B.

Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 3rd Semester
Second Year Engineering
Third Semester
Theory Practical
Subject Catego Course Name Hour Credit University Internal Hour Credit Mark
Code ry s/We Theor Marks Evaluati s/We Practic s
ek y on ek al
L/T L/T
PCE3I101 PC Fluid Flow & Flow 3-0 3 100 50 2 1 50
Measurement
PCE3I101 PC Chemical Technology 3-0 3 100 50 2 1 50
PCE3I103 PC Mechanical Operation 3-0 3 100 50 2 1 50
PCE3I104 PC Mass Transfer-I 3-0 3 100 50 2 1 50
PCE3I001 PC Chemical Process 3-1 4 100 50
Calculation
PEK3E00 HS Engineering Economics/ 2-1 3 100 50
1/ Organizational Behavior
POB3E00
2
Total 19 19 600 300 8 4 200
Total Marks: 1100
Total Credits: 23
PCE3D00 Honours Advanced Fluid 4 4 100 50
1 Dynamics
PCE3G00 Minor Solar Energy
1 Specializati Engineering
on

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 3rd Semester
Semester : 3rd
--------------
1. PCE3D001 Honours(CP) Advanced fluid dynamics 4-0-0 4
2. PEK3E001 HS(O1) Engineering Economics 3-0-0 3
3. POB3E002 HS(O1) Organizational Behavior 3-0-0 3
4. PCE3G001 Minor(CP) Solar Energy engineering 4-0-0 4
5. PCE3I001 PC(CP) Chemical Process Calculation 4-0-0 4
6. PCE3I101 PC(CP) Fluid Flow & Flow Measurement 3-0-1 4
7. PCE3I102 PC(CP) Chemical Technology 3-0-1 4
8. PCE3I103 PC(CP) Mechanical Operation 3-0-1 4
9. PCE3I104 PC(CP) Mass Transfer - I 3-0-1 4
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 3rd Semester

PCE3I101FLUID FLOW AND FLOW MEASUREMENT

Module I:
Units and dimensional analysis, Types of Fluids.
Fluid Statics: Hydrostatic Pressure, Pressure measuring Devices.
Introduction to fluids in motion, Flow in boundary layers. Its formation & growth in
tubes & plates. Basic equations of fluid flow continuity, momentum &Bernoulli’s
equation. Flow measuring devices: Venturi, Orifice, Pitot tube, and Rotameter.
Module II:
Flow of incompressible fluid in pipes, Relation between skin friction & wall shear.
Laminar flow in pipes, Hagen–Poiseuille equation, Friction factor, Friction from changes
in velocity or direction, Flow of compressible fluids, Basic equations. Flow past
immersed bodies, Drag Co-efficient. Motion of particles through fluids. Its mechanics,
Terminal velocity.
Module III:
Friction inflow through beds of solids, Fluidization, Mechanism of fluidization, pressure
drop in fluidization, Applications of fluidization.
Transportation of fluids, Reciprocating, rotary, and centrifugal pump, fans, blowers &
compressors. Characteristics curves & calculation of power & efficiency of pumps.
Concept of slip.
Text Books:
1. Unit Operations of Chemical Engineering, 7th ed. by W L McCabe, J C Smith, and
P Harriott, McGraw-Hill.
2. Fluid Mechanics for Chemical Engineers, 3rd ed. by Noel de Nevers, McGraw-
Hill.
Reference Books:
1. A Textbook of Fluid Mechanics and Hydraulic Machines, 9th ed. by R K Bansal.
2. Fluid Mechanics: Including Hydraulic Machines by AKJain.
3. Introduction to Fluid Mechanics and Fluid Machines, 3rd ed. by S K Som, G
Biswas, and S Chakraborty, McGraw-Hill, 2011.

