MP60P70
MP60P70
MP60P70
MP 60-P-70
July 1998
Scope
This Mobil Engineering Practice (MEP) covers the general requirements for the design, fabrication,
inspection, preparation for shipment and documentation of glycol dehydration systems for sweet and
sour gas service. This Practice is applicable to counter-current contactor systems and to glycol
injection systems for both stand-alone field dehydration units and for glycol dehydration units that are
a part of a production or processing facility.
This Practice is oriented toward units requiring high reliability, low maintenance and unattended
operation.
Version 0
MP 60-P-70 Glycol Dehydration Units July 1998
Table of Contents
Scope......................................................................................................................................1
Table of Contents..................................................................................................................2
1. References......................................................................................................................5
2. General............................................................................................................................8
3. Glycol Regenerator......................................................................................................10
3.1. General................................................................................................................10
3.4. Reboiler...............................................................................................................14
3.10. Insulation.............................................................................................................19
4.1. General................................................................................................................19
5. Glycol Injection.............................................................................................................22
5.2. Strainers..............................................................................................................22
6. Instrumentation............................................................................................................22
6.1. Thermowells........................................................................................................23
6.6. Shutdown.............................................................................................................25
9. Final Documentation....................................................................................................27
10.2. Sandblasting........................................................................................................29
1. References
The following publications form a part of this Practice. Unless otherwise specified herein, use the
latest edition.
T1101C01 Fired Heaters - Design & Fabrication - Process Design - Customary Units
T1101C02 Fired Heaters - Design & Fabrication - Combustion Design Conditions -
Customary Units
T1101C03 Fired Heaters - Design & Fabrication - Air Preheater Data Sheet -
Customary Units
T1101C04 Fired Heaters - Design & Fabrication - Fan Data Sheet - Customary Units
T1101M01 Fired Heaters - Design & Fabrication - Process Design - Metric Units
T1101M02 Fired Heaters - Design & Fabrication - Combustion Design Conditions -
Metric Units
T1101M03 Fired Heaters - Design & Fabrication - Air Preheater Data Sheet - Metric
Units
T1101M04 Fired Heaters - Design & Fabrication - Fan Data Sheet - Metric Units
T1201C01 Pressure Vessels - Unfired Pressure Vessels - Customary Units
T1201M01 Pressure Vessels - Unfired Pressure Vessels - Metric Units
T1310C01 Shell and Tube Heat Exchangers - Design & Construction - Unit
Performance - Customary Units
T1310M01 Shell and Tube Heat Exchangers - Design & Construction - Unit
Performance - Metric Units
T1501C01 Centrifugal Pumps (API 610) - Customary Units
T1501M01 Centrifugal Pumps (API 610) - Metric Units
T1517C01 Reciprocating Positive Displacement Pumps - Customary Units
T1517M01 Reciprocating Positive Displacement Pumps - Metric Units
T3317C01 Electrical - LV Induction Motors - Motor Design Data - Customary Units
T3317C02 Electrical - LV Induction Motors - Vendor Supplied Data - Customary Units
T3317M01 Electrical - LV Induction Motors - Motor Design Data - Metric Units
T3317M02 Electrical - LV Induction Motors - Vendor Supplied Data - Metric Units
T6070C01 Glycol Dehydration Units - Glycol Dehydration Unit Design - Customary
Units
T6070M01 Glycol Dehydration Units - Glycol Dehydration Unit Design - Metric Units
D6070C01 Glycol Dehydration Units - Documentation Requirements Sheet
API RP 14F Recommended Practice for Design and Installation of Electrical Systems for
Offshore Production Platforms Third Edition
API RP 500 Recommended Practice for Classification of Locations for Electrical
Installations at Petroleum Facilities First Edition (Supersedes RP 500A, RP
500B, RP 500C)
API RP 500B Recommended Practice for Classification of Locations for Electrical
Installations at Drilling Rigs and Production Facilities on Land and on
Marine Fixed and Mobile Platforms (See Note 1)
API RP 520 PT I Sizing, Selection, and Installation of Pressure-Relieving Devices in
Refineries Part I - Sizing and Selection Sixth Edition; Errata - 1994
API RP 520 PT II Sizing, Selection, and Installation of Pressure-Relieving Devices in
Refineries Part II - Installation Fourth Edition
API RP 521 Guide for Pressure-Relieving and Depressuring Systems Fourth Edition
API RP 550 Manual on Installation of Refinery Instruments and Control Systems,
Various Parts (See Note 2)
API STD 526 Flanged Steel Pressure Relief Valves Fourth Edition
API STD 527 Seat Tightness of Pressure Relief Valves Third Edition (R 1996)
API STD 650 Welded Steel Tanks for Oil Storage Ninth Edition; Addendum 1 - 1994;
Addendum 2 - 1995; Addendum 3 - 1996
API STD 676 Positive Displacement Pumps - Rotary Second Edition
NOTES:
1. API RP 500B shall be replaced by API RP 500 for use on offshore installations when MMS
approves.
