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Experiment 3: Redox Titration: Group: - Section: - Date

This document reports on a chemistry lab experiment involving redox titrations. The experiment measured the normality of potassium manganate (KMnO4), oxalic acid (H2C2O4), and iron(II) sulfate (FeSO4) solutions through titration. KMnO4 solution was titrated with a standard H2C2O4 solution, finding its normality to be 0.0475 N. Then H2C2O4 solution and FeSO4 solution of unknown normalities were each titrated with standard KMnO4, determining the normalities of H2C2O4 and FeSO4 through calculation.

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66 views

Experiment 3: Redox Titration: Group: - Section: - Date

This document reports on a chemistry lab experiment involving redox titrations. The experiment measured the normality of potassium manganate (KMnO4), oxalic acid (H2C2O4), and iron(II) sulfate (FeSO4) solutions through titration. KMnO4 solution was titrated with a standard H2C2O4 solution, finding its normality to be 0.0475 N. Then H2C2O4 solution and FeSO4 solution of unknown normalities were each titrated with standard KMnO4, determining the normalities of H2C2O4 and FeSO4 through calculation.

Uploaded by

argi6argi
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as DOCX, PDF, TXT or read online on Scribd
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International University, Vietnam National University - HCMC 1

GENERAL CHEMISTRY LABORATORY

REPORT
EXPERIMENT 3: REDOX TITRATION

Group: _____________ Section: ______________ Date: ____________

Group members: _______________________________

_______________________________

_______________________________

_______________________________

Score:__________
International University, Vietnam National University - HCMC 2
GENERAL CHEMISTRY LABORATORY

1. TITRATION OF KMnO4 SOLUTION WITH STANDARD H2C2O4 SOLUTION

Normality of the standard H2C2O4 solution, N(H2C2O4) = = 0.05 N

Volume of the standard H2C2O4 solution used, V(H2C2O4) = 10 mL

Trial # Burette reading (mL) Volume of KMnO4 (mL) Normality of KMnO4 (N)

1 21.00-31.40 10.40 0.048

2 31.40-42.10 10.70 0.047

Average Normality of KMnO4 = (0.048+0.047) / 2=0.0475 ( N )

Comment:

VKMnO4. NKMnO4 = VH2C2O4.NH2C2O4

Experiment 1: NKMnO4 = 10x0.05/ 10.3 = 0.048

Experiment 2: NKMnO4 = 10x0.05/ 10.7 = 0.047


International University, Vietnam National University - HCMC 3
GENERAL CHEMISTRY LABORATORY

2. TITRATION OF UNKNOWN CONCENTRATION H2C2O4 SOLUTION WITH


STANDARD KMnO4 SOLUTION

Normality of the standard KMnO4 solution, N(KMnO4) = 0.05 N

Volume of the unknown H2C2O4 solution used, V(H2C2O4) = 10 mL

Trial # Burette reading (mL) Volume of KMnO4 (mL) Normality of H2C2O4 (N)

1 42.39-46.40 4.01 0.02005

2 46.40-50.5 4.10 0.0205

Average Normality of H2C2O4 =(0.02005+0.0205) / 2=0.2275( N )

Comment:

The Normality of KMnO4 is: NH2C2O4 = (VKMnO4 x NKMnO4)/VH2C2O4

For the Trial 1: NH2C2O4 = 0.05x4.01/10 = 0.02005

For the Trial 2: NH2C2O4 = 0.05x4.1/10 = 0.0205


International University, Vietnam National University - HCMC 4
GENERAL CHEMISTRY LABORATORY

3. TITRATION OF UNKNOWN CONCENTRATION FeSO4SOLUTION WITH


STANDARD KMnO4 SOLUTION

Normality of the standard KMnO4 solution, N(KMnO4) =0.05 N

Volume of the unknown FeSO4 solution used, V(FeSO4)= 10 mL

Trial # Burette reading(mL) Volume of KMnO4 (mL) Normality of FeSO4(N)

1 36.50-50.27 13.77 0.0685

2 35.50-49.00 13.5 0.0675

Average Normality of FeSO4=(0.0685+0.0675) /2=0.068( N)


Comment:

For the Trial 1: NFeSO4 = 0.05x13.77/10 = 0.0685

For the Trial 2: NFeSO4 = 0.05x13.5/10 = 0.0675

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