample to a constant mass in a specified oven at a temperature of
2309F (1105C). After the test sample has been dried to constant mass and
cooled to room temperature determine the mass to the nearest 1 gram. Constant
mass is defined as the sample mass at which there has not been more than 0.5 gram
mass loss during 1 hour of drying. This should be verified occasionally.
8 CALCULATIONS
8.1.1 Bulk Specific Gravity Calculate the bulk specific gravity, as follows:
where:
8.1.2 Bulk Specific Gravity (Saturated-Surface-Dry) Calculate the bulk specific gravity, as
follows:
8.1.3 Apparent Specific Gravity Calculate the apparent specific gravity, as follows:
9 REPORT
1.1 Sampling. The material to be shipped should be sampled as the stockpile is being built.
Each sample shall be taken in random increments over each 1500 tons stockpiled.
1.2 Obtaining the Sample After the Stockpile Is Built. The sample shall be taken by shovel.
The sample shall be selected randomly from both the exterior and interior of the
stockpile. The producer must use the services of heavy equipment for the excavation of
interior material.
1.3 Sample Size and Sample Reduction. The field sample should be 80 to 100lbs. (35 to
45kg) in mass. From this field sample, a test sample of 20 to 25lbs. (9 to 11kg) shall be
quartered or mechanically split as detailed in Illinois Test Procedure 248.
1.4 Sampling Frequency. The sampling frequency shall be a minimum of one sample per
1500 tons of material with a five-sample minimum per stockpile.
1.5 Documentation. Stockpile location and test results shall be maintained at the plant and
shall be available to the Illinois Department of Transportation.
2.2.1 Prepare a test sample of approximately 20 to 25lbs. (9 to 11kg) from a field sample of
approximately 100lbs. (45kg).
2.2.2 The test sample should then be rinsed over a No. 4 (4.75mm) sieve to remove any fines
that may be clinging to the larger particles. If the material to be tested is a densely
graded material, eliminate this step.
2.2.3 Next, place the test sample in a bucket and fill the bucket with water until the sample is
covered by at least 1/2in. (12.5mm) of water. Allow the sample to soak for 24 hours.
2.2.4 After soaking for 24 hours, thoroughly mix the water and collect a water sample of
approximately 3.38oz. (100mL).
2.2.5 Filter the water sample to remove any suspended solids which may interfere with the
color observations.
(a) If the color of the filtered water is equal to or darker than the moderate greenish-
yellow color from the rock chart (HUE 10 Y), this material fails.
(b) If the water appears clear, allow the sample to soak another 24 hours and repeat
steps 2.2.4 and 2.2.5. If after 48 hours no color appears, the material is assumed
to have aged long enough to eliminate any leachate problems, and the sample is
acceptable.
1. SCOPE
1.1 This procedure covers the reduction of large samples of aggregate to the appropriate
size for testing, employing techniques that are intended to minimize variations in
measured characteristics between the test samples so selected and the large sample.
1.3 This standard does not purport to address all of the safety concerns, if any,
associated with its use. It is the responsibility of the user of this procedure to
establish appropriate safety and health practices and determine the applicability of
regulatory limitations prior to use.
2. REFERENCED DOCUMENTS
3. TERMINOLOGY
3.1 Definitions the terms used in this standard are defined in ASTM C 125.
4.1 Specifications for aggregates require sampling portions of the material for testing.
Other factors being equal, larger samples will tend to be more representative of the
total supply. The methods described in this standard provide for reducing the large
sample obtained in the field or produced in the laboratory to a convenient size for
conducting a number of tests to describe the material and measure its quality. These
methods are conducted in such a manner that the smaller test sample portion will be
representative of the larger sample and, thus, of the total supply. The individual test
methods provide for minimum masses of material to be tested.
4.2 Under certain circumstances, reduction in size of the large sample prior to testing is
not recommended. Substantial differences between the selected test samples
sometimes cannot be avoided, as for example, in the case of an aggregate having
relatively few large-sized particles in the sample. The laws of chance dictate that
these few particles may be unequally distributed among the reduced-size test
samples. Similarly, if the test sample is being examined for certain contaminants
occurring as a few discrete fragments in only small percentages, caution should be
used in interpreting results from the reduced-size test sample. Chance inclusion or
exclusion of only one or two particles in the selected test sample may importantly
influence interpretation of the characteristics of the original sample. In these cases,
the entire original sample should be tested.
4.3 Failure to carefully follow the procedures in these methods could result in providing a
non-representative sample to be used in subsequent testing. Selection during
splitting of an exact, predetermined mass for the sample is not permitted.
5. SELECTION OF METHOD
5.1 Fine Aggregate The preferred splitting method for fine aggregate shall be a fine
aggregate mechanical splitter (Method A). However, quartering (Method B) and
miniature stockpile sampling (Method C) may be used.
5.1.1 If the use of Method B or Method C is desired, and the sample does not have free
moisture on the particle surfaces, the sample may be moistened to achieve this
condition, thoroughly mixed, and then the sample reduction performed.
Note 1 As a quick approximation of free moisture; the fine aggregate will retain its
shape when molded in the hand, it may be considered to be wetter than saturated-
surface-dry.
5.1.2 If the use of Method A is desired and the sample has free moisture on the particle
surfaces, the entire sample may be dried to at least the surface-dry condition, using
temperatures that do not exceed those specified for any of the tests contemplated,
and then the sample reduction performed. Alternatively, if the moist sample is very
large, a preliminary split may be made using a mechanical splitter having wide chute
openings 1 1/2in. (37.5mm) or more to reduce the sample to not less than 5000g.
The portion so obtained is then dried, and reduction to test sample size is completed
using Method A.
5.2 Coarse Aggregate and Mixtures of Coarse and Fine Aggregate The required
splitting method for coarse aggregate and mixtures of coarse and fine aggregate shall
be a coarse aggregate mechanical splitter (Method A). However, quartering (Method
B) may be used for coarse aggregate moisture tests to proportion Portland cement
concrete, cement aggregate mixture II, and controlled low-strength material mixtures.
6. SAMPLING
7. APPARATUS
7.1 Sample Splitter Sample splitters shall have an even number of equal width chutes,
but not less than a total of eight for coarse aggregate, or 12 for fine aggregate, which
discharge alternatively to each side of the splitter. For coarse aggregate and mixed
aggregate the minimum width of the individual chutes shall be approximately 50
percent larger than the largest particles in the sample to be split (Note 2). For dry fine
aggregate in which the entire sample will pass the 3/8in. (9.5mm) sieve, the minimum
width of the individual chutes shall be at least 50 percent larger than the largest
particles in the sample and the maximum width shall be 3/4in. (19mm). The splitter
shall be equipped with two receptacles to hold the two halves of the sample following
splitting. It shall also be equipped with a hopper or straight-edged pan, which has a
width equal to or slightly less than the overall width of the assembly of chutes, by
which the sample may be fed at a controlled rate to the chutes. The splitter and
accessory equipment shall be so designed that the sample will flow smoothly without
restriction or loss of material (see Figure 1).
Note 2 Mechanical splitters are commonly available in sizes adequate for coarse
aggregate having the largest particles not larger than 1 1/2in. (37.5mm).
8. PROCEDURE
8.1 Place the original sample in the hopper or pan and uniformly distribute it from edge to
edge, so that when it is introduced in the chutes, approximately equal amounts will
flow through each chute. The rate at which the sample is introduced shall be such as
to allow free flowing through the chutes into the receptacles below. Reintroduce the
portion of the sample in one of the receptacles into the splitter as many times as
necessary to reduce the sample to the size specified for the intended test. The
portion of the material collected in the other receptacle may be reserved for reduction
in size for other tests.
On the final split, the mass of the two halves (after splitting) shall be within 10
percent of each other. This is determined by adding 10 percent of the mass of the
small split to the mass of the smaller split; the larger split cannot exceed this
calculated mass. If it does, both split halves shall be recombined and split until the
mass comparison requirement is met.
METHOD B QUARTERING
9. APPARATUS
10. PROCEDURE
10.1 Use either the procedure described in Section 10.1.1 or 10.1.2, or a combination of
both.
10.1.1 Mix the material thoroughly on a hard, clean, level surface by turning the entire
sample over four times using the shovel. Each shovel full shall be deposited on top of
the preceding one. This procedure shall be done three times, resulting in the
formation of a small conical pile. Carefully flatten the conical pile to a uniform
thickness and diameter by pressing down the apex with a shovel or trowel so that
each quarter sector of the resulting pile will contain the material originally in it. The
diameter should be approximately four to eight times the thickness. Divide the
flattened mass into four equal quarters with a shovel or trowel and remove two
diagonally opposite quarters, including all fine material, and brush the cleared spaces
clean. The two unused quarters may be set aside for later use or testing, if desired.
Successively mix and quarter the remaining material until the sample is reduced to
the desired size (see Figure 2).
Both halves of the final split shall meet the 10 percent comparison requirement in 8.1
herein.
10.1.2 As an alternative to the procedure in Section 10.1.1, the field sample may be placed
on a canvas blanket. Mixing may be accomplished by the shovel method listed in
10.1.1 herein or by alternately lifting each corner of the canvas and pulling over the
sample diagonally toward the opposite corner. This causes the material to be rolled
and mixed. The material shall then be flattened and divided as required in 10.1.1.
(see Figure 3) Both halves of the final split shall meet the 10 percent comparison
requirement in 8.1 herein.
11. APPARATUS
11.1 Apparatus shall consist of a straight-edge; straight-edged scoop, shovel, or trowel for
mixing the aggregate; and either a small thief, small scoop, or spoon for sampling
12. PROCEDURE
12.1 Mix the material thoroughly on a hard, clean, level surface as required in 10.1.1 or
10.1.2.
The test sample shall be obtained by selecting at least five increments in a random
X pattern over the resultant miniature sample pad using a sampling thief, small
scoop, or spoon. A sufficient number of increments shall be obtained to provide a test
sample slightly larger than the minimum test sample size when dried to a constant
mass. (see Figure 4)
For all samples from which a state monitor split will also be obtained, the number of
increments shall be doubled to provide a sample twice the minimum required test
size. This material shall then be dried to constant mass as specified in the current
ITP 11 and split in a fine aggregate mechanical splitter according to Method A
Mechanical Splitter. Alternately, the material may also be quartered according to
Method B Quartering.
Both halves of the final split shall meet the 10 percent comparison requirement in 8.1
herein.
1 SCOPE
1.1 This test procedure covers the determination of the percentage of evaporable
moisture in a sample of aggregate by drying both surface moisture and moisture in
the pores of the aggregate. Some aggregate may contain water that is chemically
combined with the minerals in the aggregate. Such water is not evaporable and is not
included in the percentage determined by this test method. Aggregate moisture
content may be run on a gradation sample prior to gradation testing or on a separate
test sample.
1.2 The values stated in SI units are to be regarded as the standard. The values in
parentheses are provided for information only.
1.3 This standard does not purport to address all of the safety concerns, if any,
associated with its use. It is the responsibility of the user of this procedure to
establish appropriate safety and health practices and determine the applicability of
regulatory limitations prior to use.
2 REFERENCED DOCUMENTS
3 TERMINOLOGY
3.1 Definitions:
3.2 For definitions of terms used in this test method, refer to ASTM C 125.
4.1 This test method is sufficiently accurate for usual purposes such as adjusting batch
quantities of ingredients for concrete. It will generally measure the moisture in the
test sample more reliably than the sample can be made to represent the aggregate
supply. In rare cases where aggregate itself is altered by heat, or where more refined
measurement is required, the test should be conducted using a ventilated, controlled-
temperature oven.
4.2 Large particles of coarse aggregate, especially those larger than 2in. (50mm), will
require greater time for the moisture to travel from the interior of the particle to the
surface. The user of this test method should determine by trial if rapid drying
methods provide sufficient accuracy for the intended use when drying large-size
particles.
5 APPARATUS
5.1 Balance The balance shall have sufficient capacity, be readable to 0.1 percent of
the sample mass, or better, and conform to the requirements of AASHTO M 231.
5.2.1 Where close control of the temperature is not required (see Section 4.1), other
suitable sources of heat may be used such as an electric or gas hot plate, electric
heat lamps, or a ventilated microwave oven. A microwave oven or an electric or gas
hot plate may be used only when drying a non-gradation test sample.
5.3 Sample Container A container not affected by the heat, and of sufficient volume to
contain the sample without danger of spilling, and of such shape that the depth of
sample will not exceed one-fifth of the least lateral dimension.
Note 1 Except for testing large samples, an ordinary frying pan is suitable for use
with a hot plate, or any shallow flat-bottomed metal pan.
6 SAMPLE
6.1 Sampling shall generally be accomplished in accordance with ITP 2, except the
sample size shall be as stated in Illinois Specification 201.
6.2 Field samples of aggregate shall be reduced to test sample size before testing
according to ITP 248.
7 PROCEDURE
7.1 The test sample shall have its mass determined to the nearest 1 gram for coarse
aggregate and to the nearest 0.1 gram for fine aggregate. This procedure provides
the Original Sample Mass, g (OSM).
7.2 The test sample shall be dried back to constant mass by the selected source of heat
as specified herein.
7.2.1 Caution When using a microwave oven, occasionally minerals are present in
aggregates that may cause material to overheat and explode. If this occurs, it can
damage the microwave oven. When a gas burner or electric hot plate is used for
drying, the technician shall continually attend the sample. The gas burner or electric
hot plate should be operated on a low-as-needed heat to prevent popping, crackling,
and/or sizzling noise from the aggregate during drying. If these noises occur, the heat
must be turned down and/or the sample must be constantly stirred during drying to
prevent potential aggregate particle breakdown.
7.3 Constant mass is defined as the sample at which there has not been more than a 0.5-
gram mass loss during a 1 hour of drying. This should be verified occasionally.
After the test sample has been dried to constant mass, the test sample shall have its
mass determined as soon as the pan or container can safely be handled to prevent
additional moisture from being pulled from the air into the aggregate structure.
7.4 Determine the mass of the test sample to the nearest 1 gram for coarse aggregate
and to the nearest 0.1 gram for fine aggregate. .
This procedure provides the Total Dry Mass, g (TDM). The TDM will also be used
for calculation of gradation samples.
8 CALCULATION
8.1 The Aggregate Moisture Content shall be determined by using the following formula:
where:
and:
Test results shall be rounded to the nearest 0.1 percent. All rounding shall be
according to ASTM E 29 (Illinois Modified)
8.2 Surface moisture content is equal to the difference between the total evaporable
moisture content and the absorption, with all values based on the mass of a dry
sample. Absorption may be determined in accordance with ITP 85, Test for Specific
Gravity and Absorption of Coarse Aggregate, or ITP 84, Test for Specific Gravity and
Absorption of Fine Aggregate.
4. Illinois Test Procedure 84, Specific Gravity and Absorption of Fine Aggregate
6. ASTM E 29 (Illinois Modified), Standard Practice for Using Significant Digits in Test Data to
Determine Conformance with Specifications
1. GENERAL
This Illinois Test procedure was developed to replace AASHTO T 142, Surface Moisture
in Fine Aggregate, which was AASHTO discontinued. The equivalent ASTM
designation is C 70. The test is a convenient procedure for field determination of free
moisture (surface moisture) of fine aggregate, if specific gravity values are known.
The accuracy of the test procedure depends upon accurate information on the bulk
specific gravity of the material in a saturated surface-dry condition.
2. EQUIPMENT
a. Balance The balance or scale shall conform to M 231 and Illinois Specification 101.
Select a representative sample of the fine aggregate to be tested for free moisture
content. The sample shall be obtained according to ITP 2 and ITP 248. Protect the
sample from moisture loss until weighing. The test sample shall have a minimum mass
of 200 grams. However, larger test samples will yield more accurate results. If a
Chapman Flask is used, as described in Section 5, then a 500 gram test sample shall be
required.
The free moisture content may be determined either by mass or by volume. In each
case, the test shall be performed at a temperature range of 18 to 29 C (65 to 85 F).
a. Determination by MassDetermine the mass of the container filled with water to the
known volume mark. Before placing the test sample into the container, reduce the
water level to prevent the water from going over the mark when the test sample is
added. Introduce the test sample into the container, and remove entrapped air.
Refill the container to the mark, and determine the mass of the container and test
sample. Calculate the amount of water displaced by the test sample as follows:
V S = WC + WS W
When a graduated flask is used, determine the combined volume of the test sample
and the water by direct reading. When a pycnometer or volumetric flask of known
volume is used, fill the container to the known volume mark with an additional
measured volume of water. The flask or pycnometer volume is then equal to the
combined volume of the test sample and water. Calculate the amount of water
displaced by the test sample as follows:
VS = V2 V1
Where:
VD = Mass of Test Sample, nearest 1 gram, Divided by the Bulk Specific Gravity
of the Fine Aggregate in a Saturated Surface-Dry Condition, nearest 0.01,
Determined According to ITP 84.
PA
PD = P (1 + )
100
Where:
Total moisture content, on a dry aggregate basis, is the sum of the free moisture, PD,
and the absorption, PA.
The Chapman Flask is graduated as discussed in Section 3b. The Chapman Flask can
be used to determine the percent of free moisture (surface moisture) of fine aggregate.
For example, assume a fine aggregate with a known saturated surface-dry specific
gravity (GS) of 2.62. The Chapman Flask is filled with water to the 200 ml line, which is
located between the two bulbs of the flask. A 500 gram test sample of fine aggregate is
then poured into the flask, and agitated to remove any entrapped air. The flask is then
placed on a level surface, and the water level is read on the neck of the flask. For this
example, assume a final reading (V) of 400 ml. The percent free moisture, P, is
calculated to the nearest 0.1 percent as follows:
500
V 200
GS
P= 100
700 V
500
400 200
P= 2.62 100
700 400
P = 3.1 percent
The percent of free moisture can also be determined from the following tables using the
above formula. Using the values from the previous example, enter the table at the final
reading from the flask (e.g. V = 400 ml), read horizontally to the specific gravity column
desired (e.g. GS = 2.62), and read the percent moisture directly as 3.1 percent.
READING GS GS GS GS GS GS GS GS GS GS GS GS GS
FROM
FLASK 2.70 2.69 2.68 2.67 2.66 2.65 2.64 2.63 2.62 2.61 2.60 2.59 2.58
391 1.9 1.7 1.4 1.2 1.0 0.8 0.5 0.3 0.1 0.0 0.0 0.0 0.0
392 2.2 2.0 1.8 1.5 1.3 1.1 0.8 0.6 0.4 0.1 0.0 0.0 0.0
393 2.5 2.3 2.1 1.9 1.6 1.4 1.2 0.9 0.7 0.5 0.2 0.0 0.0
394 2.9 2.7 2.4 2.2 2.0 1.7 1.5 1.3 1.0 0.8 0.6 0.3 0.0
395 3.2 3.0 2.8 2.5 2.3 2.1 1.8 1.6 1.4 1.1 0.9 0.6 0.4
396 3.6 3.3 3.1 2.9 2.6 2.4 2.2 1.9 1.7 1.5 1.2 1.0 0.7
397 3.9 3.7 3.4 3.2 3.0 2.7 2.5 2.3 2.0 1.8 1.5 1.3 1.1
398 4.2 4.0 3.8 3.5 3.3 3.1 2.8 2.6 2.4 2.1 1.9 1.6 1.4
399 4.6 4.4 4.1 3.9 3.7 3.4 3.2 3.0 2.7 2.5 2.2 2.0 1.7
400 4.9 4.7 4.5 4.2 4.0 3.8 3.3 3.3 3.1 2.8 2.6 2.3 2.1
401 5.3 5.1 4.8 4.6 4.4 4.1 3.7 3.7 3.4 3.2 2.9 2.7 2.4
402 5.6 5.4 5.2 4.9 4.7 4.5 4.0 4.0 3.7 3.5 3.3 3.0 2.8
READING GS GS GS GS GS GS GS GS GS GS GS GS GS
FROM
FLASK 2.70 2.69 2.68 2.67 2.66 2.65 2.64 2.63 2.62 2.61 2.60 2.59 2.58
403 6.0 5.8 5.5 5.3 5.1 4.8 4.6 4.3 4.1 3.8 3.6 3.4 3.1
404 6.4 6.1 5.9 5.7 5.4 5.0 4.9 4.7 4.4 4.2 4.0 3.7 3.5
405 6.7 6.5 6.2 6.0 5.8 5.5 5.3 5.1 4.8 4.6 4.3 4.1 3.8
406 7.1 6.8 6.6 6.4 6.1 5.9 5.6 5.4 5.2 4.9 4.7 4.4 4.1
407 7.4 7.2 7.0 6.7 6.5 6.3 6.0 5.8 5.5 5.3 5.0 4.8 4.5
408 7.8 7.6 7.3 7.1 6.9 6.6 6.4 6.1 5.9 5.6 5.4 5.1 4.9
409 8.2 7.9 7.7 7.5 7.2 7.0 6.7 6.5 6.2 6.0 5.7 5.5 5.2
410 8.6 8.3 8.1 7.8 7.6 7.4 7.1 6.9 6.6 6.4 6.1 5.8 5.6
411 8.9 8.7 8.4 8.2 8.0 7.7 7.5 7.2 7.0 6.7 6.5 6.2 6.0
412 9.3 9.1 8.8 8.6 8.3 8.1 7.8 7.6 7.3 7.1 6.8 6.6 6.3
413 9.7 9.4 9.2 9.0 8.7 8.5 8.2 8.0 7.7 7.5 7.2 7.0 6.7
4. Illinois Test Procedure 84, Specific Gravity and Absorption of Fine Aggregate
5. Illinois Test Procedure 85, Specific Gravity and Absorption of Coarse Aggregate
7. ASTM E 29 (Illinois Modified), Standard Practice for Using Significant Digits in Test Data
to Determine Conformance with Specifications
1. GENERAL
2. EQUIPMENT
a. Electronic Balance The electronic balance shall conform to M 231 and Illinois
Specification 101. The electronic balance shall have a weight below hook.
b. Tank The tank shall be made of non-corrosive material, and shall have an overflow
spout. The tank shall be of sufficient size for the pail. The pail shall not touch the
bottom or sides of the tank when submerged in the water held by the tank.
January 1, 2015 Manual of Test Procedures for Materials 71
c. Pail The pail shall be made of non-corrosive material, and shall be of sufficient size
to hold the aggregate sample.
d. Stand The stand shall be able to support the weighing operation. To allow for the
balances weigh below hook, a hole is required in the center of the stand. The stand
shall have sufficient height to easily remove the submerged pail from the tank.
The equipment is set up as illustrated in Figure 1. Fill tank A with water up to the
overflow spout B. The empty pail C is immersed in water and suspended from the
balance. Place a clean, dry scoop D on the right hand scale pan and adjust the
scales to balance. To perform the initial balance, it may be necessary to add
washers on the left hanger E to act as counterweights. Thereafter, the final
adjustment may be performed with the calibration screw on the balance.
Remove the pail from the tank. Partially fill the pail with water taken from the tank,
and slowly pour the sample into the pail. Pouring the sample into the water will
prevent the entrapping of air with the sample. The submerged sample shall be
stirred to dislodge entrapped air. If material clings to the inside of the scoop, place
the scoop in the mouth of the pail and rinse with the water. Then slowly immerse the
pail obliquely into the tank, allowing water to flow slowly over one side of the pail.
This immersion should be done carefully to prevent materiel from washing out of the
pail. Suspend the pail from the end of the left hanger. If necessary, add water to the
tank to bring the water level up to the overflow spout. Permit any excess water to
overflow. Obtain the immersed mass, by placing weights in the scoop and adjusting
the rider.
Fill the tank with water up to the overflow spout. The empty pail is immersed in
water, and suspended from the end of the electronic balance weigh below hook.
Tare the electronic balance.
Remove the pail from the tank. Partially fill the pail with water taken from the tank,
and slowly pour the sample into the pail. Pouring the sample into the water will
prevent the entrapping of air with the sample. The submerged sample shall be
stirred to dislodge entrapped air. If material clings to the inside of the scoop, place
the scoop in the mouth of the pail and rinse with the water. Then slowly immerse the
pail obliquely into the tank, allowing water to flow slowly over one side of the pail.
This immersion should be done carefully to prevent material from washing out of the
pail. Suspend the pail from the end of the electronic balance weigh below hook. If
necessary, add water to the tank to bring the water level up to the overflow spout.
Permit any excess water to overflow. Obtain the immersed mass.
The equipment is set up as illustrated in Figure 2. Be advised that the pans are not
interchangeable, and should be marked L and S respectively. L designates the
pan for the long stirrup, and S is the pan which has been balanced for the short
stirrup.
Place a clean, dry scoop D on the left hand scale pan and adjust the scales to
balance evenly. To perform the initial balance, it may be necessary to use a
counterweight constructed from a can and shot. Thereafter, the final adjustment may
be performed with the calibration screw on the balance.
Place the sample in the scoop. Determine the sample mass by placing weights in
the short stirrup pan, and adjusting the rider. The scale can measure to the nearest
0.1 gram.
Measure approximately 3,000 grams of coarse aggregate sample per Section A.4.
Soak the sample in water for 24 hours. Surface-dry the sample to a saturated
condition according to ITP 85.
Determine the mass of the immersed test sample to the nearest 1 gram per Section
A.3. This mass will be designated W for the test sample.
Or per Figure 3, which is the simpler method to use. To determine GS from Figure 3:
Project this point horizontally until it intersects the vertical line of zero free
moisture, and determine the specific gravity, GS, by interpolation, to the
nearest 0.01.
To determine the specific gravity of saturated surface-dry fine aggregate, the test is
identical to coarse aggregate, except as follows:
After soaking, spread a sample of 2,300 grams or more on a flat surface, and air dry
until the surface moisture has evaporated. Do not heat the sample to speed the
process. The saturated surface-dry condition is reached when the material will roll
freely from a scoop or trowel without sticking.
Calculate the saturated surface-dry specific gravity of the fine aggregate as follows:
1000
GS =
1000 W
1. GENERAL
This test will determine whether the aggregate has free moisture or will absorb moisture.
The test is based upon a given sample of material (not in the saturated surface-dry
condition) which will measure, when immersed in water, less or more than a sample of
the same mass of material in the saturated surface-dry condition. This depends upon
whether it contains free moisture or will absorb moisture.
To determine the free moisture or absorption of a sample of coarse aggregate, the test is
conducted in the following manner:
Determine the mass of the immersed test sample to the nearest 1 gram. The
immersed mass is obtained as per Section A.3., except the test sample shall remain
in the pail for 10 minutes. This mass will be designated W1 for the test sample.
If W1 is less than the W determined per Section A.5, the aggregate contains free
moisture; if W1 is greater than W, the aggregate will absorb moisture. The
percentage of free moisture or absorption is determined by one of the following
formulae:
0.05G S (W W1 )
If W1 < W: Free Moisture (percent) =
GS 1
0.05G S (W W1 )
If W1 > W: Absorption (percent) =
0.8G S 1
The factor, 0.8, is based on the assumption that the sample will become 80%
saturated in 10 minutes.
The simpler method is to use Figure 3 and the immersed mass (submerged weight)
W1. To determine the moisture content from Figure 3:
Project this point horizontally, until it intersects the line corresponding to the
specific gravity of the aggregate, GS.
Project this point of intersection vertically and read the percentage of free
moisture or absorption from the scale, at the bottom of the chart to the
nearest 0.1. The value is interpolated.
As an example: Suppose GS for the test sample is 2.56, and W1 is 1,170 grams.
The vertical projection of the point of intersection of the line (representing these
values) shows a free moisture content of approximately 4.0 percent.
To determine the free moisture or absorption of fine aggregate the test is identical to
coarse aggregate. However, measure a 1,000 gram test sample and use one of the
following formulae:
0.1G S (W W1 )
If W1 < W: Free Moisture (percent) =
GS 1
0.1G S (W W1 )
If W1 > W: Absorption (percent) =
0.8G S 1
Again, the simpler method is to use Figure 3 for a 1,000 gram test sample.
5. ASTM E 29 (Illinois Modified), Standard Practice for Using Significant Digits in Test Data to
Determine Conformance with Specifications
1. GENERAL
This Illinois Test procedure has been used for many years by District 2 (Dixon), but the
District is uncertain as to the origin of the test. However, this test is similar to a test
procedure used by the Iowa Department of Transportation. The test is a convenient
procedure for field determination of free moisture (surface moisture) of fine or coarse
aggregate, if specific gravity values are known.
The accuracy of the test procedure depends upon accurate information on the bulk
specific gravity of the material in a saturated surface-dry condition.
2. EQUIPMENT
a. Balance The balance or scale shall conform to AASHTO M 231 and Illinois
Specification 101.
b. Pycnometer A glass jar, gasket, and conical pycnometer top. A 0.946 L (1 qt.) jar
is used for fine aggregate, and a 1.892 L (2 qt.) jar is used for coarse aggregate.
Typically, a canning jar is used.
3. MATERIALS
a. Potable Water
c. Aggregate Sample
4. PROCEDURE
Select a representative sample of the fine or coarse aggregate to be tested for free
moisture content. The sample shall be obtained according to ITP 2 and ITP 248.
Protect the sample from moisture loss until weighing.
Apply a light coat of grease to the side of the gasket which will be in contact with
the glass jar.
Place a mark on the pycnometer top and glass jar to indicate the position of the
tightened top. Always tighten the pycnometer top to this position. If the
pycnometer top is ever tightened beyond the mark on the glass jar, re-mark the
top of the jar.
Fill the glass jar nearly full of water and screw on the pycnometer top. Finish
filling the pycnometer by pouring water until a bead of water appears above the
tops opening.
Wipe off all exterior water on the pycnometer, and then weigh to the nearest
1 gram. Record the value as M1.
Use the funnel to pour the aggregate sample into the glass jar. The jar shall
contain approximately 50 mm (2 in.) of water.
Fill the glass jar nearly full of water, and screw on the pycnometer top to the
marked position. The water temperature shall be within 1.7 C (3 F) of the
water used for calibrating the pycnometer. Finish filling the pycnometer.
January 1, 2015 Manual of Test Procedures for Materials 80
Place a finger over the pycnometer top opening, and gently roll and shake the
pycnometer several times to remove entrapped air in the aggregate sample.
When further rolling and shaking brings no more air bubbles to the top, finish
filling the pycnometer. The pycnometer is filled when a bead of water appears
above the tops opening.
Wipe off all exterior water on the pycnometer, and then weigh to the nearest
1 gram. Record the value as M2.
5. CALCULATION
VS = M1 + MS M2
Where:
b. Moisture Content
Calculate moisture content to the nearest 0.1 percent using the following
equations:
VS (1000 G S )
Fine Aggregate Free Moisture (percent) = 100
1000 VS
VS (2000 G S )
Coarse Aggregate Free Moisture (percent) = 100
2000 VS
Where:
Date: (mm/dd/yyyy)
Producer No.:
Producer Name:
Location:
Coarse Fine
Aggregate Aggregate
7. Difference, g .................................................................................................
Line 6 - Line 3
Vs (2000 )
Coarse Aggregate Surface Moisture, P =
Gs
100
2000 Vs
Vs (1000 )
Fine Aggregate Surface Moisture, P =
Gs
100
1000 Vs
1. American Concrete Institute Manual of Concrete Practice ACI 503R-93, (Reapproved 1998),
Appendix A (Test Methods).
2. Virginia Test Method for Testing Epoxy Concrete Overlays for Surface Preparation and Adhesion,
VTM-92.
3. ASTM C 1583/C 1583M-04, Standard Test Method for Tensile Strength of Concrete Surfaces and the
Bond Strength or Tensile Strength of Concrete Repair and Overlay Materials by Direct Tension (Pull-
off Method)
1. GENERAL
This test method outlines the procedure for determining the surface preparation quality of an existing
concrete surface that is to be overlaid.
2. EQUIPMENT
a. Pull-off testing device with sufficient capacity and capable of applying load at the specified rate,
g. Gloves, heat-resistant,
h. Gloves, solvent-resistant.
3. MATERIALS
a. Rapid-curing epoxy compound with a working (pot) life of 3 to 10 minutes. Pot life is the time
after mixing during which the epoxy retains sufficient workability for proper use.
b. Cleaning solvent.
a. After all cleaning has been performed in preparation for overlay placement, determine test
locations. If random sample locations for testing are required, determine according to the
Departments Method for Obtaining Random Samples for Concrete. Test locations shall be
adjusted a maximum of 0.3 m (12 inches) when they are too close to a joint, parapet, or other
obstruction, or when they are over a patch or other area that has not been mechanically scarified.
The center-to-center distance of adjacent test specimens shall be a minimum of two disk
diameters. If the concrete contains reinforcement, do not test at locations where the concrete
cover is less than 20 mm ( in.). A cover meter (pachometer) or other methods may be used to
locate reinforcement and verify the concrete cover.
b. Using a marker, mark a circle at each location using a pull-off cap as a template.
c. The test area must be thoroughly dry. No additional cleaning or surface preparation should be
performed at the test locations. A small propane torch may be used to dry an area to be tested.
Heating the surface to a temperature exceeding 50 C (120 F) may damage the surface and
result in a lower pull-off strength. Allow the surface to cool to ambient temperature before testing.
d. Mix the epoxy according to the manufacturers instructions. Place a thin layer of epoxy within the
marked area on the deck surface and on the bottom of the cap. Carefully center the cap within
the marked circle. Twist and lightly press the cap to ensure that there are no gaps between the
cap and the epoxy-covered test area. Wipe off excess epoxy around the cap.
e. Allow the epoxy to set in accordance with the manufacturers instructions. As an option when air
temperature is below 15 C (60 F), a small propane torch may be used to heat the top of the cap
for very short intervals. The temperature of the cap should not exceed 50 C (120 F). Allow the
cap to cool to air temperature before testing.
f. If the area immediately surrounding the cap is subjected to moisture (i.e. rain) after the cap has
been attached to the test area, the area must be allowed to dry before conducting the test.
Moisture can significantly reduce the tensile (pull-off) strength.
g. Attach the pull-off test equipment to the cap. Follow the manufacturers instructions. Use a
loading rate of 35 14 kPa per second (5 2 psi per second).
Failure of Epoxy Epoxy pulled away from either the cap or the surface of the concrete.
Failure of Concrete Surface Failure within 6 mm ( inch) of the top surface of the concrete. At
least 90 percent of the failure surface consists of concrete.
Failure of Underlying Concrete Failure plane is greater than 6 mm (1/4 inch) below the surface
of the concrete.
i. If the mode of failure is Failure of Epoxy or Failure of Underlying Concrete, then repeat the
test at a location at least 0.15 m (6 inch), and not more than 0.6 m (2 feet), from the previous
test. However, if the mode of failure is Failure of the Epoxy or Failure of Underlying Concrete
and the tensile (pull-off) strength is greater than the specification requirement, repeating the test
is not necessary.
k. Measure the diameter of the failed concrete surface at four evenly spaced locations around the
circumference. Average the four measurements and record as the average diameter in
millimeters (inches) to the nearest 3 mm (1/8 inch).
a. After performing a pull-off test, pull-off caps shall be cleaned properly to ensure that epoxy can
bond adequately to their surface. Cap cleaning should be performed in a well ventilated area.
b. Place the cap on a heat-resistant, non-flammable surface. Verify with the epoxy and equipment
manufacturer that a small propane torch may be used. Using the propane torch, direct the flame
on the concrete/epoxy material to be removed until the epoxy becomes pliable. Use a putty knife
to remove as much of the epoxy and concrete as possible. Warning: The use of a propane
torch to remove the epoxy from the pull-off cap may generate hazardous fumes.
c. Allow the cap to cool to room temperature (approximately 77 F) or immerse the cap in water.
Clean the cap according to instructions provided by the epoxy manufacturer, using the solvent
they recommend. The following procedure is for when acetone may be used.
d. Read and follow the label on the acetone container, which provides instructions and cautions.
Read and follow the Material Safety Data Sheet (MSDS) for acetone safety, handling, and
disposal. Warning: Acetone is extremely flammable and vapors are harmful.
e. Fill a clean metal gallon can with enough acetone to cover the caps.
f. Place a lid on the container loosely, and protect the container from tipping. Keep the container at
room temperature (approximately 77 F) and in a well ventilated area. Warning: Resident
Engineers field office is not appropriate for this step.
g. Soak the caps for 8-24 hours. The longer the soaking period, the easier the cleaning.
h. Remove the caps and clean the grooves carefully using a sharp, pointed object.
i. Once the majority of the epoxy has been removed, take a small amount of acetone and a clean
rag and wipe the surface clean. The acetone will air dry and leave no oily residue.
j. The acetone can be reused. Discontinue use and properly dispose of the acetone when it
becomes contaminated and no longer cleans effectively.
l. New pull-off caps will require cleaning with acetone. Even a small amount of oil or residue will
prevent the epoxy from bonding to the cap.
m. Disclaimer: The cleaning procedure for pull-off caps is provided as an aid for field personnel. In
all cases, field personnel are responsible for contacting the epoxy and equipment manufacturers
to determine the best method for cleaning pull-off caps.
Calculate the tensile (pull-off) strength of the concrete surface as follows, to the nearest 10 kPa (1
psi).
L
T=
(D )2
4
Where: T = tensile strength, kPa
L = load at failure, kN
= 3.1416
D = diameter, meters
L L
T= or simplified, T= 1.273
(D ) 2
D2
4
Where: T = tensile strength, psi
L = load at failure, lbs.
= 3.1416
D = diameter, inches
7. REPORT
a. Date of final cleaning of the concrete surface, and date of pull-off testing,
b. Type of equipment used for final cleaning of the concrete surface (i.e. shotblasting, high-pressure
water blasting, abrasive blasting).
e. Individual load, average diameter of failed concrete surface, and tensile strength for each
individual test.
f. Mode of failure.
8. CALIBRATION
The pull-off testing device shall be calibrated on an annual basis according to the manufacturers
recommended procedure or a procedure approved by the Department. A calibration log shall be
maintained and kept with the equipment.
1. American Concrete Institute Manual of Concrete Practice ACI 503R-93, (Reapproved 1998),
Appendix A (Test Methods).
2. Virginia Test Method for Testing Epoxy Concrete Overlays for Surface Preparation and Adhesion,
VTM-92.
3. ASTM C 1583/C 1583M-04, Standard Test Method for Tensile Strength of Concrete Surfaces and the
Bond Strength or Tensile Strength of Concrete Repair and Overlay Materials by Direct Tension (Pull-
off Method)
2. GENERAL
This test method outlines the procedure for determining the bond strength of a portland cement
concrete or thin polymer overlay.
3. EQUIPMENT
a. Coring equipment,
b. Pull-off testing device with sufficient capacity and capable of applying load at the specified rate,
d. Wire brush,
i. Gloves, heat-resistant,
j. Gloves, solvent-resistant.