2. All parts of API RP 550 are out of print and no new editions are planned. However, Mobil
considers the referenced material to be valid for Mobil's purposes, except as may be noted in this
Practice. Photocopies may be obtained from:
a) Marketing Dept., API, 1220 L Street N.W., Washington, D.C. 20005
b) UMI: University Microfilms International, 300 North Zebb Road, Ann Arbor, MI 48106.
ASME SEC VIII SISI Units (Boiler and Pressure Vessel Codes)
D1
NACE MR0175 Sulfide Stress Cracking Resistant Metallic Materials for Oilfield Equipment
NFPA 70 National Electrical Code 1996 Edition Errata #1; Tentative Interim
Amendment 1996
NFPA 70E Standard for Electrical Safety Requirements for Employee Workplaces
(National Fire Codes, vol. 3)
2. General
The design, fabrication, inspection, preparation for shipment and documentation of glycol
dehydration systems for sweet and sour gas service shall be in accordance with requirements of this
MEP, unless superceded by more stringent local regulations.
1. Regenerated glycol is pumped to the top tray or above the top bed of the contactor
(absorber).
2. The glycol flows down through the contactor, countercurrent to the gas flow.
3. Water rich glycol is removed from the bottom of the contactor, passes through the
condenser coil, flashes off gas in the flash tank and then flows through the
glycol/glycol heat exchanger to the regenerator portion of the unit.
4. In the regenerator, absorbed water is removed from the glycol at atmospheric pressure
by application of heat.
5. The regenerated glycol flows through the glycol heat exchangers for cooling and is
recirculated to the contactor by the glycol pump.
3. Glycol Regenerator
3.1. General
Each glycol regenerator shall include the following:
Stripping gas can be used either with a gas sparger in the lean glycol surge tank or, more
efficiently, with a packed column located between the reboiler and the surge tank (see
Figure 2.) The Drizo process is shown in Figure 3.
3.2.1. Preheaters
The glycol shall be preheated by the still condenser. In some applications, a
glycol/glycol heat exchanger also preheats the glycol before it enters the
glycol-hydrocarbon separator. Maximum permissible preheat temperature is
55°C (131°F) for ethylene glycol, 87°C (189°F) for diethylene glycol, 118°C
(244°F) for triethylene and 149°C (300°F) for tetraethylene glycol.
Each filter housing shall have manual inlet and outlet block valves, relief
valves and bypass piping. The filter housing shall be designed as pressure vessels.
(Refer to T1201C01 of the Mobil Data Sheets.)
For glycol injection units, a charcoal filter meeting the above specifications
shall be quoted as an optional item.
3.4. Reboiler
The reboiler shall be horizontal. The vessel shall be leak tested full of water, as a
minimum. The reboiler design pressure shall not exceed 100 kPag (14.5 psig). (Refer to
T1101C01–T1101C04 of the Mobil Data Sheets.)
Direct gas fired reboilers shall be supplied with fire box breaching
and a flame arrestor on each burner to permit stable firing operation at
the maximum design wind velocity. Burners shall be equipped with
electronic spark type ignition.
The burner design shall limit the oxides of nitrogen and effluent
impurities to levels as necessary to meet or exceed national or local
pollution control standards.
Cold glycol shall be used to condense reflux in the top of the still, with
bypass piping provided to permit condenser throughput adjustment.
Vapors from the still to atmosphere shall pass through a liquid separation
device to disengage condensables. Condensed liquids shall be disposed of in
accordance with applicable environmental regulations. The unit shall be designed to
minimize back pressure on the reboiler.