Fluid Flow Lab

1. Manometers –To find the pressure drop for flow through pipes.
2. Fluidized bed – To determine minimum fluidization velocity and pressure drop.
3. Centrifugal Pump – To draw the characteristics curves and find out the
efficiency.
4. Reciprocating Pump – To draw the characteristics curves and find out the
efficiency.
5. Venturiand Orifice Meter – To find out the flow rate of fluid flowing inside a
pipe.
6. Reynold’s Apparatus – To verify the flow whether it is laminar or turbulent.
7. Bernoulli’s Apparatus – To verify the Bernoulli’s equation.
8. Pitot tube – To find out the point velocity of fluid.
9. V-Notch – To measure the flow rate of a fluid by using V – Notch.
10. Packed Bed – To find out the pressure drop when a fluid is flowing through a
3

packed bed
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 3rd Semester

PCE3I102 CHEMICAL TECHNOLOGY

ModuleI:
Heavy Chemicals: Caustic Soda & Chlorine, HCL, Soda Ash, Sulphuric acid.

Module II:
Extraction Refining of Oil, hydrogenation of Oil.
Soap &synthetic detergents.
Pulp &paper Industry.
Technology of Pigment &dyes, Natural dyes.

Module III:
Manufacture of Sugar, Starch & its derivatives, Industrial &absolute alcohol.

Module IV:
Polymers: Polyethylene, Polypropylene, PVC, Phenol formaldehyde, Urea formaldehyde,
Polystyrene, Poly vinylacetate, Polylactic acid, and Nylons.

Text Books:
1. Dryden's Outlines of Chemical Technology for the 21st Century, 3rd ed. by
CEDryden, Edited & revised by M Gopal Rao and MSittig.
2. Shreve's Chemical Process Industries, 5th ed. by G T Austin, McGraw-Hill.

CHEMICAL TECHNOLOGY LAB

1. Manufacture of soap from vegetable oil.

2. Determination of dissolvedoxygen of the given water sample.
3. Determination of saponification value of the given oil sample.
4. Determination ofacid value of the given oil sample.
5. Determination of concentration of sugar solution by Refractometer.
6. Estimation of nitrogen in nitrogenous fertilizer.
7. Determination of total, temporary,& permanent hardness of given water sample.
8. Determination of CaO in Cement.
9. Determination of alkalinity in water sample.
10. Manufacture of phenol formaldehyde.
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 3rd Semester

PCE3I103 MECHANICAL OPERATIONS

Objectives: This course acquaints the students of the mechanical method of sizing,
separating & transportation of particles.

ModuleI:
Properties and storage of solids: Characteristics of solid particles and solids in bulk. Size
Reduction: Objectives, Methods, and Principles of size reduction, Size reduction
equipments: Coarse, Intermediate, and Fine Crushers and Ultra-fine grinders, Open &
closed circuit grinding.

ModuleII:
Solid-solid separation: Screening, Electrical separation, Classification, Gravity
concentration, and Floatation and their latest equipments.
Solid-liquid separation: Sedimentation and equipments(Thickeners and clarifiers),
Filtration: Theory and equipments.

ModuleIII:
Gas-solid separation: Principle and equipments. Transportation of solids: Conveyors
and elevators.

Module IV:
Mixing: Theory of solid and liquid mixing and their equipments. Size enlargement,
Crystallization, Feeding, Weighing, and Coagulation.

Text Book:
1. Mechanical Operations, 1st ed. by A K Swain, H Patra, and G K Roy, McGraw-
Hill.

Reference Books:
1. Unit Operations of Chemical Engineering, 7th ed. by W L McCabe, J C Smith, and
P Harriott, McGraw-Hill.
2. Mechanical Operations for Chemical Engineers, 3rd ed. by C M Narayanan and
B C Bhattacharya, Khanna Publishers.
3. Perry's Chemical Engineers' Handbook, 8th ed. by D W Green and R H Perry,
McGraw-Hill.
4. Introduction to Chemical Engineering by W L Badger and JTBanchero, McGraw-
Hill.
5. Unit Operations, by G G Brown, et. al., CBS Publishers.
6. Handbook of Mineral Dressing: Ores and Industrial Minerals by A F Taggart,
John Wiley.
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 3rd Semester

Mechanical Operation Lab

1. To find out the average size of particles in a sample (Volume-surface mean dia).
2. To determine the critical speed and time of grinding in a ball mill for producing a product
with 80% passing a given screen.
3. To separate a mixture of coal into two fractions using sink and float methodand/or
floatation method.
4. Determination of the effectiveness of a vibrating screen.
5. To verify the Rittinger’s and Kick’s law using crushing rolls and to find out the Work Index
of the coal.
6. To study the characteristics of batch sedimentation using coal sample.
7. To determine the specific cake resistance and filter medium resistance of a slurry in Plate
and frame filter press.
8. To separate a mixture of sand and iron powder by means of tabling.
9. To find out the reduction ratio in Jaw Crusher and Hammer Mill.
10. To find out the separation characteristics of Cyclone separator.

