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Iodine Value Determination Porim Test Method

This document provides a standard operating procedure for determining the iodine value of test materials using manual titration. It outlines the responsibilities of personnel, applicable references and standards, required materials and equipment, health and safety considerations, documentation, and step-by-step procedures. The iodine value is a measure of the degree of unsaturation in fatty acids and is calculated based on the titration of a sample with sodium thiosulfate solution.

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Adawiyah Ali
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695 views2 pages

Iodine Value Determination Porim Test Method

This document provides a standard operating procedure for determining the iodine value of test materials using manual titration. It outlines the responsibilities of personnel, applicable references and standards, required materials and equipment, health and safety considerations, documentation, and step-by-step procedures. The iodine value is a measure of the degree of unsaturation in fatty acids and is calculated based on the titration of a sample with sodium thiosulfate solution.

Uploaded by

Adawiyah Ali
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as DOCX, PDF, TXT or read online on Scribd
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MENA JAYA OIL & FATS SDN. BHD.

IODINE VALUE
Method : Manual Titration
1

1.0 PURPOSE
To check iodine value of test materials using manual titration

2.0 RESPONSIBILITY
2.1 Chemist is responsible to ensure the personnel are appropriately trained.
2.2 QC personnel is responsible to perform iodine value determination and generate test
report when is required.
2.3 Manager is responsible to review reports / verification report generated by QC personnel.

3.0 REFERENCES AND APPLICABLE DOCUMENTS

3.1 PORIM Test Method (1995). Test method p3.2


3.2 MPOB Test Methods p3.2:2004
3.3 ISO 3961:1996

4.0 MATERIALS AND EQUIPMENTS


4.1 Test sample
4.2 100 g L-1 potassium iodide
4.3 Cyclohexane
4.4 Wijs Solution
4.5 0.1N Sodium thiosulphate

5.0 HEALTH AND SAFETY CONSIDERATIONS

5.1 Wear and use appropriate Personnel Protective Equipment when handle test materials

5.2 Solutions very hazardous in case of skin contact (corrosive, irritator) of eye contact
(corrosive), of ingestion, of inhalation (fatal), may cause damage to organs through
prolonged and repeated exposure.

Effective date Doc No : SOP for Iodine Value


28th August 2018
Written by : Checked by : Approved by : Page 1 of ____
Adawiyah Ali
6.0 DOCUMENTATION REQUIREMENTS

6.1 Log Book


6.2 QC report / COA

7.0 PROCEDURES
7.1 Weight ~0.2-0.5 g of sample and put into a 250 mL flask.
7.2 Add 20 mL cyclohexane to dissolve the sample. Warm the flask slightly if necessary.
7.3 Add 25 mL Wijs solution, insert a stopper, shake gently and placed in the dark for 1 hour.
7.4 Add 20 mL of 100 g L-1 potassium iodide (Weigh 5 g KI, dissolve in to 50 mL water) and
100 mL distilled water.
7.5 Titrate with sodium thiosulphate solution until yellow iodine colour almost disappeared.
7.6 Add 1-2 mL starch indicator, shake vigorously until blue colour disappear. Repeat the
same for blank with no sample added.
Iodine value = [12.69N(V2 –V1)]/W
N = normality of sodium thiosulphate (Na2S2O3)
V2 = volume of Na2S2O3 solution used for blank
V1 = volume of Na2S2O3 solution used for sample
W = weight of sample in gram (g)

8.0 CARE AND MAINTENANCE


8.1 Keep away the solvents from heat/spark/open flames/hot surfaces.2

8.2 In case of skin contact, remove/take off immediately all contaminated clothing
and rinse skin with water/shower. In case of eye contact, remove contact lenses (if
present) and rinse cautiously with water for several minutes.

8.3 Dispose of waste to an appropriate treatment and disposal facility.

Effective date Doc No : SOP for Iodine Value


28th Aug 2018
Written by : Checked by : Approved by : Page 4 of ____
Adawiyah Ali

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