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Method Total Alkalinity

The document describes a method for determining total alkalinity. A 20 gram sample of FG powder is dissolved and titrated with 0.5 N HCl until a pH of 2.5 is reached. The volume of HCl consumed is used to calculate the percentage of NaOH in the sample through a provided formula, where the normality of HCl, molecular weight of NaOH, sample weight, and endpoint volume are inputs.

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0% found this document useful (0 votes)
40 views

Method Total Alkalinity

The document describes a method for determining total alkalinity. A 20 gram sample of FG powder is dissolved and titrated with 0.5 N HCl until a pH of 2.5 is reached. The volume of HCl consumed is used to calculate the percentage of NaOH in the sample through a provided formula, where the normality of HCl, molecular weight of NaOH, sample weight, and endpoint volume are inputs.

Uploaded by

fitashah2634
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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METHOD TOTAL ALKALINITY

Take 20 gram FG powder dissolve and make up in 250 ml volumetric flask ( note ph = 11.4).

Take 50 ml solution from pippete in 250 ml beaker .

Stir it and dip the electrod and titrate it against 0.5 N HCl till 2.5 PH.

Note the volume of 0.5 N HCl consumed to reached PH 2.5. ( note volume consume 59 ml )

Total alkalinity expressed as %NaOH:

% NaOH = V1 x N x 40 x100
W x 1000

5.9 = 59 X 0.5 X 40 X 100


20 X 1000
Where:
V1 =endpoint volume of titration
N =normality of hydrochloric acid titrant
40 =molecular w eight of NaOH
W =w eight of sample tested

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