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 3rd Semester

PCE3I104 MASS TRANSFER – I

Module I:
Introduction to Mass transfer operations, molecular diffusion in fluids, binary solutions,
Fick’s law, equation of continuity, steady state equimolal counter current diffusion,
Stefan-Maxwell equation, diffusivity of gases and liquids, application of molecular
diffusion, mass transfer coefficients, in laminar and turbulent flow, Interphase mass
transfer, Film theory, Penetration theory, surface-renewal theories, analogy between
mass, heat and momentum transfer.

Module II:
Absorption : Solubility of gases in liquids, two components system, multi component
system, ideal and non - ideal solutions, choice of solvent for absorption, single
component absorption material balance, counter current multistage operations, dilute
gas mixtures, non - isothermal operation, tray efficiency, continuous contact equipment,
HETP, HTU, NTU concepts for single component absorption.

Module III:
Principle of VLE for binary systems, phase diagrams, relative volatility, ideal solutions,
azeotropes, enthalpy concentration diagrams, flash vaporization, partial condensation,
differential distillation steam distillation, azeotropic and extractive distillation.
Continuous distillation: McCabe - Thiele method, Ponchon - Savarit method, Tray
efficiencies, introduction to multi component distillation.

Module IV:
Humidification operations: Definition of fundamental terms, Psychometric charts,
theory of adiabatic saturation and wet bulb temperature, Lewis relation, Gas liquid
contact, Dehumidification, Adiabatic Humidification. Equipments: Natural Circulation,
Natural draft, Mechanical draft, Spray tower, Spray chamber, Spray pond. Humidity
Measurement: Direct chemical method, Hygrometer method, Sling psychrometer, Dew
point method, Mirror method.

Reference Books:
1. Mass Transfer Operations by R E Treybal, McGraw Hill.
2. Unit Operations of Chemical Engineering, 7th ed. by W L McCabe, J C Smith, and
P Harriott, McGraw-Hill.
3. Design of Equilibrium Stage Processes by BDSmith, McGraw-Hill.
4. Principles of Mass Transfer and Separation Processesby B K Dutta, PHI.
5. Mass Transfer Operations by ASuryanarayana,New Age International.
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 3rd Semester

MASS TRANSFER - I LAB

1. To determine the diffusivity coefficient for carbon tetrachloride - air system.
2. To determine the vapour – liquid equilibrium curve for carbon tetrachloride - air system.
3. To verify Rayleigh’s equation through simple distillation for binary mixture of water and
ethanol.
4. To determine the vaporization and thermal efficiencies in steam distillation of the given
organic liquid i.e. nitrobenzene or aniline.
5. Performance of lab scale bubble cap distillation column at different reflux ratios.
6. To study the height equivalent to a theoretical plate (HETP) of packed column at total
reflux for a binary system of ethanol and water using Fenske’s equation.

PCE3I001 CHEMICAL PROCESS CALCULATIONS

Module I:
Units & dimensions, Ideal gas laws, equation of state, Vapor pressure, Clausius-
Clapeyron equation, Ideal and non-ideal solutions, humidity-relative saturation &
percentage saturation, concept of wet & dry bulbs thermometer, use of Humidity chart.

Module II:
The chemical equation &stoichiomentry, concept of limiting & excess reactants,
conversion, degree of conversion, yield etc.
Material balances &unit operations: drying, crystallization dissolution, combustion, etc.
Solving material balance (steady and unsteady state processes) without and with
chemical reactions, recycle, bypass,& purge calculations.

