Din en Iso 16925

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June 2014

DIN EN ISO 16925


D
ICS 87.040 Supersedes
DIN 55662:2009-12

Paints and varnishes –


Determination of the resistance of coatings to pressure water-jetting
(ISO 16925:2014);
English version EN ISO 16925:2014,
English translation of DIN EN ISO 16925:2014-06

Beschichtungsstoffe –
Prüfung der Beständigkeit von Beschichtungen gegen Druckwasserstrahl
(ISO 16925:2014);
Englische Fassung EN ISO 16925:2014,
Englische Übersetzung von DIN EN ISO 16925:2014-06
Peintures et vernis –
Détermination de la résistance des revêtements à un jet d’eau sous pression
(ISO 16925:2014);
Version anglaise EN ISO 16925:2014,
Traduction anglaise de DIN EN ISO 16925:2014-06
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Document comprises 22 pages

Translation by DIN-Sprachendienst.
In case of doubt, the German-language original shall be considered authoritative.

© No part of this translation may be reproduced without prior permission of


DIN Deutsches Institut für Normung e. V., Berlin. Beuth Verlag GmbH, 10772 Berlin, Germany,
has the exclusive right of sale for German Standards (DIN-Normen).
English price group 12
www.din.de !%2c("
www.beuth.de 05.14 2156405
DIN EN ISO 16925:2014-06

A comma is used as the decimal marker.

National foreword
This document (EN ISO 16925:2014) has been prepared by Technical Committee ISO/TC 35 “Paints and
varnishes”, Subcommittee SC 9 “General test methods for paints and varnishes” (Secretariat: BSI, United
Kingdom) in collaboration with Technical Committee CEN/TC 139 “Paints and varnishes” (Secretariat: DIN,
Germany). The responsible German body involved in its preparation was the Normenausschuss Beschich-
tungsstoffe und Beschichtungen (Coatings and Coating Materials Standards Committee), Working Committee
NA 002-00-07 AA Allgemeine Prüfverfahren für Beschichtungsstoffe und Beschichtungen.

The determination of the resistance of coatings to pressure water-jetting (Prüfung der Beständigkeit von
Beschichtungen gegen Druckwasserstrahl) is also expressed in German as Dampfstrahltest.

The DIN Standards corresponding to the International Standards referred to in this document are as follows:

ISO 1513 DIN EN ISO 1513


ISO 2808 DIN EN ISO 2808
ISO 4618 DIN EN ISO 4618
ISO 15528 DIN EN ISO 15528
ISO 16276-1 DIN EN ISO 16276-1
ISO 17872 DIN EN ISO 17872

Amendments

This standard differs from DIN EN 55662:2009-12 as follows:

a) the status of the standard has been changed to that of a European Standard;

b) no further modifications have been made.

Previous editions

DIN 55662: 2009-12


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National Annex NA
(informative)

Bibliography

DIN EN ISO 1513, Paints and varnishes — Examination and preparation of test samples

DIN EN ISO 2808, Paints and varnishes — Determination of film thickness

DIN EN ISO 4618, Paints and varnishes — Terms and definitions

DIN EN ISO 15528, Paints, varnishes and raw materials for paints and varnishes — Sampling

DIN EN ISO 16276-1, Corrosion protection of steel structures by protective paint systems — Assessment of,
and acceptance criteria for the adhesion/cohesion (fracture strength) of a coating — Part 1: Pull-off testing

DIN EN ISO 17872, Paints and varnishes — Guidelines for the introduction of scribe marks through coatings
on metallic panels for corrosion testing

2
EUROPEAN STANDARD EN ISO 16925
NORME EUROPÉENNE
EUROPÄISCHE NORM February 2014

ICS 87.040

English Version

Paints and varnishes - Determination of the resistance of


coatings to pressure water-jetting (ISO 16925:2014)