3. MATERIALS
b. Cleaning solvent.
a. Determine test locations. If random sample locations for testing are required, determine
according to the Departments Method for Obtaining Random Samples for Concrete. Test
locations shall be adjusted a maximum of 0.3 m (12 inches) when they are too close to a joint,
parapet, or other obstruction, or when they are over a patch or other area that has not been
mechanically scarified. The center-to-center distance of adjacent test specimens shall be a
minimum of two disk diameters. If the concrete contains reinforcement, do not test at locations
where the concrete cover is less than 20 mm ( in.). A cover meter (pachometer) or other
methods may be used to locate reinforcement and verify the concrete cover.
b. Using a marker, mark a circle at each location using a pull-off cap as a template.
c. Core completely through the overlay and at least 13 mm (1/2 inch) into the underlying concrete.
d. The top of the intact core must be thoroughly dry. A small propane torch may be used to dry an
area to be tested. Heating the surface to a temperature exceeding 50 C (120 F) may damage
the surface and result in a lower pull-off strength. Allow the surface to cool to air temperature
before testing.
e. Carefully clean the surface of the core with a wire brush to remove any debris or film left from the
coring operations.
f. Mix the epoxy according to manufacturers instructions. Place a thin layer of epoxy on both the
top of the core and the bottom of the cap. Carefully center the cap. Twist and lightly press the
cap to ensure that are no gaps between the cap and the epoxy-covered core. Wipe off excess
epoxy around the cap. Do not allow the epoxy to run down the side of the core into the annular
cut.
g. Allow the epoxy to set in accordance with the manufacturers instructions. As an option when air
temperature is below 15 C (60 F), a small propane torch may be used to heat the top of the cap
for very short intervals. The temperature of the cap should not exceed 50 C (120 F). Allow the
cap to cool to air temperature before testing.
h. Attach the pull-off test equipment to the cap. Follow the manufacturers instructions. Use a
loading rate of 35 14 kPa per second (5 2 psi per second).
Failure of Epoxy Epoxy pulled away from either the cap or the surface of the overlay.
Failure of Overlay Surface Failure within 6 mm (1/4 inch) of the top surface of the overlay.
Failure in Overlay Failure plane is deeper than 6 mm (1/4 in.) below the top surface of the
overlay and above the bond line between the overlay and underlying concrete.
Failure at Bond Line Failure plane is at the bond line between the overlay and underlying
concrete. The bottom of the overlay is covered with less than 50 percent (by area) of material
from the underlying concrete.
Failure of Underlying Concrete Surface Failure plane is just below the bond line. The bottom of
the overlay is covered with at least 50 percent (by area) of material from the underlying concrete.
The layer is less than 6 mm (1/4 inch) thick.
Failure of Underlying Concrete Failure plane is greater than 6 mm (1/4 inch) below the bond
line.
j. If the mode of failure is Failure of Epoxy, Failure of Overlay Surface, Failure in Overlay, of
Failure of Underlying Concrete, then repeat the test at a location at least 0.15 m (6 inch), and
not more than 0.6 m (2 feet), from the previous test. However, if the mode of failure is Failure of
l. Measure the diameter at four evenly spaced locations around the circumference of the core.
Average the four measurements and record as the average diameter in millimeters (inches) to the
nearest
3 mm ( 1/8 inch).
m. Measure the length of the core and record in millimeters (inches) to the nearest 3 mm (1/8 inch).
a. After performing a pull-off test, pull-off caps shall be cleaned properly to ensure that epoxy can
bond adequately to their surface. Cap cleaning should be performed in a well ventilated area.
b. Place the cap on a heat-resistant, non-flammable surface. Verify with the epoxy and equipment
manufacturer that a small propane torch may be used. Using the propane torch, direct the flame
on the concrete/epoxy material to be removed until the epoxy becomes pliable. Use a putty knife
to remove as much of the epoxy and concrete as possible. Warning: The use of a propane
torch to remove the epoxy from the pull-off cap may generate hazardous fumes.
c. Allow the cap to cool to room temperature (approximate 77 F) or immerse the cap in water.
Clean the cap according to instructions provided by the epoxy manufacturer, using the solvent
they recommend. The following procedure is for when acetone may be used.
d. Read and follow the label on the acetone container, which provides instructions and cautions.
Read and follow the Material Safety Data Sheet (MSDS) for acetone safety, handling, and
disposal. Warning: Acetone is extremely flammable and vapors are harmful.
e. Fill a clean metal gallon can with enough acetone to cover the caps.
f. Place a lid on the container loosely, and protect the container from tipping. Keep the container at
room temperature (approximately 77 F) and in a well ventilated area. Warning: Resident
Engineers field office is not appropriate for this step.
g. Soak the caps for 8-24 hours. The longer the soaking period, the easier the cleaning.
h. Remove the caps and clean the grooves carefully using a sharp, pointed object.
i. Once the majority of the epoxy has been removed, take a small amount of acetone and a clean
rag and wipe the surface clean. The acetone will air dry and leave no oily residue.
j. The acetone can be reused. Discontinue use and properly dispose of the acetone when it
becomes contaminated and no longer cleans effectively.
l. New pull-off caps will require cleaning with acetone. Even a small amount of oil or residue will
prevent the epoxy from bonding to the cap.
m. Disclaimer: The cleaning procedure for pull-off caps is provided as an aid for field personnel. In
all cases, field personnel are responsible for contacting the epoxy and equipment manufacturers
to determine the best method for cleaning pull-off caps.
Calculate the tensile (pull-off) strength of the overlay as follows, to the nearest 10 kPa (1 psi):
L
T=
( D) 2
4
Where: T = tensile strength, kPa
L = load at failure, kN
= 3.1416
D = diameter, meters
L L
T= or simplified, T= 1.273
( D) 2 D2
4
7. REPORT
b. Type of equipment used for final cleaning of the concrete surface (i.e. shotblasting, high-pressure
water blasting, abrasive blasting),
d. Individual load, average diameter of failed specimen at failure plane, and tensile strength for each
individual test.
e. Mode of failure.
8. CALIBRATION
The pull-off testing device shall be calibrated on an annual basis according to the manufacturers
recommended procedure or a procedure approved by the Department. A calibration log shall be
maintained and kept with the equipment.
4. ASTM E 29 (Illinois Modified), Standard Practice for Using Significant Digits in Test Data
to Determine Conformance with Specifications
1. GENERAL
The volume of voids per unit volume of dry rodded coarse aggregate relates experimental
data to the theory of proportioning, which produces the amount of coarse aggregate needed
in a concrete mixture. Voids may also be defined as the ratio of the volume of empty
spaces in a unit volume of dry rodded coarse aggregate to the unit volume of dry rodded
coarse aggregate.
2. EQUIPMENT
k. The measure shall be metal, cylindrical, watertight, and of sufficient rigidity to retain its
form under rough usage. The top and bottom of the measure shall be true and even,
and its sides should be provided with handles. The measure shall have a capacity of
0.014 or 0.028 m3 (0.5 or 1.0 ft3).
l. Tamping RodA round, straight steel rod 16 mm (5/8 in.) in diameter and at least 584
mm (23 in.) in length, having the tamping end or both ends rounded to a hemispherical
tip the diameter of which is 16 mm (5/8 in.).
m. The balance or scale shall conform to M 231 and Illinois Specification 101. Refer to the
requirements for unit weight.
3. PROCEDURE
n. Fill the measure with water at room temperature and cover with a piece of plate glass in
such a way as to eliminate bubbles and excess water. The measure shall be calibrated
by accurately determining the mass (weight) of water, to the nearest 0.05 kg (0.1 lb.),
required to fill it. Calculate the Measure Volume according to Section 5.0.
p. The measure shall be filled in three equal lifts. Level each lift with the fingers. Each
layer shall be rodded 25 times when the measures capacity is 0.014 m3 (0.5 ft3) or 50
times when the measures capacity is 0.028 m3 (1.0 ft3).
Rodding shall be evenly distributed over the surface of the aggregate. The rodding
should knead the layers together by the tamping rod extending slightly into the previous
layer. Care shall be taken to rod immediately above the bottom of the measure without
striking it.
q. With the final layer, the measure shall be filled to overflowing, rodded, and the surplus
aggregate struck off, using the tamping rod as a straightedge.
r. The Net Mass (Weight) of the aggregate in the measure shall then be determined to the
nearest 0.05 kg (0.1 lb.).
4. CALCULATIONS
a. The Unit Weight of the coarse aggregate is the Net Mass (Weight) of the coarse aggregate in
the measure divided by the Measure Volume. Determine the Unit Weight to the nearest
0.01 kg/m3 (0.01 lb/ft3).
b. The volume of voids per unit volume of oven-dry rodded coarse aggregate is calculated
to the nearest 0.01 as follows:
Metric:
(Ga 1000.00) Unit Wt.
Voids, V =
Ga 1000.00
English:
(Ga 62.37) Unit Wt.
Voids, V =
Ga 62.37
Gs
Ga =
A
1 +
100
Where: Unit Wt. is the unit weight of the coarse aggregate
Ga is the oven-dry specific gravity calculated to the nearest 0.01
Gs is the saturated surface-dry specific gravity of the coarse aggregate
to the nearest 0.01, which is obtained from the Departments District
office.
A is the percent absorption of the coarse aggregate to the nearest 0.1,
which is obtained from the Departments District office.
a b c
WAGa = ( x A) + ( x B) + ( x C) +
100 100 100
The weighted average of the oven-dry specific gravity shall then be used in the Voids
formula.
c. The test shall be performed at least twice. Test results with the same measure should
check within 0.01.
5. CALIBRATION OF MEASURE
The Measure Volume is calculated to the nearest 0.01 m3 (0.001 ft3) as follows:
M
Measure Volume =
W
Where: M = mass (weight) of water required to fill measure, kg (lb.)
W = unit weight of water (refer to Table 1), kg/m3 (lb/ft3)
I. SAMPLING OF CLSM
Sampling freshly mixed controlled low-strength material (CLSM) shall be performed according to
Illinois Modified AASHTO R 60, except the elapsed time for obtaining the composite sample shall not
exceed two minutes. The flow test shall start within five minutes of obtaining the composite sample.
The molding of strength test specimens shall start within ten minutes of obtaining the composite
sample. The sample is to be routinely mixed during the testing process because CLSM may
segregate.
The flow test shall consist of filling a 76 mm (3 in.) inside diameter by 152 mm (6 in.) long plastic
cylinder. The maximum variation from the normal inside diameter and length shall be 3 mm (1/8 in.).
The plastic cylinder shall be smooth, rigid, nonabsorbent, and open at both ends. The test method
shall consist of the following:
Place the cylinder on a flat, level, firm nonabsorbent surface that is free of vibration or other
disturbances.
Hold the cylinder firmly in place and fill in one lift without vibration, rodding, or tapping.
Strike off the top of the cylinder to form a level surface while holding the cylinder in place.
Remove surplus material from around the base of the cylinder.
When the material has stopped flowing, measure the maximum diameter of the resulting
spread and measure the diameter perpendicular to the maximum. Each measurement shall
be to the nearest 10 mm (0.5 in.). If the two measurements differ by more than 50 mm (2 in.),
verify working surface to be level, and test again.
Calculate the average of the two measured diameters and report to the nearest 5 mm
(0.25 in.).
The air content test shall be according to Illinois Modified AASHTO T 121 or Illinois Modified
AASHTO T 152, except the bowl shall be filled in one lift without vibration, rodding, or tapping.
Compressive strength test specimens shall be made and cured according to Illinois Modified
AASHTO T 23, except for the following:
The 152 mm x 305 mm (6 in. x 12 in.) cylinders shall be filled in one lift without vibration,
rodding, or tapping. When bleed water appears at the top of the mold after a few minutes,
the mold shall be refilled.
The curing method shall be modified by not removing the covered specimen from the mold
until the time of testing.
Compressive strength test specimens shall be tested according to Illinois Modified AASHTO T 22,
except for the following:
Neoprene caps shall be used for compressive testing, and a wire brush may be used to
flatten test specimens that are not plane.
Compressive strength shall be calculated to the nearest 1.0 kPa (1.0 psi).
1.1 This method covers the procedure for conducting the DCP test on treated and
untreated subgrade materials.
1.2 This method does not address safety problems associated with using the DCP
equipment. It is the operators responsibility to determine the limitations prior to
its use. At a minimum, the operator is cautioned not to hold the DCP from the
anvil, to avoid injury to the fingers by the falling hammer.
2.1 The DCP is used to indirectly determine the immediate bearing value (IBV) of
treated or untreated subgrade material (Note 1).
2.2 The IBV is used to evaluate the subgrade stability, and to determine the depth of
subgrade treatment according to the Departments Subgrade Stability Manual.
NOTE 1 The IBV is considered to be equivalent to the in situ Illinois Bearing Ratio
(IBR), or the laboratory IBR obtained immediately after compacting the
material, without soaking.
3.1 ASTM D 4429 (latest edition), Standard Test Method for CBR (California
Bearing Ratio) of Soils in Place
Sowers, G.F. and Hedges, C.S. (1966), Dynamic Cone for Shallow In Situ
Penetration Testing, Vane Shear and Cone Penetration Resistance Testing of In
Situ Soils, ASTM STP 399.
Maur, M.C. and de Beer, M. (1988), Computer Programs to Plot DCP Data
Users Manual, Division of Roads and Transport Technology, Pretoria.
Note 2 A disposable cone, meeting the requirements of 4.2 a), may be used in hard
materials to avoid damage to the equipment, which may be caused by driving the
hammer upward in an attempt to extract the cone from the ground.
5.1 Check the DCP components for deficiencies, replace any damaged part, and
assemble the equipment as shown in Figure 1.
5.2 Hold the DCP vertically, from the handle, and seat the cone such that the cone
base is flush with the surface of the material to be tested. The initial (reference)
reading will be taken from the cone base (Note 3). A straight edge next to the
DCP will make a good reference point. Do not record the number of blows
required to seat the cone.
Note 3 In soft materials, the cone might penetrate into a depth beyond the cone base
under the hammer weight. In this case, record the current reading, under the
hammer weight, as the initial reference point.
5.3 Raise the hammer carefully all the way to the top, without impacting the handle,
and let it drop freely on the anvil to drive the cone into the material. The cone will
penetrate the material to a depth which depends on the material resistance.
5.4 Measure the number of blows for every 150 mm (6 in.) penetration into the
material, or measure the amount of penetration after each blow if the single blow
penetration is greater than 150 mm (6 in.). This may depend on the material
variability and resistance. Penetration readings are recorded to the nearest 5
mm (0.2 in.).
6.0 CALCULATIONS
6.1 The penetration rate (PR), inches per blow, is the amount of penetration (150
mm (6 in.)) divided by the number of blows in that increment. If the single blow
penetration is greater than 150 mm (6 in.), the PR is the amount of penetration
per blow. The PR value is recorded to the nearest 5 mm (0.2 in.) per blow.
(Note 4)
Note 4 Layers of the subgrade that have similar PR values should be averaged to
determine the PR for each layer. Engineering judgment will be necessary to
group the PR values and assess the validity of high or low penetrations.
6.2 Using the average PR value and Figure 2, obtain the equivalent IBV for each
150 mm (6 in.). The IBV may be used to obtain an equivalent compressive
strength (Qu) as indicated on the DCP form (BMPR SL30).
6.3 Use the attached DCP form (BMPR SL30) to record all data obtained from 6.2 at
different stations.
10
1
0.1 1 10
Penetration Rate, PR, inches per blow - Log Scale
a
Indicate station and offset. Rate IBV Qu* Rate IBV Qu*
b
Include soil type, moisture, rutting, or cut/fill 0.5 17 5.4 1.3 5 1.6
information as applicable. 0.6 13 4.2 1.5 4 1.3
c
Depth is cumulative in inches. 0.7 11 3.5 2.0 3 1.0
d
Rate is inches of penetration per blow. 0.8 9 2.9 2.6 2 0.6
0.9 8 2.6 3.0 1.7 0.5
Comments: 1.0 7 2.2 3.3 1.5 0.5
1.1 6 1.9 4.6 1 0.3
1.2 5.5 1.8 >4.6 <1 <0.3
*Qu value calculated from IBV whole number.
IBV = 100.84 1.26 x LOG(Rate) Qu (tsf) = 0.32 x IBV
BMPR SL30 (Rev. 03/17/10)
1.1 This method covers the procedure for conducting the SCP test on treated and
untreated subgrade materials.
1.2 This method does not address safety problems associated with using the SCP
equipment. It is the operators responsibility to determine the equipment
limitations prior to its use.
2.1 The SCP is used to determine the cone index (CI) of treated or untreated
subgrade material (Note 1).
2.2 The CI is used to evaluate the subgrade stability, and to determine the depth of
subgrade treatment according to the Departments Subgrade Stability Manual.
Note 1 The CI is a strength value which is equal to the penetrometer load (in pounds)
divided by the base area (in.2), and it has the units of psi (not expressed).
4.0 EQUIPMENT
4.1 Material: The metal components of the SCP shall be made of stainless steel.
b) A graduated rod, 0.48 m (19 in.) long (variable), 16 mm (5/8 in.) diameter,
marked at 150 mm (6 in.) intervals. The bottom 150 mm (6 in.) interval is
marked at 25 mm (1 in.) subintervals.
c) A 150 lb capacity proving ring with a handle and a factory calibrated dial
indicator, calibrated direct 0 to 300 psi in 5 psi increments. Alternatively,
a displacement dial indicator may be used with a factory calibrated
proving ring and a calibration chart.
5.1 Check the SCP components for deficiencies, replace any damaged part, and
follow the manufacturers recommendations to assemble the equipment as
shown in Figure 1 (Note 2).
Note 2 - The dial indicator is a sensitive instrument which should be protected against
water, dust, and rough usage. Make sure the dial indicator is on the zero
reading prior to the test.
5.2 Hold the SCP vertically, from the handle, and seat the cone such that the cone
base is flush with the surface of the material to be tested. The initial (reference)
reading will be taken from the cone base (Note 3).
Note 3 The SCP test should be conducted after the subgrade has been stressed with
several passes of a loaded truck. Any crust formed on the subgrade, from
drying, must be removed before seating the cone. Crusted subgrades give
high readings that do not reflect the strength of the weaker underlying material.
5.3 Holding the handle firmly, push the cone down into the subgrade material at a
steady, uniform rate and record the cone index, from the dial indicator readings,
every 150 mm (6 in.) of the cone penetrations.
5.4 Continue the procedure in 5.3 until: 1) the maximum depth of 450 mm (18 in.) is
reached, or 2) high resistance is encountered, or 3) the maximum ring capacity is
reached; whichever occurs first.
5.5 Use the attached SCP form (BMPR SL31) to record the CI values at different
depths and stations. Record the CI value to the nearest whole number. The CI
can also be converted to an equivalent compressive strength (Qu) by using the
equations on the SCP form (BMPR SL31). Normally, an equivalent IBV is
determined.
Date: County:
Weather: Section:
Inspector: Route:
Company (Consultants): District:
Design No.: Contract No.:
Sheet No.: Job No.:
Contractor: Project:
Subgrade Foundation
Test Location a and Remarks b
Depth c
Dial Reading d
IBV
Qu
Depth
Dial Reading
IBV
Qu
Depth
Dial Reading
IBV
Qu
Depth
Dial Reading
IBV
Qu
Depth
Dial Reading
IBV
Qu
Depth
Dial Reading
IBV
Qu
Depth
Dial Reading
IBV
Qu
a
Indicate station and offset. Cone Index IBV Qu*
b
Include soil type, moisture, rutting, or cut/fill 320 8 2.6
information as applicable. 280 7 2.2
c
Depth is cumulative in inches. 240 6 1.9
d
Dial Reading = Cone Index (CI) 200 5 1.6
160 4 1.3
IBV = CI 40 120 3 1.0
Qu (tsf) = 0.32 x IBV 80 2 0.6
40 1 0.3
Comments: *Qu value calculated from IBV whole number.
BMPR SL31 (Rev. 03/17/10)
1 SCOPE
1.1 This test procedure covers the determination of the percentages of flat particles,
elongated particles, or flat and elongated particles in coarse aggregates.
1.2 The values stated in inch-pound units are to be regarded as standard. The values
given in parentheses are mathematical conversions to SI units that are provided for
information only and are not considered standard.
1.2.1 Exception (Regarding sieves, per ASTM E 11. The values stated in SI units shall be
considered standard for the dimensions of the wire cloth openings and the diameter of
the wires used in the wire cloth. When sieve mesh sizes are referenced, the alternate
inch-pound designations are provided for information purposes and enclosed in
parentheses.
1.3 This standard does not purport to address all of the safety concerns, if any,
associated with its use. It is the responsibility of the user of this procedure to
establish appropriate safety and health practices and determine the applicability of
regulatory limitations prior to use.
2 REFERENCED DOCUMENTS
C670, Practice for Preparing Precision and Bias Statements for Test Methods for
Construction Materials
E 11, Woven Wire Test Sieve Cloth and Test Sieves
1
For reference ASTM standards, visit the ASTM website, www.astm.org or contact ASTM Customer
Service as service #astm.org. For Annual book of ASTM Standards volume information, refer to the
standards Document Summary page on the ASTM website.
3 TERMINOLOGY
3.1 Definitions:
3.1.2 Flat and Elongated Particles of Aggregate those particles having a ratio of length to
thickness greater than a specified value.
3.1.3 Flat Particles of Aggregate those particles of aggregate having a ratio of width to
thickness greater than a specified value.
3.1.6 Width intermediate dimension of the particle. It is the maximum dimension in the
plane perpendicular to the length and thickness. The width dimensions is greater
than or equal to the thickness as illustrated in Fig.1.
4.1 Individual particles of aggregate of specific sieve sizes are measured to determine the
ratios of width to thickness, length to width, or length to thickness.
5.1 The particles shape of coarse aggregates influences the properties of some
construction materials and may affect their placement and consolidation.
5.2 This test method provides a means for checking compliance with specifications that
limit such particles or to determine the relative shape characteristics of coarse
aggregates.
6 APPARATUS
6.1 The apparatus used shall be equipment suitable for testing aggregate particles for
compliance with the definitions in 3.1, at the dimensional ratios desired.
6.1.1 Proportional Caliper Device The proportional caliper devices illustrated in Fig. 2 and
Fig. 3, are examples of devices suitable for this test method. The device illustrated in
Fig. 2 and Fig. 3 consists of a base plate with two fixed posts and a swinging arm
mounted between them so that the openings between the arms and the posts
maintain a constant ratio. The axis position can be adjusted to provide the desired
ratio of opening dimensions, Fig. 2 illustrates a device on which ratios of 1:2, 1:3, and
1:5 may be set. (see Note 1)
6.1.1.1 Verification of Ratio The ratio settings on the proportional caliper device shall be
verified by the use of a machined block, micrometer, or other appropriate device.
6.1.2 Balance The balance or scales used shall be accurate to 0.5% of the mass of the
sample.
Note 1 Fig. 2 and 3 provide examples of possible devices that may be used for this
test. Other devices may be found suitable if they are able to meet the verification
requirements listed in 6.1.1.1.
7 SAMPLING
7.1 Sample the coarse aggregate according to ITP 2. The field sample size shall meet
the minimum requirements in Illinois Specification 201.
7.2 Field samples of aggregate shall be reduced to approximate test sample size before
testing according to ITP 248. Reduction to an exact predetermined mass shall not be
permitted. Sieve the approximate test sample according to ITP 27 and retain all plus
4.75mm (No. 4) material as the test sample. The mass of the test samples shall
conform to the following:
8 PROCEDURE
8.1 The test sample shall be dried back to constant mass in an oven specifically designed
for drying, set at and capable of maintaining a uniform temperature of 1105C
(2309F). Constant mass is defined as the sample mass at which there has not
been more than a 0.5 gram mass loss during one hour of drying. This should be
verified occasionally.
8.2 Flat Particle Test and Elongated Particle Test Test each of the particles in the test
sample and place in one of three groups: (1) Flat, (2) Elongated, (3) Neither flat nor
elongated.
8.2.1 Use the proportional caliper device, positioned at the proper ratio, shown in Fig. 4, as
follows:
8.2.1.1 Flat Particle Test- Set the larger opening equal to the maximum particle width. The
particle is flat if the maximum thickness can be placed though the smaller opening.
8.2.1.2 Elongated Particle Test Set the larger opening equal to the maximum particle
length. The particle is elongated if the maximum width can be placed through the
smaller opening.
8.3 Flat and Elongated Particle Test Test each of the particles in the test sample and
place in one of two groups: (1) flat and elongated or (2) not flat and elongated.
8.3.1 Use the proportional caliper device, positioned at the proper ratio, shown in Fig. 4, as
follows:
8.3.1.1 Flat and Elongated Particle Test Set the larger opening equal to the maximum
particle length. The particle is considered flat and elongated if the maximum
thickness can be placed through the smaller opening.
8.3.2 After the particles have been classified into the groups described in 8.3, determine the
proportion of the sample in each group by count or mass, as required. The particle is
flat and elongated if the particle thickness can be completely passed through the
smaller opening.
9 Calculation
9.1 Calculate the percentage of flat, elongated, and/or flat and elongated particles to the
nearest 1 percent in using the following formula:
%= x 100
where:
GM = each group mass, and
TSM = test sample mass.
10 Report
10.1.2 Grading of the original aggregate sample, showing percentage retained on each
sieve.
10.1.3 Percentages, calculated by mass for: (1) flat particles, (2) elongated particles, and (3)
total flat and elongated particles,
11.1 Precision The precision values listed in Table 1, and Table 2, and Table 3 are
averages obtained from AMRL proficiency samples used in the Aggregate Proficiency
Sample Program (see Note 2). The 1S % and D2S % limits provided are described in
Practice C670.
11.2 Bias Since there is no accepted reference material suitable for determining the bias for
this test method, no statement on bias is being made.
1 Scope
1.1 This test procedure covers the determination of the percentage, by mass of a coarse
aggregate sample that consists of fractured particles meeting specified requirements.
1.2 The values stated in SI units are to be regarded as the standard. The values in
parentheses are provided for information only.
1.3 This standard does not purport to address all of the safety concerns, if any, associated
with its use. It is the responsibility of the user of this procedure to establish appropriate
safety and health practices and determine the applicability of regulatory limitations prior to
use.
2 Referenced Documents
3 Terminology
3.1 Definitions:
3.1.2 fractured particle, n a particle of aggregate having at least the minimum number of
fractured faces specified (usually one or two)
4.2 Specifications differ as to the number of fractured faces required on a fractured particle,
and they also differ as to whether percentage by mass or percentage by particle count
shall be used. If the specification does not specify, use the criterion of at least one
fractured face and calculate percentage by mass.
5 Apparatus
5.1 Balance A balance or scale accurate and readable to within 0.1% of the test sample
mass at any point within the range of use.
5.3 Splitter A sample splitter suitable for dividing field samples into test portion sizes in
accordance with ITP 248.
6 Sampling
7 Sample Preparation
7.1 Dry the sample sufficiently to obtain a clean separation of fine and coarse material in the
sieving operation. Sieve the sample over the 1.75mm (No. 4) sieve in accordance with
ITP 27 and then reduce the portion retained on the sieve using a splitter in accordance
with ITP 248 to appropriate size for test.
7.2 The mass of the test sample shall be at least large enough so that the largest particle is
not more than 1% of the sample mass; or the test sample shall be at least as large as
indicated below, whichever is smaller.
8 Procedure
8.1 Wash the sample over the sieve designated for determination of fractured particle to
remove any remaining fine material, and dry to constant mass. Constant mass is defined
as the sample at which there has not been more than a 0.5 gram mass loss during 1 hour
of drying. This should be verified occasionally. Determine the mass of the test sample,
and any subsequent determinations of mass, to the nearest 0.1% of the original dry
sample mass.
8.2 Spread the dried test sample on a clean flat surface large enough to permit careful
inspection of each particle. To verify that a particle meets the fracture criteria, hold the
aggregate particle so that the face is viewed directly. If the face constitutes at least one
quarter of the maximum cross-sectional area of the rock particle, consider it a fractured
face.
8.4 Determine the mass of particles in the fractured particle category, and the mass of the
particles not meeting the specified fracture criteria. Use mass to calculate percent
fractured particles.
9 Report
9.1 Report the mass percentage of the particles with the specified number(s) of fractured
faces to the nearest 0.1% in accordance with the following:
= 100
where:
P=percentage of particles with the specified number of fractured faces,
F=Mass of fractured particles with at least the specified number of fractured faces,
Q=total mass of original test specimen.
9.2 Report the specified fracture criteria against which the sample was evaluated.
9.3 Report the total mass in grams of the coarse aggregate sample tested.
9.4 Report the sieve on which the test sample was retained at the start of the test.
FIG. 6 Fractured Particle (Center) Flanked by Two Non-Fractured Particles (Chipped Only)
Standard Practice
for
Temperature of Freshly Mixed Hydraulic Cement Concrete
NOTE: This test method cannot be reproduced here due to copyright. The Contractor
shall provide a copy of the ASTM test method to the Engineer if requested.
ASTM
Section Illinois Modification
2.1 Replace as follows:
AASHTO R 60 (Illinois Modified) for ASTM C172
The ASTM standard test method is not reproduced herein, but a copy is available to individuals
who have taken the Portland Cement Concrete Level I Technician Course.
For convenience to the individual using this manual, the ASTM standard test method for
measuring the temperature of freshly mixed concrete is summarized as follows.
1. Obtain the concrete sample according to R 60. The sample size shall be sufficient to
provide a minimum 75 mm (3 in.) concrete cover around the thermometer sensor in all
directions.
2. Use an ASTM approved thermometer which is accurate to 0.5 C (1 F), and has a
range that is adequate for concrete temperatures encountered. Refer to the Standard
Specifications for Road and Bridge Construction for concrete temperature limitations.
3. Place the thermometer in the concrete sample, which was collected in a damp, non-
absorbent container. The thermometer sensor shall be submerged a minimum of 75 mm
(3 in.). The concrete temperature may also be measured in placement forms, or
anywhere the minimum 75 mm (3 in.) cover is provided.
4. Gently press the concrete around the thermometer to prevent air temperature affects.
5. Read the temperature after a minimum of 2 minutes of when the temperature readings
stabilize.
6. Complete the temperature measurement within 5 minutes after obtaining the sample.
NOTE: This test method is to be used in conjunction with and according to Illinois
Modified AASHTO T 325, Estimating the Strength of Concrete in Transportation
Construction by Maturity Tests. According to Illinois Modified AASHTO T 325, the
Contractor shall provide a copy of the ASTM test method to the Engineer if requested,
which cannot be reproduced here due to copyright.
ASTM
Section Illinois Modification
2.1 Replace as follows:
AASHTO T 22 (Illinois Modified)
AASHTO T 23 (Illinois Modified)
AASHTO T 119 (Illinois Modified)
AASHTO T 152 (Illinois Modified)
AASHTO T 177 (Illinois Modified)
AASHTO T 196 (Illinois Modified)
AASHTO T 309 (Illinois Modified)
Standard Practice
for
Use of Unbonded Caps in Determination of
Compressive Strength of Hardened Concrete Cylinders
NOTE: This test method is to be used in conjunction with and according to Illinois
Modified AASHTO T 22, Compressive Strength of Cylindrical Concrete Specimens.
According to Illinois Modified AASHTO T 22, the Contractor shall provide a copy of the
ASTM test method to the Engineer if requested, which cannot be reproduced here due to
copyright.
ASTM
Section Illinois Modification
5.3 Add as follows:
The retainers shall be free of rust and other foreign material.
Standard Method
for
Bulk Specific Gravity and Density of Compacted Bituminous Mixtures Using Coated
Samples
ASTM
Section Illinois Modification
2.1 Replace the individual Standards as follows:
IL Modified standards in the Illinois Department of Transportation Manual of
Test Procedures for Materials (current edition)
AASHTO
Section Illinois Modification
2.1 Replace the individual Standards as follows:
IL Modified ASTM Standards in the Illinois Department of Transportation
Manual of Test Procedures for Materials (current edition)
3.6 All projects containing 2750 metric tons (3000 tons) or more of a given
New mixture will require a correlation factor be determined and applied for
Section measurement of density testing.
AASHTO
Section Illinois Modification
3.7 Definitions:
Density Test Location: The random station location used for density testing.
Individual Test Result: An individual test result is the average of three to five
nuclear density readings obtained at each random density test location.
One to three individual test results will be required per density test
location depending on the following conditions:
If two confined edges are present, one individual test result
representing all five density readings across the mat shall be
reported. (Confined edge density readings are included in the
average.)
If one confined and one unconfined edge is present, two individual
test results shall be reported for each density test location.
o One individual test result representing the average of four
density readings across the mat, including the one confined
edge and excluding the unconfined edge density readings.
o One individual test result representing the average of three
density readings on the unconfined edge.
If two unconfined edges are present, three individual test results
shall be reported for each density test location.
o One individual test result representing the average of three
density readings across the mat, excluding the unconfined
edge density readings.
o One individual test result representing the average of three
density readings on the unconfined edge.
o One individual test result representing the average of three
density readings on the opposite unconfined edge.
Daily Average Density Value: The daily average density is the average of
the density readings of a given offset for the given days production.
Density Test Site: Correlation term use to describe each physical location
the nuclear density gauge is placed where a density value is determined.
AASHTO
Section Illinois Modification
3.8 When the Hot Mix Asphalt (HMA) Individual Density Site Modified QC/QA
New special provision is included, daily average density values shall also be
Section determined.
AASHTO
Section Illinois Modification
8.2.3 Replace with the following:
All reference standard counts shall consist of a 4-minute count.
8.2.5 If four reference standard counts have not been established, then the
New reference standard count shall be within 2 percent of the standard count
Section shown in the count ratio book.
8.2.6 If the reference standard count fails the established limits, the count may be
New repeated. If the second count fails also, the gauge shall not be used. The
Section gauge shall be adjusted or repaired as recommended by the manufacturer.
8.2.7 Record all daily reference standard counts in a permanent-type book for a
New gauge historical record. This also applies to direct readout gauges.
Section
AASHTO
Section Illinois Modification
9.4 Replace with the following:
Maximum contact between the base of the instrument and the surface of the
material under test is critical. Since the measured value of density by
backscatter is affected by the surface texture of the material immediately
under the gauge, a smoothly rolled surface should be tested for best results.
A filler of limestone fines or similar material, leveled with the guide/scraper
plate, shall be used to fill open surface pores of the rolled surface.
9.7 Delete.
9.8 Delete.
Note 6 Delete.
Note 7 Delete.
10.1 Delete.
10.1.1 Delete.
10.2 Delete.
AASHTO
Section Illinois Modification
11.1.2 Revise as follows:
Date of calibration data,
A1.7.1 Delete.
NOTE A1
ASTM
Section Illinois Modification
6.4.2 Revise as follows:
When the digit next beyond the last place to be retained (or reported) is equal to
or greater than 5, increase by 1 the digit in the last place retained.
6.4.3 Delete.
6.4.4 Delete.
It should be noted that strength specimens cured in the field shall be in the same
manner as the pavement or structure, which may include such thing as insulation
if used
Precast Concrete
A plastic cylinder lid shall be the preferred method to cover cylinder molds.
10.2, Replace as follows:
10.2.1, Field CuringStore test specimens as near to the point of deposit of the concrete
and represented as possible. However, some instances may require a distinct and
10.2.2 separate location. Therefore, carefully select the field location since the test
specimens will generate minimal heat from hydration.
The test specimens shall have the same curing method and shall be in the same
field environment as the construction item. If form work is removed, remove test
specimens from their molds.
At the time of testing, guard against the drying of the test specimen if appropriate.
AASHTO
Section Illinois Modification
2.1 Replace AASHTO Standard T 164 with the following:
Illinois Modified AASHTO T 164
Replace AASHTO Standard T 255 with the following:
Illinois Test Procedure 255
Replace AASHTO Standard T 308 with the following:
Illinois Modified AASHTO T 308
1. Dampen the funnel, the cone, the hand scoop or trowel, the tamping rod,
and the floor or base plate.
2. Conduct the test on a flat, level, firm, non-absorbent surface which is free
from vibration or other disturbances.
3. Hold the cone firmly in place by standing on the two foot pieces, or by
closing the clamps on the base plate. Do not allow the cone to move
during filling.
4. Immediately fill the cone in three layers, each approximately one-third the
volume of the cone. The bottom layer shall fill the cone to approximately
one-quarter its depth [67 mm (2 5/8 in.)], the middle layer to
approximately one-half its depth [155 mm (6 1/8 in.)], and the top layer to
just over the top of the cone. Each scoopful of concrete should be moved
around the top edge of the cone (or funnel, if used) to provide even
distribution of the concrete in the cone. If the funnel is used when placing
the top layer, raise it slightly to prevent it from becoming wedged inside
the cone.
6. Rod the bottom layer throughout its depth and avoid forcibly striking the
floor or base plate. To accomplish this, hold the tamping rod at the point
which will allow the desirable tamping depth.
7. Rod the middle and top layers to just penetrate into the underlying layer.
To accomplish this, hold the tamping rod at the point which will allow the
desirable tamping depth.
8. When rodding the top layer, keep the level of concrete above the cone at
all times. If the level of concrete drops below the top of the cone, stop
rodding and add more concrete. The rodding count shall resume at the
point of interruption.
9. Strike off the concrete level with the top of the cone using a screeding
and rolling motion with the tamping rod.
10. Hold the cone, without movement, by applying a downward force to the
handles. Step off the foot pieces, or unclamp the base plate clamps, and
immediately raise the cone above the concrete. This shall be performed
in a steady upward lift with no lateral movement or rotation. The cone
shall be lifted within 3 to 7 seconds. Step 4 through 10 shall performed
within 2 minutes.
11. If a significant falling away or shearing off of concrete from one side
occurs, do not measure the slump. Repeat the test on another portion of
the sample. If the same result occurs, the concrete probably lacks the
cohesiveness for the slump test to be applicable.
12. To measure the slump, invert the cone and place it on the floor or base
plate near the slumped concrete. Place the tamping rod across the cone
and immediately measure the distance between the bottom of the rod
and the displaced original center of the top surface of the concrete. A
base plate with a swing handle may also be used to measure the
distance.
Revise as follows:
Illinois Test Procedure 19 replaces T 19M/T 19
AASHTO T 23 (Illinois Modified)
AASHTO T 119 (Illinois Modified)
AASHTO R 60 (Illinois Modified)
AASHTO T 152 (Illinois Modified)
AASHTO T 196 (Illinois Modified)
Remove as follows:
AASHTO R 11 (replaced by Illinois Modified ASTM E 29)
Add as follows:
AASHTO M 231 Weighing Devices Used in the Testing of
Materials
Fill the container about half full of water, pour the fine aggregate slowly into the
container and stir vigorously by hand for five minutes so that the fine aggregate
will be completely inundated with no entrapped air around or between the
particles. It is very difficult to remove all of the entrapped air and much care
should be taken in performing this operation or the test will show erroneous
results.
Finish filling the container with water. Wipe the contact surfaces clean and clamp
the cover of the apparatus firmly to the container.
Close the lower petcock and open the upper petcock and the funnel valve. Pour
water through the funnel until it stands at a level slightly above the arrow mark on
the graduated scale. Close the funnel valve and adjust the water level to the
arrow mark on the graduated scale by means of the lower petcock.
Close the upper petcock and apply pressure with the bicycle tire pump until the
gage reads 103 kPa (15 psi). Read and record the subsidence of the water level.