Module III:
Energy balance concepts: Heat capacity, Calculation of enthalpy changes without change
of phase, Energy balance with chemical reaction, Standard heat of reaction at constant,
pressure & constant volume, effect of T and P on heat of reaction, Adiabatic reaction of
temperature,heat of solution & mixing.

Text Books:
1. Stoichiometry and Process Calculations by B Lakshmikutty and K V Narayanan,
PHI.
2. Stoichiometry, 5th ed. by B I Bhatt and S B Thakore, McGraw-Hill.

References Books:
1. Elementary Principles of Chemical Processes, 3rd ed. by R M Felder and R W
Rousseau, John Wiley.
2. Chemical Process Principles: Material and Energy Balances (Part - 1), 2nd ed. by O
A Hougen, K M Watson, and R A Ragatz, CBS.
3. Principles of Chemical Engineering Processes by N Ghasem and R Henda, CRC.
4. Basic Principles and Calculations in Chemical Engineering, 8th ed. by D M
Himmelblau and J B Riggs, PHI.
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 3rd Semester

PEK3E001 ENGINEERING ECONOMICS

Module I:
Engineering Economics: Nature and scope, general concepts on micro & macro-
economics. The theory of demand, demand function, Law of demand and its exceptions,
elasticity of demand, law of supply and elasticity of supply. Determination of
equilibrium price under perfect competition (simple numerical problems to be solved).
Theory of production, Law of variable proportion, Law of returns to scale.

ModuleII:
Time value of money: Simple and compound interest, cash flow diagram, principle of
economic equivalence. Evaluation of engineering projects: Present worth method,
Future worth method, Annual worth method, internal rate of return method, Cost-
benefit analysis in public projects. Depreciation policy, Depreciation of capital assets,
Causes of depreciation, Straight line method and declining balance method.

Module III:
Cost concepts, Elements of costs, Preparation of cost sheet, Segregation of costs into
fixed and variable costs. Break-even analysis-Linear approach(simple numerical
problems to be solved). Banking: Meaning and functions of commercial banks; functions
of Reserve Bank of India. Overview of Indian Financial system.

Text Books:
1. Engineering Economics, 4th ed. by J L Riggs,D D Bedworth, and S U Randhwa,
McGraw-Hill.
2. Principles of Economics by D M Mithani, Himalaya Publishing.

Reference Books:
1. Engineering Economics and Costing, 2nd ed. by S Mishra, PHI.
2. Engineering Economy, 16th ed. by W G Sullivan, E M Wicks, and C P Koelling,
PHI.
3. Engineering Economics, 2nd ed. by R Panneerselvam, PHI.
4. Managerial Economics, 2nd ed. by G Gupta, McGraw-Hill.
5. Cost Accounting, 4th ed. by J Lal and S Srivastava, McGraw-Hill.
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 3rd Semester

POB3E002 ORGANIZATIONAL BEHAVIOR

Module I:
The study of Organizational Behaviour: Definition and meaning, Why study OBLearning
?Nature of Learning, How Learning occurs ? Learning and OB. Foundations of individual
behavior. Personality: Meaning and definition, Determinants of personality, Personality
traits, Personality and OB.Perception: Meaning and definition, Perceptual process,
Importance of perception in OB. Motivation: Nature and importance, Herzberg’s Two
Factor Theory, Maslow’s Need Hierarchy Theory, Alderfer’s ERG Theory, Evaluations.

Module II:
Organizational Behaviour Process: Communication – Importance, Types, Gateways and
Barriers to Communication, Communication as a tool for improving Interpersonal
Effectiveness, Groups in Organizations – Nature, Types, Why do people join groups,
Group Cohesiveness and Group Decision-making Managerial Implications, Effective
Team Building. Leadership-Leadership & Management, Theories of Leadership-Trait
theory, Leader Behaviour theory, Contingency Theory, Leadership and Followership,
How to be an effective Leader, Confict-Nature of Conflict and Conflict Resolution. An
Introduction to Transactional Analysis (TA).

Module III:
Organization: Organizational Culture – Meaning and Definition, Culture and
Organizational Effectiveness. Introduction to Human Resource Management-Selection,
Orientation, Training and Development, Performance Appraisal, Incentives
Organizational Change – Importance of Change, Planned Change and OB techniques.
International OrganisationalBehaviour – Trends in International Business, Cultural
Differences and Similarities, Individual and Interpersonal Behaviour in Global
Perspective.

