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    Experiment 3 Hydrolysis of Methyl Acetate

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    Eugene Laude Canencia
    This document summarizes an experiment to determine the specific rate constant of methyl acetate hydrolysis at different temperatures. Methyl acetate was added to an acid solution and samples were taken over time and titrated with sodium hydroxide. The volume of sodium hydroxide needed decreased over time as the methyl acetate hydrolyzed. Results from trials at 25°C and 35°C are presented, showing higher reaction rates at the higher temperature. The data collected will allow calculation of the specific rate constant at each temperature.

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    Experiment 3 Hydrolysis of Methyl Acetate

    Uploaded by

    Eugene Laude Canencia
    319 views3 pages
    This document summarizes an experiment to determine the specific rate constant of methyl acetate hydrolysis at different temperatures. Methyl acetate was added to an acid solution and samples were taken over time and titrated with sodium hydroxide. The volume of sodium hydroxide needed decreased over time as the methyl acetate hydrolyzed. Results from trials at 25°C and 35°C are presented, showing higher reaction rates at the higher temperature. The data collected will allow calculation of the specific rate constant at each temperature.

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    PhyCHem

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    This document summarizes an experiment to determine the specific rate constant of methyl acetate hydrolysis at different temperatures. Methyl acetate was added to an acid solution and samples were taken over time and titrated with sodium hydroxide. The volume of sodium hydroxide needed decreased over time as the methyl acetate hydrolyzed. Results from trials at 25°C and 35°C are presented, showing higher reaction rates at the higher temperature. The data collected will allow calculation of the specific rate constant at each temperature.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    319 views3 pages

    Experiment 3 Hydrolysis of Methyl Acetate

    Uploaded by

    Eugene Laude Canencia
    This document summarizes an experiment to determine the specific rate constant of methyl acetate hydrolysis at different temperatures. Methyl acetate was added to an acid solution and samples were taken over time and titrated with sodium hydroxide. The volume of sodium hydroxide needed decreased over time as the methyl acetate hydrolyzed. Results from trials at 25°C and 35°C are presented, showing higher reaction rates at the higher temperature. The data collected will allow calculation of the specific rate constant at each temperature.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
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    The experiment determined the specific rate constant of hydrolysis of methyl acetate at different temperatures through titration.

    The experiment determined the specific rate constant of hydrolysis of methyl acetate at 25°C and 35°C.

    Standardized sodium hydroxide and hydrochloric acid solutions, methyl acetate, thermostats, pipettes and timers were used to titrate aliquots of the reaction mixture at set time intervals.

    HYDROLYSIS OF METHYL ACETATE

    KRIZIA MAE Y. KONNO

    Department of Chemical Engineering

    College of Engineering and Architecture

    Cebu Institute of Technology -University

    N. Bacalso Ave. Cebu City, 6000 Philippines

    In this experiment, the specific rate constant at two or more different temperatures
    were determined. The concentration of methyl acetate was determined at a given time
    through titration samples with a standard sodium hydroxide solution.
    1. INTRODUCTION

    2. MATERIALS AND METHODS

    MATERIALS:

    Thermostats at 25 and 30
    Three 250 ml Erlenmeyer Flasks
    Two 125 ml Erlenmeyer Flasks
    5-ml pipette
    100-ml pipette
    Stopwatch or electric timer
    Methyl acetate
    2 liter 0.2 N sodium hydroxide solution
    500 ml 1 N hydrochloric acid
    Distilled water
    Ice

    METHODS:

    The sodium hydroxide solution was prepared by the dilution of a saturated stock
    solution to minimize the amount of carbonate present and hence seduced the fading of the
    phenolphthalein end point.

    12 ml methyl acetate was contained in a test tube, set into a thermostat at 25 C. 250
    ml of standardized 1 N hydrochloric acid in a flask. After thermal equilibrium was
    established, an aliquot of an acid was titrated with a standard sodium hydroxide solution. In
    two 250 ml flasks, clamped in a thermostat, 100 ml of the acid was added and allowed to
    come to thermal equilibrium for 5 minutes. 5 ml of methyl acetate was transferred to one of
    the flasks with a clean, dry pipette. When the pipette was half emptied, the timing watch was
    started. The reaction mixture was shaken to provide thorough mixing.

    3. RESULTS

    @ 25 C VHcl (ml) VH2O (ml) Valiq (ml) VNaOH (ml) t (min) VNaOH (ml)
    1 50 50 5 44.2 10.17 12.77
    2 50 50 5 45.35 10.33 12.77
    3 50 50 5 48.10 10.93 12.77
    @ 35 C VHcl (ml) VH2O (ml) Valiq (ml) VNaOH (ml) t (min) VNaOH (ml)
    1 50 50 5 54.68 9.58 12.77
    2 50 50 5 61.19 10.10 12.77
    3 50 50 5 65.10 10.22 12.77

    4. DISCUSSION

    5. CONCLUSSION

    6. REFERENCES

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