Scribd Logo
Upload

Welcome to Scribd!

  • 40 views

    Exp # 11

    Uploaded by

    Aasia Farrukh
    This document describes an experiment to determine the acid value of an oil sample. The experiment involves titrating a sample of oil dissolved in neutralized alcohol with N/10 NaOH solution using phenolphthalein as an indicator. The volume of base added is recorded and used to calculate the acid value of the oil sample based on the reaction of fatty acids with the base. The acid value provides a measure of how acidic the oil is.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd

    Exp # 11

    Uploaded by

    Aasia Farrukh
    40 views2 pages
    This document describes an experiment to determine the acid value of an oil sample. The experiment involves titrating a sample of oil dissolved in neutralized alcohol with N/10 NaOH solution using phenolphthalein as an indicator. The volume of base added is recorded and used to calculate the acid value of the oil sample based on the reaction of fatty acids with the base. The acid value provides a measure of how acidic the oil is.

    Original Description:

    chemical process industries

    Copyright

    © © All Rights Reserved

    Available Formats

    DOCX, PDF, TXT or read online from Scribd

    Did you find this document useful?

    Is this content inappropriate?

    This document describes an experiment to determine the acid value of an oil sample. The experiment involves titrating a sample of oil dissolved in neutralized alcohol with N/10 NaOH solution using phenolphthalein as an indicator. The volume of base added is recorded and used to calculate the acid value of the oil sample based on the reaction of fatty acids with the base. The acid value provides a measure of how acidic the oil is.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    40 views2 pages

    Exp # 11

    Uploaded by

    Aasia Farrukh
    This document describes an experiment to determine the acid value of an oil sample. The experiment involves titrating a sample of oil dissolved in neutralized alcohol with N/10 NaOH solution using phenolphthalein as an indicator. The volume of base added is recorded and used to calculate the acid value of the oil sample based on the reaction of fatty acids with the base. The acid value provides a measure of how acidic the oil is.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    You are on page 1of 2

    Chemical Process Industries (lab)

    Department of Chemical Engineering Course No. Ch.E-201


    Wah Engineering College wahcantt.

    EXPERIMENT# 11

    Experiment Title: Oil analysis

    Objectives: To determine acid value in the given sample of oil.

    Apparatus required: Oil sample, titration flask, burette, pipette, beaker, weighing balance.

    Chemicals required: N/10 NaOH, 1% alcoholic solution of phenolphthalein, neutralized alcohol.


    Procedure:

    Take 4-5 grams of given sample of oil in a titration flask. Add 50 ml of neutralized
    alcohol in the titration flask , thoroughly mix it. Heat the contents of titration flask on water bath to boiling
    temperature followed by the addition of 1% alcoholic solution of phenolphthalein. Titrate it against N/10
    NaOH till pink colour which persist for about 10 seconds arises. . The boiling should be carried out very
    slowly on oxidizing flame and titration is carried out at boiling point. The volume of N/10 NaOH is
    noted down and take three readings.

    Observations and Calculations:


    1. Weight of oil sample taken = 4.1 g
    2. Volume of neutralized alcohol added = 50 mlIndicator = erichrome Black-T
    3. Standard solution = N/10 NaOH
    4. Indicator used = phenolphthalein
    5. Initial colour = colourless
    6. End point colour of the solution = pink (which persist only for about 10 seconds)
    7. Solution taken in the burette = N/10 NaOH

    Reactions:
    RCOOH + NaOH → RCOONa + H2O

    [Type text] Page 1


    Chemical Process Industries (lab)
    Department of Chemical Engineering Course No. Ch.E-201
    Wah Engineering College wahcantt.

    Sr.No. Initial Burette Reading Final Burette Reading Volume of N/10 NaOH used
    (ml) (ml) (ml)

    Mean Reading = ________

    Volume of N/10 NaOH solution used = (x) ________________________ml

    x ml of N/10 NaOH solution = x ml of N/10 KOH solution

    1000 ml of 1 N KOH = 56 g = 56000mg

    x ml of 1/10 N KOH = (56*1000/10*1000) * (x) * mg of KOH = y mg of KOH

    Acid Value = y/weight of oil sample taken =

    [Type text] Page 2

    You might also like

    pFad - Phonifier reborn

    Pfad - The Proxy pFad of © 2024 Garber Painting. All rights reserved.

    Note: This service is not intended for secure transactions such as banking, social media, email, or purchasing. Use at your own risk. We assume no liability whatsoever for broken pages.


    Alternative Proxies:

    Alternative Proxy

    pFad Proxy

    pFad v3 Proxy

    pFad v4 Proxy