Release the pressure by opening the upper petcock. Release the water by
opening the C-clamps. Repeat the test on other samples until it is apparent from
the results obtained that all the air entrapped between the fine aggregate particles
is being stirred out.
The sum of the readings obtained for the two samples is the subsidence of the
water level due to the air held within the aggregate particles, and is the correction
to be applied in determining the air content of the concrete. The test can be
made on the samples of fine and coarse aggregate combined, but more difficulty
will be experienced in stirring out entrapped air.
2. Close the lower petcock. Open the upper petcock and the funnel valve.
Add water through the funnel until the level is slightly above the index
mark, or until water flows from the upper petcock.
3. Close the funnel valve. Using the lower petcock, adjust the bottom of the
meniscus (water level) to be level with the index mark. The index mark is
to account for the expansion of the air meter, and is above the zero mark.
The expansion is primarily a result of the C-clamps elongating. Always
read the water level at the bottom of the meniscus. Close the lower
petcock.
5. Using the hand pump, apply 103 kPa (15 psi) pressure.
6. Read the water level and record the apparent air content to the nearest
tenth of a percent. If the water level cannot be read at 103 kPa (15 psi),
reduce the air pressure to 69 kPa (10 psi) and multiply the reading by
1.25. If the water level cannot be read at 69 kPa (10 psi), reduce the air
pressure to 34 kPa (5 psi) and multiply the reading by 2.00.
If the water glass needs cleaning, remove the valve from the funnel valve
assembly. Clean the inside of the glass with a strip of cloth and one of the wire
guards of the water glass.
AASHTO
Section Illinois Modification
2.1 Replace AASHTO Standard T 84 with the following:
Illinois Test Procedure 84
7.4 Delete
Note 4 Delete
Note 9 Delete
AASHTO
Section Illinois Modification
12.3 Replace the first sentence with the following:
Cover the test portion in the bowl with trichloroethylene, methylene chloride,
or normal-propyl bromide extractant, and allow sufficient time for the solvent
to disintegrate the test portion (not more than 1 h).
(W1 W2 ) (W3 + W4 )
Asphalt Binder Content, % = x100
W1 W2
Where:
When method B or E is used and the amount of mineral matter in the extract
is not determined, then the percent asphalt binder content in the test portion
shall be calculated as follows:
AASHTO
Section Illinois Modification
14.1.1.2 Revise the first sentence as follows:
Cylindrical Metal Frames, two.
Test Delete:
Method D Test Method D
18 Delete
19 Delete
20 Delete
Note 18 Delete
AASHTO
Section Illinois Modification
A1.2.2.1 Replace the third sentence with:
Transfer all of the extract (from Method A, B, or E as appropriate) to an
appropriate (feed) container suitably equipped with a feed control (valve or
clamp, etc.).
AASHTO
Section Illinois Modification
2.1 Replace with the following:
Referenced Illinois modified AASHTO Standards:
M231, Weighing Devices Used in the Testing of Materials
5.3.1 For immersing the specimen in water while suspended under the weighing
New device, equipped with an overflow outlet for maintaining a constant water
Section level.
5.3.2 Constant Temperature Water Bath Shall meet the requirements listed in
New the Illinois Department of Transportation document, Bituminous Concrete
Section QC/QA Laboratory Equipment.
AASHTO
Section Illinois Modification
8 Delete
9 Delete
10 Delete
Footnote1 Delete
AASHTO
Section Illinois Modification
3.1.2 Replace with the following:
Residual Pressure the pressure remaining in the vacuum vessel after a
vacuum (negative pressure) is applied. The residual pressure is based on,
and measured with, an absolute manometer.
Figure 2 Delete
AASHTO
Section Illinois Modification
Figure 3 Delete
8.3 Delete
8.3.1 Delete
8.3.2 Delete
8.3.3 Delete
Note 5 Delete
13.1 Replace with the following: Mass Determination in Water - Suspend the
container and contents in the 25 1C (77 1.8F) water bath and
determine the mass after 10 1 min immersion. Designate the mass of the
container and the sample in water as B.
Note 8 Delete
Note 9 Delete
AASHTO
Section Illinois Modification
14.1.1 Replace with the following:
Mass Determination in Water:
A
Theoretical Maximum Specific Gravity =
A (B C)
where:
14.1.3.1 Delete
14.1.3.2 Delete
Figure 5 Delete
Figure 6 Delete
Note 10 Delete
Note 11 Delete
Appendix Delete
AASHTO
Section Illinois Modification
3.3 Replace with the following:
Compaction HammerThe compaction hammer (figure 2) shall be an
automatic hammer with a fixed (non-rotating) base. The compaction
hammer shall have a flat, circular tamping face and a 4536 9 g (10 0.02
lb) sliding weight with a free fall of 457.2 1.524 mm (18 0.06 in.). The
compaction hammer shall be equipped with a finger safety guard. The
automatic hammer consists of the mechanical compactor, with an automatic
counter, and a flat-foot hammer assembly.
AASHTO
Section Illinois Modification
4.5.2 Revise the fifth sentence as follows:
After compaction, let mold and sample cool for 1 hour 15 minutes before
extracting the sample from the mold.
5.2 Delete reference to manually recording the maximum load and flowmeter
reading; it is not required.
Note 1: Burning the soil may drive off organic material, which will result in moisture
measurements higher than the true value. Rapid heating of the soil may cause
particles to explode and loss of material, which will also result in moisture
measurements higher than the true value. Therefore, stir the soil sample when
drying to accelerate the operation and avoid localized overheating.
5.1, 7.1, Add as follows:
9.1, and For field tests, sieving according to t 99 or as referenced herein is not required. As
11.1 an alternative, thoroughly break up soil aggregations until no piece is larger than
12 mm (0.5 in.). Discard any piece larger than 12 mm (0.5 in.).
6.1 and Add the following after the first sentence:
10.1 The need for adding water is determined by moisture content of the field sample.
6., 8., Add as follows:
10., and All rounding shall be according to ASTM E 29.
12.
AASHTO
Section Illinois Modification
1.1 Replace the first sentence with the following:
This method covers preparation of specimens and the measurement of the
change of diametral tensile strength resulting from the effects of water
saturation and accelerated water conditioning of compacted asphalt
mixtures.
5.5 Delete
5.6 Delete
5.7 Delete
6.3.3 Odor neutralizing additives, if used, shall be added to the asphalt binder
New according to the manufacturers recommended dosage rate and procedure
Section prior to mixing the asphalt with the heated aggregates.
6.4 Delete
8.1.1 The pavement may be cored with the objective of performing a forensic
New analysis of the in-situ conditions of the in-place, compacted mixture. In that
Section case, the core specimens should be kept in a leak-proof plastic bag until
testing to preserve the in-situ conditions. The testing should be conducted
as soon as possible after coring.
10.3.7 Delete.
AASHTO
Section Illinois Modification
2.1 Replace the individual AASHTO Standards with the appropriate Illinois
modified AASHTO Standards:
2.1 Replace AASHTO Standard T 2, T 11, T 27, and T248 with the following:
Illinois Test Procedure 2
Illinois Test Procedure 11
Illinois Test Procedure 27
Illinois Test Procedure 248
3.4 Replace the second and third sentences with the following:
The moisture sample shall be weighed immediately, prior to beginning the
test count, and this value shall be recorded as the original sample weight.
The sample to be tested for moisture content shall be placed in a 110 5 C
(230 9 F) oven at the time the mixture test count is being performed.
Drying of the moisture sample shall continue until it reaches constant mass.
Constant mass (oven dry) is defined as less than 0.5 g loss in 1 hour. This
weight shall be recorded as the oven-dry weight. Moisture content is
determined as follows:
AASHTO
Section Illinois Modification
4.1 Replace with the following:
Nuclear asphalt binder content gauge system, capable of at least a 3-point
calibration, consisting of:
4.6.2 Delete
5.2 Add the following between the second and third sentences:
The location of the gauge for field-testing requires the gauge to be in the
exact location used during calibration.
AASHTO
Section Illinois Modification
8.1 Replace with the following:
Obtain samples of freshly produced asphalt concrete according to Illinois
Department of Transportation document, "HMA QC/QA Initial Daily Plant
and Random Samples".
AASHTO
Section Illinois Modification
Annexes Replace with the following:
APPENDICES
A3.5 Delete
A3.5.1 Delete
A3.5.2 Delete
A3.5.3 Delete
A4.3 Delete
A4.3.1 Delete
A4.3.2 Delete
AASHTO
Section Illinois Modification
A6.1 Replace with the following:
Note A3 Note A3 - To find an appropriate starting mass, place the dry aggregate in a
gauge-sample pan. Fill the sample pan one-half full, evenly distributing the
sample in the pan. Level the HMA mixture with a trowel or spatula. Fill the
remainder of the pan until the weight of the HMA mixture in the pan equals
the dry aggregate weight. If the pan is not full, fill the pan to the point that
the HMA mixture is mounded slightly above the top of the pan. Record the
weight of the HMA mixture in the pan. This is the weight that is to be used
for all calibration and test samples using this calibration. Level the top of the
HMA mixture using a spatula or trowel. Use the metal plate or plywood to
consolidate the HMA mixture until it is even with the top edge of the pan. All
specimens should be compacted at a temperature between 121 and 149
6C (250 and 300 10F) to ensure that the mix will compact properly.
AASHTO
Section Illinois Modification
A10 Delete Entire Section
B2 Fill the sample pan one-half full of hot dry aggregate dried to constant
New weight and at the temperature of the aggregate sample used during
Section calibration 6C (10F). Place the dry hot aggregate in a tared sample pan
in two equal layers. For each layer, raise and drop the pan approximately
one inch, four times. Be sure that the pan bottom strikes evenly. Use a
spatula to distribute the aggregate to avoid segregation. Add to or remove
aggregate until the weight of aggregate in the pan is equal to the weight of
aggregate used in the calibration. Using a straightedge, level the top of the
aggregate sample until it is even with the top of the sample pan. Obtain and
record the temperature of the sample.
B3 Place the hot blended aggregate into the gauge and proceed as per
New manufacturers instruction for operation of the equipment and the sequence
Section of operation. This dry aggregate count is used to determine changes in
aggregates which affect counts.
AASHTO
444 North Capitol Street, N. W.
Suite 249
Washington, D.C. 20001
(202) 624-5800
www.transportation.org
AASHTO
Section Illinois Modification
1.1 Revise the first sentence as follows:
This test method covers the determination of asphalt binder content of HMA
by ignition of the asphalt binder at 482 C (900 F) in a furnace.
AASHTO
Section Illinois Modification
7.2 Replace with the following:
Obtain and split a HMA sample(s) according to Sections 6.2, 6.4, and A2.2
herein.
( ) ( )
% ( ) = 100
AASHTO
Section Illinois Modification
8.2 Replace with the following:
Obtain and split a HMA sample(s) according to Sections 6.2, 6.4, and A2.2
herein.
( ) ( )
% ( ) = 100
8.9 Delete.
through
8.15
AASHTO
Section Illinois Modification
9.3 Correct the aggregate gradation by subtracting the degradation computed in
New Section 9.2 herein from the percent passing on the respective sieves.
Section
A2.8.1 Delete.
The following procedures shall be used for measurements using the nuclear
method in trenches, and around abutments, culverts or other objects either
buried or protruding from the surface of the ground.
9.5.1.1 OBJECTS BURIED BELOW THE SURFACE OF MATERIAL TO BE TESTED
Standard Method
for
Preparing and Determining the Density of Hot-Mix Asphalt (HMA) Specimens
by Means of the Superpave Gyratory Compactor
AASHTO
Section Illinois Modification
2.1 Replace with the following:
Referenced Illinois modified AASHTO Standards:
M 231, Weighing Devices Used in the Testing of Materials
R 30, Mixture Conditioning of Hot-Mix Asphalt (HMA)
R 35, Superpave Volumetric Design for Hot-Mix Asphalt (HMA)
T 166, Bulk Specific Gravity of Compacted Hot-Mix Asphalt Using
Saturated Surface-Dry Specimens
T 209, Theoretical Maximum Specific Gravity and Density of Hot-Mix
Asphalt Paving Mixtures
Standard Method
for
Preparing and Determining the Density of Hot-Mix Asphalt (HMA) Specimens
by Means of the SHRP Gyratory Compactor
(continued)
Reference AASHTO T 312-12
AASHTO
Section Illinois Modification
6. Replace entire section with the following:
CalibrationThe gyratory compactor internal angle shall be calibrated
according to the Illinois Procedure for Internal Angle Calibration of
Superpave Gyratory Compactors (SGCs) using the Dynamic Angle Validator
(DAV-2). The ram pressure, height and rate of gyration shall be calibrated
according to the manufacturers instructions and shall be completed prior to
the internal angle calibration. The internal angle, ram pressure, height and
rate of gyration shall be calibrated at a minimum frequency of once per
month. The monthly internal angle calibration may be conducted utilizing
the external angle verification as outlined in the Illinois Procedure for
Internal Angle Calibration of Superpave Gyratory Compactors (SGCs) using
the Dynamic Angle Validator (DAV-2).
8.1.2.1 Delete.
NOTE 4
8.1.4.1 When necessary, reduce the sample according to Illinois Test Procedure
New 248 and the following:
Section
Place the splitter on a level surface. The splitter and accessory equipment
may be heated, not to exceed 110C (230F), as determined by a
noncontact temperature device. Surfaces of the mechanical splitter that will
come in contact with the HMA shall be lightly coated with an approved
asphalt release agent to prevent a buildup and loss of asphalt binder and
fines. The release agent shall not contain any solvents or petroleum-based
products that could affect asphalt binder properties.
Standard Method
for
Preparing and Determining the Density of Hot-Mix Asphalt (HMA) Specimens
by Means of the SHRP Gyratory Compactor
(continued)
Reference AASHTO T 312-12
AASHTO
Section Illinois Modification
8.2.3 Replace with the following:
Reduce the sample according to Illinois Test Procedure 248 and the
following:
Place the splitter on a level surface. The splitter and accessory equipment
may be heated, not to exceed 110C (230F), as determined by a
noncontact temperature device. Surfaces of the mechanical splitter that will
come in contact with the HMA shall be lightly coated with an approved
asphalt release agent to prevent a buildup and loss of asphalt binder and
fines. The release agent shall not contain any solvents or petroleum-based
products that could affect asphalt binder properties.
A1.2 Each district shall own and operate an Internal Bore Gauge. A Three-Point
New gauge is recommended although a Two-Point gauge is allowed. Care must
Section be exercised during operation to ensure accuracy and precision regardless
which gauge is selected.
Standard Method
for
Preparing and Determining the Density of Hot-Mix Asphalt (HMA) Specimens
by Means of the SHRP Gyratory Compactor
(continued)
Reference AASHTO T 312-12
AASHTO
Section Illinois Modification
A3.2.2 Replace the fifth sentence with the following:
When using the three-point gauge, while extending the gauge contacts, use
a small circular motion at the top of the gauge to align the contact tips with
the master ring bore.
A3.4 Replace from the third sentence of the second paragraph to the end of the
section with the following:
At each elevation, measurements designated as A shall have one of the
gauge contacts aligned with the mark made in A3.3, measurements
designated as B shall have the contact rotated from the mark 90 degrees
for a Three-Point gauge or 120 degrees for a Two-Point gauge, and
measurements designated as C shall have the contact rotated from the
mark 180 degrees for a Three-Point gauge or 240 degrees for a Two-Point
gauge.
For best accuracy and consistency, each bore measurement should use the
same firmness and technique applied in Section A3.2.2 for gauge
standardization.
Standard Method
for
Preparing and Determining the Density of Hot-Mix Asphalt (HMA) Specimens
by Means of the SHRP Gyratory Compactor
(continued)
Reference AASHTO T 312-12
AASHTO
Section Illinois Modification
A3.4.2 Replace the first sentence with the following:
Release the gauge; rotate it 90 degrees (Three-Point gauge) or 120 degrees
(Two-Point gauge) and obtain the measurement in this orientation.
A3.4.4 Replace the second sentence with, Repeat Section A3.4 through A3.4.3 for
Elevations 2 and 3.
AASHTO
Section Illinois Modification
2.1 Revise as follows:
AASHTO M 231 Weighing Devices Used in the Testing of Materials
Illinois Test Procedure 84
Illinois Test Procedure 85
AASHTO T 121 (Illinois Modified)
AASHTO R 60 (Illinois Modified)
AASHTO T 255 (Illinois Modified)
(continued)
Reference AASHTO T 318-02 (2011)
AASHTO
Section Illinois Modification
9.4 Replace as follows:
Leave the tray and glass lid on the balance. Record the tare weight. Place
the 1500 100 gram test specimen in the ceramic tray, and cover with the
glass lid.
(continued)
Reference AASHTO T 318-02 (2011)
AASHTO
Section Illinois Modification
9.11 Replace as follows:
Remove the tray, glass lid, and test specimen from the microwave oven.
Take off the glass lid, and wipe off any moisture on the lid. Determine the
mass of the tray, glass lid, and specimen together. If the change in mass
is 1 g or more, repeat the 2 minute drying period until the change in mass
is less than 1 g. Record the mass of the tray, glass lid, and dry test
specimen together (WD).
Where:
Example For CA
Saturated Surface-Dry Mass per Volume for Coarse Aggregate (A) = 1,140
kg/m
Coarse Aggregate Absorption (B) = 1.2 %
1,140 3
= = = 1,126 3
1 + (100) 1 + (1.2100)
(continued)
Reference AASHTO T 318-02 (2011)
AASHTO
Section Illinois Modification
10.4 All Rounding shall be according to ASTM E 29.
New
Section
11.1.3 Replace as follows:
Total water content, nearest 1 kg/m (1 lb/yd).
AASHTO
Section Illinois Modification
1.2 Revise the last sentence as follows:
Alternatively, field cores with a diameter of 150 mm (5.91 in.), 255 mm (10
in.), 300 mm (12 in.), or saw-cut slab specimens may be tested.
2.1 Revise the individual AASHTO Standards with the appropriate Illinois
modified AASHTO Standards:
R 30, Mixture Conditioning of Hot Mix Asphalt (HMA)
T 166, Bulk Specific Gravity of Compacted Hot Mix Asphalt (HMA)
Using Saturated Surface-Dry Specimens
T 209, Theoretical Maximum Specific Gravity and Density of Hot Mix
Asphalt (HMA)
T 312, Preparing and Determining the Density of Hot Mix Asphalt
(HMA) Specimens by Means of the Superpave Gyratory Compactor
AASHTO
Section Illinois Modification
6.2.6.2 Replace with the following:
Compacting SGC Cylindrical Specimens--Material shall be compacted into
specimens using an SGC according to IL Modified AASHTO T 312. A
specimen thickness of 622 mm (2.40.1 in.) shall be used. The specimen
thickness shall be at least twice the nominal maximum aggregate size. Two
150 mm (5.91 in.) diameter specimens are needed for each wheel.
Compacted specimens shall be cooled at room temperature on a clean, flat
surface until the specimen is cool to the touch.
AASHTO
Section Illinois Modification
Note 1 Replace the second sentence with the following:
In order for the total sample height to be 622 mm (2.40.1 in.), the sample
must be trimmed with a wet saw if it is too tall. If the sample is too short
then it must be shimmed up with Plaster of Paris (or equivalent).
6.4.2 Delete the first sentence referring to minimum time after compaction.
It may be useful to run every test for 20,000 wheel passes to collect
additional data on moisture sensitivity.
AASHTO
Section Illinois Modification
8.8.4 Replace with the following:
Each wheel on the wheel-tracking device shall shut off independent of the
other wheel. The end of a test for each wheel can occur when the specified
number of wheel passes listed in Section 8.6.1.1 or the number of passes
otherwise specified has occurred on that wheel. Further, each wheel on the
device shall be set to lift independently when the LVDT displacement is 14.0
mm (0.55 in.) for that wheel. The HWTD measures the rut depth at multiple
points per pass across the specimen. The maximum rut depth is defined as
the average rut depth of the point with the deepest rut depth and the rut
depth of the two points physically closest to it. The testing device software
automatically saves the test data file for each wheel.
If the test was conducted using a single wheel, a passing test from that
wheel shall have a rut depth less than or equal to 12.5 mm at the prescribed
number of passes in section 8.6.1.1.
AASHTO
Section Illinois Modification
All Replace all references to AASHTO Standards with the appropriate Illinois
Sections Modified AASHTO Standard, except as noted below.
2.1 Delete reference to AASHTO T 176 and AASHTO T 304
Replace AASHTO Standards T 11 and T 27, and ASTM Standards D 4791 and D
5821 with the following:
Illinois Test Procedure 11
Illinois Test Procedure 27
Illinois Test Procedure 4791
Illinois Test Procedure 5821
2.2 Delete
5.1.1 Delete
5.1.2 Delete
Note 3 Delete
5.1.3 Delete
5.2 Delete
Table 1 Delete
and all
footnotes
Note 4 Delete
If the RAP / RAS Asphalt Binder Replacement (ABR) exceeds 20 percent, the
high and low virgin asphalt binder grades shall each be reduced by one grade
(i.e. 25 percent ABR would require that a virgin asphalt binder grade of PG64-22
be reduced to a PG58-28).
5.3.1 Delete
Note 5 Delete
Table 2 Delete
5.3.2 Delete
Note 7 Delete
6.2 Delete
6.3 Delete
6.4 Delete
6.5 Delete
Note 8 Delete
Table 6 Delete
Appendix Delete
X1
Appendix Delete
X2
Standard Specification
for
Stone Matrix Asphalt (SMA)
AASHTO
Section Illinois Modification
Whole This AASHTO Provisional document shall only be used in conjunction with a
Document Special Provision that includes Illinois SMA mix design and ingredient materials
details.
Standard Specification
for
Stone Matrix Asphalt (SMA)
AASHTO
Section Illinois Modification
8.1 Insert after Note 3:
Standard Specification
for
Stone Matrix Asphalt (SMA)
AASHTO
Section Illinois Modification
8.1 Insert at end:
Standard Practice
for
Mixture Conditioning of Hot Mix Asphalt (HMA)
AASHTO
Section Illinois Modification
1.1 Replace with the following:
This standard practice describes procedures for mixture conditioning of
uncompacted hot mix asphalt (HMA). Conditioning requirements for
volumetric mixture design, specimens for Hamburg Wheel testing, and
specimens for strength and TSR testing are addressed.
2.1 Revise the individual AASHTO Standards with the appropriate Illinois
Modified AASHTO Standards:
Standard Practice
for
Mixture Conditioning of Hot Mix Asphalt (HMA)
7.1.1 Delete
Note 1
For testing of all mixtures with low-absorptive aggregate, place the mixture
and pan in the conditioning oven pre-heated to the mixtures specified
compaction temperature 5 F ( 3 C) for 1 hr. 5 min. prior to
compaction. (1 hr. of oven time, not the time the mixture was held at
compaction temperature, is used.)
For testing of all mixtures with high-absorptive aggregate, place the mixture
and pan in the conditioning oven pre-heated to the mixtures specified
compaction temperature 5 F ( 3 C) for 2 hrs. 5 min. prior to
compaction. (2 hrs. of oven time, not the time the mixture was held at
compaction temperature, is used.)
Standard Practice
for
Mixture Conditioning of Hot Mix Asphalt (HMA)
7.1.2 Note 2D Condition Hamburg Wheel specimens from WMA mixtures from
New Note both lab-produced mix and plant-produced mix for two hours in addition to
the requirements for HMA.
1/ When two different values are present within a single cell, the correct
value is based on whether low or high absorptive aggregates are used.
Standard Practice
for
Superpave Volumetric Design for Hot Mix Asphalt (HMA)
AASHTO
Section Illinois Modification
ALL All references to calculations involving Nini and Nmax do not apply at
Sections this time.
Replace all references to AASHTO or ASTM standards with the
appropriate Illinois-modified specification or Illinois Test Procedure.
Replace all references to design air voids of 4.0% with the design air
voids content specified in Illinois-modified M323.
4.1 Delete
Note 3
6.1 Delete
6.2 Delete
Standard Practice
for
Superpave Volumetric Design for Hot Mix Asphalt (HMA)
(continued)
Reference AASHTO R 35-12
AASHTO
Section Illinois
IllinoisModification
Modification
6.8 Replace with the following:
Prepare a minimum of three trial aggregate blend gradations and confirm
that each trial blend meets M 323 gradation controls. An example of three
acceptable trial blends in the form of a gradation plot is given in Figure 1.
6.9 Delete
6.9 Delete
Note 6
8.1 Note 7a
New Note The design number of gyrations will be determined by the Department and
specified in the plans.
Standard Practice
for
Superpave Volumetric Design for Hot Mix Asphalt (HMA)
(continued)
Reference AASHTO R 35-12
Standard Practice
for
Superpave Volumetric Design for Hot Mix Asphalt (HMA)
(continued)
Reference AASHTO R 35-12
AASHTO
Section Illinois Modification
8.3 Delete
Note 9
8.3 Delete
Note 10
Standard Practice
for
Superpave Volumetric Design for Hot Mix Asphalt (HMA)
(continued)
Reference AASHTO R 35-12
AASHTO
Section Illinois Modification
X2.5.1 Delete the last sentence
X2.6.3 Delete
Note X8 Delete
X2.6.4 Delete
X2.6.4.1 Delete
X2.6.4.2 Delete
X2.6.4.3 Delete
AASHTO
Section Illinois Modification
Whole This AASHTO document shall only be used in conjunction with a Special
Document Provision that includes Illinois SMA mix design and ingredient materials details.
Note 3 Delete
Note 5 Delete
POINT OF SAMPLING
The field sample shall be obtained at or near the point of discharge by the delivery
equipment and prior to incorporation of the concrete into the work, except when
concrete is placed by pump or conveyor.
When concrete is placed by pump or conveyor, the field sample for strength tests
shall be obtained at the discharge end of the pump or conveyor. Per
specifications, a slump test (or applicable self-consolidating concrete tests), air
content test, and temperature test shall be performed on the same sample
obtained for strength tests.
Note: Field samples for strength test are taken at the discharge end of the
pump or conveyor because air content is likely to change during transport.
Typically, if air content increases 1 percent, compressive strength will
decrease approximately 2 to 6 percent and flexural strength will decrease
approximately 2 to 4 percent. These sampling and testing procedures are
mandatory for bridge deck concrete transported by pump or conveyor. For
some construction items, it may not be feasible or practical to obtain a field
sample at the discharge end of the pump or conveyor. These samples may
be obtained prior to pumping or conveying at the discretion of the Engineer.
7. Clean all test equipment with water and allow to drain, or wipe dry. Never
assemble wet test equipment before storing.
8. Clean all test equipment with water and allow to drain, or wipe dry. Never
assemble wet test equipment before storing.
Sampling freshly mixed self-consolidating concrete (SCC) shall be performed according to Illinois
Modified AASHTO R 60, except the elapsed time for obtaining the representative sample shall not
exceed two minutes. The number of testing personnel shall be such that all tests shall start within
five minutes of obtaining the representative sample.
The yield test shall be according to Illinois Modified AASHTO T 121, except the measure shall be
filled in one lift without vibration, rodding, or tapping. The air content test shall be according to Illinois
Modified AASHTO T 152 or T 196, except the bowl shall be filled in one lift without vibration, rodding,
or tapping.
Strength test specimens shall be made according to Illinois Modified AASHTO T 23 or R 39, except
for the following:
a. The specimen molds shall be filled using a suitable container in one lift without vibration,
rodding, or tapping.
b. Strike off the surface of the concrete level with the top of the mold using the strike-off bar
or tamping rod.
c. The slump flow, VSI, air content, and temperature of each batch of concrete, from which
specimens are made, shall be measured immediately after remixing.
1. Illinois Test Procedure SCC-1, Sampling, Determining Yield and Air Content, and Making and Curing
Strength Test Specimens of Self-Consolidating Concrete
3. ASTM E 29 (Illinois Modified), Standard Practice for Using Significant Digits in Test Data to
Determine Conformance with Specifications
1. GENERAL
This test method covers the determination of flowability and stability of fresh self-consolidating
concrete (SCC). The average diameter of the slump flow is a measure of the filling ability (flowability)
of SCC. The Visual Stability Index (VSI) is a measure of the dynamic segregation resistance
(stability) of SCC.
2. EQUIPMENT
a. Mold and Tamping Rod The mold and tamping rod shall conform to that described in T 119.
b. Strike-Off Bar Optional. The strike-off bar shall be a flat straight bar at least 3 mm (0.125 in.) x
20 mm (0.75 in.) x 300 mm (12 in.).
c. Base Plate The base plate shall be of a smooth, rigid, and nonabsorbent poly methyl
methacrylate (e.g. Plexiglas, Lucite, etc.) or high-density overlay (HDO) plywood material, and
be of sufficient dimensions to accommodate the maximum slump flow. Optional: Centered on the
testing surface of the base plate shall be a marked circle of diameter 500 mm (20 in.).
e. Measuring Tape The measuring tape shall have a minimum gradation of 10 mm (0.5 in.).
f. Stopwatch Optional. The stopwatch shall have a minimum reading of 0.2 seconds.
3. MATERIALS
The sample of SCC from which test specimens are made shall be obtained according to Section I of
Illinois Test SCC-1.
4. PROCEDURE
a. Dampen the slump cone and base plate. Ensure excess water is removed from the testing
surface as too much water may influence the Visual Stability Index (VSI) rating.
d. Strike off the surface of the concrete level with the top of the mold using the tamping rod or strike-
off bar. Remove surplus concrete from around the base of the mold and base plate surface.
g. When the concrete has stopped flowing, measure the maximum diameter of the resulting slump
flow and measure the diameter perpendicular to the maximum. Each measurement shall be to
the nearest 10 mm (0.5 in.). If the two measurements differ by more than 50 mm (2 in.), verify
base plate to be level, and test again.
h. Calculate the average of the two measured diameters. This is the slump flow.
i. By visual examination, rate the Visual Stability Index (VSI) of the SCC using the criteria in Table 1
and illustrated in Figures 2 9.
No mortar halo or coarse aggregate heaping in the slump flow, but some slight
1
bleeding and/or air popping is evident on the surface of the slump flow, or concrete in
stable
the mixer drum/pan or sampling receptacle (e.g. wheelbarrow).
Slight mortar halo, 10 mm (0.5 in.) wide, and/or coarse aggregate heaping in the
2
slump flow, and highly noticeable bleeding in the mixer drum/pan or sampling
unstable
receptacle (e.g. wheelbarrow).
Clearly segregated by evidence of a large mortar halo, > 10 mm (0.5 in.), and/or large
3
coarse aggregate pile in the slump flow, and a thick layer of paste on the surface of the
unstable
concrete sample in the mixer drum or sampling receptacle (e.g. wheelbarrow).
5. REPORT
a. Report the slump flow (average of two measured diameters) to the nearest 5 mm (0.25 in.).
1. Illinois Test Procedure SCC-1, Sampling, Determining Yield and Air Content, and Making and
Curing Strength Test Specimens of Self-Consolidating Concrete
2. Illinois Test Procedure SCC-2, Slump Flow and Stability of Self-Consolidating Concrete
4. ASTM E 29 (Illinois Modified), Standard Practice for Using Significant Digits in Test Data to
Determine Conformance with Specifications
1. GENERAL
This test method covers the determination of the flowability and passing ability of self-consolidating
concrete (SCC) using the J-Ring and Slump Cone. The diameter of the unobstructed slump flow
versus the obstructed slump flow passing through the J-Ring is a measure of the passing ability of
SCC.
2. EQUIPMENT
The sample of SCC from which test specimens are made shall be obtained according to Section I of
Illinois Test SCC-1.
4. PROCEDURE
b. Place the base plate on level, stable ground. Center the J-Ring on the base plate. The mold
shall be centered within the J-Ring and inverted with the smaller diameter opening down.
c. Strike off the surface of the concrete level with the top of the mold using the tamping rod or strike-
off bar. Remove surplus concrete from around the base of the mold and base plate surface.
g. Calculate the average of the two measured diameters. This is the J-Ring flow.
h. Calculate the difference between the J-Ring flow and the unobstructed slump flow, as tested
according to Illinois Test SCC-2, of the same representative sample. This is the J-Ring value.
Rate the passing ability of SCC using the criteria in Table 1.
5. REPORT
a. Report the unobstructed slump flow (average of two measured diameters) and J-Ring flow
(average of two measured diameters) to the nearest 5 mm (0.25 in.).
4. Illinois Test Procedure SCC-1, Sampling, Determining Yield and Air Content, and Making and Curing
Strength Test Specimens of Self-Consolidating Concrete
6. ASTM E 29 (Illinois Modified), Standard Practice for Using Significant Digits in Test Data to
Determine Conformance with Specifications
3. GENERAL
This test method covers the determination of the flowability and passing ability of self-consolidating
concrete (SCC) using the L-Box. The flow heights ratio is a measure of the passing ability of SCC.
The flow times (T20 and T40) are a measure of the flowability of SCC.
a. L-Box See Figure 1. The inside surface of the L-Box walls shall be of a smooth, rigid,
nonabsorbent material.
b. Tamping Rod or Strike-Off Bar The tamping rod shall conform to that described in T 119. The
strike-off bar shall be a flat straight bar at least 3 mm (0.125 in.) x 20 mm (0.75 in.) x 300 mm (12
in.).
d. Measuring Tape The measuring tape shall have a minimum gradation of 10 mm (0.5 in.).
e. Stopwatch Optional. The stopwatch shall have a minimum reading of 0.2 seconds.
The sample of SCC from which test specimens are made shall be obtained according to Section I of
Illinois Test SCC-1.
c. Ensure the sliding gate is shut, and fill the vertical of the L-Box in one lift without vibration,
rodding, or tapping.
d. Strike off the surface of the concrete level with the top of the L-Box using the tamping rod or
strike-off bar.
f. Raise the sliding gate. Complete the test procedure from the start of filling through opening of the
sliding gate without interruption and within 5 minutes.
g. Optional. Determine the time in seconds it takes for the concrete flow to travel 200 mm (8 in.)
and 400 mm (16 in.), as measured from the time the sliding gate is lifted. These are the T20 and
T40 times, respectively. Refer to Figure 2.
h. When the concrete has stopped flowing, measure the height of the resulting flow at the sliding
gate, H1, and at the end of the horizontal, H2, to the nearest 5 mm (0.25 in.).
a. Report the filling heights, H1 and H2, to the nearest 5 mm (0.25 in.).
c. Report observations of bleeding, and/or air popping on the surface of the concrete flow.
d. Optional. Report the T20 and T40 flow times to the nearest 0.2 second.
1. Illinois Test Procedure SCC-1, Sampling, Determining Yield and Air Content, and Making and
Curing Strength Test Specimens of Self-Consolidating Concrete
2. AASHTO T 22 (Illinois Modified), Compressive Strength of Cylindrical Concrete Specimens
3. AASHTO T 23 (Illinois Modified), Making and Curing Concrete Test Specimens in the Field
4. AASHTO T 24, Obtaining and Testing Drilled Cores and Sawed Beams of Concrete
5. AASHTO T 119 (Illinois Modified), Slump of Hydraulic-Cement Concrete
6. AASHTO R 39 (Illinois Modified), Making and Curing Concrete Test Specimens in the Laboratory
1. GENERAL
This test method covers the determination of the static segregation resistance (stability) of self-
consolidating concrete (SCC). The visual assessment, using a Hardened Visual Stability Index
(HVSI), of cast or cored hardened cylinders cut lengthwise in two is a measure of the stability of SCC.
2. EQUIPMENT
a. Mold The mold shall be a 6 x 12 in. (150 x 300 mm) cylinder mold and conform to T 23 or R 39.
b. Tamping Rod or Strike-Off Bar The tamping rod shall conform to that described in T 119. The
strike-off bar shall be a flat straight bar at least 0.125 x 0.75 x 12 in. (3 x 20 x 300 mm).
c. Suitable container for filling specimen molds.
d. Saw The saw shall have a diamond or silicon-carbide cutting edge and shall be capable of
cutting specimens without excessive heating or shock.
e. Core Drill The core drill shall have diamond impregnated bits attached to a core barrel.
3. MATERIALS
The sample of SCC from which fresh test specimens are made shall be obtained according to Section
I of Illinois Test SCC-1. Cored specimens from hardened concrete shall be obtained according to T
24 and have a minimum diameter of 50 mm (2 in.). When necessary as determined by the Engineer,
the core may be taken so that its axis is perpendicular to the concrete as it was originally placed as
long as the core diameter is sufficiently large enough to assess extent of static segregation.
1
Test method developed by the Illinois Department of Transportation (Original Effective Date: August 12, 2004). Test
method submitted to AASHTO by Illinois Department of Transportation. The AASHTO version is similar and is known
as AASHTO PP 58.
a. A minimum of two fresh test specimens shall be made according to T 23 or R 39, except for the
following:
i. The specimen molds shall be filled in one lift using a suitable container without vibration,
rodding, or tapping.
ii. Strike off the surface of the concrete level with the top of the mold using the strike-off bar or
tamping rod.
iii. The slump flow, VSI, air content, and temperature of each batch of concrete, from which
specimens are made, shall be measured immediately after remixing.
b. Immediately after being struck off, the specimens shall be capped with a plastic cylinder lid and
moved to the storage place where they will remain undisturbed. The specimens shall be
assigned an identification number, and the date of molding, location of concrete, and mix design
number shall be recorded.
c. Before being subjected to sawing, the specimens shall have had a minimum curing period of
24 hours at a minimum temperature of 16 C (60 F) or attained a minimum compressive strength
of 6200 kPa (900 psi) according to T 22.
d. The specimens shall be saw cut lengthwise down the center through its diameter. If the
specimen cannot be satisfactorily sawed smooth from lack of curing, then the remaining
specimen(s) shall remain undisturbed for an additional minimum curing period of 24 hours before
being subjected to sawing.
e. Make a visual assessment of the cut plane of the hardened concrete cylinder(s) using the criteria
in Table 1 and illustrated in Figures 1 8. The cut plane shall be wetted to facilitate visual
inspection.
0 No mortar layer at the top of the cut plane and no variance in size and percent area of
stable coarse aggregate distribution from top to bottom.
Slight mortar layer, less than or equal to 6 mm (1/4 in.) tall, at the top of the cut plane and
1
slight variance in size and percent area of coarse aggregate distribution from top to
stable
bottom.
2 Mortar layer, less than or equal to 25 mm (1 in.) tall, at the top of the cut plane and distinct
unstable variance in size and percent area of coarse aggregate distribution from top to bottom.
Clearly segregated as evidenced by a mortar layer greater than 25 mm (1 in.) tall and
3
considerable variance in size and percent area of coarse aggregate distribution from top to
unstable
bottom.
5. REPORT
a. Report the identification number and required information for each hardened specimen.
b. Report the Hardened Visual Stability Index (HVSI) for each hardened specimen.
1
Test method developed by the Illinois Department of Transportation (Original Effective Date: August 12, 2004). Test
method submitted to AASHTO by Illinois Department of Transportation. The AASHTO version is similar and is known
as AASHTO PP 58.
No mortar layer.
Uniform distribution
of coarse aggregate
from top to bottom.