Peintures et vernis - Détermination de la résistance des Beschichtungsstoffe - Prüfung der Beständigkeit von
revêtements à un jet d'eau sous pression (ISO 16925:2014) Beschichtungen gegen Druckwasserstrahl
(ISO 16925:2014)

This European Standard was approved by CEN on 20 December 2013.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same
status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United
Kingdom.
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EUROPEAN COMMITTEE FOR STANDARDIZATION


COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels

© 2014 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 16925:2014 E
worldwide for CEN national Members.
DIN EN ISO 16925:2014-06
EN ISO 16925:2014 (E)

Contents
Page

Foreword ............................................................................................................................................................. 3
1 Scope ....................................................................................................................................................... 4
2 Normative references............................................................................................................................. 4
3 Terms and definitions ............................................................................................................................ 4
4 Principle .................................................................................................................................................. 5
5 Apparatus and materials ....................................................................................................................... 5
6 Sampling ................................................................................................................................................. 6
7 Preparation of test specimens .............................................................................................................. 7
7.1 Test specimens ...................................................................................................................................... 7
7.2 Preparation and coating ........................................................................................................................ 7
7.3 Thickness of coating.............................................................................................................................. 7
8 Procedure ................................................................................................................................................ 7
8.1 Introducing the cut or the scribe .......................................................................................................... 7
8.2 Testing ..................................................................................................................................................... 8
9 Evaluation ............................................................................................................................................... 9
9.1 General .................................................................................................................................................... 9
9.2 Evaluation with pictures to compare ................................................................................................... 9
10 Precision ................................................................................................................................................. 9
10.1 General .................................................................................................................................................... 9
10.2 Repeatability limit (r) ........................................................................................................................... 10
10.3 Reproducibility limit (R) ....................................................................................................................... 10
11 Designation ........................................................................................................................................... 10
12 Test report ............................................................................................................................................. 10
Annex A (normative) Calibration of the test apparatus ............................................................................... 17
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Bibliography ...................................................................................................................................................... 20

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DIN EN ISO 16925:2014-06
EN ISO 16925:2014 (E)

Foreword

This document (EN ISO 16925:2014) has been prepared by Technical Committee ISO/TC 35 “Paints and
varnishes” in collaboration with Technical Committee CEN/TC 139 “Paints and varnishes” the secretariat of
which is held by DIN.

This European Standard shall be given the status of a national standard, either by publication of an identical
text or by endorsement, at the latest by August 2014, and conflicting national standards shall be withdrawn at
the latest by August 2014.

Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights.

According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech
Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece,
Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,
Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom.

Endorsement notice

The text of ISO 16925:2014 has been approved by CEN as EN ISO 16925:2014 without any modification.
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DIN EN ISO 16925:2014-06
EN ISO 16925:2014 (E)

1 Scope
This International Standard specifies a test method for the assessment of the resistance of coatings to
pressure water-jetting. The test method simulates the effects pressure water-jetting has on a coating.

2 Normative references
The following documents, in whole or in part, are normatively referenced in this document and are
indispensable for its application. For dated references, only the edition cited applies. For undated
references, the latest edition of the referenced document (including any amendments) applies.
ISO 1513, Paints and varnishes — Examination and preparation of test samples
ISO 2808, Paints and varnishes — Determination of film thickness
ISO 4618, Paints and varnishes — Terms and definitions
ISO 15528, Paints, varnishes and raw materials for paints and varnishes — Sampling
ISO  17872, Paints and varnishes  — Guidelines for the introduction of scribe marks through coatings on
metallic panels for corrosion testing

3 Terms and definitions


For the purposes of this document, the terms and definitions given in ISO 4618 and the following apply.
3.1
fracture strength
force required to exceed the attachment forces
— between coats or between coat and substrate (adhesion) and/or
— within a coat (cohesion)
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[SOURCE: ISO 16276‑1:2007, 3.1]


3.2
adhesion
phenomenon of attachment at the interface between a solid surface and another material caused by
molecular forces
Note 1 to entry: Adhesion should not be confused with cohesion.