The length of the exchanger shall be selected such that the exchanger does
not overhang the skid.
Exchangers shall cool the lean glycol to at least 11°C (20°F) below the
maximum allowable temperature recommended by the pump manufacturer. (Refer to
T1310C01 of the Mobil Data Sheets.)
The vendor shall quote, as an option, an automatic startup system for the
standby pump on signal of low-glycol flow.
The rate of flow shall be adjustable. For electrically driven pumps, this may
be accomplished by either bypass control or motor speed control.
The surge tank shall be gas blanketed with its pressure equalized to that of
the reboiler.
The surge tank may be either integral with the reboiler or supplied as a
separate vessel. Vessel configuration shall be horizontal.
The surge tank shall be leak tested full of water, as a minimum. The surge
tank design pressure shall not exceed 100 kPag (14.5 psig). Refer to MP 11-P-01 for
integral surge tanks.
3.10. Insulation
The still, reboiler and surge tank shall be thermally insulated with calcium silicate
insulation with a minimum thickness of 1.5 in.
Other surfaces with a temperature of 71°C (160°F) or hotter shall be insulated for
personnel protection, as given in the Appendix to this MEP.
4.1. General
Each glycol contactor unit shall include a gas scrubber, a contactor and a glycol cooler.
Mist eliminator elements shall be installed in the scrubber and contactor. Wire mesh mist
eliminators are common and various vane pack mist eliminators are acceptable. Wire
mesh mist eliminators shall be designed to remove 99.9 percent of 10 droplets
minimum. Mist eliminator thickness is 6 in (150 mm). For more information on design
and installation of wire mesh eliminators, refer to MP 12-P-21. Vane packs shall remove
99.9 percent of 20 droplets. Vane packs require two support rings, one above and one
below the vanes. Material of construction shall be 304 or 316 SS.
4.1.1. Scrubber
The scrubber shall be located upstream of the contactor. If an integral
scrubber is used, a leakage test of the chimney tray shall be made to verify a
proper seal. Note that the chimney tray shall be seal-welded at site. The
chimney tray shall have sufficient volume to prevent glycol overflow into the
scrubber during shutdown. A centrifugal type separator may be used, subject
to Mobil approval.
4.1.2. Contactor
The base unit shall use either structured packing or bubble cap trays.
Structured packing is preferred and will reduce the diameter and height of the
contactor. Acceptable packing includes Sulzer Mellapak 250Y, Koch
Flexipak 2Y, Norton Intalox 2T, Nutter BSH-250 or equivalent. Packing
shall be selected based on the vapor/liquid loadings, physical properties and
desired efficiency. Bubble cap trays shall only be used for dirty services.
Please refer to MP 12-P-21 for additional packing and tray specifications.
Only gravity flow trough type distributors are acceptable for tower
diameters >36 in. For tower diameters <36 in, drio tube orifice pan
If the rich glycol is taken from the bottom head of the contactor, a
grating vortex breaker shall be included. See MP 12-P-21 for additional
information.
5. Glycol Injection
The spray nozzle shall be inserted through flanged openings, so that nozzles
may be installed or removed without removing the heat exchanger head.
Mobil shall approve spray nozzle selection and geometry before spray nozzle
openings are located in the heat exchanger head.
The temperature of glycol entering the injection point shall be at least 10°C
(50°F).
Glycol injection into pipelines shall be done in such a manner that uniform
distribution is ensured.
5.2. Strainers
A "Y" strainer shall protect each glycol injection point. Each strainer shall be sized for
full flow. One strainer may serve several spray nozzles. Strainer openings shall be 1/4 to
1
/2 of the freepassage area of the spray nozzles.
6. Instrumentation
All instrumentation devices with visual indication shall be located facing the active area for ease of
observation.
6.1. Thermowells
Thermowells with temperature indicating devices shall be installed at the following
locations, as a minimum:
3. Reboiler
4. Still outlet
5. Inlet and outlet of the still reflux coil
6. Reboiler stack or, for indirectly heated reboilers, the heating medium inlet and outlet
Gauge glasses shall be the armored reflex type for absolute levels and the
armored transparent type to indicate interfaces.
Rating
Differential pressure gauges shall be supplied on each filter case and on the
contactor gas inlet/outlet and between packed beds (if applicable).