Note contrast
at top. This is
Visible Mortar layer
a layer of
> 1 in. (25 mm) and
foam, which
considerable variance
may be visible
of coarse aggregate
in any stable or
distribution from top to
unstable mix.
bottom.
1
Test method developed by the Illinois Department of Transportation (Original Effective Date: August 12, 2004). Test
method submitted to AASHTO by Illinois Department of Transportation. The AASHTO version is similar and is known
as AASHTO PP 58.
1. Illinois Test Procedure SCC-6, Standard Test Method for Static Segregation of Hardened Self-
Consolidating Concrete Cylinders
2. Illinois Specification 101, Minimum Requirements for Electronic Balances
3. AASHTO M 92, Standard Specification for Wire Cloth Sieves for Testing Purposes
4. AASHTO T 23 (Illinois Modified), Making and Curing Concrete Test Specimens in the Field
5. AASHTO T 119 (Illinois Modified), Slump of Hydraulic-Cement Concrete
6. ASTM E 29 (Illinois Modified), Standard Practice for Using Significant Digits in Test Data to
Determine Conformance with Specifications
1. GENERAL
This test method covers the evaluation of the dynamic segregation resistance (stability) of self-
consolidating concrete (SCC). The visual assessment using a Hardened Visual Stability Index (HVSI)
or the coarse aggregate weight (mass) retained ratio are measures of the stability of SCC.
2. EQUIPMENT
a. Specimen Mold The mold shall be a 6 x 12 in. (150 x 300 mm) cylinder mold and conform to
T 23.
b. Tamping Rod or Strike-Off Bar The tamping rod shall conform to that described in T 119. The
strike-off bar shall be a flat straight bar at least 0.125 x 0.75 x 12 in. (3 x 20 x 300 mm).
c. Suitable container for filling specimen molds.
d. Saw Procedure Option A onl y, The saw shall have a diamond or silicon-carbide cutting edge
and shall be capable of cutting specimens without excessive heating or shock.
e. Sieve Procedure O ption C onl y, The sieve shall be a No. 4 (4.75 mm) rectangular sieve of
minimum dimensions 13 x 25 in. (330 x 635 mm) manufactured according to AASHTO M 92.
f. Balance Procedure Option C only, The balance shall be according to Illinois Specification 101
for portland cement concrete unit weight measurements.
3. MATERIALS
Test specimens shall be made from separate samples of SCC obtained at or near 1) the point of
discharge by deliver equipment, and 2) the point of flow termination as approved by the Engineer.
1
Test method developed by the Illinois Department of Transportation (Original Effective Date: May 1, 2006).
Option AFor each of the two samples obtained (i.e., one at or near the point of discharge and
another at point of flow termination), conduct testing according to Illinois Test SCC-6 for assessment
of Hardened Visual Stability Index (HVSI).
Option BReserved.
Option CObtain two samples (i.e., one at or near the point of discharge and another at point of flow
termination) and determine the Dynamic Segregation Index as follows:
b. Strike off the surface of the concrete level with the top of the mold using the tamping rod or
strike-off bar.
c. Wet wash over the No. 4 (4.75 mm) sieve the sample collected at or near the point of
discharge.
d. Blot any free water from the retained coarse aggregate particles surface with a towel to
achieve a saturated surface dry (SSD) condition.
e. Determine the weight (mass) of the coarse aggregate to the nearest 0.1 lb. (50 g).
f. Repeat a. e. for the sample collected at the point of flow termination.
g. Calculate the Dynamic Segregation Index (DSI) as follows:
(CA1 CA2 )
DSI = 100
CA1
Where: CA1 = weight (mass) of coarse aggregate collected at or near the point of discharge
CA2 = weight (mass) of coarse aggregate collected at the point of flow termination
5. REPORT
1
Test method developed by the Illinois Department of Transportation (Original Effective Date: May 1, 2006).
1. Illinois Test Procedure SCC-1, Sampling, Determining Yield and Air Content, and Making and Curing
Strength Test Specimens of Self-Consolidating Concrete
2. Illinois Specification 101, Minimum Requirements for Electronic Balances
3. AASHTO M 92, Standard Specification for Wire Cloth Sieves for Testing Purposes
4. AASHTO T 23 (Illinois Modified), Making and Curing Concrete Test Specimens in the Field
5. AASHTO R 39 (Illinois Modified), Making and Curing Concrete Test Specimens in the Laboratory
6. ASTM E 29 (Illinois Modified), Standard Practice for Using Significant Digits in Test Data to
Determine Conformance with Specifications
1. GENERAL
This test method covers the determination of the dynamic segregation (stability) of self-consolidating
concrete (SCC) using the flow trough. The Dynamic Segregation Index (DSI) is a measure of the
dynamic segregation of SCC. A minimum slump flow of 24 in. (610 mm) is recommended to perform
the test.
1
Test method developed by the Illinois Department of Transportation (Original Effective Date: August 1, 2007).
1
Test method developed by the Illinois Department of Transportation (Original Effective Date: May 1, 2006).
1. SCOPE
1.1 This method covers the measurement of formwork pressure of fresh self-consolidating concrete (SCC)
using pressure transducers attached to formwork.
1.2 This is a field test with the intention of measuring formwork pressure during placement of SCC.
1.3 The text of this standard references notes and footnotes that provide explanatory information. These
notes shall not be considered as requirements for this standard.
1.5 This standard may involve hazardous materials, operations, and equipment. This standard does not
purport to address all of the safety concerns, if any, associated with its use. It is the responsibility of the
user of this standard to establish appropriate safety and health practices and determine the applicability
of regulatory limitations prior to use.
2. REFERENCED DOCUMENTS
3.1 This method is applicable when there is a concern about SCC form pressures that may exceed the rated
strength of the formwork. SCC shall be defined by ASTM C 125.
Note 1 Formwork less than or equal to 3 m (10 ft) tall constructed of commercial forms rated at
57.5 kPa (1200 psf) or greater may be able to resist the SCC pressures encountered in the field.
However, the engineer is still responsible for the formwork design.
1
Test method developed by the Illinois Department of Transportation (Original Effective Date: January 1, 2008).
The test method provided is based on the version submitted to AASHTO by Illinois Department of
Transportation. The AASHTO version is similar and is known as AASHTO TP 93.
4.1 Pressure Transducer a suitable pressure transducer for measuring pressure from SCC.
4.2 Data Acquisition System a suitable data acquisition interface for obtaining pressure readings from
pressure transducers.
4.3 Bracket a bracket conforming to the pressure transducer and formwork geometry shall be used for
attaching the pressure transducer to the formwork. Figures 2 and 3 show one such bracket system.
4.4 Portable Hand Drill and Bit a suitable drill and bit for drilling pressure transducer access holes.
4.5 Baby Powder and Cellophane Wrap suitable materials for covering the pressure transducer face.
Note 2 A Vishay Model P3 Strain Indicator and Recorder with Honeywell Model AB/HP pressure
transducers have been used for measuring pressures from SCC. The Vishay unit will accommodate four
pressure transducers, and the required access hole for the Honeywell Model AB/HP pressure transducer
is 35 mm (1 3/8 in.) in diameter.
5. PROCEDURE
5.1.1 Drill an appropriate size access hole through the formwork for the pressure transducer which will allow
measurement of pressure.
5.2.1 Mount the pressure transducer to the formwork using the bracket system. The pressure transducer face
shall extend through a hole drilled in the formwork, and shall align flush with the inside form surface.
5.2.2 The face of the pressure transducer shall be protected with a light dusting of baby powder and a single
layer of cellophane wrap on top.
Note 3This technique prevents direct contact of the SCC with the pressure transducer face while
ensuring measurement of pressure.
5.3.1 Install a minimum of one pressure transducer at or near each point of SCC placement. The first pressure
transducer below the point of SCC placement shall be approximately 300 mm (12 in.) above the base of
the formwork. Additional pressure transducers shall be installed above the bottom transducer at the
direction of the formwork design engineer.
5.4.1 The pressure shall be observed and recorded periodically to ensure that the pressure remains under the
rated strength of the formwork during the pour. The calculation and recording of form filling rate during
the pour should also be performed periodically to evaluate the pour rate influence.
Note 5 The measured pressure will rise as the formwork is filled with SCC, but will eventually slow
down and start falling as the SCC begins to gel and stiffen.
Formwork pressure is also a function of the form filling rate. If the rate is low, the maximum pressure will
be relatively low. If the rate is very high, the pressure may approach hydrostatic pressure. It is cautioned
that if the form filling rate is significantly increased later in the day, formwork pressure above a pressure
transducer location will likely be higher than the pressure at the transducer. In addition, stopping and
subsequently starting a pour will cause the pressure to fluctuate. Therefore, it is important to maintain
relatively constant pour rates through the day.
6. REPORT
6.1.2 The measured pressure at various times during the pour, and
7. KEYWORDS
7.1 Self-consolidating concrete (SCC); formwork pressure; pressure transducer; data acquisition system;
bracket; form filling rate; measured pressure; hydrostatic pressure.
A. Scope
Quality Control Plans for QC/QA Contracts normally require incoming aggregate to
be checked for gradation compliance before use in mix plants. Aggregate is
produced to tight gradation bands at the source but will degrade during handling and
shipment.
B. Purpose
The Contractor shall obtain certified aggregate gradation bands (including master
band, if required) from the aggregate source for all certified aggregates prior to any
shipment of material to the mix plant. Natural sand gradation bands shall be obtained
from the appropriate District Materials Engineer.
D. General Procedure
The Contractor may modify the aggregate source gradation bands according to the
following procedures, if necessary, to check incoming aggregate for gradation
compliance at the mix plant. If not modified, the aggregate source gradation bands
shall be considered the mix plant gradation bands when checking incoming
aggregate.
1. Coarse AggregateThe Contractor may shift the aggregate source master band
a maximum of three percent (3%) upwards to establish a Mix Plant Master Band
for each coarse aggregate used. All other aggregate source gradation bands,
except for the top sieve and bottom sieve bands in the gradation specification,
may also be shifted upward a maximum of three percent (3%). The top sieve and
bottom sieve bands shall not be changed, except as follows:
3. Natural SandThe gradation bands obtained from the Department for each
natural sand shall not be changed.
E. Department Approval
All aggregate source gradation bands and mix plant gradation bands must be sent to
the District Materials Engineer for approval prior to any shipment of aggregate to the
mix plant. Once approved, the mix plant gradation bands shall not be changed
without approval of the District Materials Engineer.
The following table denotes the responsibilities and the person responsible.
7.2 Quality Sampling / Testing. IDOT will continue to sample and test all
aggregates for quality. The IDOT Aggregate Inspector shall sample any certified
stockpile at the frequency designated in the Manual for Aggregate Inspection. All
quality samples are sent to the Central Bureau of Materials and Physical
Research for testing. The tests run were discussed previously in Chapter 3.0
herein. Any certified stockpile must meet the designated quality before shipment.
Willful shipment of out-of-specification material shall be handled according to
Section 11.2 of the Departments current Policy Memorandum, Aggregate
Gradation Control System (AGCS), in Chapter 8.0.
The production plant, from the primary crusher to the final screening/logwashing,
is visited next. This stop verifies that the correct production method is being
used to produce the required quality and gradation. Problems with equipment,
such as screen cloth, etc., can be observed and corrected.
7.3.2 This quick type of inspection helps the Aggregate Technician/AGCS Technician/
Inspector keep a handle on the aggregate being produced. It does not take
away from actual testing of the aggregate but enhances the inspection to ensure
quality aggregate.
7.4.1 Under the Aggregate Gradation Control System, the Aggregate Technician, the
AGCS Technician, the Mixture Aggregate Technician, and the IDOT Aggregate
Inspector must know how to correctly sample aggregate for gradation testing.
The Aggregate Technician/AGCS Technician/Mixture Aggregate Technician will
have to sample at a specified frequency from both production and stockpiles.
They may choose one of the approved production sampling methods described
in Illinois Test Procedure 2, (Chapter 5.0 of the AGCS). The stockpile sampling
method noted in Chapter 5.0 is the only method allowed for sampling a stockpile.
The IDOT Aggregate Inspector will sample on a very infrequent basis. Most of
the IDOT monitor samples will be split samples taken and split by the Aggregate
Technician/AGCS Technician/Mixture Aggregate Technician. However, the IDOT
Aggregate Inspector may take a sample at any time under the program.
The IDOT Aggregate Inspector is required to keep a personal diary on his daily
inspection trips. Much of the same information required for the Aggregate
Technician/AGCS Technician diary is noted by the IDOT Aggregate Inspector.
7.8 Safety. It is the responsibility of the QC Manager, the Aggregate Technician, the
AGCS Technician, the Mixture Aggregate Technician, the IDOT Aggregate
Inspector, and the Gradation Technician to perform their respective duties in a
safe manner. To assure that this condition is met, the QC Manager, the
Aggregate Technician, the AGCS Technician, the Mixture Aggregate Technician,
and the IDOT Aggregate Inspector should be familiar with any an all safety
regulations in force. Great care should be taken when sampling around moving
equipment, e.g., conveyor belts, screen decks, hopper grates, etc. Due to poor
visibility and large truck/equipment traffic, caution should also be used when
driving around the plants and stockpiles.
The QC Manager, the Aggregate Technician, the AGCS Technician, the Mixture
Aggregate Technician, and the IDOT Aggregate Inspector must have a
knowledge of applicable Mine Safety and Health Administration (MSHA)
regulations. The IDOT Aggregate Inspector is also regulated by Departmental
policies covered in the Employee Safety Code handbook.
EXAMPLE
Company Name: _______________________________
Date:
Plant Name:
Weather:
Ledge Information:
Material Being Produced:
VISUAL INSPECTION: 1ST VISIT 2ND VISIT 3RD VISIT ADDITIONAL VISITS
Time:
Stockpile/Loadout:
Degradation YES/NO YES/NO YES/NO YES/NO
Segregation YES/NO YES/NO YES/NO YES/NO
Contamination YES/NO YES/NO YES/NO YES/NO
Plant:
Pit Area:
Graph(s):
Samples Taken:
Production
Loadout:
Resample:
SIGNATURE:
Problems:
(Init./Time)
Action Taken:
(Init./Time)
Comments:
Gradation control charts provide an effective way to monitor the aggregate production
process and can present a graphical record of aggregate gradation during continuous
production and stockpiling. Specific changes or gradual trends in a product's gradation
can be readily identified before major trouble occurs. Other benefits that may also be
realized by using control charts include but are not limited to:
Under the Illinois Aggregate Producer Control Chart Procedure, all gradation test results
(percent passing) for each required gradation/production point tested shall be recorded
on a control chart within one working day of sampling. The control chart/s for any
gradation in the program must therefore have each required sieve represented on the
chart.
The gradation control charts are to be readily accessible at the source and/or approved
laboratory and available for inspection upon request by the Aggregate Inspector or a
representative of the Department. Computer-maintained charts shall be printed and
displayed once per week or at the request of the Department. Control charts are the
property of the Department and shall not be removed or altered in any manner. The
Aggregate Inspector shall check the control charts on a regular basis.
The Illinois Specification 201 Aggregate Gradation Sample Size Table & Quality Control
Sieves document from the Manual of Test Procedures for Materials designates the
required sieves for coarse and fine aggregate gradations.
9.1 Definitions
9.1.1 Average: The sum of a series of test results or measurements divided by the number of
values or measurements included in the sum, also, known as the arithmetic mean.
9.1.2 Check Samples: Samples taken for a specific purpose, other than required by Table 1.
This information may be used to verify an observation or conclusion, or as a means of
confirmation of corrective action, other than required by Table 1. Such samples are
permitted under any circumstances except to replace samples required by Table 1.
9.1.4 Master Band or Control Limits: Mathematical limits placed on gradations, based on
established Master Band limits, which when exceeded initiate action by those
responsible for process control, and/or acceptance of aggregate products. These limits
may be established on the basis of previous historical experience or by start of
production results.
9.1.6 Table 1: Table 1 of the current Bureau of Materials and Physical Researchs Policy
Memorandum, Aggregate Gradation Control System (AGCS) found in Manual of Test
Procedures for Materials
9.1.7 Trend: When two or more points move away from the mid-point target values in either
direction (), thus producing either a steep angled line or three points moving with a
gradual angle. This is usually associated with the moving average points but can also be
determined from individual test points. Trends are indications that a problem(s) are or
will be present if corrective action is not taken.
9.1.8 Warning Band or Moving Average: The average of 5 consecutive values (sample
results) obtained per Table 1 requirements, based on established Warning Band limits.
Such values always represent the most recently obtained test results or measurements
within the prescribed group of observations. These limits may be established on the
basis of previous historical experience or by start of production results.
9.2 Control Chart Paper / Size. Control charts for the Gradation Control Program, when
created by hand, must be placed on 10 x 10 cross-sectional graph paper measuring 420
mm x 280 mm (16-1/2" x 11") or 216 mm x 280 mm (8-1/2" x 11"). Graph paper, used for
this purpose, can be ordered through office supply specialty stores, companies dealing
in drafting materials or ordered thru the internet. An example of a control chart is found
on the last page of this document.
9.3 Chart Preparation. At the top of the control chart, the aggregate product material code
and the Master Band target (when known) will be noted.
The vertical distance between these lines must accurately represent the difference
between the upper and lower limits for each sieve using a vertical scale of one division
(square) which will equal one percent (1%) passing on all sieves except the 75-m (No.
200), see Article 9.3.1.
On the left side of the control chart, the upper and lower specification lines of each sieve
shall be connected by a drawn vertical double arrow.
The specification limits for the each sieve, e.g., 45% for upper limit and 15% for lower
limit, must be indicated at the top (for upper limit) and bottom (for lower limit) of the
arrow. The sieve size, e.g., 4.75 mm (No. 4), shall also be indicated between the limits
on the far left side of the chart.
The vertical scale [(1% = 1 division (square) or for 75m (No. 200), 0.1% = 1 division
(square)] shall be noted below each required sieve.
Each test value will be spaced horizontally every 1/2 or 5 horizontal divisions (squares).
9.3.1 The 75-m (No. 200) sieve, when plotted, shall be plotted for washed tests only.
9.3.2 Master Bands and Warning Bands shall be drawn across the graph for the critical sieve,
when required, as defined in Article 9.5.1 herein. Master Band limits, once known, shall
be represented by a solid line and the Warning Band limits shall be represented by a
broken line.
9.4 Plotting of Test Values. The Gradation Control Program allows the producer to run
both washed and dry gradation tests. The percent passing results for each different kind
of gradation test run shall be plotted on the control chart using specific symbols. All
symbols must measure approximately 2.5 mm (1/10") on each side/diameter.
9.4.1 The symbols to be used for each test type are as follows:
9.4.3 The moving average will be calculated and plotted on the last five consecutive
washed production test values on each critical sieve and is only plotted when a new
washed production test is ran.
The moving average will be started by taking the fifth test value after the start of yearly
production, or production restarted after a protracted shutdown, and averaging it with the
four preceding test values. Once the moving average is established, the moving average
will be calculated and plotted each time a new washed production test value is ran and
plotted.
9.4.4 Each individual test result that is ran and plotted shall have the following information
located at the bottom of the chart below the respective plotted test result.
Every resample was taken. (An R shall be placed under the test result that it
represents
9.4.5 Stockpile load out test results may be plotted or summarized on a separate control chart,
graph, or table. The reporting format may be developed by the Source. The reporting
format shall include the information required in this article (sample type, time, and date).
The control limits and deviation from the established Master Band shall be identified.
9.5 Master Band/Warning Band. During Start of Production, Master Bands/Warning Bands
must be developed and placed on the control chart after five tests or within the first
9,100 metric tons (10,000 tons), whichever occurs first, for each product's critical
sieve, when required. Any production or equipment change after development of a
Master Band may necessitate the development of a new Master Band.
Historical data from washed production samples may also be used, at the Source's
request, to establish Master Band targets. The average, rounded to the nearest whole
number, used to establish the Master Band shall be based only on washed production
critical sieve test results.
9.5.1 Master Bands/Warning Bands will be drawn plus/minus using the below-listed
percentages from a rounded average for each listed coarse aggregate sieve/gradation.
If the critical sieve and the plus/minus percentages for coarse aggregates is not listed,
this information will be assigned by the Bureau of Materials and Physical Research on
an as-needed basis.
9.5.2 When a production change is made, a vertical line shall be drawn through the Master
Band. The change shall be noted on the chart and documented in the Source plant
diary.
9.5.3 A Master Band, when established, shall take precedence over the Standard
Specification limits set for that sieve/gradation.
9.6 Test Values at Master Band/Warning Band Limits. When an individual test value on a
Master Band exceeds the Master Band limits, the producer must treat that test result as
a failure. Article 6.5 of the current Department Policy Memorandum "Aggregate
Gradation Control System" (AGCS) shall be enacted. Article 6.5 of the AGCS requires
resamples/corrective action be taken in response to the initial failing test.
The situation of the moving average hitting or exceeding a Warning Band is different
than a failing individual test and Master Bands. When the moving average hits or
exceeds the Warning Bands, the Source must decide whether to take corrective action
to bring the gradation back within the Warning Bands or to develop a new Master Band.
The Source must notify the District what action was taken.
If a new Master Band is developed, the material shall be stockpiled separately from the
previous production.
The development of a new Master Band may necessitate new HMA or PCC mix designs.
15
21 23 21 23 24 23 21 23 24 27 31 31 29 26 25 24 24 23 22
#16 Sieve
4
2 3 2 2 3 1 2 3 2 2 3 2 2 3 3 2 2 2 1
10/3 10/4 10/5 10/6 10/7 10/10 10/11 10/12 10/14 10/15 10/18 10/18 10/18 10/18 10/19 10/20 10/21 10/22 10/23
AM AM AM PM AM AM AM AM PM AM AM AM PM PM AM AM PM AM AM
R R R
Scale: 1 square = 1%
Comparison Method
Calculate size fraction between consecutive sieves, including cutter sieves, for both the
State Monitor and Producer test results (% Passing).
Show the fraction retained between consecutive sieves for both gradations, the fraction
difference on each consecutive sieve grouping between the Monitor and Producer
gradation, the applicable tolerance (if coarse aggregate, use coarse aggregate
tolerances and, if fine aggregate, use fine aggregate tolerances- If size fraction between
consecutive sieves exceeds largest fraction shown, use tolerance for largest size
fraction), and whether they are in-tolerance or out-of-tolerance.
If the comparison has no out-of-tolerance fractions, both sample results are considered
valid. If and out-of-tolerance situation has been identified, both the producer certified
technician and the State inspector shall immediately investigate the splitting procedure,
test equipment, test method, and calculations for possible equipment failure or
procedure errors. The State Monitor Sample shall always take precedence unless
shown to be invalid during investigation.
Example:
Comparison Data
Consecutive Monitor Producer Fraction Applicable
Sieve Sizes Fraction Fraction Difference Tolerance Disposition
25 mm and 19 mm 13 11 2 5 OK
(1 and 3/4")
19 mm and 16 mm 20 22 2 5 OK
(3/4 and 5/8)
16 mm and 12.5 mm 31 23 8 7 Out
(5/8 and 1/2")
12.5 mm and 9.5 mm 23 30 7 6 OUT
(1/2 and 3/8)
9.5 mm and 6.3 mm 9 9 0 3 OK
(3/8 and 1/4")
6.3 mm and 4.75 mm 2 2 0 2 OK
(1/4 and #4)
4.75 mm and 1.18 mm 1 1 0 2 OK
(#4 and #16)
1.18 mm and 75 m 0.3 0.7 0.4 2 OK
(#16 and #200)
75 m and Pan 0.7 1.3 0.6 2 OK
(#200 and Pan)
Model Annual Quality Control (QC) Plan for Hot-Mix Asphalt (HMA) Production
Appendix B1
Producer Name:
Producer/Supplier No.:
Address:
City/State/ZIP Code:
Phone No.:
A. Contractor Responsibilities
In joint ventures, where one Contractor is producing the mix and another is
responsible for the laydown, the Quality Control Manager, from either party, who is
ultimately responsible for the Quality Control should be identified in the Quality
Control Addendum.
B. Materials
All materials proposed for use are from approved sources. Material sources are
identified below for coarse aggregate, fine aggregate, mineral filler, asphalt binder,
prime, anti-strip additive, and release agent. This includes the mix type,
Producer/Supplier Number, firm name, and firm location.
Producer/
Material Mix Type Supplier No. Firm Name Location
(1)
(2)
(3)
(4)
(5)
(6)
(7)
Model Annual Quality Control (QC) Plan for Hot-Mix Asphalt (HMA) Production
Appendix B1
(continued)
Effective: May 1, 1993
Revised: January 1, 2008
Producer/
Material Mix Type Supplier No. Firm Name Location
(8)
(9)
(10)
1. Aggregates
The incoming aggregate gradation bands have been developed from the
source gradation bands and are attached. Listed below are the contact
persons for the aggregate sources furnishing mixture aggregates.
All aggregate stockpiles will be built using procedures that will minimize
segregation and degradation. All coarse and fine aggregate will be placed
in single-layer truck-dumped stockpiles at the mix plant. QC personnel will
pay special attention to the loadout, replenishing, and remixing of the
aggregate stockpile.
A washed gradation test will be performed for each 500 (tons 450 metric
tons) for the first 1,000 tons (900 metric tons) for each aggregate
received. Additional gradation tests (every third test will be a washed
Model Annual Quality Control (QC) Plan for Hot-Mix Asphalt (HMA) Production
Appendix B1
(continued)
Effective: May 1, 1993
Revised: January 1, 2008
gradation test) will be run on the frequency of one test per 2,000 tons
(1,800 metric tons) for each aggregate received while the stockpiles are
being built or aggregate is being shipped in. Gradation correction factors
will be developed from washed gradation test results and applied to all dry
gradation results. All aggregate (correction factors applied) will meet the
mix plant gradation bands as developed according to the current
Department policy, "Development of Gradation Bands on Incoming
Aggregate at Mix Plants", before being used in mix production at the mix
plant. All incoming aggregate gradation results shall be recorded in the
plant diary. If a failing sample is encountered, the following resample
procedure will be followed:
(2) If the first resample passes, the required frequency will be continued.
(3) If the first resample fails, shipment of the aggregate will be halted,
and corrective action will be taken. Corrective action may be
rejection of the material, remixing or addition of material by
feeder/conveyor system, or any other action approved by the
Engineer. The aggregate producer will be notified of the problem. A
second resample will be taken immediately after corrective action.
(5) If the second resample fails, the aggregate represented will not be
used in the QC/QA HMA mixture. The material will be removed from
the certified aggregate stockpile.
Model Annual Quality Control (QC) Plan for Hot-Mix Asphalt (HMA) Production
Appendix B1
(continued)
Effective: May 1, 1993
Revised: January 1, 2008
After mix production has started, all aggregate stockpiles will be checked
with a required washed gradation sample on a weekly basis. This testing
will be waived if the mixture is classified as a small tonnage item
according to the special provision. The test results shall be compared to
the mix plant gradation bands for compliance. These gradation results will
be noted in the Plant Diary, and a copy will be provided to the District
Engineer.
(2) If the first resample passes, mix production may continue. Several
additional check samples will be taken to monitor the stockpile.
(3) If the first resample fails, mix production will be halted, and corrective
action will be taken on the stockpile. Corrective action may include
rejection of the material, remixing or addition of material by
feeder/conveyor system before use in the plant, or any other action
approved by the Engineer. The aggregate contact person will be
notified of the problem. A second resample will be obtained
immediately after corrective action.
(4) If the second resample passes, mix production will begin. Several
additional check samples will be taken to monitor the stockpile.
(5) If the second resample fails, the stockpile will not be used in the
QC/QA HMA mixture.
Aggregate not meeting the mix plant gradation bands shall not be used in
the QC/QA HMA mixtures.
Model Annual Quality Control (QC) Plan for Hot-Mix Asphalt (HMA) Production
Appendix B1
(continued)
Effective: May 1, 1993
Revised: January 1, 2008
C. Mix Design
All requirements of the Standard Specifications Section 1030, and the items listed
in the Department's current "QC Personnel Responsibilities and Duties Checklist"
will be met by the QC personnel. All personnel being utilized to run the Quality
Control sampling and testing shall have taken and passed the appropriate HMA
QC/QA level of training. The QC Manager will assign duties in accordance with the
"QC Personnel Responsibilities and Duties Checklist". The QC Manager will assure
the listed duties are performed and documented. Additional duties, when
necessary, will be assigned and monitored by the QC Manager. Sufficient QC
personnel will be provided to run the QC Plan. Additional QC personnel will be
added when necessary.
All equipment has been calibrated, and the supporting documentation is on file at
the QC laboratory. The QC Laboratory was approved by the Department's Bureau
of Materials and Physical Research and by District __________ on
___________________________. The laboratory/equipment will be available for
inspection by the Engineer.
Model Annual Quality Control (QC) Plan for Hot-Mix Asphalt (HMA) Production
Appendix B1
(continued)
Effective: May 1, 1993
Revised: January 1, 2008
F. Mix Plant/Production
Manufacturer
Model Number
Serial Number
Batch Size
Tons Per Hour
Approved By
Approval Date
It is our intent to run the day following start-up. Production will not begin until the
acceptable nuclear/core correlation is complete, all other required tests are
acceptable, the targets are established, and the results are reviewed and agreed to
by the Department.
The aggregate feeders will be calibrated prior to the start of production using the
aggregates and approximate percentages approved in the Job Mix Formula (JMF).
At this time aggregate samples will be taken and compared with the JMF.
At the start of mix production or when adjustments are made to the mix, the QC
Manager will give the aggregate proportions to the plant operator, and then,
periodically throughout the day, checks will be made of the actual proportions used.
This will be especially noted and recorded when a nuclear asphalt and/or a mix
sample is taken. The results will be immediately reported to the Resident Engineer
and/or other designated Department personnel upon completion of the test.
All scale and sensitivity checks will be performed in accordance with the Hot-Mix
Asphalt Level II Technician Course manual. Surge bins may be utilized as part of
the overall plant operation. The QC Manager shall contact the Department for
approval when material will be stored overnight.
All sampling and testing, including all required plant tests, resamples, and additional
check tests (when necessary), will be performed in accordance with Department
test methods in the time frame required in Section 1030 of the Standard
Specifications. The "Radioactive Material License" required for nuclear density and
asphalt binder content determinations are attached. District Materials or the Bureau
of Materials and Physical Research personnel are welcome to observe all testing by
the QC personnel. Time permitting, split samples will be shared with Department
Model Annual Quality Control (QC) Plan for Hot-Mix Asphalt (HMA) Production
Appendix B1
(continued)
Effective: May 1, 1993
Revised: January 1, 2008
personnel prior to start-up. Coring will be performed using a truck-mounted drill rig
or by suitable equipment as approved by the Engineer. An adjustment of 1-1/2% to
2% for minus No. 200 (0.075 mm) material of washed samples vs. dry gradations
will be used until a gradation correction factor is established based on preliminary
aggregate sampling and testing.
All Department split samples will be stored on site. These samples will be identified
with the date and time the material was sampled, Sequence Number, Contract
Number, mix plant Producer/Supplier Number, aggregate source
Producer/Supplier Number, and the initials of the individual who sampled the
material.
Only approved equipment will be used in the placement and compaction of the mix
in accordance with the Standard Specification requirements.
The QC Manager will verify that all laydown equipment conforms to Department
requirements prior to start-up. At the start of laydown, Two Growth Curves will be
run on a test strip to determine the suitability of the mix. Mix samples shall be taken
and tested from trucks representing material between both Growth Curves. From
Growth Curve information, a rolling pattern will be established. Nuclear tests and
cores will be taken from the start-up area to verify density and correlation of the
nuclear density gauge. Temperatures of the mix will be taken and duly recorded.
After the start-up data is approved by the Department and actual production has
begun, daily nuclear density tests will be taken at the start of each day's production,
along with temperature readings, to verify continued conformance with density
requirements. Nuclear density tests according to the Section 1030 will be performed
to assure compliance with specified density requirements. Testing will be conducted
within the project traffic control, or by use of flaggers, as needed.
Start-up and construction of the test strip is planned to be performed in the morning
of the first day. If no problems are encountered, cores for nuclear/core correlation
will be taken. The mat will be cooled with ice or dry ice. All tests will be completed
for anticipated production the next day.
Should any adverse mix characteristics be observed, the QC Manager shall make
mix adjustments as needed to correct the situation.
Model Annual Quality Control (QC) Plan for Hot-Mix Asphalt (HMA) Production
Appendix B1
(continued)
Effective: May 1, 1993
Revised: January 1, 2008
The QC Manager or his representative will check laydown equipment daily for
specification compliance and immediately repair or replace nonconforming
equipment.
I. Corrective Action
All test results will be reported daily to the Resident Engineer and other designated
personnel as requested by the Department. The data will be reported on the
following forms or on forms generated by the Department's current QC/QA
software:
The completed forms will be forwarded to the District Engineer within three days of
test completion.
Model Annual Quality Control (QC) Plan for Hot-Mix Asphalt (HMA) Production
Appendix B1
(continued)
Effective: May 1, 1993
Revised: January 1, 2008
K. Control Charts
In addition, control charts will be posted at the laboratory and kept updated for the
following test parameters in accordance with the Department's current "Hot-Mix
Asphalt QC/QA Control Charts/Rounding Test Values".
1. Gradations
Hot-Bins/Combined Belt
Percent Passing 1/2-in. (12.5-mm) Sieve
Percent Passing No. 4 (4.75-mm) Sieve
Percent Passing No. 8 (2.36-mm) Sieve
Percent Passing No. 30 (600-m) Sieve
Percent Passing No. 200 (75-m) Sieve
Ignition Oven
Total Dust Content
2. Gravities
4. Density
6. Stockpile Gradations
In the event the Total Dust Content is out of tolerance, measures will be taken to
correct the problem, which may include adding Positive Dust Control Equipment.
Model Quality Control (QC) Addendum for Hot-Mix Asphalt (HMA) Production
Appendix B2
Contract No.:
Marked Route:
Route:
Section:
County:
Contractor:
Address:
City/State/ZIP Code:
Phone No.:
A. Contractor Responsibilities
This Quality Control Addendum to the Annual Quality Control Plan further explains
how ________________________________ proposes to control the equipment,
ingredient materials, and production methods to ensure the specified product is
obtained. All requirements in Section 1030, the Annual QC Plan, and this QC
Addendum will be adhered to.
RAP will meet the requirements of Sections 406, 1030 and 1102 of the Standard
Specifications and any Special Provisions in the Contract. ______ percent of RAP
is proposed for use in the ____________________________ course.
Model Quality Control (QC) Addendum for Hot-Mix Asphalt (HMA) Production
Appendix B2
(continued)
Effective: July 1, 1995
Revised: May 1, 2007
C. Mix Design
The project QC Manager will have overall responsibility and authority for Quality
Control at both the plant and on the road and will make the necessary adjustments
in the mix production, placement, and compaction to assure conformance with the
Standard Specifications and Contract Special Provisions.
The QC personnel and/or consulting firm that will be utilized, as well as the backup
QC personnel and/or consulting firm, are as follows:
Level of Phone
Name Training Firm Number
(1)
(2)
(3)
(4)
(5)
(backup)
E. Mix Plant/Production
The mix for this project will be produced by Producer/Supplier No. _____________.
F. Control Charts
A copy of the Control Charts will be submitted to the Engineer upon completion of
the Contract.
A. Scope
1. This method covers the proper procedures for correlating nuclear gauge densities to
core densities. Procedures are applicable to both direct transmission and backscatter
techniques.
2. The procedure shall be used on all projects containing 3000 tons (2750 metric tons) or
more of any hot-mix asphalt mixture. It may also be used on any other project where
feasible. The direct transmission method shall be used for thick-lift layers. "Thick-lift" is
defined as a layer 6 in. (152.4) mm or greater in compacted thickness.
B. Applicable Documents
2. The density test procedure shall be in accordance with the Department's "Illinois-
Modified ASTM D 2950, Standard Test Method for Determination of Density of
Bituminous Concrete In-Place by Nuclear Method".
C. Definitions
Test site: Individual test site where a single density is determined. Five (5) test sites are
located at each test location.
Nuclear Density: The average of 2 or possibly 3 density readings on a given test site.
1. Density results from a nuclear gauge are relative. If an approximation of core density
results is required, a correlation must be developed to convert the nuclear density to
core density.
E. Site Selection
1. The nuclear density tests and cores necessary for nuclear/core correlation shall be
obtained during the start-up of each specific mixture for which a density specification
is applicable.
2. Three correlation locations shall be selected. Two sites will be located on the two
growth curves from the first acceptable test strip. The third location shall be chosen
after an acceptable rolling pattern has been established and within the last 100 tons
(90 metric tons) of material placed during start-up. The material from the third site
shall correspond to the same material from which the second hot-mix sample was
taken.
3. If a mixture start-up is not required, two of the three correlation locations shall be in an
area containing a growth curve.
1. Backscatter Mode
a. At each of the three correlation locations, five individual sites shall be chosen and
identified as shown in Figure 1.
b. Two nuclear readings shall be taken at each of the 15 individual sites. (See
Figure 1.) The gauge shall be rotated 180 degrees between readings at each
site. (The two uncorrected readings taken at a specific individual site shall be
within 1.5 lbs/ft3 [23 kg/m3). If the two readings do not meet this criterion, one
additional reading shall be taken in the desired direction. The nuclear densities
are to be recorded on the correlation form (Figure 3).
c. One core in good condition shall be obtained from each of 15 individual sites
(Figure 1). Care should be exercised that no additional compaction occurs
between the nuclear testing and the coring. The cores shall be tested for density
in accordance with Illinois-Modified AASHTO T 166 or T 275. The core densities
are to be entered on the correlation form.
For quality assurance purposes, the Department may direct the Contractor to
take additional cores adjacent to those above or to submit the quality control
cores for Department testing.
d. Extreme care shall be taken in identifying which location each of the density
readings represents. The data points have to be paired accurately or the
correlation process will be invalid.
a. At each of the three correlation locations, five individual sites shall be chosen
across the mat as shown on Figure 1.
b. A smooth hole in the pavement, slightly larger than the probe, shall be formed to
a depth 2 in. (50 mm) greater than the test depth. The probe shall be inserted so
that the side of the probe facing the center of the gauge is in intimate contact with
the side of the hole. Two nuclear readings shall be taken at each of the 15
individual sites. (See Figures 1 and 2)
The gauge shall be rotated 180 degrees (see Figure 2) around the core area at
each site. (The two uncorrected readings taken at a specific individual site shall
be within 2.0 lbs/ft3 [30 kg/m3] (see Figure 2). If the two readings do not meet this
criterion, one additional reading shall be taken in the desired direction. The
nuclear densities are to be recorded on the correlation form (Figure 3).
c. One core in good condition shall be obtained from each of the 15 individual sites.
(See Figures 1 and 2) The cores shall be obtained from beneath the center of the
gauge no closer than 3-1/2 in (87.5 mm) from either access hole. The thickness
of the core should represent the thickness of the layer being tested. The layer
shall be carefully separated for testing in accordance with Illinois-Modified
AASHTO T 166. Care should be exercised that no additional compaction occurs
between the nuclear testing and the coring. The cores shall be tested for density
in accordance with Illinois-Modified AASHTO T 166 or T 275.