[SOURCE: ISO 4618:2006, 2.6]


3.3
cohesion
forces that bind a film into an integral entity
Note 1 to entry: Cohesion should not be confused with adhesion.

Note 2 to entry: Breaks in cohesion can occur within the coating as well as the substrate. In case of breaks within
the substrate, it is subsumed under the term material delamination.

[SOURCE: ISO 4618:2006, 2.54, modified — Note 2 to entry has been added.]

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EN ISO 16925:2014 (E)

4 Principle
The resistance of a coated test specimen to the loss of adhesive strength is tested by means of defined
pressure water-jetting.
The extent of the damage of the test specimen primarily depends on, besides the adhesive strength, the
space between nozzle and test piece, the volumetric flow rate, the test time, the geometry of the nozzle,
the impact area, the angle of impact, and the water temperature of the jet, as well as the cutting and
scribing tool.
The evaluation is carried out by means of a visual comparison of pictures, in which characteristic values
are related to the peeled-off areas.
The parting line (plane) of the peeling shall be indicated in the test report (e.g. substrate/priming coat).

5 Apparatus and materials


Ordinary laboratory apparatus, together with the following:

5.1 Pressure water-jet, consisting of a high-pressure pump and a nozzle.

A high-pressure pump conveys the water from a storage bin. To avoid influences from variations in
pressure, it is necessary that the pressure and the volumetric flow rate be adjustable at the nozzle
described below.
The water temperature shall be adjustable to ± 2 °C.
The temperature shall be adjusted in accordance with Annex A. Necessary safety devices on the pressure
side of the unit, as e.g. pressure relief valve and by-pass valve, shall exist. If the jetting is unsteady, a flow
calming section may be installed in front of the nozzle. A pulsation of the water jet at the opening of the
pump is inadmissible. In order to reach a reproducible result, the nozzle shall be solidly mechanically
fixed and the test specimen shall be secured against slipping. For the adjustment of the volumetric flow
rate, a nozzle with a jet angle of 25° and a volumetric flow rate of 6 l/min at 2 MPa (20 bar) is required
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(see Annex A).
The following technical data should be attainable:
— volumetric flow rate: 8 l/min to 14 l/min

— pressure: 4 MPa (40 bar) to 13 MPa (130 bar)

— temperature: 20 °C to 80 °C

— jetting time: 10 s to 300 s

Figure 1 shows the schematic construction of a pressure water-jet apparatus which is specially built for
these tests.

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EN ISO 16925:2014 (E)

Key
1 flow calming section 8 heating
2 high-pressure valve, height adjustable 9 base frame, moveable
3 test specimen 10 temperature sensor
4 clamping element 11 high-pressure pump
5 feed tank 12 by-pass valve
6 floating valve with filter 13 pressure relief valve
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7 water shortage safeguard 14 pressure transmitter

Figure 1 — Schematic construction of a pressure water-jet apparatus

5.2 Cutting or scribing tool, to be agreed by the interested parties.

The following cutting and scribing tools are appropriate: cutter knife (“C”), scribing tool according to
van Laar (“L”) or scribing tool according to Sikkens (“S”), in accordance with ISO 17872.
The tool should be safely usable.

5.3 Time measuring device (stopwatch).

6 Sampling
Take a representative sample of the product being tested in accordance with ISO 15528.
Examine and prepare each sample for testing in accordance with ISO 1513.

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EN ISO 16925:2014 (E)

7 Preparation of test specimens

7.1 Test specimens


The test specimens should preferably be plane. The size of the test specimens as well as the number of
tests shall be agreed by the interested parties.
Test specimens (building components) can have different adhesive strengths. It is recommended that
different parts of the test specimen (building components) be tested.