6.6. Shutdown
As a minimum, any one of the following conditions shall initiate a reboiler shutdown:
All instruments and other equipment that might be damaged in shipment shall be removed,
packed separately, individually tagged and match marked for field assembly. Detailed field
assembly instructions shall be provided for such items.
In no instance shall equipment and/or auxiliaries extend beyond the base plate of the shipping
pallet edge.
All spare parts furnished by the vendor shall be wrapped and packaged so that they are
preserved in original condition and properly tagged and coded so that they can later be identified.
They shall be packaged separately and shipped at the same time as the equipment. Packing lists
shall be furnished so that the parts can be handled without uncrating, if desired.
9. Final Documentation
The documentation required shall include the items indicated on the DRS (see the Mobil Data Sheets
for this MEP).
Skid design shall take into account lifting requirements. The unit may be mounted on more
than one skid, if necessary, for space and weight considerations.
The skid shall be designed to hold the full weight of the equipment with the reboiler reservoir
full of glycol and the tower full of water. The runners and cross pieces shall be of the same depth.
The design shall provide for ease of loading and unloading. The tower shall not be attached to
the skid while in transit to or from locations. All equipment shall be bolted to the skid and piping
shall be clamped to the skid.
Where standby equipment is installed, bypass piping and/or valving shall be provided to
allow isolation of the equipment without interrupting normal unit operation. This includes, but is
not limited to, pumps, filters, strainers and control valves.
ASME SEC VIII D1 shall be the minimum acceptable where local codes do
not cover pressure relief valves or are less stringent.
Pressure relief valves shall be of carbon steel with stainless steel trim and
carbon steel springs. Construction materials for sour gas service shall conform to
NACE MR0175.
Pressure relief valves shall be tested for set pressure and leakage in the
manufacturer's shop. Cold differential set pressures shall be given on the valve data
sheet and stamped on the nameplate in accordance with API STD 526.
10.2. Sandblasting
All equipment and piping, including skid members, shall be sandblasted to near-white
condition and painted in accordance with the job specifications. Special care shall be
taken not to sandblast or paint instrumentation, controls, valve stems, nameplates or any
other prepainted and/or stainless steel equipment.
the skid to a header to allow a single tie-in. Each line feeding the drain header shall be
provided with a check valve.
The unit shall be designed for continuous, unattended operation for the
conditions detailed on the Mobil Data Sheets. If not otherwise stated, the gas shall be
assumed to be water saturated, as a minimum.
All piping, vessels and equipment operating below the ambient dew point,
stated on the Mobil Data Sheets, shall be thermally insulated.
The design and construction of all equipment shall conform to all applicable
regulatory requirements of the government bodies having jurisdiction.
Mobil reserves the right to inspect vessels and piping at any time during their
fabrication to assure that the materials and workmanship are in accordance with this
Practice and the governing codes.
1. Within the United States: NFPA 70, NFPA 70E, local codes/regulations
and as applicable, API RP 500.
2. Within the Outer Continental Shelf of the United States: API RP 500B,
API RP 14F and as applicable, 29 CFR 1910 Subpart S.
3. Outside the United States: Codes and regulations of the locality where
installed. In the absence of recognized codes or regulations, the
requirements of items 1 and 2 (above) shall be applied.
Unless waived in writing, Mobil or its authorized representative shall witness all hydrostatic
testing. Hydrostatic tests shall be performed in accordance with ASME SEC VIII D1 or ASME
B31.3, as applicable.
The vendor shall facilitate the Mobil inspector's work by furnishing copies of specified
certifications for materials, shop test data, etc., to verify compliance with specifications. The
vendor shall maintain for the inspector's review such other records as are needed to insure
compliance with material and fabrication specifications.
Prior to pressure testing, equipment shall be thoroughly cleaned internally and external
surfaces shall be free of weld spatter, scale and other foreign material. Gasket compounds other
than graphite, oil or grease shall not be used.
For hydrostatic tests or surface inspections of equipment, all exterior surfaces and welds
subject to pressure shall be clean and dry.
New gaskets shall be installed in equipment joints that are opened for any reason after
assembly or pressure test, except that ring-type joint gaskets may be reused if undamaged.
Version 0
MP 60-P-70 Glycol Dehydration Units July 1998