For quality assurance purposes, the Department may direct the Contractor to
take additional cores adjacent to those above or to submit the quality control
cores for Department testing.
d. Extreme care shall be taken in identifying which location each of the density
readings represents. The data points have to be paired accurately or the
correlation process will be invalid.
1. The two (or possibly three) nuclear readings at each individual site shall be entered on
the correlation form and then averaged. The core density taken at each individual site
shall be entered on the correlation form. After the averaging, there will be 15 paired
data points, each pair containing the average nuclear density and core density for
each of the 15 individual sites.
2. The paired density values shall be correlated using the Department's linear regression
program. (Disks are available from the Bureau of Materials and Physical Research) or
an approved and equivalent calculating method.
3. For the purpose of this procedure, standard statistical methods for measuring the
"best fit" of a line through a series of 15 paired data points consisting of core density
and nuclear density shall be used.
5. Correlation coefficients (r) may range from minus 1.0 to plus 1.0. An "r" value greater
than 0.715 is considered acceptable.
FIRST GROWTH CURVE IS BETWEEN 200 AND 225 METRIC TONS (225 AND 250 (BACKSCATTER)
TONS), THE SECOND GROWTH CURVE IS BETWEEN 250 AND 275 METRIC TONS
(275 AND 300 TONS).
300 mm (1 FT.) 300 mm (1 FT.)
FIGURE 1
3 (8) A 3 (8) B 13A 13B
PAVING DIRECTION
1 CORRELATION
2 CORRELATION LOCATIONS LOCATION IN AN AREA
IN GROWTH CURVE AREAS 1 (6) A 1 (6) B REPRESENTING A 11A 11B
REGULAR ROLLING
PATTERN.
2 of 3 sites
1 of 3 sites
NUCLEAR/CORE CORRELATION TEST LOCATIONS
FIGURE 2
1A 1B
DIRECT TRANSMISSION
NUCLEAR SITE CORE PROBE HOLE
NUCLEAR/CORE CORRELATION
Date:
Contract: Gauge No.:
Job No.: Layer Thickness:
Route: Gmm
Base Material: Milled Binder Aggregate Other:
Mix No.:
Mix Code:
Use: (surface, 1st lift binder, etc.)
STATION:
6A) 6B) 6A) 6B) 6) 6)
STATION:
11A) 11B) 11A) 11B) 11) 11)
For mixtures where the quantity exceeds 3000 tons (2750 metric tons), the Contractor and the
Department shall evaluate the mixture to be produced for each contract using a 300 ton test
strip. The Contractor shall follow the following procedures for constructing a test strip.
A team of both Contractor and Department personnel shall construct a test strip and
evaluate mix produced at the plant.
1. Resident Engineer
2. District Construction Supervising Field Engineer, or representative
3. District Materials Mixtures Control Engineer, or representative
4. Contractor's QC Manager, required
5. Contractor's Density Tester
6. Bureau of Materials and Physical Research representative when requested
7. Bureau of Construction representative when requested
B. Communications
The Contractor shall advise the team members of the anticipated start time of production
for the mix. The QC Manager shall direct the activities of the test strip team. A Department-
appointed representative from the test strip team will act as spokesperson for the
Department.
C. Acceptance Criteria
1. Mix Design and Plant Proportioning - The mix design shall be approved by the
Department prior to the test strip. Target values shall be provided by the Contractor
and will be approved by the Department prior to constructing the test strip.
2. Evaluation of Growth Curves - Mixtures which exhibit density potential less than or
greater than the density ranges specified in Article 1030.05(d)(4) shall be considered
to have a potential density problem which is normally sufficient cause for mix
adjustment.
If an adjustment has been made, the Engineer may require an additional test strip be
constructed and evaluated. This information shall then be compared to the AJMF and
required design criteria for acceptance.
3. Evaluation of Required Plant Tests - If the results of the required plant tests exceed
the JMF target value control limits, the Contractor shall make allowable mix
adjustments/plant changes, resample, and retest. If the Engineer determines
additional adjustments to the mix will not produce acceptable results, a new mix
design may be required.
The Contractor shall produce 300 tons (275 metric tons) of mix for the test strip. The
test strip will be included in the cost of the mix and will not be paid for separately since
the Contractor may continue production, at their own risk, after the test strip has been
completed.
a. Location of Test Strip - The test strip shall be located on a relatively flat portion of
the roadway. Descending/ascending grades or ramps should be avoided.
b. Constructing the Test Strip - After the Contractor has produced and placed
approximately 225 to 250 tons (200 to 225 metric tons) of mix, paving shall cease
and a growth curve shall be constructed. After completion of the first growth
curve, paving shall resume for the remaining 50 to 75 tons (45 to 70 metric tons),
and the second growth curve shall be constructed within this area. The
Contractor shall use normal rolling procedures for all portions of the test strip
except for the growth curve areas which shall be compacted solely with a
vibratory roller as directed by the QC Manager.
c. Required Plant Tests - A set of mixture samples shall be taken at such a time as
to represent the mixture in between the two growth curve trucks.
The mixture sampled to represent the test strip shall also include material
sufficient for the Department to conduct a Hamburg Wheel test according to
Illinois modified AASHTO T 324.
E. Compaction Requirements
1. Compaction Equipment - The Contractor shall provide a vibratory roller meeting the
requirements of Article 1101.01(g) of the Standard Specifications. It shall be the
responsibility of the test strip team to verify specification compliance before
commencement of growth curve construction. An appropriate amplitude shall be
selected on the basis of roller weight and mat thickness to achieve maximum density.
The vibratory roller speed shall be balanced with frequency so as to provide
compaction at a rate of not less than 10 impacts per 1 ft. (300 mm).
3. Compaction and Testing - The Contractor shall direct the roller speed and number of
passes required to obtain a completed growth curve. The nuclear gauge shall be
placed near the center of the hot mat and the position marked for future reference.
With the bottom of the nuclear gauge and source rod clean, a 1-minute nuclear
reading (without mineral filler) shall be taken after each pass of the roller. Rolling shall
continue until a growth curve can be plotted, the maximum density determined, and
three consecutive passes show no appreciable increase in density or evident
destruction of the mat.
4. Final Testing - A core shall be taken and will be secured by the Department from each
growth curve to represent the density of the in-place mixture. Additional random cores
may be required as determined by the Engineer.
F. Nuclear/Core Correlation
A correlation of core and nuclear gauge test results may be performed on-site as defined in
the Department's "Standard Test Method for Correlating Nuclear Gauge Densities with
Core Densities". All correlation locations should be cooled with ice or dry ice so that cores
can be taken as soon as possible. Three locations should be selected. Two sites should be
located on the two growth curves from the first acceptable test strip. The third location
should be in an area corresponding to the second set of mixture samples taken at the
plant. This correlation should be completed at the same time by the Contractor prior to the
next day's production. Smoothness of the test strip shall be to the satisfaction of the
Engineer.
H. Documentation
All test strips, required plant tests, and rolling pattern information (including growth curves)
will be tabulated by the Contractor with a copy provided to each team member and the
original retained in the project files.
The following checklists detail the required minimum duties of Contractor Quality Control (QC)
personnel. The QC Manager has overall responsibility to ensure that the listed duties are
performed and documented. The QC Manager shall not perform sampling and/or testing except
in emergency situations or in any other situation approved by the Engineer. Additional duties, as
necessary, may be required to control the quality of production and placement of the Hot-Mix
Asphalt (HMA) mixtures. A Level II Technician may be used to perform any Level I Technician
duties.
Note: Testing frequency denoted as "P" = "Prior to Start-up" and as "D" = "Daily".
A. Level I Technician
1. Checklist
e. Take required samples when required using proper procedures. (D) ___
2. Required Tests. The minimum test frequency shall be according to Section 1030 of
the Standard Specifications. However, additional tests may be required by the
Engineer.
a. Stockpiles
(washed gradations minimum one per week for each material used) ___
e. Gmb ___
f. Gmm ___
1. Material Source
It is necessary to identify the source of the ingredients to ensure that they have been
inspected and the correct quality of aggregate, grade of asphalt binder, and anti-strip
additive are being used in the specified mix. Sources shall be verified.
2. Aggregate Quality
The Level II Technician may confirm the quality of the aggregate by requesting current
quality information from the District Materials office.
3. Stockpiling
Sites for stockpiles shall be grubbed and cleaned prior to storing the aggregates.
Separate stockpiles shall be provided for the various sources and kinds of aggregates.
Stockpiles shall be separated to prevent intermingling at the base (width of endloader
bucket). If partitions are used, they shall be of sufficient heights to prevent
intermingling. Aggregates for HMA mixtures shall be handled, in and out of the
stockpiles, in such a manner that will prevent contamination and degradation.
Coarse aggregate stockpiles shall be built in layers not exceeding 1.5 m (5 ft) in height
and each layer shall be completely in place before the next layer is started. A stockpile
may be expanded by again starting the expansion from the ground and building layers
as before. End-dumping over the sides will not be permitted. Use of steel track
equipment on Class B Quality, Class C Quality and all blast furnace slag aggregate
stockpiles shall not be permitted where degradation is detected. When loading out of
stockpiles, vertical faces shall be limited to reasonable heights to eliminate
segregation due to tumbling. Segregation or degradation due to improper stockpiling
or loading out of stockpiles shall be just cause for rejecting the material.
4. Gradations
The Level II Technician shall obtain the average gradations as well as the Master
Bands from the aggregate source. He/She shall run the required gradation's test
frequency on incoming aggregate as required in Section 1030 of the Standard
Specifications.
5. Asphalt Binder
a. Incoming Asphalt Binder: The Level II Technician shall periodically check the
grade and temperature of asphalt binder as received at the plant. If the asphalt
binder is shipped by truck, the driver should have in his possession a numbered
ticket showing the name and location of the refinery, the name of the material,
date shipped, loading temperature, quantity, specific gravity or weight/L
(weight/gal), and the number of the tank from which the asphalt was loaded. It is
the responsibility of the refinery to load trucks only from tanks that have been
tested and approved by the Department. If shipment is made by rail, a tag usually
will be found on the top of the dome of the tank car indicating that it has been
sampled at the refinery.
b. Asphalt Binder Storage: The Level II Technician shall check the temperature of
the asphalt binder in storage. The temperatures shall be maintained in
accordance with the Standard Specifications. The Level II Technician should be
aware of the grade of asphalt binder in each storage tank. Asphalt binders of
different sources and grades shall not be intermixed in storage, and the tanks
shall be identified.
6. Testing Equipment
Care of the laboratory testing equipment is the responsibility of the Level I Technician.
Equipment shall be furnished by the Contractor or Consultant, kept clean, and kept in
good working condition. At the start of the project, the technician shall check that all
equipment required to be furnished is available and in good condition. Acceptance
and, ultimately, performance of a mixture may be dependent on the accuracy of the
field tests. Defective equipment could result in erroneous, as well as untimely, results.
7. Asphalt Plant
a. Plant Approval: Plant must be approved and calibrated prior to production each
construction season. The QC Manager shall review this information. If it is not
available or current, the District Hot-Mix Asphalt Supervisor shall be notified.
b. Cold Aggregate Bins: The cold aggregate bins or bulkheads shall be checked for
aggregate intermingling. Each bin or compartment in a bin shall contain only one
source and type of aggregate. The bins should be checked each day to ensure
the charging of the compartments remains the same as it was for previous
operations for the same mix. The QC Manager shall notify the state inspector of
changes in aggregate source and gradation and/or gate settings.
c. Dust Collector: The Level II Technician shall check that the dust from the primary
collector is returned to the boot of the hot elevator by a metering system as
required by Article 1102.01(a)(5) of the Standard Specifications. This metering
system should be such as to require a few adjustments in maintaining a uniform
rate of collected dust returned to the hot elevator. The primary dust-feed shall
occur only when aggregate is being discharged from the drier.
Plants having dry secondary collectors shall return this material to a storage silo
or the mineral filler bin if it will meet the requirements of the mineral filler
specifications (Section 1011 of the Standard Specifications).
e. Hot-Bins: The Level II Technician is to ensure that each hot-bin overflow pipe is
working to prevent back-up of material into other compartments or bins. An
overflow or sudden shortage of material in a bin may indicate a broken or
clogged screen, a change in feeding rate, or a change in gradation of the
aggregate being used. Overflow pipes shall not be discharged into the hot
elevator.
g. Timers: The timers used for recycling the wet and dry mixing times for a batch
plant shall be checked and set at the required mixing times. On continuous
plants, the pugmill dam gate shall be in the raised position. The required times
are in the appropriate articles of the Standard Specifications.
h. Batching: The Level II Technician shall observe the batching operation to ensure
the approved batch weights are being met. Manually operated batch plants shall
have markers on the scales to indicate the approved batch weight of each
ingredient material. Automatic batching plants shall have posted near the scales
the approved weights per bin. On continuous plants, the gate openings shall be
checked for the proper setting. It is recommended that batch counters and/or ton
counters be set at "zero" or that initial and final readings be taken and recorded
each day.
i. Surge and Storage Bins: When a surge and storage bin are used, approval and
scale calibration information should be available. They shall be inspected for
compliance with Article 1102.01(a)(6) of the Standard Specifications. Trucks shall
be loaded in such a manner as to minimize segregation.
j. The platform and/or suspended weigh hopper scale shall be checked for proper
zero. The scales shall be cleaned off before starting each day.
k. The anti-strip additive system calibration shall be checked and the proper flow
rate determined.
l. The weigh ticket printer shall be checked for information required by the
specifications.
m. The computer and/or control system shall be checked to see if the correct
percentages of materials have been entered. The automatic printer for the
computer of the drier drum should be turned on and working.
8. Trucks
A Level I Technician, under the direct supervision of the QC Manager or the Level II
Technician, shall inspect the trucks used to transport the HMA mix. The technician
shall see that each truck is provided with a cover and is properly insulated, if specified,
before it is permitted to be used in the transportation of the mixture from the plant to
the job. The truck bed shall be observed for foreign material before the bed is
lubricated. He/She shall observe the spraying of the inside of the trucks with a release
agent and shall see that no pools of release agent remain in the truck beds before
loading.
9. Mixture Inspection
The Level II Technician shall inspect the mixture at the plant, which includes
observing the weighing of the materials; checking the temperature of the mixture; and
visually inspecting for coating of the aggregates, segregation, and moisture in the
mixture. The Level I Technician shall sample and determine the gradation of the hot-
bins and/or cold-feeds and the proper amount of asphalt binder being used to ensure
conformity to the mix formula. The Level II Technician shall also verify and document
the addition rates of the anti-strip additives.
In addition, the Level I Technician shall perform the required core density tests and,
when required, extraction tests at the field laboratory.
The QC Manager shall furnish the Contractor with the mixing formulas which have
been established for a specific combination of sources of ingredients. The formulas
shall state the percentage of aggregate for each sieve fraction and the percentage of
asphalt binder. These formulas are to be used in proportioning the ingredient
materials for HMA mixtures within the specified tolerances. Changes in the mix
formulas are to be made only by the QC Manager.
It is important that the QC Manager observe the laying and compaction of the mixture.
Mixture variations are noticeable in the completed work, and variations that are not
apparent in the mixture at the plant sometimes show up as defects in the texture and
uniformity of the surface. Flushing of the mixture is a defect that can be detected only
on the road.
It is the duty of both the Level I and Level II Technicians to establish and maintain an
open line of communications.
11. Samples
The Level I Technician shall take check samples of the mixture in addition to the
required samples. He/She must also store split samples in a dry storage area for the
Engineer. Section 1030 of the Standard Specifications discusses sampling
procedures and sampling frequency.
12. Reports
The Quality Control Manager is responsible for completion of a "Daily Plant Output
Report" (MI 305) for each day of production for each type of mix. Other reports, when
required, are "Sample Identification" (LM-6), and Scale Checks.
Initial Daily Plant and Random Samples shall be obtained at the frequency specified in Section
1030 of the Standard Specifications.
A. Truck samples shall be taken of the mixture for testing. Two sampling platforms (one on
each side of the truck) shall be provided for sampling of the mix. In order to obtain a
representative sample of the entire truck, an equal amount of material shall be taken from
each quarter point around the circumference of each pile in the truck to obtain a composite
sample weighing approximately 150 lbs (70 kg). All truck samples shall be obtained by
using a "D"-handled, square-ended shovel with built-up sides and back (1 to 1 in. [25 to
37.5 mm]).
B. After the sample has been obtained, it shall be divided into two approximately equal size
(split) samples by the use of an approved mechanical sample splitter. One of the split
samples shall be placed in a Department-approved sample container provided by the
Contractor and shall be properly identified for use by the Department. These split samples
shall be retained by the Contractor for assurance testing by the Engineer and may be
disposed of only with the permission of the Engineer. The split samples shall be stored in a
dry, protected location. The remaining split will be used for those tests described in Section
1030 of the Standard Specifications.
C. Starting with the first day of production (excluding start-up), the initial daily required plant
sample shall be obtained between the first to 1 hours of daily production of a particular
mixture. These daily plant test samples shall be tested for, but not limited to, the following:
4. Aggregate Gradations
a. Combined Belt
b. Individual Cold-Feeds
c. Hot-Bins
D. The second daily required plant sample shall be taken at a randomly selected time within
the third quarter of the anticipated production day using the "Random Numbers" table on
the following page or the Department's QC/QA computer software. For HMA mixtures
classified as All Other the Contractor shall use the anticipated full production day when
calculating the random sampling time. The anticipated full production day shall be the time
from a hour after production begins to a hour before production ends. The following
procedure shall be used to calculate the second daily required plant sampling time.
1. Multiply the quarter production day (in minutes) by a three digit random number,
expressed as a decimal, selected from the "Random Numbers" table or the
Department's QC/QA computer software.
2. The number obtained (rounded to a whole number) shall be added to the starting time
of the third quarter. The time represented by this addition is the randomly selected
sampling time.
If the plant is producing HMA mixtures intermittently, the samples shall be taken as
close to the determined time as possible.
RANDOM NUMBERS
0.576 0.730 0.430 0.754 0.271 0.870 0.732 0.721 0.998 0.239
0.892 0.948 0.858 0.025 0.935 0.114 0.153 0.508 0.749 0.291
0.669 0.726 0.501 0.402 0.231 0.505 0.009 0.420 0.517 0.858
0.609 0.482 0.809 0.140 0.396 0.025 0.937 0.301 0.253 0.761
0.971 0.824 0.902 0.470 0.997 0.392 0.892 0.957 0.040 0.463
0.053 0.899 0.554 0.627 0.427 0.760 0.470 0.040 0.904 0.993
0.810 0.159 0.225 0.163 0.549 0.405 0.285 0.542 0.231 0.919
0.081 0.277 0.035 0.039 0.860 0.507 0.081 0.538 0.986 0.501
0.982 0.468 0.334 0.921 0.690 0.806 0.879 0.414 0.106 0.031
0.095 0.801 0.576 0.417 0.251 0.884 0.522 0.235 0.389 0.222
0.509 0.025 0.794 0.850 0.917 0.887 0.751 0.608 0.698 0.683
0.371 0.059 0.164 0.838 0.289 0.169 0.569 0.977 0.796 0.996
0.165 0.996 0.356 0.375 0.654 0.979 0.815 0.592 0.348 0.743
0.477 0.535 0.137 0.155 0.767 0.187 0.579 0.787 0.358 0.595
0.788 0.101 0.434 0.638 0.021 0.894 0.324 0.871 0.698 0.539
0.566 0.815 0.622 0.548 0.947 0.169 0.817 0.472 0.864 0.466
0.901 0.342 0.873 0.964 0.942 0.985 0.123 0.086 0.335 0.212
0.470 0.682 0.412 0.064 0.150 0.962 0.925 0.355 0.909 0.019
0.068 0.242 0.777 0.356 0.195 0.313 0.396 0.460 0.740 0.247
0.874 0.420 0.127 0.284 0.448 0.215 0.833 0.652 0.701 0.326
0.897 0.877 0.209 0.862 0.428 0.117 0.100 0.259 0.425 0.284
0.876 0.969 0.109 0.843 0.759 0.239 0.890 0.317 0.428 0.802
0.190 0.696 0.757 0.283 0.777 0.491 0.523 0.665 0.919 0.146
0.341 0.688 0.587 0.908 0.865 0.333 0.928 0.404 0.892 0.696
0.846 0.355 0.831 0.281 0.945 0.364 0.673 0.305 0.195 0.887
0.882 0.227 0.552 0.077 0.454 0.731 0.716 0.265 0.058 0.075
0.464 0.658 0.629 0.269 0.069 0.998 0.917 0.217 0.220 0.659
0.123 0.791 0.503 0.447 0.659 0.463 0.994 0.307 0.631 0.422
0.116 0.120 0.721 0.137 0.263 0.176 0.798 0.879 0.432 0.391
0.836 0.206 0.914 0.574 0.870 0.390 0.104 0.755 0.082 0.939
0.636 0.195 0.614 0.486 0.629 0.663 0.619 0.007 0.296 0.456
0.630 0.673 0.665 0.666 0.399 0.592 0.441 0.649 0.270 0.612
0.804 0.112 0.331 0.606 0.551 0.928 0.830 0.841 0.702 0.183
0.360 0.193 0.181 0.399 0.564 0.772 0.890 0.062 0.919 0.875
0.183 0.651 0.157 0.150 0.800 0.875 0.205 0.446 0.648 0.685
Note: Always select a new set of numbers in a systematic manner, either horizontally or
vertically. Once used, the set should be crossed out.
Density tests (core or nuclear gauge) shall be performed at randomly located sites based on the
frequency specified in Section 1030 of the Standard Specifications. The random test locations
shall be determined as follows:
A. The beginning station number shall be established daily and the estimated paving distance
computed for the day's production. The total distance to be paved shall then be subdivided
into units representing 2640-ft. (800-m) or 1320-ft. (400-m) frequency.
B. The length of each unit shall be multiplied by the three digit random number expressed as
a decimal from the "Random Numbers" table on the following page or from the
Department's QC/QA computer software. The number obtained shall be added to the
beginning station number for the unit to determine the center of the test site location.
C. This process shall be repeated for the subsequent units for the day's production using a
new random number for each location.
D. The partial unit at the end of each day shall be considered a whole unit, and the test
location shall be determined by multiplying the partial distance by the next available
random number.
RANDOM NUMBERS
0.576 0.730 0.430 0.754 0.271 0.870 0.732 0.721 0.998 0.239
0.892 0.948 0.858 0.025 0.935 0.114 0.153 0.508 0.749 0.291
0.669 0.726 0.501 0.402 0.231 0.505 0.009 0.420 0.517 0.858
0.609 0.482 0.809 0.140 0.396 0.025 0.937 0.301 0.253 0.761
0.971 0.824 0.902 0.470 0.997 0.392 0.892 0.957 0.040 0.463
0.053 0.899 0.554 0.627 0.427 0.760 0.470 0.040 0.904 0.993
0.810 0.159 0.225 0.163 0.549 0.405 0.285 0.542 0.231 0.919
0.081 0.277 0.035 0.039 0.860 0.507 0.081 0.538 0.986 0.501
0.982 0.468 0.334 0.921 0.690 0.806 0.879 0.414 0.106 0.031
0.095 0.801 0.576 0.417 0.251 0.884 0.522 0.235 0.389 0.222
0.509 0.025 0.794 0.850 0.917 0.887 0.751 0.608 0.698 0.683
0.371 0.059 0.164 0.838 0.289 0.169 0.569 0.977 0.796 0.996
0.165 0.996 0.356 0.375 0.654 0.979 0.815 0.592 0.348 0.743
0.477 0.535 0.137 0.155 0.767 0.187 0.579 0.787 0.358 0.595
0.788 0.101 0.434 0.638 0.021 0.894 0.324 0.871 0.698 0.539
0.566 0.815 0.622 0.548 0.947 0.169 0.817 0.472 0.864 0.466
0.901 0.342 0.873 0.964 0.942 0.985 0.123 0.086 0.335 0.212
0.470 0.682 0.412 0.064 0.150 0.962 0.925 0.355 0.909 0.019
0.068 0.242 0.777 0.356 0.195 0.313 0.396 0.460 0.740 0.247
0.874 0.420 0.127 0.284 0.448 0.215 0.833 0.652 0.701 0.326
0.897 0.877 0.209 0.862 0.428 0.117 0.100 0.259 0.425 0.284
0.876 0.969 0.109 0.843 0.759 0.239 0.890 0.317 0.428 0.802
0.190 0.696 0.757 0.283 0.777 0.491 0.523 0.665 0.919 0.146
0.341 0.688 0.587 0.908 0.865 0.333 0.928 0.404 0.892 0.696
0.846 0.355 0.831 0.281 0.945 0.364 0.673 0.305 0.195 0.887
0.882 0.227 0.552 0.077 0.454 0.731 0.716 0.265 0.058 0.075
0.464 0.658 0.629 0.269 0.069 0.998 0.917 0.217 0.220 0.659
0.123 0.791 0.503 0.447 0.659 0.463 0.994 0.307 0.631 0.422
0.116 0.120 0.721 0.137 0.263 0.176 0.798 0.879 0.432 0.391
0.836 0.206 0.914 0.574 0.870 0.390 0.104 0.755 0.082 0.939
0.636 0.195 0.614 0.486 0.629 0.663 0.619 0.007 0.296 0.456
0.630 0.673 0.665 0.666 0.399 0.592 0.441 0.649 0.270 0.612
0.804 0.112 0.331 0.606 0.551 0.928 0.830 0.841 0.702 0.183
0.360 0.193 0.181 0.399 0.564 0.772 0.890 0.062 0.919 0.875
0.183 0.651 0.157 0.150 0.800 0.875 0.205 0.446 0.648 0.685
Note: Always select a new set of numbers in a systematic manner, either horizontally or
vertically. Once used, the set should be crossed out.
A. Scope
1. All required Contractor test results, including resample tests and mixture start-
up, described in Article 1030.05(g) of the Standard Specification shall be split
samples and plotted on Control Charts. (No check tests shall be plotted on
these Control Charts.) In addition, the Engineer's "assurance" test results shall
also be displayed. The minimum frequency of such tests shall be according to
Section 1030 of the Standard Specifications.
B. General Procedures
Air Voids, Field VMA, Minus No. 200 (Minus 75-m), Field Density
- 0.1% per division (1 in. [25 mm] = 1.0%).
2. The horizontal scale shall be arranged such that each randomly selected test
value obtained is plotted at in. (12.5-mm) intervals. (See Figure 1.)
The moving average for minus 200 (minus 75 m) for HMA production control
shall include both washed ignition oven gradation and adjusted dry gradation
individual results. When a given sublot includes both washed ignition and dry
gradation test results for the minus 200 (minus 75 m), only the washed
ignition shall be used in the moving average.
The moving average for Gmm of a new mixture shall be established initially with
the results from the start-up and shall include more tests in the moving
average as they occur until the moving average of four is established. Unless
otherwise specified by the Engineer, the moving average for Gmm of a
previously placed mixture shall begin with the most recent moving average of
four and shall be averaged with subsequent test results.
2. At the bottom of the chart under the line on which the individual test data is
plotted, the following information shall be listed:
b. Lot Number.
c. Test Sequence.
1. Test values obtained during start-up and the Job Mix Formula (JMF)
adjustment period shall be placed at the beginning of the Control Charts. Once
all these required tests have been completed and their values recorded, two
vertical double black lines shall be drawn on the graph in. (12.5 mm) apart.
This constitutes the field verification process for the mixture.
F. Adjusting Targets
2. When an adjustment to the Target value is made, two vertical double black
lines shall be drawn on the graph in. (12.5 mm) apart. The new target value
plus upper and lower control values will be placed on the chart. The moving
average will continue as though the adjustment had not taken place.
The Contractor resample tests for a failed individual test shall be the only biased process
control test placed on the Control Chart. It shall be denoted by a circle (closed for washed
gradations and open for all other tests) with its value placed on the vertical line which
corresponds to the time or lot from which the resample was taken. A circle shall be drawn
around this value and the failed test value which the resample represents. Both the failed
test value and the resample test value shall be used as individual points in determining
moving averages.
The following are the appropriate significant digits to which test values are to be
rounded for parameters described in the Section 1030:
1.0 GENERAL
Contractors shall provide all hot-mix asphalt (HMA) mix designs for use on
Department contracts. All mix designs must provide mixture meeting Department
mix criteria. The Department will provide current aggregate bulk specific gravity. The
Engineer reserves the right to be present for the sampling of all aggregates for mix
designs. Once verified, a mix design will be approved for use for a three year period.
After three years, the mix design shall be redesigned if necessary, and re-verified.
2.0 PURPOSE
3.1 The Contractor shall provide a mix design prepared by a Hot-Mix Asphalt Level III
Technician in accordance with the Department's "Hot-Mix Asphalt Design Procedure"
in the current Hot-Mix Asphalt Level III Tec hnician Course manual. All testing shall
be performed by Hot-Mix Asphalt Level I Technicians or higher. The mix design shall
be submitted with the following design data:
B. The Contractor shall provide the average mix plant stockpile gradations and
aggregate blend percentages used to design the mix. Each of the individual
aggregate gradations used in the Contractor design shall be an average of a
minimum of 5 (five) stockpile gradations from existing stockpiles at the plant.
Adjusted average aggregate source gradations (stockpile gradations preferred)
may be substituted if aggregate has not been shipped to the mix plant. The
adjustment shall be based on the amount of aggregate degradation during
shipment to, and handling at, the mix plant. A design using gradation information
not comparing to mix plant or aggregate source gradations shall be considered
unacceptable.
C. The Contractor shall provide a summary of design test data and optimum design
data utilizing a design package with the same output format as CARE-AC.
(1) Design sheet. The design shall contain a minimum of four design
points, two of which shall bracket the optimum design asphalt binder
(AB) content by at least 0.5%. Under remarks include: short-term
aging time, dust correction factor, compaction temperature, and
mixing temperature.
(3) Actual graph paper from the stability machine and actual Gmm lab
worksheets (original copy unless otherwise specified).
(e) Asphalt Binder Content vs. Voids Filled with Asphalt (VFA).
3.2 The Contractor shall provide samples of blended aggregate, asphalt binder, and
additives which represent the materials in the mix design. The representative
samples shall be identified and submitted as follows:
A. Aggregate (including mineral filler/collected dust) -- Dried, split into the individual
sizes specified for the Batching Worksheet as stated in the current Hot-Mix
Asphalt Level III Technician Course manual, and then blended to the chosen
gradation. The amount submitted shall be two (2) 10,000-gram samples of dry
aggregate, with an additional 2,000 grams for gradation testing if requested by
the District. All material shall be bagged in plastic bags or other airtight
containers. Each container shall be identified with the source names, source
locations, source Producer/Supplier Numbers, material codes, sample location,
and sample date.
3.3 All design data and material samples shall be submitted to the Department a
minimum of 30 calendar days prior to production.
3.4 The Contractor shall certify in writing that all materials submitted for mix design
verification meet Department requirements and represent the materials to be used
during mix production.
3.5 Previously verified mix designs shall be resubmitted for verifications as per
Section 4.1 herein.
4.1 At the option of the Department, mix designs may be verified using either Method A
or Method B listed below:
Method A. Department verification for mix designs will include review of all mix
design data (including all aggregate field gradations) submitted by the Contractor,
mixing the component materials submitted by the Contractor, and testing of the
asphalt mixture. Verification testing will include volumetric, TSR and Hamburg Wheel
on a mixture made from the individual materials submitted by the Contractor. The
mixture at the optimum design asphalt binder content shall meet the mix design
criteria for the following: VMA, VFA, Gmb, Gmm, Pa (voids), Tensile Strengths, TSR
values, and Hamburg Wheel.
4.2 The Contractor mix design data and Department verification testing shall meet the mix
design criteria in the Standard Specifications, any Special Provision in the Contract,
and the following tolerances (where applicable):
Gradation Tolerance
12.5 mm (1/2 in) 3.0
4.75 mm (No. 4) 2.0
2.36 mm (No. 8) 2.0
600 m (No. 30) 1.0
75 m (No. 200) 0.5
Pb (Asphalt Binder Content) 0.15
4.3 The Department will notify the Contractor in writing within 30 calendar days of
receiving the design data/materials as to the acceptability of the submitted
Contractor mix design. If the verification fails, the 30-calendar-day time for the
Department to notify the Contractor starts over. Acceptable designs may be used in
Department contracts, provided the design is reproducible in the mix plant.
1.0 SCOPE
1.1 The purpose of this procedure is to evaluate the effect of 20-hour storage on hot-
mix asphalt.
1.2 Article 1102.01(a)(10) of the IDOT Standard Specifications for Road and B ridge
Construction allows for the storage of hot-mix asphalt in surge systems designed
and operated to prevent segregation and loss of temperature. The specification
allows for a maximum retention of eight hours. Longer retention times must be
approved in writing by the Engineer.
3.0 EQUIPMENT
3.1 One-quart (1-liter) and 1-gallon (4-liter) metal containers with lids for sample
storage and transportation.
4.0 PROCEDURE
4.1 The Bureau of Materials and Physical Research will evaluate the effect of
additional storage time on the mixture. The Engineer will direct the Contractor to
sample the mixture based on the following procedure. The Engineer reserves the
right to witness the sampling.
4.3 The bin must be filled with a binder mixture at a time mutually agreed upon by
the Contractor and Engineer.
4.4 A 1-quart (1-liter) sample of the asphalt binder shall be taken at this time.
4.5 A 1-gallon (4-liter) sample of the mixture shall be taken at this time.
4.6 An additional 1-gallon (4-liter) mixture sample will be taken 20 hours after initial
storage.
4.7 Samples shall be drawn from the silo by dumping the mixture into a truck and
sampling from the truck. All samples should be large enough to fill the metal
container.
4.8 Each sample container shall be sealed immediately and marked with the
producer's or supplier's name and number, plant location, date, time, type of
mixture, mixture temperature, and asphalt binder source and grade.
Note: If the sample container does not stay sealed, the container may be cooled
with the sample before sealing.
4.9 The samples should be immediately forwarded to the Bureau of Materials and
Physical Research for evaluation.
4.10 Asphalt binder recovered from the mixture samples will be tested for the effects
of increased storage time on viscosity.
Viscosity at 60 C,
Grade
Pascal Seconds, Maximum
PG 64-28 125
PG 58-28 250
PG 58-22 500
PG 64-22 1000
PG 70-22 (neat) 2000
4.11 The test results of the initial mixture sample shall be used for informational
purposes only.
4.12 Approval will be based on the test results from the final mixture sample.
4.14 The procedure for recovery of the extracted asphalt shall be Illinois Modified
AASHTO T 170, "Recovery of Asphalt from Solution by Abson Method."
A. Scope
The Contractor may be required to use the nuclear gauge or ignition oven to
determine the asphalt binder content of a Hot-Mix Asphalt (HMA) mixture. To
ensure consistency, both the Contractor and the Department shall calibrate the
device(s) in the same manner using the same mixture.
B. Purpose
1. Department Verification
d. Testing shall include, at the option of the Engineer, one or both of the
following test procedures:
(1) The District has the option of witnessing the Contractor's calibration
procedures as outlined in Section 7 of Illinois Modified AASHTO
T 287.
(2) Prior to calibrating the nuclear asphalt binder content gauge, the
Contractor shall submit the following to the District office at least 2
weeks prior to production:
Sieve Tolerance
12.5 mm (1/2 in.) 3.0
4.75 mm (No. 4) 2.0
2.36 mm (No. 8) 1.5
600 m (No. 30) 1.0
75 m (No. 200) 0.5
Pb (Asphalt Content) 0.15
2. Calibration
b. The Contractor shall retain the calibration pans. These pans shall be
covered with plastic bags and stored in a dry, secure place.
D. Ignition Oven
1. Department Verification
c. Calibrations shall consist of, at the option of the Engineer, one or both of
the following procedures:
(1) The District has the option to witness the mixing and burning of the
calibration sample. The Contractor shall mix enough mixture to
provide the Department with calibration samples.
(2) The Contractor shall submit the following to the District office at least
two weeks prior to production:
A dust correction factor (DCF) shall be determined and applied to each new mix design
using the procedure listed below. This procedure will be used to supplement the Hot-Mix
Asphalt Level III Technician Course manual to account for additional minus No. 200
(minus 75-m) material present as a result of batching with unwashed aggregates.
It is important to note the Adjusted Blend Percentages are temporary percentages used
during laboratory batching only. The original Blend Percentages on the Design
Summary Sheet remain unchanged.
Note: When adjusting percentages to equal 100, the largest percentage should be
adjusted accordingly.
1. Batch a combined aggregate sample matching the job mix formula (JMF). Test
sample size shall be determined using Illinois Specification 201 and based on the
nominal maximum size of the largest coarse aggregate.
2. Perform a washed test on the combined aggregate sample using Illinois Modified
AASHTO T 11.
3. The DCF shall be the difference between the percent passing the No. 200 (75-m)
sieve of the washed test and the JMF.
4. Determine the mineral filler reduction (MFR) by dividing the DCF by the percent (in
decimal form) mineral filler gradation passing the No. 200 (75-m) sieve.
6. Adjust the remaining blend percentages to sum to 100 by dividing each by the
quantity (1 - MFR).
Example
Step 3. Determine the Dust Correction Factor (DCF). The DCF is the difference in
the percent passing the No. 200 (75-m) sieve between the washed test and
the JMF:
Step 4. Determine the Mineral Filler Reduction (MFR) by dividing the DCF (%) by
the percent (in decimal form) mineral filler gradation passing the No. 200
(75-m) sieve:
MFR (%) = 1.6 / 0.88 = 1.8%
Step 5. Determine the adjusted mineral filler blend percentage by subtracting the
MFR (%) from the blend percentage of mineral filler:
Step 6. Adjust the remaining blend percentages to sum to 100 by dividing each by
the quantity [1 - MFR (in decimal form)]:
Adjusted
Blend Blend
Percentage Percentage1
032CMM11 38.0 38.7
032CMM16 35.0 35.6
038FAM20 14.5 14.8
037FAM01 10.0 10.2
004MFM01 2.5 0.7
100.0 100.0
6. The DCF shall be the difference between the percent passing the No. 200
(75-m) sieve of the washed test and the RJMF.
10. Determine the batching blend percentages with RAP by multiplying the
adjusted virgin aggregate blend percentages by the VAF.
RAP Example
VAF = 0.763
Step 3. Determine the RAP adjusted JMF (RJMF). Combine gradation using the
adjusted virgin aggregate blend percentages.
1 100.0
89.4
66.8
3/8 53.9
#4 28.5
#8 19.2
#16 17.4
#30 14.6
#50 7.8
#100 3.8
#200 3.4
Step 4. Batch the virgin aggregates according to the adjusted blend percentages
matching the RJMF. Illinois specification 201 requires a 5000-gram sample
when CM11 is present.
Step 6. Determine the dust correction factor (DCF). The DCF is the difference
between the percent passing the No. 200 (75-m) sieve of the washed test
and the RJMF.
DCF = 0.9
Step 7. Determine the mineral filler reduction (MFR)RAP. The (MFR)RAP is determined
by dividing the DCF by the percent (in decimal form) mineral filler gradation
passing the No. 200 (75-m) sieve.