7.2 Preparation and coating


The conditions of coating, drying/hardening, as well as stoving, shall be agreed.
Before testing, the coated test specimens shall be conditioned either 48 h at 60 °C or 7 days at room
temperature. In case of conditioning at 60 °C, the specimen shall be cooled down to room temperature
before the cut or scribe (see 8.1) is introduced.

7.3 Thickness of coating


Determine the dry film thickness of the coating, in micrometres, in accordance with one of the procedures
specified in ISO 2808.

8 Procedure

8.1 Introducing the cut or the scribe


Make sure that the test specimen is securely fastened when introducing the cut or the scribe.
Introduce both of the cuts or scribes vertically through the coating into the substrate using the cutting
or scribing tool, as shown in Figure 2. The depth of the cut or scribe into the substrate should be as
minimal as possible. The length of the first cut or scribe shall be at least 100 mm, if the geometry of the
part allows that. At an angle, introduce a second cut or scribe with a minimum length of 20 mm. The
cuts or scribes shall be introduced straight-line at an angle of approximately 30°. An automatic cutting
or scribing device may be used. Residues of the coating shall be removed from the cut or scribe.
NOTE The depth of the cut or scribe into the substrate influences the result.
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The cutting or scribing tools should be checked regularly and replaced if necessary.

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Dimensions in millimetres

Figure 2 — Introducing the cuts or scribes (St Andrew’s cross)

8.2 Testing
After inserting the test specimen into the apparatus (e.g. using a spacer block), calibrate the space
between test specimen and nozzle.
Operate the pressure water-jetting apparatus at room temperature.
Three test methods (A, B, or C – see Table 1) are preferred as well as three possible scribing tools (C, L, or
S – see 5.3 N1)). The test method to be applied, the scribing or cutting tool to be used, and the water pressure
shall be agreed.

Table 1 — Test methods


Space between
Water Duration of
Test method Impact angle nozzle and Flow rate
temperature jetting
sample
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°C mm l/min s
A 60 ± 2 90° ± 2° 100 ± 1 11,3 ± 0,2 30 ± 1
B 60 ± 2 90° ± 2° 100 ± 1 11,3 ± 0,2 60 ± 1
C 60 ± 2 90° ± 2° 130 ± 1 11,3 ± 0,2 60 ± 1

For jetting, deionized water should be used.


When using automatic and manual devices, fasten the test specimen so that the water jet impacts as
shown in Figure 3. The jet impacts in the middle above the point of intersection onto the longer one of
both cuts/scribes.

N1) National footnote: It should be corrected to read: “see 5.2”.

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EN ISO 16925:2014 (E)


Figure 3 — Jetting area

9 Evaluation

9.1 General
Damage is recognizable when the coating loosens or flakes, regardless of which coat sustains the damage.

9.2 Evaluation with pictures to compare


Carry out the evaluation visually, comparing the specimen with the pictures.
In the course of the visual evaluation, a characteristic value is laid down by comparing with the
illustrations in Figures 4 to 9. A characteristic value between 1 and 5 results, depending on the degree
of damage. No damage corresponds to the characteristic value 0. In addition to the evaluation, if
applicable, the attribution of the separation from the main separation level or to the respective film
shall be indicated.
The result of the visual assessment is indicated in dependence of the applied method, for example:
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— method A: characteristic value A;


— method B: characteristic value B;
— method C: characteristic value C.
NOTE In addition, by measuring the areas of flaking (maximum width, in millimetres, or area, in square
millimetres), the overall damage can be evaluated. The overall damage is calculated by summing up all damaged
areas of the test specimen. Even the smallest areas of flaking are measured and calculated, and all areas added to
the overall damage.