Text Books:
1. Organizational Behavior: Human Behavior at Work by J W Newstrom and K
Davis, McGraw-Hill.
2. OrganisationalBehaviour: Text, Cases & Games, 11th ed. by K Aswathappa,
Himalaya Publishing House.

Reference Books:
1. Organizational Behavior, 15th ed. by S P Robbins, T A Judge, and N Vohra,
Pearson.
2. Organizational Design for Excellence by P N Khandwalla, McGraw-Hill.
3. Organizational Behaviour: Text and cases, 2nd ed. by U Sekaran, McGraw-Hill.
4. Organizational Behavior: Eemerging knowledge and practice for the real
world, 5th ed. by S McShane, M A V Glinow, and R Sharma, McGraw-Hill.
5. Organizational Behaviour, 2nd ed. by D K Bhattachayya, Oxford University Press.
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 3rd Semester

PCE3D001ADVANCED FLUID DYNAMICS

(MAJOR)
Module I:
Properties of fluids and multiphase flow: Fluids and fluid properties, Kinematics:
Motion, streamlines, pathlines, and streaklines. Newtonian, non-Newtonian, and non-
viscous fluids. Continuity equation in cartesian, cylindrical, and spherical coordinates.
Derivation of general momentum equation for Newtonian fluids in cartesian
coordinates.

Module II:
Eulers’ equation, principles of rotational and irrotational flow, velocity potential,
Bernoulli’s equation, Laplace equations, stream function, vorticity, Cauchy-Rieman
equation. Analytical solutions for simple two dimensional incompressible, irrotational
fluid flows: flow along two inclined plates, point source or sink in an infinite fluid.
Stokes law of viscosity, Navier-stokes equation, creeping flow around a solid sphere,
expression for total drag.

Module III:
Turbulent flow: Transition to turbulence, Prandtl’s mixing length, Turbulence models.
Boundary layer on immersed bodies, two dimensional boundary layer equation, laminar
boundary layer on flat plate (Blasius’ exact solution), Von-Karmann’s integral
momentum equation, boundary layer separation flow and pressure drag, Flow of
compressible fluids, thermodynamic considerations, continuity and momentum
equation for one dimensional compressible flow, one dimensional normal shock, flow
through fluidized beds. Navier-Stokes equation and various approaches of simulation
(stream velocity, primitive variable).

Reference Books:
1. Introduction to Fluid Mechanics,8th ed. by RWFox, ATMcDonald, and
PJPritchard, John Willey& Sons.
2. Fluid Dynamics and Heat Transfer by JGKnudsen and DLKatz, McGraw-Hill.
3. Transport Phenomena, 2nd ed. by RBBird, WEStewart, and ENLightfoot, John
Wiley and Sons.
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 3rd Semester

PCE3G001 SOLAR ENERGY ENGINEERING

(Minor)

Module I:
Sources of radiation, solar constant, solar charts, Measurement of diffuse, global and
direct solar radiation: pyrheliometer, pyranometer, pyregeometer, net pyradiometer-
sunshine recorder.

Module II:
Solar non-concentrating collectors: Design considerations. Classification, Air and liquid
heating collectors. Derivation of efficiency and testing of flat plate collectors. Analysis of
concentric tube collector. Solar green house: Design and classification. Concentrator
mounting: Focusing solar concentrators, Heliostats.

Module III:
Solar powered absorption A/C system, water pump, chimney, drier, dehumidifier, still,
cooker. Photo-voltaic cell: Characteristics, cell arrays. Power electric circuits for output
of solar panels, choppers, inverters, batteries, charge regulators, construction concepts.
Energy Storage: Sensible, latent heat, and thermo-chemical storage, pebble bed, etc.
Solar ponds.

Text Books:
1. Principles of Solar Engineering 2nd ed. by DY Goswami, F Kreith, and JFKreider,
Taylor & Francis.
2. Fundamentals for Solar Energy Conversion by EE Anderson, Addison-Wesley
Publ. Co.