0.9
MFRRAP = = 1.1%
0.85
Step 8. Determine the mineral filler blend percentage by subtracting the MFRRAP from
the blend percentage of mineral filler.
Step 9. Adjust the remaining blend percentages to sum to 100% by dividing each by
the quantity [1-MFRRAP (in decimal form)]:
Step 10. Determine the batching blend percentages with RAP by multiplying the
adjusted virgin blend % by the VAF.
VAF = 0.763
1.0 GENERAL
1.1 This method covers the calibration of the ignition oven for characterization
of reclaimed asphalt pavement (RAP). Correction factors for both
gradation and asphalt content are determined by conducting parallel
ignition and extraction testing.
2.1 The ignition oven may be used in place of solvent extractions at the
frequency stated in Section 1031 of the Standard Specifications.
2.2 This method may be used only with the approval of the Engineer.
2.3 Each RAP stockpile shall require a separate ignition oven calibration.
2.4 All RAP stockpiles and sampling frequencies shall meet the requirements
stated in Section 1031 of the Standard Specifications.
4.0 PROCEDURE
4.3.1 Calculate the average Asphalt Binder (AB) percentage of the two
extractions, Pext. Calculate the average AB percentage of the four
ignition oven burns, Pign. Assuming the average AB content from the
extraction to be correct, subtract the average extraction AB
percentage from the average ignition oven AB percentage to
determine the asphalt correction factor, Cf.
Cf = Pign - Pext
Use the asphalt correction factor to adjust the ignition oven asphalt
content on all subsequent testing of that stockpile.
4.4.1 From the two extractions, calculate the average percent passing the
applicable sieve, Gext. Calculate the average percent passing each
applicable sieve from the four ignition oven burns, Gign. Subtract the
extraction average percent passing each sieve from the ignition oven
average of the corresponding sieve to determine a correction factor,
GCf, for gradation for each sieve.
5.0 REPORT
6.1 The estimates of precision and bias shall be considered those that apply
to the referenced documents.
7.0 USE
7.1 Use the correction factor for percent passing the No. 200 (75-m) sieve to
adjust the minus No. 200 (75-m) material from the ignition oven on all
subsequent testing of that stockpile.
7.2 Use the asphalt correction factor to adjust the ignition oven asphalt
content on all subsequent testing of that stockpile.
7.3 The ignition oven washed gradations may be used uncorrected for all
sieves except for the No. 200 (75-m) sieve.
A. Scope
The Contractor will be required to provide production gradation test results for both
washed ignition oven gradations (WIOG) and dry combined belt / hot bin gradations
on the same control chart according to Section 1030 of the Standard Specifications.
In order for this data to be meaningful, the dry combined belt / hot bin gradations
shall be calibrated to the WIOG using the windage factor established below.
B. Purpose
A windage factor (WF) shall be determined and applied to dry gradation production
test results in order to establish a WIOG equivalency. The WF accounts for the
difference, in minus #200 (minus 75m) material, between dry combined belt/hot bin
gradations and WIOG due to the following:
variability in the addition of Mineral Filler
washed vs. dry gradation (cling-on dust)
generation of dust through plant aggregate degradation
C. Procedure
1. Obtain two combined belt/hot bin aggregate samples and perform two dry
gradation (DG) tests. The DG shall include the theoretical amount of mineral
filler to be added. Average the two test results for the minus #200 (minus
75m) material.
2. Obtain two samples of HMA representing, near as possible, material from step
one. Perform WIOG testing on the HMA samples and average the two results
for minus the #200 (minus 75m) material.
(continued)
Effective: May 1, 2004
Revised: May 1, 2007
4. Add WF to all combined belt/hot bin gradation test results prior to plotting on
the Minus #200 (minus 75m) Control Chart. All, (including WIOG test results
used to establish WF, are plotted directly on the Minus #200 (minus 75m)
Control Chart. When both the DG and WIOG test results represent the same
material, the WIOG are the results to be included in the moving average.
Example:
Given:
WIOG#1 (minus #200) = 4.8% (Truck sample taken between growth curves)
WIOG#2 (minus #200) = 4.6% (Truck sample taken from outside Test Strip
area during startup)
DG#1 (minus #200) = 2.7% (Combined belt sample taken to correspond to
material sampled for WIOG#1)
DG#2 (minus #200) = 2.1% (Combined belt sample taken to correspond to
material sampled for WIOG#2)
Step 1. Average the two DG test results for the minus #200 (minus 75m)
material.
Step 2. Average the two WIOG test results for the minus #200 (minus 75m)
material.
Step 4. Add WF = 2.3% to all combined belt/hot bin gradation test results prior to
plotting on the Minus #200 (minus 75m) Control Chart.
The following instructions describe the method to be used for visually identifying and classifying
the effect of moisture damage on the adhesion of asphalt binder to the aggregate in Hot-Mix
Asphalt (HMA) mixtures. This procedure provides the means to rate this phenomenon in
numerical terms. This procedure is applicable to both laboratory compacted specimens and
pavement cores 1.
INSTRUCTIONS
1. This procedure shall only be applied to freshly split specimen faces, such as those obtained
from split tensile testing. The observation of cored, sawed, or chiseled faces shall be
avoided, as the true condition of the stripping will be obscured.
2. The rating shall be completed within 10 minutes of splitting for maximum clarity. When the
specimens dry out, they may look considerably different. The aggregate surfaces shall be
examined carefully to determine if the asphalt binder was stripped from the aggregate as a
result of being washed by water before the specimen was split or if the asphalt binder was
ripped apart near the asphalt/aggregate interface during the split tensile test. Also,
aggregate surfaces with small, relatively isolated, globules of asphalt binder are quite likely
not stripped.
3. Special attention shall be given to fractured and broken aggregates. Fractured aggregates
are those that were cracked during compaction. These fractured aggregates will have a
distinct face with a dull or discolored surface. Broken aggregates are those that were
broken during the split tensile test. Broken aggregates often occur near the outside surface
of the specimen where the compressive forces are greatest. These broken aggregates will
also have a distinct broken face, but will have a bright, uncoated surface. The broken
aggregates may be a continuation of a crack that was started during compaction. There is
no evidence that a broken aggregate was broken entirely under the compressive force of the
split tensile test.
4. Coarse aggregate particles shall be defined as those particles retained on the #8 sieve.
Fine aggregate particles shall be defined as those particles that will pass through a #8 sieve.
5. When examining the split face, use the entire face area of all the fine particles separately
from all the coarse particles on the split face to determine the percentage of the total area
that is stripped. Do not use the percent of the area of each individual stone that is stripped
to collectively determine the percentage of stripped aggregate particles on the entire split
face of the specimen. Also, do not estimate the percentage of aggregate particles that are
stripped based on the total number of aggregate particles. (i.e., a small stripped aggregate
particle does not affect the entire specimen the same as a large stripped aggregate particle.)
1
Pavement cores taken from the field shall be sealed in plastic bags immediately after coring in order to retain their
in-situ moisture. Pavement cores shall be split and visually rated as soon as possible after coring to avoid any
healing of the asphalt to the aggregate surfaces.
PROCEDURE
2. Observe the coarse aggregate of the split face with the naked eye. Pay special attention to
the coarse aggregate that is broken or fractured. These particles are not stripped.
3. Assign a strip rating to the coarse aggregate of the split face based on the following
descriptions:
1 - Less than 10% of the entire area of all the coarse aggregate particles is
stripped (no stripping to slight stripping).
2 - Between 10% and 40% of the entire area of all the coarse aggregate particles
is stripped (moderate stripping).
3 - More than 40% of the entire area of all the coarse aggregate particles is
stripped (severe stripping).
4. Observe the fine aggregate particles and rate the particles for percent of the area showing
moisture damage. A microscope or magnifying glass with a total magnification of 10X shall
be used to aid in viewing the specimens. Observe the fine aggregate particles and mentally
rate the particles present in the field of view. Move the specimen to a new field of view and
rate the particles present. Repeat this process once more, ensuring a new field of view is
chosen. Average the three observations.
5. Assign a strip rating to the fine aggregate of the split face based on the following
descriptions:
1 - Less than 10% of the entire area of all the fine aggregate particles viewed is
stripped (no stripping to slight stripping).
2 - Between 10% and 25% of the entire area of all the fine aggregate particles
viewed is stripped (moderate stripping).
3 - More than 25% of the entire area of all the fine aggregate particles viewed is
stripped (severe stripping).
6. Report the individual strip ratings for both the coarse and fine aggregate on the strip rating
form. Include any comments or special notes about the observations from that specimen.
7. Average all the individual strip ratings for the conditioned specimens (typically 3) for a given
test sample. Calculate a separate average for both coarse and fine aggregates. The
average coarse and fine strip ratings for the unconditioned specimens (typically 3) may also
be calculated for a given test sample. These average ratings give a quick overall appraisal
of the moisture susceptibility of the sample. Note that the averaged ratings may not be
simple whole numbers.
GENERAL COMMENTS
1.0 GENERAL
2.0 PURPOSE
A. This procedure applies to using additives in hot mix asphalt (HMA) mixtures and
testing those mixtures in the lab. This procedure includes the dry method of
hydrated lime addition as well as the wet method and the slurry method. Also,
this procedure includes specimens containing no additive, liquid anti-strip,
polymer-modified asphalt, and polymer-modified asphalt with hydrated lime or
liquid anti-strip.
B. Four levels of conditioning are included in this procedure and are used when
specified. These four levels are no conditioning (or control), submerging in a hot
water bath, one cycle of freezing followed by submerging in the hot water bath,
and five freeze and hot water bath cycles. The conditioned samples are all
partially saturated with water before the freeze and hot water bath cycles begin.
D. Tensile strengths are determined and the tensile strength ratio (TSR) is
calculated. The tensile strength of the unconditioned specimens is compared
with the tensile strength of the specimens from each of the applicable levels of
conditioning to determine the TSR. The TSR is a measure of the relative effect
that each additive type and conditioning method has on the moisture
susceptibility of the samples. The results are used to compare the various
additives and their effect on the stripping potential of each mix and to determine
the best additive to be used for a specific mixture containing a specific blend of
materials.
3.0 MATERIALS
The HMA Mix Design shall be performed using the hydrated lime addition
method and / or the liquid anti-strip type that will be used during actual production
in the field.
B. The liquid anti-strip and / or hydrated lime method used must result in:
1) A conditioned tensile strength that is equal to, or greater than, the original
conditioned tensile strength for the same mixture without the additive,
2) A TSR value that is equal to, or greater than, 0.85 for 6-inch (150 mm)
diameter specimens, and
3) Hamburg Wheel test results for rut depth and number of wheel passes
according to Illinois modified AASHTO T-324.
A. Dry Aggregates:
Dry the aggregate samples in a 230 9 F (110 5 C) oven so that the batch
weights and additive amounts can be accurately determined.
B. Split Aggregates:
The aggregate samples will then be split according to Illinois-modified AASHTO
T-248.
C. Blend Aggregates:
The aggregates will be blended into the correct batch size. Because of the large
size of the gyratory specimens, each batch will contain enough material for two
gyratory specimens (approximately 8000 - 8500 grams for tensile strength and
TSR and approximately 5000 5500 grams for the Hamburg Wheel
test). Several batches will need to be prepared to produce the required number
of gyratory specimens (six for strength and TSR and four for Hamburg Wheel
testing as well as pilot specimens). Also, include sufficient material in one of the
batches for a maximum specific gravity (Gmm) test run according to Illinois-
modified AASHTO T-209 (approximately 2000 grams).
D. Mix Samples:
1. With No Additive:
a. Heat the asphalt binder and the dry aggregate blend to a mixing
temperature of 295 5 F (146 2.8C) for neat asphalt.
b. Remove the blend from the oven and make a small crater in the top of the
hot, dry aggregates.
c. Add the correct amount of asphalt binder to the batch.
d. Mix the aggregates and asphalt binder.
a. List the hydrated lime in its own column on the Aggregate Blending Sheet
and enter the percent passing each sieve in the corresponding line on the
form.
b. 1.0% hydrated lime is added to the mix. The 1.0% hydrated lime is based
on the total dry weight of aggregate in the mix and is added in addition to
the mineral filler specified in the mix design.
e. Heat the asphalt binder and the dry aggregates (not including mineral
filler) to a mixing temperature of 295 5 F (146 2.8C) for neat asphalt
or 325 5 F (163 2.8C) for polymer modified asphalt.
f. Make a small crater in the top of the hot, dry aggregates.
g. Add the correct amount of dry hydrated lime to the crater in the
aggregates.
h. Mix the hydrated lime and aggregates until the aggregates are completely
coated (approximately 10 to 15 seconds).
i. If the blend of aggregates and hydrated lime cools below the mixing
temperature, place the blend back in the oven until the blend is returned
to the mixing temperature (approximately 10 minutes).
j. Remove the blend from the oven and make a small crater in the top of the
hot, dry aggregates and hydrated lime.
k. Add the correct amount of mineral filler, (if required in the mix design), to
the crater in the aggregates.
l. Mix the mineral filler with the aggregates and hydrated lime until the
mineral filler is uniformly dispersed in the blend (approximately 10 to 15
seconds).
m. If the blend of aggregates, hydrated lime, and mineral filler cools below
the mixing temperature, place the blend back in the oven until the blend is
returned to the mixing temperature (approximately 10 minutes).
n. Make a crater in the aggregates and add the correct amount of asphalt
binder to aggregates, hydrated lime, and mineral filler.
o. Mix the asphalt binder with the blend of aggregates, hydrated lime, and
mineral filler.
a. List the hydrated lime in its own column on the Aggregate Blending Sheet
and enter the percent passing each sieve in the corresponding line on the
form.
b. 1.0% hydrated lime is added to the mix. The 1.0% hydrated lime is based
on the total dry weight of aggregate in the mix and is added in addition to
the mineral filler specified in the mix design.
aggregate, similar to mineral filler, and the gradation of all of the hydrated
lime contributes to the overall blend gradation.
l. Mix the mineral filler with the hydrated lime-covered aggregates until the
mineral filler is uniformly dispersed in the blend (approximately 10 to 15
seconds).
m. If the blend of hydrated lime-coated aggregates and mineral filler cools
below the mixing temperature, place the blend back in the oven until the
blend is returned to the mixing temperature (approximately 10 minutes).
n. Make a crater in the aggregates and add the correct amount of asphalt
binder to the mixture of hydrated lime-covered aggregates and mineral
filler.
o. Mix the hydrated lime-coated aggregates, mineral filler, and asphalt
binder together until the aggregates are completely coated with the
asphalt binder.
a. List the hydrated lime in its own column on the Aggregate Blending Sheet
and enter the percent passing each sieve in the corresponding line on the
form.
b. 1.0% hydrated lime is added to the mix. The 1.0% hydrated lime is based
on the total dry weight of aggregate in the mix and is added in addition to
the mineral filler specified in the mix design.
5. Liquid Anti-strip
a. Add 0.5% of liquid anti-strip (by weight of asphalt) to the asphalt binder
and mix together until the liquid anti-strip is distributed thoroughly in the
asphalt binder.
6. Polymer
E. Split Samples:
Split the batches into the correct sample size which will make a gyratory
specimen 3 in. (95 mm) high (approximately 4200 grams).
F. Compact Samples:
1. Run a maximum specific gravity (Gmm) for each of the additive mix types
being evaluated.
3. Pilot bricks from the mixes for each type of additives being evaluated will be
made to determine the correct compaction level to achieve 7.0 0.5% air
voids.
5. Compact samples to 7.0 0.5% air voids for each mix additive type using the
number of gyrations determined above.
6. A total of 12 individual samples will be compacted for each additive mix type
for each complete round of testing.
7. Run a Gmb on each sample to verify that the air voids are within the range of
7.0 0.5%.
5.0 TESTING
a. Placed in a 77F (25C) water bath for a minimum of two hours to bring
the sample to room temperature.
b. Placed between the loading heads and loaded at 2 in. (50 mm) per
minute until failure.
4. The indirect tensile strength (ITS) will be calculated using the equation:
2 P
ITS =
t d
where:
P = Load (pounds)
= 3.1416
t = Sample Thickness (inches)
d = Sample Diameter (inches)
5. Within 10 minutes after breaking the sample in the indirect tensile tester, the
split samples will be inspected visually to evaluate the amount and degree of
moisture damage. This will be done according to the IDOT procedure,
Stripping of Hot Mix Asphalt Mixtures - Visual Identification and
Classification.
C. AASHTO T-283 Sample Set (with one freeze-thaw cycle) (Only use when
specified):
D. AASHTO T-283 Sample Set (with five freeze-thaw cycles) (Only use when
specified):
1. Three bricks will be tested as in Testing; C above except that five complete
freeze thaw cycles will be completed instead of only one.
2. The plastic bag and plastic wrap should stay on the sample throughout the
test and should not be removed until the beginning of the final thaw cycle in
the 140F (60C) bath. If the plastic bag tears or if the plastic wrap comes
loose, replace them prior to the next freeze cycle and add 10 mL of water.
3. After the final thaw cycle is complete, follow the steps above in Testing; A; 2,
3, 4, & 5.
Illinois Modified AASHTO T-324: Perform a Loaded Wheel test according to Illinois
modified AASHTO T-324.
A. All the data from testing will be collected and will/may include:
1. Gmm
2. Gmb
3. Voids
a. Unconditioned
b. Conditioned
5. The standard TSR, for each additive type (calculated with the unconditioned
strength in the denominator and with the conditioned strength in the
numerator). For each additive type the TSR is calculated separately for each
level of conditioning.
6. The combined TSR, which is similar to the standard TSR except that it is
calculated by always using the unconditioned strength from samples with no
additive in the denominator, regardless of the additive type used.
B. Evaluate the strengths, TSRs, rut depths, and wheel passes for each additive
type, for each aggregate type tested, to determine if:
2. One of the additive types consistently gives higher strengths, TSR ratings, rut
depths, and wheel passes.
Dolomite aggregates that contain significant amounts of Magnesium Carbonate, when used
in Hot-Mix Asphalt, have been found to undergo mass loss during ignition oven testing,
which causes highly variable results in asphalt binder content. This procedure utilizes the
ignition oven to identify these types of aggregates.
B. Procedure
1. Obtain a 3000 gram sample of the aggregate to be tested and oven dry to a constant
mass in an oven set at 110 C 5 (230 F 9). Constant mass is achieved by drying
sample until further drying does not alter the mass by more than 0.5 g in one hour as
stated in IL Modified AASHTO T-30.
3. Place one of the 1000 gram samples into the ignition oven catch pan.
4. Record the initial weight of the sample and catch pan at room temperature to the nearest
0.1 gram.
5. Place the sample and catch pan into an ignition oven preheated to 625 C. Do not
push the start button on the oven. Allow sample to remain in ignition oven for one
hour.
6. After one hour, remove the sample and catch pan, allow it to cool to room temperature
and record the weight to the nearest 0.1 gram.
7. Repeat steps 3 through 10 for the two remaining 1000 gram samples.
8. Calculate the aggregate mass loss for each run according to the following:
Wi Wf
W = 100
Wi
Where: W = Aggregate mass loss in percent
Wi = Initial weight of the aggregate sample in grams
Wf = Final weight of the aggregate sample in grams after
exposure to 625 C
10. Aggregates exhibiting average mass loss in excess of 4% are likely to contain significant
amounts of Magnesium Carbonate and will likely cause high variability in ignition oven
test results for asphalt content.
January 1, 2015 Manual of Test Procedures for Materials B91
Appendix B18
This Page Reserved
In the following sections, the terms top and bottom angles, first position, and turned 90
degrees will be used. This refers to the position where the DAV-2 will be collecting angle data.
The following diagrams will display how the DAV-2 will be oriented in the gyratory specimen mold
and will help avoid confusion in the midst of testing:
Basic method for all compactors (additional instructions included for early model Troxler 4140s)
1. Attach the HMS sphere to the top of the DAV-2 using the supplied bolt. Tighten the bolt
enough so that the sphere will not turn, but do not over tighten as this could strip out the
bolt. The HMS plates are referred to by their eccentricity, or how far (in mm) from the
center of the sphere the load is applied. The 22 mm plate (the one labeled 21, referring
to the angle in degrees ground into the bottom of the plate) will be the only plate used in
this calibration. Apply lubricant to the top of the sphere and to the angled surface on the
bottom of the plate, as this will help to reduce wear from metal on metal contact.
Petroleum jelly is the best lubricant to use with the DAV-2 and HMS.
2. Prior to testing, select two good, clean specimen molds to use for calibration. Make sure
these molds are not too worn, are within specifications, and are used for production
testing. The molds will be referred to as mold A and mold B. Place molds A and B
o o
into an oven set at 305 F / 154 C for a minimum of 30 minutes. Connect the DAV-2 to a
CPU using the supplied interface cable. If the CPU doesnt have a serial port, a serial to
USB adapter may be used; these adapters, however, need software in order to function
and this software must be installed before they will operate. There are three buttons in
the Test Quip software that will be used. They are as follows:
3. Open the Test Quip DAV-2 software and start data collection in the DAV-2 (Start Button
in the illustration above). When data collection has been successfully initialized,
disconnect the cable from the DAV-2. The DAV-2 has ~26 minutes of memory for data
collection, so begin testing quickly so all test points will be collected within that time
frame. Before placing the DAV-2 into a mold, apply lubricant to the bottom of the DAV-2.
As the DAV-2 will spin during gyration, the lubricant will allow for free movement and help
to reduce wear from metal on metal contact.
5. Remove mold B from the oven. Repeat the same process as with mold A for the
second bottom and top angles; but for both these angles, line the prongs up with a point
90 degrees counter-clockwise from the first position, as in the turned 90 degrees
illustration on the previous page. After running the second bottom and top angles,
extrude the DAV-2 and put mold B back into the oven to reheat for possible further
testing. These internal angles will yield a total of four test points for one run.
6. Connect the DAV-2 to the CPU with the interface cable and stop the data collection in the
DAV-2 (Stop Button in the illustration on the previous page). Download the data to the
CPU (Download Data Button in the illustration on the previous page). Label the data
sheet as needed and save it to a pre-labeled file that has been set up for internal angle
data. The data will look something like this:
7. Open the DAV-2 Excel spreadsheet. Be sure to choose Enable Macros when prompted
so the integrated buttons will function. A prompt should pop up asking to open a file.
Choose the desired saved file and click OK. If the prompt doesnt come up or an error
occurs, simply click on the Add Data button. After the data imports to the spreadsheet,
the initial page will look something like this:
10. If the average internal angle is not within the specified 1.16o +/- 0.02o range, the SGCs
angle must be physically adjusted accordingly using the manufacturers specified
method. This adjustment often has to be done on a trial and error basis; some
manufacturers have detailed documentation on changing the angle, so be sure to refer to
that when possible. State per sonnel will not perform t he phy sical angl e adjustment t o
contractor or consultant SGCs under any circumstances.
11. When the angle is physically adjusted, repeat steps #2 #10 after both molds have had a
minimum of 30 minutes to reheat in the oven. This may take more than one additional
attempt to get to the desired internal angle. Adjust the SGCs angle until the average of
the four internal angles from the 22 mm HMS plate is at 1.16o +/- 0.02o. The SGC is now
within internal angle specifications.
The DAV-2 and HMS must be used a minimum of once every two years for gyratory angle
calibration. It is suggested that this calibration take place during a material labs inspection,
which may be annually or biennially depending on how the individual district conducts its
inspections. Routine monthly angle calibration verification of SGCs may be performed one of two
ways:
2. After the final angle is set and calibrated with the DAV-2 and HMS, an external angle
verification procedure may be run according to the SGC manufacturers specifications. If
HMA is needed for this procedure, an N90 surface mix commonly used in the testing
labs area should be utilized. The external angle measurement from this procedure will
become the reference angle for verification purposes. For example: the DAV-2 and HMS
o
gives an internal angle of 1.16 and the external angle procedure gives an external angle
o
of 1.23 . When verifying using the external angle from then on, the external angle should
measure 1.23o +/- 0.02o. This method addresses concerns of possible mold wear due to
the use of the DAV-2 and HMS as well as giving labs that do not own a DAV-2 an
accepted method of routine gyratory angle verification.
1. Start data collection in the DAV-2. Load the DAV-2 and HMS into the mold, and place in
the SGC sample chamber.
2. Hit the MENU button on the keypad. Hit 2 to adjust the maximum pressure setting.
Type 200, then hit the ENTER key to input the value. Hit the ESC key to exit the
menu.
4. When the ram reaches ~130 mm, hit the ESC key to stop the ram. Make sure the ram
head and collar are seated squarely in the top of the mold, with the pin on the collar fully
down into the notch on the top of the mold.
5. Hit the ANGLE ON key to induce the angle. Be sure that the angle stop block (inside
the compactor) fully engages. Hit the ESC key after the tray stops rotating.
6. Hit the RAM DOWN key. The ram will travel down and contact the DAV-2 and HMS.
Hit the ESC key when the ram has stopped completely.
7. Hit the MENU button on the keypad. Hit 2 to adjust maximum pressure setting. Type
600, then hit the ENTER key to input the value. Hit the ESC key to exit the menu.
8. Hit the START button to use automatic compaction to complete the rest of the internal
angle measurement.
Calibration verification on the DAV-2 units will be performed by BMPR annually. The units
are to be sent to the Central Bureau HMA Lab in the late fall or early winter after the construction
season ends. The calibration verification will be performed and the units will be returned to the
districts in time for winter mix design verifications and lab inspections.
1. Keep the DAV-2, the ram head, and the molds being used as clean as possible. Any
debris on the bottom (or top) plate of the mold or on the ram head will have an effect on
the angle when the bottom of the DAV-2 contacts it. A quick spray of WD-40 and a wipe
down with a rag on the inside of the mold, the plate(s), and the ram head will ensure
good angle data.
3. While the standard hydraulic jack set up may be used for extruding the DAV-2 and other
contents from the mold after testing, there is a more efficient way using Marshall molds.
Start with a base plate, followed by a collar, then a mold, then another collar; then place
your gyratory mold (with base plate) over the stack. This will give you enough height on
most SGC molds to bring the gyratory mold base plate to the upper lip of the gyratory
mold without coming out. Another Marshall base plate may be added to the top of the
stack to give a little more height for taller gyratory molds (Troxler 4141, Pine compactors).
This stack is also helpful in loading the DAV-2 into the mold without having to drop it
down into the mold. Experiment to find the best setup to work with different models of
SGCs.
4. Some early model Troxler 4140s have been noted to release the angle when the HMS is
used. This is attributed to a worn main bearing in the compactor. This causes the angle
stop block inside the compactor to start moving away from the fixed angle screw block
that is supposed to be pushing it to keep the angle on. As the angle stop block moves
farther away from the fixed angle screw block, the angle is reduced. This is seen mostly
when using the 25.8 mm HMS plate or when the SGC exhibits excessive pressure. This
issue shouldnt be a problem when calibrating with the 22 mm HMS plate at 600 kPa
(using the alternate manual start procedure), but it is good to be aware of the potential for
this problem. A symptom of a worn main bearing can be observed during compaction of
hot mix when the angle stop block inside the compactor chatters (causing a rapping
noise) and can physically be seen moving a little bit during gyration. It seems to not be a
problem when compacting hot mix as the angle will stay engaged despite the
chattering, but this can pose a problem with HMS testing. While not recommended, the
following technique has been used as a way to continue testing until the main bearing
could be replaced. To physically keep the angle block engaged, a shop rag was first
folded in half twice. When the compactor induced the angle, the protruding collar inside
the compactor was gripped with the rag. Pressure was then applied in the opposite
direction of gyration. This held the angle block in place and kept the angle on.
5. When calibrating the angle on a contractor or consultants SGC, be sure to let their
personnel perform the physical angle adjustments when they are needed. This way the
state is not held liable for any mechanical problems that may occur afterwards.
QC/QA Document
Segregation Control of Hot-Mix Asphalt
Appendix B20
1.0 SCOPE
1.1 This work shall consist of the visual identification and corrective action to
prevent and/or correct segregation of hot-mix asphalt.
2.0 DEFINITIONS
2.4.1 Low. A pattern of segregation where the mastic is in place between the
aggregate particles; however, there is slightly more coarse aggregate in
comparison with the surrounding acceptable mat.
3.0 PROCEDURE
3.1 When medium or high segregation of the mixture is identified by the Contractor,
the Engineer, or the daily evaluation, the following specific corrective actions
shall be taken as soon as possible. The corrective actions shall be reported to
the Engineer before the next days paving proceeds.
3.1.1 End of Load Segregation. When medium or high end of load segregation is
identified, the following actions as a minimum shall be taken.
QC/QA Document
Segregation Control of Hot-Mix Asphalt
Appendix B20
(continued)
3.2 When the corrective actions initiated by the Contractor are insufficient in
controlling medium or high segregation, the Contractor and Engineer will
investigate to determine the cause of the segregation.
Any verification testing necessary for the investigation will be performed by the
Department according to the applicable project test procedures and
specification limits.
3.3 The District Construction Engineer will represent the Department in any dispute
regarding the application of this procedure.
1. GENERAL
If the RAP consists of natural aggregates only, the RAP aggregate bulk specific gravity shall be
as follows:
If the RAP contains slag aggregate the following procedure shall be used by an independent
AASHTO accredited laboratory to determine the RAP aggregate bulk specific gravity (Gsb).
2. SUMMARY of METHOD
A representative slag RAP sample shall be thoroughly prepared prior to testing by reheating and
remixing the reclaimed material. A solvent extraction, including washed gradation for
Department comparison, and two maximum theoretical specific gravity (Gmm) tests are
performed so that an effective specific gravity (Gse) can be calculated. The Gse value is used in
the calculation to determine the bulk specific gravity (Gsb) of the RAP.
3. SAMPLING
The slag RAP stockpile, in its final usable form, shall be sampled by obtaining a minimum of five
representative samples from the slag RAP stockpile. The samples shall be thoroughly blended
and split into two- 20,000 gram samples. One of the samples shall be submitted to an
independent AASHTO accredited IDOT approved laboratory for the subsequent preparation and
testing as specified herein. The other sample shall be submitted to the Department for optional
verification testing.
4. EQUIPMENT
Equipment including oven balances, HMA sample splitter, vacuum setup and solvent extractor
shall be according to the HMA QC/QA Laboratory Equipment document in the Manual of Test
Procedures for Materials. In addition the following equipment will also be required:
A. Sample pans - Large, flat and capable of holding 20,000 grams of RAP material.
B. Chopping utensil Blade trowel or other utensil used to separate the large
conglomerations of a RAP sample into a loose-flowing condition.
A. Transfer the entire 20,000 gram sample into a large flat pan(s).
B. Place sample into a preheated oven at 230 9 F. (110 5 C.) and heat for 30 to 45
minutes.
C. Remove the sample from the oven and begin breaking up the larger conglomerations of
RAP with the chopping utensil.
D. As the material begins to soften, blend the heated RAP by mixing the freshly chopped
material with the fines in the pan.
E. Return the RAP into the oven and continue heating for another 15 - 20 minutes.
F. Remove the RAP from the oven and repeat the chopping of the conglomerations and
blending of the fines until the RAP sample is homogeneous and conglomerations of fine
aggregate complies with Illinois Modified AASHTO T-209.
G. Place the loose RAP into a hopper or pan and uniformly pour it through a riffle splitter.
Take each of the halves and re-pour through the splitter. Thoroughly blend the sample
by repeating this process 2 - 3 times.
6. TESTING
7. CALCULATIONS
A. Calculate the adjusted Pb of the RAP to account for the addition of the 1.5 percent
virgin asphalt binder as follows:
1. Calculate mass of RAP Asphalt Cement (AC):
Pb
Mass of RAP AC = Dry RAP mass
100
(100 Adjusted Pb )
Gse (RAP) =
100 Adjusted Pb
Gmm 1.040
Calculate Gse:
Adjusted Pb = 6.3%
Rice Test, Gmm = 2.505
Appendix B22
Effective January 31, 2008
Revised January 1, 2014
GENERAL
When cores are removed from a pavement, and a solvent extraction or ignition oven
burn is conducted on the cored material, the gradation of the resulting aggregate is finer
than the original pavement because the perimeter of the core was cut by the core barrel.
Also, breakdown may occur as a result of the aggregate being subjected to the high
temperatures in the ignition oven. The following Core Correction Factors are used to
estimate the gradation of the in-place pavement from the gradation of the core after a
solvent extraction or an ignition oven burn has been conducted. The Core Correction
Factors were determined from four-inch diameter cores cut from 150 mm gyratory
compacted lab specimens. The six-inch Factors were estimated from the four-inch
Factors.
APPLICABLE DOCUMENTS
Percent Passing
EXTRACTION IGNITION OVEN *
Sieve BINDER SURFACE BINDER SURFACE
4-inch 6-inch 4-inch 6-inch 4-inch 6-inch 4-inch 6-inch
1" / 25.0mm 0.0 0.0 0.0 0.0 0.0 0.0 0.0 0.0
3/4" / 19.0mm 1.0 0.7 0.0 0.0 0.0 0.0 0.0 0.0
1/2" / 12.5mm 1.5 1.0 0.0 0.0 2.3 1.5 0.0 0.0
3/8" / 9.5mm 1.4 0.9 0.0 0.0 2.5 1.7 0.1 0.1
#4 / 4.75mm 0.9 0.6 2.2 1.5 1.9 1.3 2.1 1.4
#8 / 2.36mm 0.7 0.5 1.0 0.7 1.0 0.7 0.9 0.6
#16 / 1.18mm 0.6 0.4 0.6 0.4 0.7 0.5 0.6 0.4
#30 / 0.600mm 0.4 0.3 0.4 0.3 0.5 0.3 0.5 0.3
#50 / 0.300mm 0.4 0.3 0.4 0.3 0.4 0.3 0.3 0.2
#100 / 0.150mm 0.3 0.2 0.2 0.1 0.3 0.2 0.3 0.2
#200 / 0.075mm 0.17 0.11 0.16 0.11 0.20 0.13 0.20 0.13
The gradation of the aggregate from the extraction or ignition oven burn of the core is finer than the gradation of the original in-
place pavement. Therefore, subtract the designated amount from the measured percent passing of the core to estimate the in-
place gradation prior to coring.
* This testing was conducted on a limited number of aggregate sources. A larger amount of degradation in the ignition oven is
possible from aggregates from other sources.
Given: 4-inch BINDER mix cores where an IGNITION OVEN Burn has been conducted.
Percent Passing
IGNITION OVEN
Subtract Correction
Ignition Binder Estimated In-place
Factor from Ignition
Sieve Oven Correction Pavement Gradation
Oven Gradation
Gradation Factor
1" / 25.0mm 100.0 0.0 100.0 - 0.0 100.0
3/4" / 19.0mm 97.9 0.0 97.9 - 0.0 97.9
1/2" / 12.5mm 77.2 2.3 77.2 - 2.3 74.9
3/8" / 9.5mm 63.6 2.5 63.6 - 2.5 61.1
#4 / 4.75mm 38.5 1.9 38.5 - 1.9 36.6
#8 / 2.36mm 25.0 1.0 25.0 - 1.0 24.0
#16 / 1.18mm 18.1 0.7 18.1 - 0.7 17.4
#30 / 0.600mm 14.0 0.5 14.0 - 0.5 13.5
#50 / 0.300mm 10.1 0.4 10.1 - 0.4 9.7
#100 / 0.150mm 6.9 0.3 6.9 - 0.3 6.6
#200 / 0.075mm 5.60 0.20 5.60 - 0.20 5.40
Given: 6-inch SURFACE mix cores where a SOLVENT EXTRACTION has been conducted.
Percent Passing
EXTRACTION
Subtract Correction
Surface Estimated In-place
Extracted Factor from Extracted
Sieve Correction Pavement Gradation
Gradation Gradation
Factor
1" / 25.0mm 100.0 0.0 100.0 - 0.0 100.0
3/4" / 19.0mm 100.0 0.0 100.0 - 0.0 100.0
1/2" / 12.5mm 100.0 0.0 100.0 - 0.0 100.0
3/8" / 9.5mm 95.6 0.0 95.6 - 0.0 95.6
#4 / 4.75mm 60.6 1.5 60.6 - 1.5 59.1
#8 / 2.36mm 35.3 0.7 35.3 - 0.7 34.6
#16 / 1.18mm 23.8 0.4 23.8 - 0.4 23.4
#30 / 0.600mm 17.8 0.3 17.8 - 0.3 17.5
#50 / 0.300mm 12.8 0.3 12.8 - 0.3 12.5
#100 / 0.150mm 9.2 0.1 9.2 - 0.1 9.1
#200 / 0.075mm 7.10 0.11 7.10 - 0.11 6.99
When required, an off-site preliminary test strip and modified start-up shall be performed
as follows:
(a) Team Members. The start-up team, if required, shall consist of the following:
(b) Communication. The Contractor shall advise the team members of the
anticipated start time of production for both the off-site preliminary test strip and
subsequent modified start-up for both the surface and binder courses. The QC
Manager shall direct the activities of the start-up team. A Department-appointed
representative from the start-up team will act as spokesperson for the
Department.
(c) Off-site Preliminary Test Strip. The off-site preliminary test strip shall consist of
272 metric tons (300 tons). It shall contain two growth curves which shall be
tested as outlined herein.
(1) Mix and Gradation Test Strip Samples. The first and second sets of mixture
and gradation samples shall be taken by the Contractor at such times as to
represent the mixture of the two growth curves, respectively. All off-site
preliminary test strip samples shall be processed by the Contractor for
determination of mixture composition and air voids. This shall include
washed ignition gradation and asphalt content test results. This information
shall then be compared to the JMF and required design criteria.
All rolling equipment intended for use on a project shall be utilized on the off-
site preliminary test strip.
(3) Constructing the Off-site Preliminary Test Strip. After the Contractor has produced
the mix, transported the mix, and placed approximately 90 to 140 metric tons (100 to
150 tons) of mix, placement of the mix shall stop, and a growth curve shall be
constructed. After completion of the first growth curve, paving shall resume for 45 to
90 metric tons (50 to 100 tons) of mix, placement shall stop, and the second growth
curve shall be constructed within this area. Additional growth curves may be required
if an adjustment/plant change is made during the off-site preliminary test strip. The
Contractor shall use the specified rolling procedures for all portions of the test strip
except for the growth curve areas which shall be compacted as directed by the QC
Manager.
(4) Location of Off-site Preliminary Test Strip. The off-site preliminary test strip shall be
located on a pavement type similar to the contract pavement and acceptable to the
Engineer. It shall be on a relatively flat portion of the roadway.
(6) Compaction and Testing. The QC manager shall specify the roller(s) speed and
number of passes required to obtain a completed growth curve. The nuclear gauge
shall be placed near the center of the hot mat and the position marked for future
reference. With the bottom of the nuclear gauge and the source rod clean, a one-
minute nuclear reading (without mineral filler) shall be taken after each pass of the
roller. Rolling shall continue until the maximum density is achieved and three
consecutive passes show no appreciable increase in density or no evidence of
destruction of the mat. The growth curve shall be plotted. No testing of initial passes
shall be taken until the third pass is completed.