10 Precision

10.1 General
The data regarding the repeatability and reproducibility limits have been determined in an interlaboratory
test. Representatives of the automotive industry have been involved in the interlaboratory test.
The interlaboratory test aimed at determining the precision of the test method. As a standard substrate,
polycarbonate/polybutylene terephthalate (PC/PBT) panels were coated with coating materials
exclusively produced for this interlaboratory test. The interlaboratory test was conducted in accordance

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EN ISO 16925:2014 (E)

with three different methods. In this International Standard, the data relative to precision were
obtained by method A (see Table 1). The test panels were centrally produced. The St Andrew’s cross was
introduced into the coating with a defined new utility knife. Each participant conducted the testing with
his own pressure water-jetting apparatus device. The test panels were visually assessed in comparison
to the pictures (see 9.2). Also, the overall damage area was calculated (see 9.2, note).
The data relative to the repeatability limit and the reproducibility limit do not account for the influence
of the preparation of test specimens (see Clause 7).
Deviations of precision can occur due to different substrates.

10.2 Repeatability limit (r)


The repeatability limit r is the value below which the absolute difference between two test results
(each the mean of valid duplicates) can be expected to lie when this method is used under repeatability
conditions. In this case, the test results were obtained on identical material by one operator in one
laboratory within a short interval of time using the standardized test method. In this International
Standard, the repeatability limit r is one characteristic value with a preset probability of 95 %.

10.3 Reproducibility limit (R)


The reproducibility limit R is the value below which the absolute difference between two single test
results (each the mean of valid duplicates) can be expected to lie when this method is used under
reproducibility conditions. In this case, the test results are obtained on identical material by operators
in different laboratories using the standardized test method. In this International Standard, the
reproducibility limit R is two characteristic values with a preset probability of 95 %.

11 Designation
The example below shows the designation of the test method in accordance with this International
Standard.
EXAMPLE
Method A (in accordance with ISO 16925:2013, Table 1 N2) ), with scribes introduced using a scribing tool
according to Sikkens (S) (in accordance with ISO 16925:2013 N2), 5.2):
Pressure water-jetting test ISO 16925:2013 N2) — A — S
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12 Test report
The test report shall contain at least the following information.
a) all details necessary to identify the tested coating (manufacturer, product designation, batch
number, coating process, etc.);
b) a reference to this International Standard (ISO 16925:2013 N2) );
c) the type of substrate (manufacturer, product designation, batch number, injection moulding process,
etc.) and preparation of surface;
d) the conditions of coating, drying/hardening or stoving as well as the ageing time and conditioning
before the testing;
e) the test method, the cutting or scribing tool and the water pressure used (see 8.2);
f) the result of the test as indicated in Clause 9, including the parting line;
g) any deviation from the specified test method;

N2) National footnote: It should be corrected to read: “ISO 16925:2014”.

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EN ISO 16925:2014 (E)

h) any special agreements between the interested parties, that are not included in c) and d);
i) any unusual features (anomalies) observed during the test;
j) the date of the test;
k) the person who undertakes the test.

Characteristic value 0

Figure 4 — Characteristic value 0 for pressure water-jet damage


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DIN EN ISO 16925:2014-06
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a) Characteristic value 1a

b) Characteristic value 1b
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c) Characteristic value 1c

Figure 5 — Characteristic value 1 for pressure water-jet damage

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EN ISO 16925:2014 (E)

a) Characteristic value 2a

b) Characteristic value 2b
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c) Characteristic value 2c

Figure 6 — Characteristic value 2 for pressure water-jet damage

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EN ISO 16925:2014 (E)

a) Characteristic value 3a

b) Characteristic value 3b
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c) Characteristic value 3c

Figure 7 — Characteristic value 3 for pressure water-jet damage

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EN ISO 16925:2014 (E)

a) Characteristic value 4a

b) Characteristic value 4b
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c) Characteristic value 4c

Figure 8 — Characteristic value 4 for pressure water-jet damage

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EN ISO 16925:2014 (E)

a) Characteristic value 5a

b) Characteristic value 5b
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c) Characteristic value 5c

Figure 9 — Characteristic value 5 for pressure water-jet damage

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EN ISO 16925:2014 (E)

Annex A
(normative)

Calibration of the test apparatus

A.1 Apparatus and materials


Ordinary laboratory apparatus, as well as the following.

