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    Vtotal X 10 (E/m) vs. VSTD: External Calibration Method

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    Aria Carino
    This document contains the results of an external calibration and standard addition method to determine the concentration of fluoride (F-) in an unknown sample. The external calibration generated a linear regression line with a slope of -45.4974 and intercept of 50.1267 to relate the voltage measurements to the log of the F- standard concentrations. The standard addition method involved adding increasing volumes of a F- standard to the unknown sample and generated a linear regression line with a slope of 253.95 and intercept of 5.3259 relating the total voltage measurements to the added F- concentrations. This line was used to calculate the F- concentration in the unknown sample as 0.02097 ppm.

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    Vtotal X 10 (E/m) vs. VSTD: External Calibration Method

    Uploaded by

    Aria Carino
    64 views4 pages
    This document contains the results of an external calibration and standard addition method to determine the concentration of fluoride (F-) in an unknown sample. The external calibration generated a linear regression line with a slope of -45.4974 and intercept of 50.1267 to relate the voltage measurements to the log of the F- standard concentrations. The standard addition method involved adding increasing volumes of a F- standard to the unknown sample and generated a linear regression line with a slope of 253.95 and intercept of 5.3259 relating the total voltage measurements to the added F- concentrations. This line was used to calculate the F- concentration in the unknown sample as 0.02097 ppm.

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    dfgh

    Original Title

    DATA-ISE

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    This document contains the results of an external calibration and standard addition method to determine the concentration of fluoride (F-) in an unknown sample. The external calibration generated a linear regression line with a slope of -45.4974 and intercept of 50.1267 to relate the voltage measurements to the log of the F- standard concentrations. The standard addition method involved adding increasing volumes of a F- standard to the unknown sample and generated a linear regression line with a slope of 253.95 and intercept of 5.3259 relating the total voltage measurements to the added F- concentrations. This line was used to calculate the F- concentration in the unknown sample as 0.02097 ppm.

    Copyright:

    © All Rights Reserved
    Download as XLSX, PDF, TXT or read online from Scribd
    Download as xlsx, pdf, or txt
    64 views4 pages

    Vtotal X 10 (E/m) vs. VSTD: External Calibration Method

    Uploaded by

    Aria Carino
    This document contains the results of an external calibration and standard addition method to determine the concentration of fluoride (F-) in an unknown sample. The external calibration generated a linear regression line with a slope of -45.4974 and intercept of 50.1267 to relate the voltage measurements to the log of the F- standard concentrations. The standard addition method involved adding increasing volumes of a F- standard to the unknown sample and generated a linear regression line with a slope of 253.95 and intercept of 5.3259 relating the total voltage measurements to the added F- concentrations. This line was used to calculate the F- concentration in the unknown sample as 0.02097 ppm.

    Copyright:

    © All Rights Reserved
    Download as XLSX, PDF, TXT or read online from Scribd
    Download as xlsx, pdf, or txt
    of 4

    Buffer 138 mV

    EXTERNAL CALIBRATION METHOD

    Standard (ppm) Trial 1 Trial 2 Trial 3 log[F-]


    0.5 61.3 59 56.8 -0.3010299957
    1 59.5 57.3 55.5 0
    2 39.5 38 35.9 0.3010299957
    3 25.1 24.7 23.8 0.4771212547

    Trial 1 Trial 2 Trial 3 ave. mV


    Sample -15.5 -14.7 -14.2 -14.8

    slope -45.497460409
    intercept 50.1269513492

    -45.497460409 50.1269513492
    stdev of slope 11.5124837545 3.6807681313 stdev of intercept
    0.8864822466 6.8300339648
    15.6183895532 2
    728.5879387453 93.2987279214

    STANDARD ADDITION METHOD

    Sample 0: No addition (mV) 1st: 25L (mV) 2nd: 50L (mV) 3rd: 75L (mV)
    1 10.4 -0.2 -8.1 -13.9
    2 8.5 -2.9 -10.8 -16.1
    3 5.8 -5.8 -12.9 -18.5
    average mV 8.2333333333 -2.9666666667 -10.6 -16.1666666667
    Vtotal 10 10.025 10.05 10.075
    slope -45.497460409

    y values 6.5923084357 11.649022549 17.1848639621 22.8336974875


    x values 0 0.025 0.05 0.075

    slope
    Vtotal x 10^(E/m) vs. Vstd intercept
    50
    40 V'
    Vtotal x 10^(E/m)

    f(x) = 253.9510775714x + 5.3258947752 [F-]


    30
    R = 0.9884757483
    20
    10
    0
    0 0.02 0.04 0.06 0.08 0.1 0.12 0.14
    Volume of Standard Added
    f(x) = 253.9510775714x + 5.3258947752

    Vtotal x 10^(E/
    30
    R = 0.9884757483
    20
    10
    0
    0 0.02 0.04 0.06 0.08 0.1 0.12 0.14
    Volume of Standard Added
    average mV per std
    59.0333333333
    mV vs. log[F-]
    57.4333333333 70
    37.8 60
    f(x) = - 45.497460409x + 50.1269513492
    24.5333333333 50
    R = 0.8864822466

    millivolts
    40
    30
    calculated [F-] in ppm
    20
    26.7328717289
    10
    0
    -0.4 -0.3 -0.2 -0.1 0 0.1 0.2 0.3 0.4 0.5 0.6
    Concentration of Standard F- (in log[F-])

    of intercept

    4th: 100L (mV) 5th: 125L (mV)


    -21.5 -28.9
    -20.8 -24.6
    -22.4 -26.2
    -21.5666666667 -26.5666666667
    10.1 10.125

    30.0843411778 38.8427891283
    0.1 0.125

    253.9510775714
    5.3258947752

    0.0209721291
    2.0972129066
    ]
    13492

    0.3 0.4 0.5 0.6


    in log[F-])

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