(7) Final Testing. After the growth curve information is obtained, a final nuclear reading,
using mineral filler to eliminate surface voids, shall be taken at the marked position.
This reading is used to adjust the maximum density reading obtained during the
growth curve.
(8) Evaluation of Growth Curves. Mixtures which exhibit density potential outside of the
specified density range shall be considered as sufficient cause for mix adjustment. If
a mix adjustment is made, an additional test strip may be constructed, and
associated tests shall be performed. This information shall then be compared to the
AJMF and required design criteria.
If the density potential of the mixture not meet the minimum specified, the operation
shall cease until all test data is analyzed or a new mix design is produced.
(d) Documentation. All off-site preliminary test strip, modified start-up, and rolling pattern
information (including growth curves) will be tabulated by the QC manager with copies
provided to each team member, and the original retained in the project files. Any
changes to the rolling pattern shall be by the Contractor and the Engineer and recorded.
(e) Modified Start-Up. At the start of placement on the jobsite, the Contractor shall construct
a growth curve in between the first 90 to 140 metric tons (100 to 150 tons) for the
purposes of evaluating the properties of the mixture and ensuring that the established
rolling pattern was valid.
The placement shall stop until the growth curve has been evaluated. A hot-bin or a
combined aggregate belt sample and a mix sample representative of the growth curve
shall be obtained and tested expediently for determination of mix composition and air
voids. This information shall then be compared to the preliminary test strip data.
If the growth curve and visual evaluation of the mix are satisfactory, the placement may
be resumed. If the growth curve and visual evaluation of the mix are unsatisfactory,
placement shall remain on hold until the plant samples are completed and reviewed by
the QC Manager and the Engineer. If agreed by the Engineer, the Contractor shall
make appropriate adjustments, resample and retest, construct another growth curve,
and evaluate the mixture. This procedure will be followed until satisfactory test results
are obtained.
A. Purpose
This procedure provides a means for determining the amount of asphalt binder
remaining after a tack coat or prime coat cures. The remaining asphalt binder is
termed residual asphalt. This procedure shall be used for verifying specification
compliance when the tack coat or prime coat application rate is specified based on
residual asphalt.
B. Procedure
11. Cut and label a 12.0 inch by 12.0 inch square piece of non-woven geotextile
fabric or cardboard. Place the square in a 230 9 F (110 5 C) oven and dry
to constant weight. Remove the square from the oven and record the weight Wi
to the nearest 0.1 gram within 5 minutes after removal.
Notes:
Oven drying is necessary because cardboard especially can retain
considerable moisture in humid conditions.
Constant weight is defined as the weight at which further drying does not
alter the mass more than 0.5 gram in 1 hour.
12. Place the pre-weighed square at a random transverse location prior to tack or
prime coat application.
13. After the prime or tack has been applied, remove the square from the pavement
and protect from damage during transport. Place the square in a 230 9 F (110
5 C) oven and dry to a constant weight.
14. Remove the square from the oven and record the final weight Wf to the nearest
0.1 gram within 5 minutes after removal from the oven.
15. Subtract the initial weight Wi determined in step 1 from the final weight Wf
determined in step 4. Divide this value by 454 to get the residual asphalt binder
application rate in lbs/ ft2.
INSTRUCTIONS: The Contractor shall respond to all items addressed in this model. This is
applicable to work performed by the Contractor or subcontractor(s).
Examples are provided to assist the Contractor, and any innovations to the
quality control process may be presented.
County:
Section:
Route:
District:
Contract No.:
Job No.:
Project:
Contractor:
P.O. Box:
Street Address:
City/State/Zip Code:
Telephone No.:
Fax No.:
I. FIELD OFFICE
Location:
Contact Person:
Telephone Number:
Individual's Name:
Department Training:
Company Name:
Telephone Number:
Primary or Back Up
The Level II PCC Technician who will be responsible for plant mixture control and
adjustments is indicated in Part 2.
INSTRUCTIONS: Indicate whether beams and/or cylinders will be cast, as well as how the
specimens will be initially cured.
Note: In some instances, such as Articles 503.05 and 503.06, only a flexural strength is
specified. An equivalent compressive strength may be used if approved by the Engineer.
Example:
Plastic cylinder molds [6 by 12 in. (152 by 305 mm)] will be used to cast strength
specimens. The plastic cylinder mold will be covered with a plastic cylinder lid. A curing
box will be used to maintain the specimens within 60 to 80 F (16 to 27 C). The
specimens will be transported after 24 hours for standard curing.
INSTRUCTIONS: Indicate the final location for standard curing and testing of the strength
specimens, and the method of curing.
Example:
The strength specimens will be transported to the consultant's lab for standard curing in a
water storage tank, and testing.
Example:
In the event of failing tests or observation of defective work at the jobsite, the Level I PCC
Technician will be responsible for notifying the Superintendent and the Quality Control
Manager. The Superintendent will be responsible for notifying the Resident Engineer.
In the event of failing tests at the plant, the Level II PCC Technician will be responsible for
notifying the Superintendent and the Quality Control Manager. The Superintendent will be
responsible for notifying the Resident Engineer.
V. COMMUNICATION
INSTRUCTIONS: For concurrent pours, indicate how each Concrete Tester will be able to
contact the Level I PCC Technician.
Indicate how jobsite personnel will be able to contact the Level II PCC Technician.
Example:
For concurrent pours, each Concrete Tester will be able to contact the Level I PCC
Technician by two-way radio. Jobsite personnel will use two-way radio to contact the Level
II PCC Technician, when he/she is at the plant. When the Level II PCC Technician is not at
the plant, jobsite personnel and the Level II PCC Technician will use a cellular phone.
INSTRUCTIONS: Indicate the forms, the bound hardback field books, and bound hardback
diaries that will be used to maintain documentation at the jobsite.
Example:
A bound hardback field book will be used for all documentation at the jobsite.
Examples:
A meeting will be scheduled the day before the bridge deck pour to discuss mix, concrete
delivery, pumped concrete, finishing equipment and requirements, labor, deficiencies,
curing, weather conditions (i.e. temperature, humidity, wind), and other pertinent issues.
Or
A meeting will be scheduled two months, two weeks, and two days before the bridge deck
pour. The meetings will discuss mix, concrete delivery, pumped concrete, finishing
equipment and requirements, labor, deficiencies, curing, weather conditions (i.e.
temperature, humidity, wind), and other pertinent issues.
If applicable:
I. MATERIALS
INSTRUCTIONS: The wording for A) Aggregates is provided for the Contractor. Indicate
the material sources for B) Coarse Aggregates and C) Fine Aggregates. If applicable,
attach proposed mix plant gradation bands in accordance with the Departments
Development of Gradation Bands on Incoming Aggregate at Mix Plants.
A) Aggregates
B) Coarse Aggregates
Example:
Coarse aggregates are shipped by rail to the plant, in a uniform gradation condition.
Upon delivery of the coarse aggregate, it will be transferred to a stockpile by a
movable conveyor system. The stockpile will be built according to Article 1004.01 (e),
of the Standard Specifications for Road and Bridge Construction (January 1, 2012).
Fine aggregates are shipped by truck to the plant, in a uniform gradation condition.
The fine aggregate will be truck dumped into a stockpile. The truck stockpile will be
built according to Article 1003.01 (e) of the Standard Specifications for Road and
Bridge Construction (January 1, 2012).
All stockpiles will be separated with concrete block walls, sufficient in width, length,
and height to prevent contamination. The maximum height of the walls will be ___ ft
(___ m).
Example:
Coarse and fine aggregates will be stockpiled and allowed to drain for 12 hours, before
placement in the plant bins. However, during hot weather, the aggregate stockpiles
will be periodically sprinkled with water.
NOTE: Fine aggregate moisture testing is specified in the Special Provision for
Quality Control/Quality Assurance of Concrete Mixtures.
INSTRUCTIONS: Indicate how and where you will sample aggregates to assure they
will meet current Department gradation specifications.
Example:
For aggregates arriving at the plant, truck-dump sampling will be performed for fine
and coarse aggregate gradation tests.
For aggregates used during concrete production, on-belt sampling will be performed
for fine and coarse aggregate gradation tests. The conveyor belt beneath the bin will
be used.
NOTE: The frequency of gradation testing to check the production of concrete, for
aggregates stored at the plant in stockpiles or bins, is specified in the Special
Provision for Quality Control/Quality Assurance of Concrete Mixtures.
Plant Name:
Plant Location:
Producer No.:
NOTE: The plant and delivery trucks are to be approved according to the Bureau of
Material and Physical Researchs Policy Memorandum, Approval of Concrete
Plants and Delivery Trucks. Contact the Departments District office to obtain the
required forms.
Location:
Contact Person:
Telephone Number:
The quality control laboratory is sq. ft. [The Department suggests 200 ft (20 m)].
Individual's Name:
Department Training:
Company Name:
Telephone Number:
Primary or Back Up
NOTE: Include personnel who have been trained by the Level II PCC Technician to
sample and test aggregate for moisture.
The Level I PCC Technician who will be responsible for jobsite mixture control and
adjustments is indicated in Part 1.
The Quality Control Manager who will be responsible for overall project quality control is
indicated in Part 1.
INSTRUCTIONS: Provide mix design information as stated in 1.1 Volumetric Mix Design
and Mix Design Submittal of the Portland Cement Concrete Level III Technician Course
Manual of Instructions for Design of Concrete Mixtures.
Otherwise state: Only mix designs previously verified by the Department will be used.
INSTRUCTIONS: Based on the ASTM C 1260 test information provided for the
aggregates, indicate the mixture option selected for minimizing the risk of alkali-silica
reaction. Refer to Article 1020.05(d).
INSTRUCTIONS: Indicate the plant start-up testing frequency, and the plant testing
frequency thereafter, to control production. This is required for slump, air content, unit
weight, yield, and temperature tests performed at the plant. Indicate any other tests that
will be performed.
NOTE: Plant start-up situations are defined in the Portland Cement Concrete Level II
Technician Course manual. Indicate if the manuals plant start-up situations will
be applicable, or if other start-up situations will apply.
INSTRUCTIONS: If the Level II will supervise more than one plant, indicate his/her
attendance at the various plants for large or critical pours.
VIII. COMMUNICATION
INSTRUCTIONS: Indicate how plant personnel will be able to contact the Level II PCC
Technician, when he/she is not at the plant.
Example:
Plant personnel will use a land phone, to contact the Level II PCC Technician by cellular
phone.
INSTRUCTIONS: Indicate the forms, the bound hardback field books, and bound hardback
diaries that will be used to maintain documentation at the plant, and at the laboratory.
Example:
A loose-leaf binder will be used to maintain any Department form which is required at the
plant, or at the laboratory. A bound hardback field book will be used to record test results
at the plant, and at the laboratory. A bound hardback diary will be used to document
observations, inspections, adjustments to the mix design, and corrective actions at the
plant.
(IF AN INDIVIDUAL)
Firm Name
Print Name of Owner
Signature of Owner
Date:
(IF A CO-PARTNERSHIP)
Firm Name
Print Name of Partner
Signature of Partner
Date:
(IF A CORPORATION)
Corporate Name
Print Name of Authorized Representative
Signature of Authorized Representative
Date:
(ALL)
Business Address:
P.O. Box:
Street Address:
City/State/Zip Code:
County:
Section:
Route:
District:
Contract No.:
Job No.:
Project:
Contractor:
P.O. Box:
Street Address:
City/State/Zip Code:
Telephone No.:
Fax No.:
ADDENDUMS
(IF AN INDIVIDUAL)
Firm Name
Print Name of Owner
Signature of Owner
Date:
(IF A CO-PARTNERSHIP)
Firm Name
Print Name of Partner
Signature of Partner
Date:
(IF A CORPORATION)
Corporate Name
Print Name of Authorized Representative
Signature of Authorized Representative
Date:
(ALL)
Business Address:
P.O. Box:
Street Address:
City/State/Zip Code:
This document summarizes the qualifications and duties of quality control personnel for Portland
Cement Concrete (PCC) mixtures, Cement Aggregate Mixture II (CAM II), and Controlled Low-
Strength Material (CLSM). Duties shall be performed daily, or as required, according to the
QC/QA specifications and related documents.
QUALITY CONTROL MANAGER: An individual who has the experience, responsibility, and
authority to make decisions regarding quality control of Portland Cement Concrete, Cement
Aggregate Mixture II, and Controlled Low-Strength Material. This individual is required to
have successfully completed the Department's Portland Cement Concrete Level I Technician
Course, the Portland Cement Concrete Level II Technician Course, and either the 3-day
Mixture Aggregate Technician Course or 5-day Aggregate Technician Course.
3. Ensure the laboratory, concrete plant, and delivery trucks are approved by the
Engineer.
6. Ensure good communication between the plant and jobsite to quickly resolve
quality control problems. Failure to resolve quality control problems shall
result in mixture production suspension.
10. Supervise the Level III PCC Technician, Level II PCC Technician, Level I PCC
Technician, Concrete Tester, Gradation Technician, Mixture Aggregate
Technician, and Aggregate Technician.
LEVEL III PCC TECHNICIAN: An individual who has successfully completed the
Department's Portland Cement Concrete Level I Technician Course, the Portland Cement
Concrete Level II Technician Course, the Portland Cement Concrete Level III Technician
Course, and either the 3-day Mixture Aggregate Technician Course or 5-day Aggregate
Technician Course.
2. Read contract special provision(s) for project specific mix design information.
2. Check the operation of the concrete plant and condition of the delivery trucks.
7. Verify the specified mix design is used, and the correct proportions of
aggregates, cement, finely divided minerals, water, admixtures, and fiber
reinforcement are batched.
10. Supervise the Gradation Technician, or assign the task to the Mixture
Aggregate Technician or Aggregate Technician.
9. Observe the discharge of a mixture by the delivery truck, and take appropriate
action if a problem is identified.
10. For a mixture which is not mixed on the jobsite, ensure the required
information is recorded on the delivery truck ticket.
11. Document all observations, inspections, adjustments to the mix design, test
results, retest results, and corrective actions promptly, and in the specified
format.
12. Maintain communications with plant personnel to control the mixture, for
compliance with the specifications.
5. Observe the mixture and notify the Level I or Level II PCC Technician of any
problems.
7. For a mixture which is not mixed on the jobsite, ensure the required
information is recorded on the delivery ticket.
NOTE: The duties listed are for assisting the Level II PCC Technician, and are not to be
confused with the Aggregate Gradation Control System program.
NOTE: The duties listed are for assisting the Level II PCC Technician, and are not to be
confused with the Aggregate Gradation Control System program.
This document applies to cast-in-place, precast, and precast prestressed operations. This
document summarizes the minimum requirements for sampling and testing Portland Cement
Concrete (PCC) mixtures, Cement Aggregate Mixture II (CAM II), and Controlled Low-Strength
Material (CLSM). Refer to the Manual of Test Procedures for Materials for detailed equipment
information.
Shovel
Thermometer
Ruler
Definition of High Volume Aggregate Testing Operation The high volume aggregate testing
equipment may be used for multiple concrete plants, if approved by the Engineer. The decision
will be based on specification requirements for providing test results.
Electronic Balance2
(2 Check weights are recommended.)
Sieve Shaker, 305 mm (12 in.) sieve capacity and sufficient inside height to accept typical sieve
stock
1 5/8 in. nominal height4 9.5 mm (3/8 in.), 6.25 mm (1/4 in.),
4.75 mm (No. 4), 1.18 mm (No. 16) two required,
0.3 mm (No. 50), 0.15 mm (No. 100),
0.075 mm (No. 200) two required
4
Distance from the top of the frame to the sieve cloth surface
Two Pans
Lid
Definition of Low Volume Aggregate Testing Operation The low volume aggregate testing
equipment may be used only for a single concrete plant. If a reduced testing time is desired, the
high volume aggregate testing equipment is recommended, since the low volume 200 mm
(8 in.) sieves will normally require the coarse aggregate sample to be sieved in parts to prevent
overloading.
Electronic Balance2
(2 Check weights are recommended.)
Sieve Shaker, 200 mm (8 in.) sieve capacity and sufficient inside height to accept typical sieve
stock
Two Pans
Lid
Shovel
Thermometer
Ruler
Plastic Cylinder Lids, 150 mm (6 in.), 100 mm (4 in.), or other material per Illinois Modified
AASHTO T 23
-------------OR-------------
Steel or Plastic Beam Molds (typical length)
152 x 152 x 457 mm (6 x 6 x 18 in.),
152 x 152 x 483 mm (6 x 6 x 19 in.),
152 x 152 x 508 mm (6 x 6 x 20 in.),
152 x 152 x 533 mm (6 x 6 x 21 in.), or
152 x 152 x 762 mm (6 x 6 x 30 in.)
Plastic Cover with Absorbent Pad, or other material per Illinois Modified AASHTO T 23
------------AND------------
Tamping Rod or Vibrator (as appropriate)
Mallet
Recording Thermometer
Self-Consolidating Concrete
For dry cast operations, the slump kit is optional and the air meter kit is not required.
Applicable Products When cores are used to determine compressive strength, the core drill
shall have diamond impregnated bits attached to the core barrel.
Applicable Specification(s):
b) Divide the total quantity by the random sample testing frequency. Round up to the nearest whole
number.
i.e. Total quantity of bridge substructure is 395 yd (302 m). The random sample testing
frequency is 50 yd (40 m) for slump and air.
302/40 = 7.6
Obtain 8 random samples.
c) Obtain a random number from a calculator, a computer, or the Department's random numbers
table and multiply this number by the random sample testing frequency. Round the result to the
nearest whole number and document the random number used.
d) Determine which truck is to be sampled by maintaining a cumulative total of the amount placed
during the pour.
Cumulative Total_
1st truck 6.5 yd (5.0 m) 6.5 yd (5.0 m)
2nd truck 6.5 yd (5.0 m) 13.0 yd (10.0 m)
3rd truck 6.5 yd (5.0 m) 19.5 yd (15.0 m)
4th truck 6.5 yd (5.0 m) 26.0 yd (20.0 m)
**5th truck 6.5 yd (5.0 m) 32.5 yd (25.0 m)
** Sample this truck since the random sample calculation is at 29 yd (23 m). It is not
necessary to sample exactly at 29 yd (23 m). Therefore, the slump and air test may be
performed upon arrival of the truck. Sampling is to be performed according to Illinois
Modified AASHTO R 60.
c) For each random sample location, determine the corresponding station location and
document.
d) For each random sample location, the process shall be repeated for additional test locations
using new random numbers for each location.
NOTE: Always select a new set of numbers in a systematic manner, either horizontally or
vertically. Once used, the set should be crossed out.
POLICY MEMORANDUM
1.0 DEFINITIONS
CONSULTANT - A Private firm which performs construction materials testing for the
Department, Producer, or Contractor. Department prequalification and AASHTO
accreditation requirements apply where Department construction testing is
performed directly for the Department under a Department contract or subcontract.
FIELD TESTS Tests that may be performed outside of a laboratory, for example, a
portland cement concrete (PCC) or hot-mix asphalt (HMA) test performed at the
jobsite.
QUALITY CONTROL LABORATORY - Any laboratory used for Quality Control (QC)
testing (Contractor or Producer tests) required by the Department. Required tests
for quality control laboratories are listed in Table 1.
This policy governs the minimum qualifications for materials Quality Control and
Quality Assurance Laboratories operated by Contractors, Producers and
Consultants. It applies to aggregate, hot-mix asphalt (HMA) and Portland cement
concrete (PCC) testing laboratories.
3.0 PURPOSE
4.0 AUTHORITY
Federal regulations (23 CFR Part 637) require the Department to establish a
program for "qualifying" construction laboratories involved in tests which are used for
acceptance. Under the Department's QC/QA specifications, Contractor/Producer
test results are used in the acceptance process
6.1.1 All testing for Department contracts shall be performed by Qualified Personnel as
specified in the contract.
6.1.2 The Department will maintain a computer database of Qualified Personnel who
have successfully passed the appropriate QC/QA classes.
6.2.1 The Department shall approve all Private Laboratories used on Department
projects.
6.2.3 Each Private Laboratory shall have adequate floor space to efficiently conduct
required tests. Suggested minimum floor space is provided under Model Quality
Control Plans in the Manual of Test Procedures for Materials.
6.2.4 Each Private Laboratory shall have HVAC equipment capable of maintaining a
room temperature of 20 to 30 C (68-86 F). A Private Laboratory that performs
only aggregate gradation and/or aggregate moisture testing is exempt from this
requirement.
6.2.5 All equipment shall be as specified in the current Manual of Test Procedures for
Materials.
7.1 AASHTO R 18
Each Private Laboratory shall establish and implement a quality system which
meets the criteria from AASHTO R 18. Accredited Laboratories shall comply with all
of AASHTO R 18 for AMRL, and ASTM C 1077 for CCRL, with the exception of
Sections 6.1.7.4 and Section 6.1.7.5 of ASTM C 1077. The Private Laboratory
shall document staff technical proficiency in line with the requirements of AASHTO
R-18 section 5.5.2.
Each Private Laboratory shall have a Technical Manager (however titled) who has
overall responsibility for the technical operations of the Private Laboratory. The
Technical Manager shall be responsible for equipment maintenance and
calibration, maintaining records, and ensuring that current test procedures are
utilized. If the Private Laboratory is prequalified in a Professional Consultant
service category, a licensed Illinois Professional Engineer shall have direct
supervision of the laboratory.
The Private Laboratory shall calibrate or verify all testing equipment associated
with tests performed by the Private Laboratory. Table 3 includes a maximum
interval for calibrating most laboratory equipment. Heavy use or specific test
requirements may justify more frequent checks.
7.5.1 Test Records Each Private Laboratory shall maintain test records which contain
sufficient information to permit verification of any test report.
7.5.2 Records Retention - Each Private Laboratory shall maintain documentation of the
internal quality controls. At a minimum, the records shall include:
7.5.3 Equipment Calibration and Verification Records - Calibration records shall include
the minimum information listed below. AASHTO R 18 and ASTM Standard C 1077
provide additional guidance for calibration of most testing equipment.
1. Description
2. Model & Serial Number
3. Name of person calibrating
4. Calibration equipment used
(e.g., standard weights, proving rings, thermometers)
5. Date calibrated & next due date
6. Reference procedure used
7. Results of calibration / verification
7.6 Publications
Each Approved Private Laboratory shall maintain current copies of all test
procedures performed. This requirement shall include a current copy of the Manual
of Test Procedures for Materials.
8.1 General
AASHTO accreditation does not waive the right of the Department to conduct
inspections and/or re-inspections.
8.4.1 The Private Laboratory shall submit a written request for an inspection to the
District. The request shall indicate the following:
The location of the Private Laboratory.
The type of Private Laboratory, i.e., aggregate, HMA, or PCC.
The name of the Technical Manager, who will be present for the inspection.
The date the Private Laboratory will be ready for inspection.
8.4.2 The District will notify the BMPR Laboratory of the inspection request. BMPR
personnel will establish a tentative date to perform the inspection.
8.4.3 The District will perform a brief visual inspection approximately seven calendar days
before the BMPR inspection. The District will verify that the Private Laboratory is
ready for inspection and notify the BMPR Laboratory.
8.4.4 BMPR personnel will perform the inspection and prepare a preliminary report.
Standard inspection forms and a preliminary report, developed and maintained by
the BMPR Laboratory, will be used.
8.4.5 BMPR personnel will assign identification numbers to all test equipment. Unless a
District has an established numbering system, the following sequences will be used.
Sieves
e.g., IL07 -1418-01
where: IL = State
07 = inspection year
1418-01 = Producer/Supplier Number
Sieves are engraved on the inside of the bottom lip directly beneath the label.
HMA Equipment
e.g., IL07B1 - 123
where: IL = State
07 = inspection year
B = hot mix asphalt (bituminous)
1 = district number
123 = sequential numbers
PCC Equipment
e.g., IL07C1 - 123
where: IL = State
07 = inspection year
C = concrete
1 = district number
123 = sequential numbers
*The numbering system prior to 2007 was IL07-123 for HMA and
IL07CND1-123 for PCC. The change was made to make the numbering
system more uniform.
8.4.7 If a review of the preliminary report indicates there are no deficiencies, BMPR will
provide written notification to the Private Laboratory indicating the Private
Laboratory is now an approved private laboratory. The notification will include an
equipment list. A copy of the notification will be provided to the District.
8.4.8 If the preliminary report indicates there are deficiencies, BMPR will provide written
notification to the Private Laboratory, indicating the deficiencies and that corrective
action is required. A copy of the written notification will be provided to the District.
8.4.9 After correction of all cited deficiencies, the Private Laboratory shall notify the
District. The District will inspect the Private Laboratory to verify the deficiencies
have been corrected and will notify BMPR in writing.
8.4.10 BMPR will provide written notification to the Private Laboratory, indicating the
private laboratory is now an approved private laboratory. The notification will include
an equipment list. A copy of the written notification will be provided to the District.
8.6.2 The District may not waive any requirements for Private Laboratories or test
equipment for Required Tests.
8.6.4 At any time, if the District identifies deficiencies in the facility, equipment, or test
procedures that could affect the results of any QC or QA tests, the District will
require the Private Laboratory to take immediate action to correct the deficiency.
The Department will maintain a computer database to monitor the approval status of
Private Laboratories. The database will include the following information:
Attachments
MG/jy
Note 1: Required for laboratories that test Air Cooled Blast Furnace Slag.
Note 2: Required for laboratories that run the Departments Slag Producers Self-Testing Program.
Surface-Dry Specimens
Maximum Specific Gravity of Bituminous
T 209 (IL)
Paving Mixtures
Resistance to Plastic Flow of Bituminous
T 245 (IL)
Mixtures Using Marshall Apparatus
Resistance of Compacted Bituminous Mixture
T 283 (IL)
to Moisture Induced Damage
Asphalt Content of Bituminous Concrete
T 287 (IL) Or T164 or Mixtures by the Nuclear Method
T 3082
T 312 (IL)
Superpave Gyratory Compaction
T 308 (IL) Asphalt Binder Content of Hot-Mix Asphalt by
or T164 or
the Ignition Method
T 2872
D 2950 Determination of Density of Bituminous
______ (IL) Concrete In-Place by Nuclear Method Field
Test; not observed during Lab Inspection
Note 1: Method B shall be used for quantitative extraction. Method A or E shall be used to recover binder for qualitative analysis.
Note 2: Determined by which piece of equipment is more appropriate for the lab to determine asphalt content.
Note 1: For an exception to the strength testing requirement of performing compressive or flexural testing
(example: labs at Concrete Producer Plants), refer to the Departments Required Sampling and Testing Equipment for
Concrete document and check with district for approval of exception.
Note 2: Required for laboratories that run the Departments Slag Producers Self-Testing
Program.
Note 3: Requirement determined on case to case basis by district in which lab is located.
Note 2: The AAP on-site assessment is not required for Illinois type portable beam
breakers but is required for all other types of beam breakers. Additional
Information regarding use of portable PCC labs and their approval is provided
In Department Policy MAT-15, Quality Assurance Procedures for Construction.
Note 3 Test equipment must be presented during an inspection if the consultant lab
has the ability to perform the test.
Note 4 Test equipment must be presented during an inspection if consultant lab has
the ability to verify PCC mix designs.
Note 5 Test must be performed if consultant lab has the ability to perform the test.
All equipment listed is required unless noted otherwise. This list recommends 12 sieves and
12 shakers. Individual needs may vary for the specific products. Eight-inch sieves and other
alternate equipment may be substituted provided they conform to Illinois Test Procedure or
ASTM requirements and are approved by the Engineer.
Quantity Description
1 Mechanical Sieve Shaker 12 sieve capacity
1 Coarse Aggregate Sample Splitter (Illinois Test Procedure 248, Method A)
4 Splitter Pans, for coarse aggregate
1 Fine Aggregate Sample Splitter (as required)
4 Splitter Pans, for fine aggregate
1 Sink and clear Water Supply
1 Oven, electric drying, capable of maintaining a uniform temperature of 110 5 C
(230 9 F), (optional see Hot Plate)
2 Hot Plate, electric, or burner, gas in lieu of Oven, if approved by the Engineer
1 Gloves, pair, insulated
1 Balance, electronic, 8000 g capacity, 0.1 g readability
15 Sample Pans, (constructed to minimize loss of material during testing)
This document summarizes the minimum requirements for Hot-Mix Asphalt (HMA) quality
control, quality assurance, and design laboratories. It is the contractors responsibility to ensure
that all equipment complies with the applicable test specification in the Manual of Test
Procedures for Materials.
The QC laboratory will be 600 ft2 (55 m2) or greater in size and be located at the mix production
site. The laboratory will have running water and controlled heating and air conditioning capable
of maintaining a temperature between 68 86 F (20 - 30 C). The laboratory will be properly
maintained and contain the necessary equipment and supplies for performing the Quality
Control testing. All testing will be performed at the QC laboratory.
1. Balance (1): As defined by Illinois Specification 101. Balances used for Illinois
Modified AASHTO T 166, Illinois modified AASHTO T 209 (weight in water method),
and Illinois Modified AASHTO T 85 shall also include the following:
3. Freezer (1):
c. Capillary lid.
d. Small piece of fine wire mesh over the vacuum hose opening.
5. Ovens:
7. Sample Splitters:
b. Hot-mix asphalt (1): As defined by Illinois Modified AASHTO T 248 with the
following additional requirements:
8. Sieve Shaker (Mary Ann type or equivalent) (1): Capable of holding 12 in. (305 mm)
sieves.
b. Sieves No. 4 (4.75mm) and larger will be checked with go/no-go gauges for
compliance with minimum and maximum size openings.
c. Sieves below the 3/8 in. (9.5mm) may be 1 5/8 in. nominal height*.
10. Thermometers:
12. Vacuum Pump (1): Capable of removing entrapped air to a residual pressure of 30
mm Hg.
13. Gyratory Compactor (1) meeting the requirements of Illinois Modified AASHTO
T 312.
15. Gyratory Specimen Molds (2): As defined by Illinois Modified AASHTO T 312.
b. Diameter of extruding disk must not be less than 5.4 in. (138mm).
18. Ignition Oven (1): Gilson Binder Ignition Furnace, Model HM-378;
Barnstead/Thermolyne Furnace, Models F 85930 or F 85938; CEM Max Furnace;
Carbolite Furnace, Model ABA 7/35; or Troxler Furnace, Models 4730 or 4731 as
defined by Illinois AASHTO T 308.
Note: Other available furnace types may be used if acceptably evaluated by an
IDOT-approved research laboratory.
20. Sampling Shovel with sides and back built up 1 1 1/2 in. (25 40 mm).
21. Nuclear Asphalt Density Gauge (1): As defined by Illinois Modified ASTM D 2950.
22, Nuclear Asphalt Content Gauge (1) and Related Apparatus: As defined by the
Departments Procedure for Asphalt Content of HMA Mixtures by the Nuclear Method.*
*Note: Only required if lab utilizes Illinois Modified AASHTO T 287 (in place of
Illinois Modified AASHTO T 308) to determine asphalt content of HMA mixtures.
2. Extraction Apparatus (1), if utilizing recycled asphalt materials (RAP and/or RAS) :
As defined by Illinois Modified AASHTO T 164, Test Methods A and B.
6. Loading Strips ( one set for 6 in. specimens): As defined by Illinois Modified
AASHTO T 283.
7. Oven for short term aging (1): Capable of maintaining 325 5 F (163 3 C).
8. Water Bath (1): As defined by Illinois Modified AASHTO T 283 with the following
additional requirements:
b. Having perforated false bottom or equipped with a shelf at least 2 in. (51 mm)
above bottom of bath.
c. Thermostatically controlled.
10. Baking Pans (2): Each providing a minimum surface area of 140 in.2 (903 cm2).
*11. Mixing Apparatus (1): As defined by Illinois Modified AASHTO T 245 with a
minimum capacity of 12000 g.
*Optional
Electronic balances approved for Illinois Department of Transportation use prior to the
effective date of this specification may be utilized until replaced.
* A maximum 50-gram (0.1 lb.) readability is permitted to calibrate the unit weight measure
(Illinois Modified AASHTO T 121) and the air meter measuring bowl (Illinois Modified AASHTO
T 152). However, if the capacity of the unit weight measure and the air meter measuring bowl
is less than 0.009 cubic meter (0.3 cu.ft.), a 20-gram (0.05 lb.) or smaller readability is
preferable for calibration.
1
* The weighing equipment may be a balance or scale, and it does not have to be electronic.
***The weighing of cylinder strength specimens prior to compressive strength testing is optional.
2
Sufficient capacity.
A 20-gram (0.05 lb.) or smaller readability shall be required for unit weight measures which
have a capacity less than 0.009 cubic meter (0.3 cu.ft.). A 50-gram (0.1 lb.) or smaller
readability shall be required for unit weight measures which have a capacity greater than or
equal to 0.009 cubic meter (0.3 cu.ft.).
AASHTO
444 North Capitol Street, N. W.
Suite 249
Washington, D.C. 20001
(202) 624-5800
www.transportation.org
AASHTO
Section Illinois Modification
2.1 Revise as follows:
AASHTO T 23 (Illinois Modified)
AASHTO R 39 (Illinois Modified)
AASHTO R 18 test method, Establishing and Implementing a Quality Management System for
Construction Materials Testing Laboratories, cannot be reproduced in this manual due to
copyright. AASHTO standards may be requested from the address below:
AASHTO
444 North Capitol Street, N. W.
Suite 249
Washington, D.C. 20001
(202) 624-5800
www.transportation.org
This stand-alone document explains the statistical analysis and procedure used to determine
the pay factor for a hot-mix asphalt (HMA) mixture on Pay for Performance (PFP) project. HMA
materials specified to be sampled and tested for percent within limits payment adjustment
(voids, VMA, and in-place density) and dust/AC adjustments will be evaluated for acceptance in
accordance with this document.
Pay parameters evaluated using percent within (PWL) limits will be analyzed collectively and
statistically by the Quality Level Analysis method using the procedures listed to determine the
total estimated percent of the lot that is within specification limits. Quality Level Analysis is a
statistical procedure for estimating the percent compliance to a specification and is affected by
shifts in the arithmetic mean and the sample standard deviation. Two measures of quality are
required to establish the contract unit price adjustment. The first measure is the Acceptable
Quality Level (AQL) which is the PWL at which the lot will receive 100 percent pay. The second
measure of quality is the Rejectable Quality Level (RQL) at which the Department has
determined the material may not perform as desired and may be rejected.
The pay factor on full-depth projects shall be determined by weighting each mixture equally.
Material placed at the same gyrations values but with and without polymer will be evaluated as
two separate mixtures. For example: one surface mix and one binder mix will be weighted
50/50 regardless of tonnage. Additionally, one surface mix, one polymer binder mix and one
non-polymer mix will be evaluated as three equally (1/3) weighted mixtures even if the polymer
binder is the only difference between binder lifts.
Pay adjustments for Dust/AC ratio will be applied using the Dust/AC Pay Adjustment Table
found in the Hot Mix Asphalt Pay for Performance Using Percent within Limits special provision.
Note: Table 1: Pay Attributes and Price Adjustment Factors contain the UL, LL, and pay factor f
weights.
Items 1 through 8 of the following procedure will be repeated for each lot of the various pay
factor parameters.
x=
x
n
Where:
= summation of
x = individual test value
n = total number of test values
n . ( x)
2 2
s=
( x)
n( n 1)
Where:
(x 2
) = summation of the squares of individual test values
(5) Determine PU (percent within the upper specification limit which corresponds to a given
QU) from Table 2. (Note: Round up to nearest QU in table 2.)
(6) Determine PL (percent within the lower specification limit which corresponds to a give
QL) from Table 2. (Note: Round up to nearest QL in table 2.)
(7) Determine the Quality Level or PWL (the total percent within specification limits).
(8) To determine the pay factor for each individual parameter lot:
(9) Once the project is complete determine the Total Pay Factor (TPF) for each parameter
by using a weighted lot average by tons (mix) or distance (density) of all lots for a given
parameter.
Where:
W1,W2 = weighted percentage of material evaluated
PF = Pay factor for the various lots
TPF = Total pay factor for the given parameter
(10) Determine the Composite Pay Factor (CPF) for each mixture. The CPF shall be rounded
to 3 decimal places.
[ (
CPF = f VMA (TPFVMA ) + f voids (TPFvoids ) + f density TPFdensity )] / 100
Substituting from Table 1:
[ (
CPF = 0.3(TPFVMA ) + 0.3(TPFvoids ) + 0.4 TPFdensity )] / 100
Where:
fVMA, fvoids, and fdensity = Price Adjustment Factor listed in Table 1
TPFVMA, TPFvoids, and TPFdensity = Total Pay Factor for the designated measured
attribute from (9)
Determine the Pay factor for the given lot of a N90 HMA surface being placed at 1.5 inches thick
as an overlay. The project consists of 10,000 tons over 17 miles.
Note that mix sample and density lots are independent of each other.
In this example the mix sample lot represents 10,000 tons while the density lot represents 6
miles (N= 30). The project would have two additional density lots following the same
calculations as the first lot. All three lots are combined as per item (9).
Density: Each density test interval represents 0.2 mile thus N= 30 in which 5 cores are taken
per mile would represent 6 miles of paving.
Density
Lot Test
# Interval Density
1 91.5
2 93.0
3 92.9
4 93.5
5 93.0
1 6 94.0
7 92.8
8 93.5
9 91.0
30 92.7
Average: 92.79
Standard Deviation: 0.910
Voids:
QU =
(4.0 + 1.35) 4.16 = 1.44
0.825
PU = 94
PL = 98
PWL = 92
PF = 53 + 0.5 (92)
PF = 99.0
PFVoids = 99.0
VMA:
QU =
(14.5 + 3.0) 14.42 = 6.18
0.498
PU = 100
PL = 90
PWL = 90
PF = 53 + 0.5 (90)
PF = 98
PFVMA = 98.0
Density:
97.0 92.79
QU = = 4.63
0.910
92.79 91.5
QL = = 1.42
0.910
PU = 100
PL = 93
PWL = 93
PF = 53 + 0.5 (93)
PF = 99.5
PFDensity = 99.5
Determine the total pay factors for each parameter. In this example 10,000 tons of mix
represents the entire project so only one lot exists for VMA and voids. If more mix lots occurred
on a project they would be combined just like density as shown.
TPFDensity= (31680/88000)(99.5)+(31680/88000)(101.4)+(24640/88000)(97.3)
TPFDensity= 99.6
Combine the three Total Pay Factors to determine the Composite Pay Factor for the mix.
CPF = 0.989
Given that the mixture bid price per ton = $65.00 and 10,000 tons were placed.
Determine the difference between the adjusted pay and the plan unit pay.
If the difference is a positive value this will be the incentive paid. If the difference is a
negative value this will be the disincentive paid. In this case a $7,150 disincentive would
be paid as per policy memorandum 9-4.
Given a full-depth project with two mixtures whose combined pay factors were determined to be
101.5% and 99.2%. The full-depth pay factor shall be calculated as follows:
Given that the bid price per square yard = $25.00 and 1400 yd2 were placed.