A.1.1 Temperature measuring device, with sensor, capable of measuring to 0,5 °C.

A.1.2 Balance, weighing to 10 g.

A.1.3 Time measuring device (stopwatch), capable of measuring ± 0,1 s.

A.1.4 Container, for the determination of the volumetric flow rate for at least 20 l of water.

A.1.5 Plastic block, made of polystyrene rigid plastic foam.

The kind of the polystyrene rigid plastic foam shall be agreed by the interested parties.

A.1.6 Length measuring device, capable of measuring ± 0,1 mm.

A.2 Procedure
A.2.1 General
For calibration, adjust the pressure water-jet apparatus in accordance with method B (according to 8.2).

A.2.2 Calibration of water temperature


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Bring the pressure water-jetting apparatus to the operating temperature and let water jet for at least
1 min. Subsequently, let water jet for 1 min into a container containing the temperature sensor. Read off
the temperature immediately. Conduct the determination in quintuplicate. The water temperature shall
remain constant during the course of the calibration.
The water temperature shall be (60 ± 2) °C.

A.2.3 Calibration of volumetric flow rate


Calibrate the volumetric flow rate, qV, in litres per minute, by differential weighing.
Determine the tare weight, m0, of the container on the balance precisely to 10 g. Adjust the pressure water-
jet apparatus in accordance with method B. Collect the water in the container entirely. Subsequently,

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determine the mass of the container with the water, m1, on the balance precisely to 10 g. The difference
equals the mass of the collected water, m2, as given in Formula (A.1):

m2 = m1 − m0 (A.1)

Since the water density, ρwater, is approximately equal to 1,0 g/cm3, the collected volume, Vwater, is given
by Formula (A.2):

V water ≈ m2 (A.2)

For a jetting time of 60 s (equal to 1 min), and given the relationship in Formula (A.3), it can be determined
that the collected mass m2 should equal the volumetric flow rate, expressed in litres per minute.

dV
qV = (A.3)
dt
The volumetric flow rate shall be (11,3 ± 0,2) l/min.

A.2.4 Calibration of the water jet


The conditions for the calibration of the jetting are in accordance with method B. For the calibration of
the jetting, a stainless steel precision flat film extrusion die with a volumetric flow rate of the nozzle of
6 l/min at 2 MPa (20 bar) and a jet angle 25° is used. This nozzle is required to produce an even liquid
distribution during the entire jetting.
When using an automatic pressure-water apparatus, fasten the polystyrene rigid plastic foam in the
apparatus so that the jet cannot move the block. When using a manual apparatus, fasten the block in a
similar fixture.
After jetting, the length and the width of the impact are measured. See Figure A.1.
The mean length of the impact shall be (73 ± 5) mm and the mean width (8 ± 1) mm on average.
Dimensions in millimetres
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Figure A.1 — Measures of the washed-out areas in the polystyrene rigid plastic foam

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Additionally, the homogeneity of the jetting is assessed visually. The jetting shall be evenly deep and
straight. Frayed edges and sinuous lines are not acceptable and suggest uneven pressure (see Figure A.2).

a) With complaints

b) Without complaints

Figure A.2 — Jetting in comparison


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EN ISO 16925:2014 (E)

Bibliography

[1] ISO 4618:20061), Paints and varnishes — Terms and definitions


[2] ISO 16276-1:2007, Corrosion protection of steel structures by protective paint systems — Assessment
of, and acceptance criteria for, the adhesion/cohesion (fracture strength) of a coating — Part 1: Pull-
off testing
Normen-Download-Beuth-Kansai Altan-KdNr.7552972-LfNr.7890111001-2017-03-14 14:58

1) Under revision.

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