Given a full-depth project with three mixtures whose pay factors were determined to be 98.9%,
101.5% and 99.2%. The full depth pay factor shall be calculated as follows:
Given that the bid price per square yard = $25.00 and 1400 yd2 were placed.
Note: For negative values of QU or QL, PU or PL is equal to 100 minus the table PU or PL. If the value of QU or QL does
not correspond exactly to a figure in the table, use the next higher value.
Samples shall be obtained at the frequency specified in the Hot Mix Asphalt Pay for
Performance Using Percent within Limits special provision.
A. The random plant samples shall be taken at the randomly selected tonnage within a sublot.
The random tonnage will be determined by the Engineer using the Random Numbers
table as specified herein or an approved software program. The tonnage shall be
calculated according to the following:
1. Unless otherwise known, determine the random locations for a tonnage in excess of
five percent over plan quantity by multiplying the plan quantity tonnage by 1.05 to
determine an over-projected final quantity. If the over-projected final quantity is not
achieved, disregard the additional random values.
2. Determine the maximum number of sublots needed for the given mixture by dividing
the over-projected tonnage calculated above by the sublot size in tons (metric tons).
This will determine the maximum number of sublots for the given mixture.
4. The individual sublot random tonnages shall then be converted to the cumulative
random tonnages. This is accomplished by using the following equation for each
sublot.
CT = [(ST ) * (n 1)] + RT
n n
B. If the paving is completed for a particular mixture before the specified sampling tonnage for
the last sublot is achieved, the partial sublot shall be omitted.
C. Plant truck samples shall be taken of the mixture for testing. Two sampling platforms (one
on each side of the truck) shall be provided for sampling of the mix. In order to obtain a
representative sample of the entire truck, an equal amount of material shall be taken from
each quarter point around the circumference of each pile in the truck to obtain a composite
sample weighing approximately 200lbs. (95 kg). All truck samples shall be obtained by
using a "D"-handled, square-ended shovel with built-up sides and back (1 to 1-1/2 in. [25 to
38 mm]). The sample shall be taken out of the truck containing the random tonnage as
determined by the Engineer following the procedure described herein. The sample
tonnage will be disclosed no more than 30 minutes prior to sampling. Sampling shall be
performed by the Contractor under the supervision of the Engineer.
D. The truck sample shall be divided into three approximately equal size (split) samples by the
use of an approved mechanical sample splitter. The Engineer will witness all splitting. Two
split samples for Department testing shall be placed in Department-approved sample
containers provided by the Contractor and identified as per the Engineer's direction. The
Engineer will gain immediate possession of both Department split samples. The Contractor
may store, discard, or test the remaining split as described in Section 1030 of the Standard
Specifications. However, the Contractor must test and provide the sample results in order
to initiate the dispute resolution process as described in the Hot Mix Asphalt Pay for
Performance Special Provision.
Example:
Given: - Plan quantity = 10,000 tons for a given mixture. - Sublot = 1000 tons
(725 metric tons).
2. Determine the maximum number of sublots needed for the project based on the over-
projected tonnage.
3. Obtain random numbers from the table and apply a different random number to each
sublot.
The following contains a completed table for the eleven plant random samples:
RANDOM NUMBERS
0.576 0.730 0.430 0.754 0.271 0.870 0.732 0.721 0.998 0.239
0.892 0.948 0.858 0.025 0.935 0.114 0.153 0.508 0.749 0.291
0.669 0.726 0.501 0.402 0.231 0.505 0.009 0.420 0.517 0.858
0.609 0.482 0.809 0.140 0.396 0.025 0.937 0.301 0.253 0.761
0.971 0.824 0.902 0.470 0.997 0.392 0.892 0.957 0.040 0.463
0.053 0.899 0.554 0.627 0.427 0.760 0.470 0.040 0.904 0.993
0.810 0.159 0.225 0.163 0.549 0.405 0.285 0.542 0.231 0.919
0.081 0.277 0.035 0.039 0.860 0.507 0.081 0.538 0.986 0.501
0.982 0.468 0.334 0.921 0.690 0.806 0.879 0.414 0.106 0.031
0.095 0.801 0.576 0.417 0.251 0.884 0.522 0.235 0.389 0.222
0.509 0.025 0.794 0.850 0.917 0.887 0.751 0.608 0.698 0.683
0.371 0.059 0.164 0.838 0.289 0.169 0.569 0.977 0.796 0.996
0.165 0.996 0.356 0.375 0.654 0.979 0.815 0.592 0.348 0.743
0.477 0.535 0.137 0.155 0.767 0.187 0.579 0.787 0.358 0.595
0.788 0.101 0.434 0.638 0.021 0.894 0.324 0.871 0.698 0.539
0.566 0.815 0.622 0.548 0.947 0.169 0.817 0.472 0.864 0.466
0.901 0.342 0.873 0.964 0.942 0.985 0.123 0.086 0.335 0.212
0.470 0.682 0.412 0.064 0.150 0.962 0.925 0.355 0.909 0.019
0.068 0.242 0.777 0.356 0.195 0.313 0.396 0.460 0.740 0.247
0.874 0.420 0.127 0.284 0.448 0.215 0.833 0.652 0.701 0.326
0.897 0.877 0.209 0.862 0.428 0.117 0.100 0.259 0.425 0.284
0.876 0.969 0.109 0.843 0.759 0.239 0.890 0.317 0.428 0.802
0.190 0.696 0.757 0.283 0.777 0.491 0.523 0.665 0.919 0.146
0.341 0.688 0.587 0.908 0.865 0.333 0.928 0.404 0.892 0.696
0.846 0.355 0.831 0.281 0.945 0.364 0.673 0.305 0.195 0.887
0.882 0.227 0.552 0.077 0.454 0.731 0.716 0.265 0.058 0.075
0.464 0.658 0.629 0.269 0.069 0.998 0.917 0.217 0.220 0.659
0.123 0.791 0.503 0.447 0.659 0.463 0.994 0.307 0.631 0.422
0.116 0.120 0.721 0.137 0.263 0.176 0.798 0.879 0.432 0.391
0.836 0.206 0.914 0.574 0.870 0.390 0.104 0.755 0.082 0.939
0.636 0.195 0.614 0.486 0.629 0.663 0.619 0.007 0.296 0.456
0.630 0.673 0.665 0.666 0.399 0.592 0.441 0.649 0.270 0.612
0.804 0.112 0.331 0.606 0.551 0.928 0.830 0.841 0.702 0.183
0.360 0.193 0.181 0.399 0.564 0.772 0.890 0.062 0.919 0.875
0.183 0.651 0.157 0.150 0.800 0.875 0.205 0.446 0.648 0.685
Note: Always select a new set of numbers in a systematic manner, either horizontally or
vertically. Once used, the set should be crossed out.
Density tests using cores shall be obtained at the frequency specified in the Hot Mix Asphalt
Quality Control for Performance (QCP) and Pay for Performance (PFP) Using Percent within
Limits special provisions. The random test locations shall be determined as follows:
A) The random core locations shall be taken at the randomly selected test location within each
density testing interval. The random test location will be determined by the Engineer using
the Random Numbers table as specified herein or an approved software program. This
may be performed each day or predetermined for the project. Regardless of when the
values are determined, the values are to be considered confidential and are not to be
disclosed to anyone outside of the Department. Disclosing the information prior to finish
rolling would be in direct violation of federal regulations.
Each core location shall be randomly located both longitudinally and transversely within
each density testing interval. Each core location within the density testing interval shall be
determined with two random numbers. The first random number is used to determine the
longitudinal distance to the nearest 1 ft into the density testing interval. The second random
number is used to determine the transverse offset to the nearest 0.1 ft from the left edge of
the paving lane.
To determine the longitudinal location of a core, multiply the length of the prescribed density
interval by the random number selected from the Random Number table. Determine the
random transverse offset as follows:
1. PFP. The effective lane width of the pavement shall be used in calculating the
transverse offset. The effective lane width is determined by subtracting 1.0 ft for
each unconfined edge from the entire paved lane width (i.e. If a 12.0 ft wide paved
lane has two unconfined edges, the effective lane width would be 10.0 ft.)
Determine the transverse offset by multiplying the effective width by the random
number selected from the Random Number table.
The transverse offset is measured from the left physical edge of the paved lane to
locate the core on the pavement. If the left edge was unconfined, it will be omitted
by adding 1.0 ft to the calculated transverse offset measurement.
Random locations that fall within 4.0 inches of a confined edge shall be moved to 4.0
inches off the edge. Areas outside the mainline pavement that are paved
concurrently with the mainline pavement (i.e. three-ft wide left shoulders, driveways,
etc.) are not considered part of the paved mainline mat. See PFP example
calculation herein.
The core density location for the outer 1.0 ft of an unconfined edge will be randomly
selected within each 0.5 mile section for each unconfined edge. Longitudinal joint
testing shall be located at a distance equal to the lift thickness or a minimum of 4.0
in. (100 mm), from each pavement edge. (i.e. for a 5 in. (125 mm) lift the near edge
of the core barrel shall be within 5.0 in. (125 mm) from the edge of pavement.)
2. QCP. The entire width of the pavement shall be used in calculating the transverse
offset. No offset movement is to be used for random locations that lie within 1.0 ft
from an unconfined edge. Cores taken within 1.0 ft from an unconfined edge will
have 2.0% density added for pay adjustment calculation purposes. Random
locations that fall within 4.0 in. of an edge shall be moved to 4.0 in. off the edge. See
QCP example calculation herein.
B) This process shall be repeated for all density intervals on a given project.
C) Example Calculations.
PFP Example.
This PFP example illustrates the determination of the core locations within the first mile of a
lot.
Given 1.5 in. thickness would require a density testing interval of 0.2 miles. The pavement
consists of a 13.0 ft-wide mat with the left edge confined and the right edge unconfined.
The random numbers for the longitudinal direction are 0.917, 0.289, 0.654, 0.347, and
0.777. The random numbers for the transverse direction are 0.890, 0.317, 0.428, 0.998,
and 0.003.
The individual density test interval distances can be converted to the cumulative random
distance using the following equation:
CDn = [ D (n 1)] + Rn
Where:
The longitudinal core locations are determined by multiplying the longitudinal random
numbers by 1056 ft (0.2 mile). The transverse core locations are determined by multiplying
the transverse random number by the effective width of the paved mat.
Determine the effective lane width by subtracting 1.0 ft, for each unconfined edge, from the
entire paved lane width. In this case only the right edge is unconfined, so subtract 1.0 ft
from the entire paved lane width of 13.0 ft.
The random location for the first mile measured from the beginning of the lot and the left
(confined) edge of the paved mat are as follows:
Core
Longitudinal Location Cumulative Distance Transverse Location
#
1 1056 x 0.917 = 968 ft 1056 x (1-1) + 968 = 968 ft 12.0 x 0.890 = 10.7 ft
2 1056 x 0.289 = 305 ft 1056 x (2-1) + 305 = 1361 ft 12.0 x 0.317 = 3.8 ft
3 1056 x 0.654 = 691 ft 1056 x (3-1) + 691 = 2803 ft 12.0 x 0.428 = 5.1 ft
4 1056 x 0.347 = 366 ft 1056 x (4-1) + 366 = 3534 ft 12.0 x 0.998 = 11.7 ft
5 1056 x 0.777 = 821 ft 1056 x (5-1) + 821 = 5045 ft 12.0 x 0.003 = 0.0 ft = 0.3 ft1/
1/ The 0.0 ft for Core #5 was moved in to 0.3 ft due to the 4 in. minimum from the edge
requirement.
QCP Example.
This QCP example illustrates the determination of the core locations within the first mile of a
project.
Given 1.5 thickness would require a density testing interval of 0.2 miles. The pavement
consists of a 13.0 ft-wide mat with the left edge confined and the right edge unconfined.
The random numbers for the longitudinal direction are 0.904, 0.231, 0.517, 0.253, and
0.040. The random numbers for the transverse direction are 0.007, 0.059, 0.996, 0.515,
and 0.101.
The individual density test interval distances can be converted to the cumulative random
distance using the following equation:
CDn = [ D (n 1)] + Rn
Where:
The longitudinal core locations are determined by multiplying the longitudinal random
numbers by 1056 ft (0.2 mile). The transverse core locations are determined by multiplying
the transverse random number by the width of the paved lane (13.0 ft).
The random location for the first mile measured from the beginning of the lot and the left
(confined) edge of the paved mat are as follows:
Core
Longitudinal Location Cumulative Distance Transverse Location
#
1 1056 x 0.904 = 955 ft 1056 x (1-1) + 955 = 955 ft 13.0 x 0.007 = 0.1 ft = 0.3 ft1/
2 1056 x 0.231 = 244 ft 1056 x (2-1) + 244 = 1300 ft 13.0 x 0.059 = 0.8 ft
3 1056 x 0.517 = 546 ft 1056 x (3-1) + 546 = 2658 ft 13.0 x 0.996 = 13.0 ft = 12.7 ft2/
4 1056 x 0.253 = 267 ft 1056 x (4-1) + 267 = 3435 ft 13.0 x 0.515 = 6.7 ft
5 1056 x 0.040 = 42 ft 1056 x (5-1) + 42 = 4266 ft 13.0 x 0.101 = 1.3 ft
1/ The 0.1 ft offset for Core #1 was moved in to 0.3 ft due to the 4 in. minimum from the
edge requirement.
2/ The 13.0 ft offset for Core #3 was move in to 12.7 ft due the 4 in. minimum from the edge
requirement. Since this core is within 1 ft from an unconfined edge 2% will be added to
the measured core density.
RANDOM NUMBERS
0.576 0.730 0.430 0.754 0.271 0.870 0.732 0.721 0.998 0.239
0.892 0.948 0.858 0.025 0.935 0.114 0.153 0.508 0.749 0.291
0.669 0.726 0.501 0.402 0.231 0.505 0.009 0.420 0.517 0.858
0.609 0.482 0.809 0.140 0.396 0.025 0.937 0.301 0.253 0.761
0.971 0.824 0.902 0.470 0.997 0.392 0.892 0.957 0.040 0.463
0.053 0.899 0.554 0.627 0.427 0.760 0.470 0.040 0.904 0.993
0.810 0.159 0.225 0.163 0.549 0.405 0.285 0.542 0.231 0.919
0.081 0.277 0.035 0.039 0.860 0.507 0.081 0.538 0.986 0.501
0.982 0.468 0.334 0.921 0.690 0.806 0.879 0.414 0.106 0.031
0.095 0.801 0.576 0.417 0.251 0.884 0.522 0.235 0.389 0.222
0.509 0.025 0.794 0.850 0.917 0.887 0.751 0.608 0.698 0.683
0.371 0.059 0.164 0.838 0.289 0.169 0.569 0.977 0.796 0.996
0.165 0.996 0.356 0.375 0.654 0.979 0.815 0.592 0.348 0.743
0.477 0.535 0.137 0.155 0.767 0.187 0.579 0.787 0.358 0.595
0.788 0.101 0.434 0.638 0.021 0.894 0.324 0.871 0.698 0.539
0.566 0.815 0.622 0.548 0.947 0.169 0.817 0.472 0.864 0.466
0.901 0.342 0.873 0.964 0.942 0.985 0.123 0.086 0.335 0.212
0.470 0.682 0.412 0.064 0.150 0.962 0.925 0.355 0.909 0.019
0.068 0.242 0.777 0.356 0.195 0.313 0.396 0.460 0.740 0.247
0.874 0.420 0.127 0.284 0.448 0.215 0.833 0.652 0.701 0.326
0.897 0.877 0.209 0.862 0.428 0.117 0.100 0.259 0.425 0.284
0.876 0.969 0.109 0.843 0.759 0.239 0.890 0.317 0.428 0.802
0.190 0.696 0.757 0.283 0.777 0.491 0.523 0.665 0.919 0.146
0.341 0.688 0.587 0.908 0.865 0.333 0.928 0.404 0.892 0.696
0.846 0.355 0.831 0.281 0.945 0.364 0.673 0.305 0.195 0.887
0.882 0.227 0.552 0.077 0.454 0.731 0.716 0.265 0.058 0.075
0.464 0.658 0.629 0.269 0.069 0.998 0.917 0.217 0.220 0.659
0.123 0.791 0.503 0.447 0.659 0.463 0.994 0.307 0.631 0.422
0.116 0.120 0.721 0.137 0.263 0.176 0.798 0.879 0.432 0.391
0.836 0.206 0.914 0.574 0.870 0.390 0.104 0.755 0.082 0.939
0.636 0.195 0.614 0.486 0.629 0.663 0.619 0.007 0.296 0.456
0.630 0.673 0.665 0.666 0.399 0.592 0.441 0.649 0.270 0.612
0.804 0.112 0.331 0.606 0.551 0.928 0.830 0.841 0.702 0.183
0.360 0.193 0.181 0.399 0.564 0.772 0.890 0.062 0.919 0.875
0.183 0.651 0.157 0.150 0.800 0.875 0.205 0.446 0.648 0.685
Note: Always select a new set of numbers in a systematic manner, either horizontally or
vertically. Once used, the set should be crossed out.
Hot-mix asphalt (HMA) samples shall be obtained at the frequency specified in the Hot Mix
Asphalt Quality Control for Performance (QCP) and Pay for Performance (PFP) Using Percent
within Limits special provisions.
The random jobsite mixture samples shall be taken at the randomly selected test location within
a sublot. The random test location will be determined by the Engineer using the Random
Numbers table as specified herein or an approved software program. This may be performed
each day or predetermined for the project as per the Engineer. Regardless of when the values
are determined, the values are to be considered confidential and are not to be disclosed to
anyone outside of the Department. Disclosing the information would violate the intent of this
procedure and federal regulations.
The sample location shall be determined by calculating the longitudinal distance the truck would
travel to produce the random sample tonnage. The starting station for the longitudinal distance
measurement is the location of the paver where the truck begins to unload the mixture into the
paver or Material Transfer Device (MTD). Computations are made to the nearest foot (see
examples in appendix herein).
If the paving is completed for a mixture before the specified sampling test location for the last
mixture sublot is completed, a test will not be taken and the tonnage will be added to the current
lot.
The Contractor may select either sampling behind the paver or sampling from the MTD
discharge chute. The Contractor shall provide the necessary equipment and HMA Level I
personnel to obtain the required samples, for whatever method is chosen, as specified herein.
This method covers the procedures for sampling HMA paving mixtures at the point of
delivery immediately behind the paver and before initial compaction. This method is
intended to provide a single composite sample that is representative of the mixture as
produced (i.e. excludes paver effects).
1. Equipment
b) Sample Containers (4 each). Metal sample buckets with a minimum capacity of 3.5
gallons (13 liters).
1) Sampling Plates (4 each). The sampling plates shall be rectangular and have a
minimum size of 14 x 28 inches (360 x 720 mm). Plates shall have a hole
approximately 0.25 inches (6 mm) in diameter drilled through each of the four
corners.
2) Lifting Handles and Wire Lead. A 24 inch (600 mm) length of wire shall be
attached to the two holes on one side of the plate to serve as lifting handle. An
additional wire lead shall be attached to one of the lifting handles for locating the
buried plate in the pavement. This wire shall extend to the edge of the
pavement.
3) Hammer and masonry nails for securing plates and wire lead.
2. Shovel Sample Sampling Procedure (Without Plates). This method shall be used when
sampling over smooth HMA and concrete surfaces.
a) The sampling shovel shall be used at each of the four offsets illustrated in Figure 2.
to dig directly downward into pavement until it comes into contact with the previous
pavement surface. When in contact, the shovel shall be pushed forward until it is
full. The shovel shall be lifted up slowly and carefully place the mix into the sample
container in order to prevent any loss of HMA.
January 1, 2015 Manual of Test Procedures for Materials E26
Appendix E4
Illinois Department of Transportation
3. Shovel/Plate Sampling Procedure (With Plates). This method shall be used when
sampling HMA directly over aggregate base, stabilized subbase, rubblized concrete, or a
milled surface. This method may not be appropriate for 3/4 in. level binder over a milled
surface. In the case of IL-4.75 mm or IL-9.5 FG mixtures, if approved by the Engineer,
these mixtures may be shovel sampled from the auger area at the designated random
location. Intentions of sampling IL-4.75 mm or IL-9.5 FG mixtures in this manner shall
be listed in the approved QC Plan.
a) Each plate with the wire lead attached to handle shall be placed at four locations
according for Figure 2. at the designated location ahead of the paver. If conditions
on the project require restricting movement of the plate, a nail shall be driven through
one of the holes in the plate and into the pavement.
b) The wire lead shall be extended beyond the edge of the pavement. Trucks, pavers,
and/or materials transfer devices will be allowed to cross over the pate and/or wire
lead.
c) After the HMA is placed, the wire lead shall be used to locate the plate. Once
located, the wire handles shall be lifted out of the pavement. This will locate the four
corners of the plate.
d) Once the plate edges are defined, the shovel shall be used to dig downward through
the thickness of the pavement until it is in contact with the plate. The shovel shall be
pushed forward until it is full. The shovel shall be lifted up slowly and carefully place
the mix into the sample container in order to prevent any loss of HMA.
Paving Width
Direction of Paving
10 feet
4. Composite/Lab Sample.
a) HMA samples shall be taken, blended and split, using an IDOT approved HMA
splitter, onsite by the Contractor and witnessed by the Engineer. The sample shall
be taken immediately behind the paver and before initial roller compaction. One
composite sample consists of four increments collected within 10 feet longitudinally
and diagonally across the width of the paving operation (Fig. 2). The four increments
shall be blended according to HMA Level I procedures to provide a single composite
sample.
b) Composite Sample.
1) PFP. If the contractor elects to have the option to dispute test results by the
Engineer, a composite sample size shall be a minimum of 200 lbs. (90 kg),
allowing 50 lbs (23 kg) for District testing, 50 lbs. (23 kg) for Contractor testing,
50 lbs (23 kg) for dispute resolution testing, and 50 lbs. (23 kg backup for
Department testing).
2) QCP. A composite sample size shall be a minimum of 100 lbs. (45 kg), allowing
50 lbs. (23 kg) for District testing, and 50 lbs. (23 kg) for Contractor testing.
c) Lab Sample.
1) PFP. The minimum lab sample size of 50 lbs. (23 kg) shall be obtained by
splitting the composite samples into four equal lab samples using an IDOT
approved HMA splitter. The Engineer will secure three Department lab samples
for the Contractor to transport to the District Materials Laboratory.
2) QCP. The minimum lab sample size of 50 lbs. (23 kg) shall be obtained by
splitting the composite samples into two equal lab samples using an IDOT
approved HMA splitter. The Engineer will secure the Department lab sample for
the Contractor to transport to the District Materials Laboratory.
a) HMA from the paver auger system shall be used to fill the voids left in the pavement
from sampling. To reduce segregation and low density in the finished mat, buckets
shall be used to fill the voids left by the samples.
1) HMA from the augers system shall be placed in clean metal buckets just prior to
sampling the pavement.
2) The metal buckets shall be filled with approximately 25% more HMA than will be
removed from the void.
c) The HMA shall be slightly leveled to provide a gradual hump over the filled void to
allow compression of the mix by the roller.
d) Unacceptable site repair shall be removed and replaced at the Contractors expense.
B. MTD Sampling.
This method covers the procedures for sampling HMA paving mixtures at the point of
delivery from a material transfer device (MTD).
1. Equipment.
a) MTD Sampling Device. A portable device mounted either in the bed of a pickup
truck or on a trailer. The device shall be equipped with a funnel large enough to
capture the full stream of HMA from the MTD discharge chute without spillage and
shall be capable of capturing a minimum composite HMA sample of 200 lbs (90 kg).
See appendix for illustrations of various MTD sampling device configurations.
The Engineer will identify the truck containing the sample tonnage immediately prior to
sampling. Immediately after the truck containing the random HMA tonnage has finished
unloading, the MTD shall pull forward away from the paver far enough to allow the
sampling device to be positioned under the MTD discharge chute. The sampling device
shall be positioned as level as possible in a safe location readily accessible by the MTD.
The MTD shall discharge without spillage a minimum of 200 lbs. (90 kg) of HMA for PFP
or 100 lbs. (45 kg) for QCP into the funnel of the sampling device.
3. Composite/Lab Sample.
a) Composite Sample. HMA from all four sample containers of the sampling device
shall be blended into one composite sample and split to lab sample size by the
Contractor onsite using an IDOT approved HMA splitter. The blending and splitting
shall be according to HMA Level I procedures and will be witnessed by the Engineer.
1) PFP. If the contractor elects to have the option to dispute test results by the
Engineer, a composite sample size shall be a minimum of 200 lbs. (90 kg),
allowing 50 lbs (23 kg) for District testing, 50 lbs. (23 kg) for Contractor testing,
50 lbs (23 kg) for dispute resolution testing, and 50 lbs. (23 kg backup for
Department testing).
2) QCP. A composite sample size shall be a minimum of 100 lbs. (45 kg), allowing
50 lbs. (23 kg) for District testing, and 50 lbs. (23 kg) for Contractor testing.
b) Lab Sample.
1) PFP. The minimum lab sample size of 50 lbs. (23 kg) shall be obtained
by splitting the composite samples into four equal lab samples using an
IDOT approved HMA splitter. The Engineer will secure three Department
lab samples for the Contractor to transport to the District Materials
Laboratory.
2) QCP. The minimum lab sample size of 50 lbs. (23 kg) shall be obtained
by splitting the composite samples into two equal lab samples using an
IDOT approved HMA splitter. The Engineer will secure the Department
lab sample for the Contractor to transport to the District Materials
Laboratory.
C. Documentation After the sample has been obtained, the following information shall be
written on each sample bag or box with a felt tip marker.
Contract #: _______________
Lot #:__________ Sublot #:__________
Date: ___________ Time: ___________
Mix Type (binder, surface): _________
Mix Design #: _____________________
Sampled By: ______________________
D. Sample Security Each sample bag will be secured by the Engineer using a locking ID tag.
Sample boxes will be sealed/taped using a security ID label.
E. Sample Transportation The Contractor shall deliver the secured sample to the district
laboratory, during regular working hours, for testing within two days of sampling.
F. Examples:
1. Behind Paver Sampling. Determination of random sample location for behind paver
sampling.
This example illustrates the determination of the random behind the paver test location
within a sublot:
Given a surface mix with a design Gmb of 2.400 is being placed 12 feet wide and 1.5
inches thick. The Engineer has elected to determine all the undisclosed random
January 1, 2015 Manual of Test Procedures for Materials E30
Appendix E4
Illinois Department of Transportation
tonnages prior to production. The plan quantity on the project was 10,000 tons and
enough random values were determined to allow for a 5% overrun assuring enough
random tonnages were generated. Ignore any random tonnages beyond what was
placed on the project.
The truck containing the mix representing the 167 tons shall be the first sublot tested.
The truck in question contains 160 to 172 cumulative tonnage to be placed on the
project. Determine the random location by dividing the value of the selected truck
tonnage to determine the random distance value to 3 decimal places.
167 160 = 7 (where the random ton falls within the truck)
Determine the distance using 58.3% of the distance the truck will pave using the
following formula:
384.6 Tons RD
Longitudinal Distance =
Gmb width thickness
Where:
Longitudinal Distance = Random distance from starting station (ft)
Tons = total tons within the sample truck
RD = random distance value as calculated above
Gmb = design Gmb for the mix being placed
Width = width of mat being paved (ft)
Thickness = thickness of mat being paved (in)
384.6 12 .583
Longitudinal Distance =
2.400 12 1.5
Measure the calculated longitudinal distance from the starting station where the truck
began to unload. Determine and document the random sample station and obtain the
random mix sample as outlined herein.
0.576 0.730 0.430 0.754 0.271 0.870 0.732 0.721 0.998 0.239
0.892 0.948 0.858 0.025 0.935 0.114 0.153 0.508 0.749 0.291
0.669 0.726 0.501 0.402 0.231 0.505 0.009 0.420 0.517 0.858
0.609 0.482 0.809 0.140 0.396 0.025 0.937 0.301 0.253 0.761
0.971 0.824 0.902 0.470 0.997 0.392 0.892 0.957 0.040 0.463
0.053 0.899 0.554 0.627 0.427 0.760 0.470 0.040 0.904 0.993
0.810 0.159 0.225 0.163 0.549 0.405 0.285 0.542 0.231 0.919
0.081 0.277 0.035 0.039 0.860 0.507 0.081 0.538 0.986 0.501
0.982 0.468 0.334 0.921 0.690 0.806 0.879 0.414 0.106 0.031
0.095 0.801 0.576 0.417 0.251 0.884 0.522 0.235 0.389 0.222
0.509 0.025 0.794 0.850 0.917 0.887 0.751 0.608 0.698 0.683
0.371 0.059 0.164 0.838 0.289 0.169 0.569 0.977 0.796 0.996
0.165 0.996 0.356 0.375 0.654 0.979 0.815 0.592 0.348 0.743
0.477 0.535 0.137 0.155 0.767 0.187 0.579 0.787 0.358 0.595
0.788 0.101 0.434 0.638 0.021 0.894 0.324 0.871 0.698 0.539
0.566 0.815 0.622 0.548 0.947 0.169 0.817 0.472 0.864 0.466
0.901 0.342 0.873 0.964 0.942 0.985 0.123 0.086 0.335 0.212
0.470 0.682 0.412 0.064 0.150 0.962 0.925 0.355 0.909 0.019
0.068 0.242 0.777 0.356 0.195 0.313 0.396 0.460 0.740 0.247
0.874 0.420 0.127 0.284 0.448 0.215 0.833 0.652 0.701 0.326
0.897 0.877 0.209 0.862 0.428 0.117 0.100 0.259 0.425 0.284
0.876 0.969 0.109 0.843 0.759 0.239 0.890 0.317 0.428 0.802
0.190 0.696 0.757 0.283 0.777 0.491 0.523 0.665 0.919 0.146
0.341 0.688 0.587 0.908 0.865 0.333 0.928 0.404 0.892 0.696
0.846 0.355 0.831 0.281 0.945 0.364 0.673 0.305 0.195 0.887
0.882 0.227 0.552 0.077 0.454 0.731 0.716 0.265 0.058 0.075
0.464 0.658 0.629 0.269 0.069 0.998 0.917 0.217 0.220 0.659
0.123 0.791 0.503 0.447 0.659 0.463 0.994 0.307 0.631 0.422
0.116 0.120 0.721 0.137 0.263 0.176 0.798 0.879 0.432 0.391
0.836 0.206 0.914 0.574 0.870 0.390 0.104 0.755 0.082 0.939
0.636 0.195 0.614 0.486 0.629 0.663 0.619 0.007 0.296 0.456
0.630 0.673 0.665 0.666 0.399 0.592 0.441 0.649 0.270 0.612
0.804 0.112 0.331 0.606 0.551 0.928 0.830 0.841 0.702 0.183
0.360 0.193 0.181 0.399 0.564 0.772 0.890 0.062 0.919 0.875
0.183 0.651 0.157 0.150 0.800 0.875 0.205 0.446 0.648 0.685
Note: Always select a new set of numbers in a systematic manner, either horizontally
or vertically. Once used, the set should be crossed out.
A. Scope
The following guidelines are provided to clarify the district submittal requirements for dispute
resolution samples; and expedite the testing process for HMA mix and/or core samples.
B. Procedure
When submitting HMA mix and/or core samples include the following:
All District and Contractor split sample test results on attached PFP Dispute Resolution Form,
Submit entire dispute resolution HMA mix split sample,
Cores must be split or sawed to lift testing thickness,
QC Package template and dailies sent electronically for mix being tested.
Any sample sent to BMPR without the above listed information will not be processed until all
requested information is received.
Gmb
% Voids
Gsb
Field VMA
This document explains the procedure used to determine the pay adjustment for a hot-mix
asphalt (HMA) mixture for Quality Control for Performance (QCP) projects.
The following steps are used to determine the pay deduction for each QCP mixture:
Table 1
Pay Factor
Parameter 103% 100% 95% 90%
IL-9.5FG at < 1.25 in. 93.5% to 94.5% 91.0% to 96.5% 90.0% to 97.0% 89.0% to 98.0%
PFVoids, PFVMA, and PFDensity = Average sublot pay factors for the pay
parameters
The QCP deduction for a given mixture is calculated by multiplying the Mixture Unit Price by the
Quantity and the CPF according to Equation 2 below.
Example:
Determine the QCP pay deduction for the given N70 HMA IL-12.5 surface mixture being placed
at 1.5 inches thick as an overlay. The project consists of 6,900 tons placed over a distance of
12 lane miles.
Note that mix sample lots and density lots are independent of one another.
In this example the first mix lot represents 4,000 tons while the second lot represents 2,900
tons. There are 12 density sublots representing 12 lane miles (N=12, representing 12 miles x 5
cores/mile = 60 cores).
Mix sample: Each sublot represents 1000 tons except for lot 2, sublot 3 which represents 900
ton.
Density: Since this pavement is < 3 inches thick, cores are taken randomly every 0.2 mile
which is 5 cores per mile. Each density sublot represents 1 mile. Therefore with cores taken
every 0.2 mile, the density sublot will represent the average of 5 density cores.
12 91.5 93.5 92.7 93.8 92.1
Voids:
Since the District randomly selected and tested the split from sublot 2 in Lot 1, and the void
results were 1) within the 100% pay factor tolerance and 2) within Precision Limits of the
Contractors results, the District does not need to test the remaining sublots in Lot 1 and the
entire Lot receives a Pay Factor of 100%.
For the second Lot the District randomly selected and tested the split from sublot 1. Since the
District void results were not within the 100% pay factor tolerance, the District had to test all of
the remaining Sublot splits. (see completed table below):
Calculate the void deviation from target for each of the District sublot split results.
Lot 1:
Sublot 2: Deviation = 3.2% - 4.0% = -0.8%
Lot 2:
Sublot 1: Deviation = 2.5% - 4.0% = -1.5%
Sublot 2: Deviation = 2.2% - 4.0% = -1.8%
Sublot 3: Deviation = 3.6% - 4.0% = -0.4%
Using Table 1 and the deviation from Target, determine the corresponding Void sublot Pay
Factor for each District test result.
Lot 1:
Sublot 2: Pay Factor associated with -0.8% in Table 1 is 100%
Lot 2:
Sublot 1: Pay Factor associated with -1.5% in Table 1 is 95%
Sublot 2: Pay Factor associated with -1.8% in Table 1 is 90%
Sublot 3: Pay Factor associated with -0.4% in Table 1 is 103%
Target Voids = 4.0%
Lot Sublot Contractor District Deviation Sublot PF
1 4.1
1 2 3.9 3.2 -0.8 100.0
3 2.8
4 3.0
1 2.3 2.5 -1.5 95
2 2 2.1 2.2 -1.8 90
3 3.8 3.6 -0.4 103
Note: Bolded and italicized test results denote the sublot split that
was randomly selected by the District for testing.
Calculate the average sublot Pay Factor for Voids. (Note: The 100% in Lot 1 represents four
sublots and therefore is multiplied by four)
Ave Sublot Pay Factor (PFVoids) = ((100% X 4) + 95% + 90% + 103%) / 7 sublots = 98.3%
VMA:
Since the District randomly selected and tested the split from Sublot 2 in Lot 1, and the VMA
results were 1) within the 100% pay factor tolerance and 2) within Precision Limits of the
Contractors results, the District does not need to test the remaining sublots in Lot 1 and the
entire Lot receives a Pay Factor of 100%.
For the second Lot the District randomly selected and tested the split from Sublot 1. Since the
District results were not within the 100% pay factor tolerance for Voids, the District had to test
all of the remaining sublot splits. (see completed table below):
Calculate the VMA deviation from target for each of the District sublot split results.
Lot 1:
Sublot 2: Deviation = 13.3% - 14.0% = -0.7%
Lot 2:
Sublot 1: Deviation = 13.4% - 14.0% = -0.6%
Sublot 2: Deviation = 13.1% - 14.0% = -0.9%
Sublot 3: Deviation = 13.6% - 14.0% = -0.4%
Using Table 1 and the deviation from Target, determine the corresponding VMA sublot pay
factor for each District test result.
Lot 1:
Sublot 2: Pay Factor associated with -0.7% in Table 1 is 100%
Lot 2:
Sublot 1: Pay Factor associated with -0.6% in Table 1 is 100%
Sublot 2: Pay Factor associated with -0.9% in Table 1 is 90%
Sublot 3: Pay Factor associated with -0.4% in Table 1 is 100%
Calculate the average sublot pay factor for VMA. (Note: The 100% in Lot 1 represents four
sublots and therefore is multiplied by four)
Ave Sublot Pay Factor (PFVMA) = ((100% X 4) + 100% + 90% + 100%) / 7 sublots = 98.6%
Density:
Determine the sublot pay factor using the average sublot density and Table 1 (see completed
table below).
Determine the Density pay factor by averaging the sublot pay factors.
12 91.5 93.5 92.7 93.8 92.1 92.7 100
Average Density Sublot PF = 99.9
CPF = 99.1%
QCP Deduction:
Determine the QCP deduction pay for the given mixture using Equation 2.
QCP Deduction = (Mixture Unit Price x Mixture Quantity x CPF/100) (Mixture Unit Price x
Mixture Quantity)
QCP Deduction = ($65.00/ton x 6,900 tons x 99.1 / 100) ($65.00/ton x 6,900 tons)
= - $4,036.50
In this case a $4,036.50 disincentive would be paid as per Construction Memorandum 10-4.
Given a full-depth project with two mixtures whose combined pay factors were determined to be
100.0% and 98.2%. The full-depth pay factor shall be calculated as follows:
Given that the bid price per square yard = $25.00 and 1400 yd2 were placed.
Given a full-depth project with three mixtures whose pay factors were determined to be 98.9%,
100.0% and 99.2%. The full depth pay factor shall be calculated as follows:
Given that the bid price per square yard = $25.00 and 1400 yd2 were placed.
Best Practices
For
Pay-For-Performance (PFP) and Quality Control for Performance (QCP)
Implementation
Appendix E7
Effective Date: April 1, 2012
Purpose
This document is intended to aid district personnel in successfully preparing for and
implementing the Pay-For-Performance (PFP) and Quality Control for Performance (QCP)
specifications.
Lab
Since payment on PFP and QCP projects is based on Department test results, attention to
laboratory equipment, qualified lab personnel and laboratory efficiency becomes paramount.
Review of results from recent Annual Bituminous Uniformity Studies (aka Round Robins) and
dispute resolutions and addressing any district lab issues resulting in poor comparisons will
prove beneficial.
1) Equipment - It is imperative to inspect and calibrate all laboratory testing equipment
according to frequencies listed in Policy Memorandum 21-08.0 Minimum
Requirements For Construction Materials Testing Laboratories - Department
Operated Laboratories at a minimum. Inspection and calibration immediately prior
to PFP and QCP testing is highly recommended. Always use the same gyratory
compactor for a given PFP or QCP contract.
4) Efficiency PFP and QCP are based on Department testing which results in a higher
testing frequency for the district laboratory. An internal audit of your district
laboratory for efficiency may help identify ways to improve productivity. This activity
should be conducted by district materials staff that are not involved in day-to-day
testing, or BMPR staff if requested.
Also, it will be important to make sure Construction personnel have copies of all the
necessary supporting documents.