Reference Books:
1. Solar Engineering of Thermal Processes by J A Duffie and W A Beckman, John
Wiley.
2. Fundamentals of Renewable Energy Sources by GNTiwari and
MKGhosal,Narosa Publishing House.
3. Energy Studies 2nd ed. by WShepherd and DWShepherd, Imperial College Press. 12
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 4th Semester
Fourth Semester
Theory Practical
Code Course Name Hours/ Credit University Internal Hours/ Credit Marks
Week Theory Marks Evaluation Week Practical
L/T L/T
HS Purely Applied 3-0 3 100 50
Mathematics for
Specific Branch of
Engineering
PC Mass Transfer-II 3-0 3 100 50 2 1 50
PC Heat Transfer 3-0 3 100 50 2 1 50
PC Chemical Engineering 3-0 3 100 50 2 1 50
Thermodynamics
PC Fuel & Energy 3-0 3 100 50 2 1 50
Technology
HS Engineering Economics/ 2-1 3 100 50
Organizational
Behaviour
*Skill Project and Hands 6 3 100
on
Total 18 18 600 300 14 7 300
Total Marks: 1200
Total Credits: 25
Honours Advance 4 4 100 50
Mass
Transfer
Minor Separation
Process

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 4th Semester
Semester : 4th
--------------
1. PCE4D001 Honours(CP) 4-0-0 4
2. PMA4E001 HS(CP) Applied Mathematics - III 3-0-0 3
3. PEK4E002 HS(O1) Engineering Economics 3-0-0 3
4. POB4E003 HS(O1) Organizational Behavior 3-0-0 3
5. PCE4I101 PC(CP) Mass Transfer - II 3-0-1 4
6. PCE4I102 PC(CP) Heat Transfer 3-0-1 4
7. PCE4I103 PC(CP) Chemical Engineering Thermodynamics 3-0-1 4
8. PCE4I104 PC(CP) Fuel & Energy Technology 3-0-1 4
9. PCE4I201 PC(CP) Skill Project and Hands on 0-0-3 3
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 4th Semester

PCI4E001 APPLIED MATHEMATICS - III

Module-I
Complex Analysis:
Analytic function, Cauchy-Riemann equations, Complex integration: Line integral in the
complex plane, Cauchy’s integral theorem, Cauchy’s integral formula, Derivatives of
analytic functions, Taylor’s series, Maclaurin’s series, Laurent’s series, Singularities and
zeros.

Module-II
Complex Analysis:
Residue integration method, evaluation of real integrals
Numerical Methods:
Errors of numerical results, error propagation,., Lagrange Interpolation, Newton divided
difference interpolation, Newton’s forward and backward interpolation, Spline
interpolation.

Module-III
Numerical Methods:
Numerical integration: The trapezoidal rule, The Simpson’s rules, Gauss Integration
formulas.
Solution of ordinary differential equation: Euler’s method, Improvement of Euler’s
method, Runge-Kutta methods, multi step methods, Methods for system and higher
order ordinary differential equations.

Module-IV
Probability Theory and Its Applications: Probability, Random variables, Probability
distributions, Mean and variance; Features of Probability Distribution: Binomial,
Poisson, Uniform and Normal distribution, Distribution of several random variables.

Statistical Techniques and Its Applications: Scope of Statistics, Random sampling,

Sampling Distribution,Correlation analysis, Regression Analysis,Fitting Straight Lines,
Estimation of Parameters, Statistical Hypothesis.

Text books:
1. E. Kreyszig,” Advanced Engineering Mathematics:,Tenth Edition, Wiley India
2. S.Pal and S.C. Bhunia, “Engineering Mathematics” Oxford University Press
3.Jay L. Devore, “Probability and Statistics for Engineering and Sciences”, Seventh
Edition, Thomson/CENGAGE Learning India Pvt. Ltd

Reference books:
1. E.B. Saff, A.D.Snider, “Fundamental of Complex Analysis”, Third Edition, Pearson
Education, New Delhi
2. P. V. O’Neil, “Advanced Engineering Mathematics”, CENGAGE Learning, New
Delhi
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 4th Semester

PCE4I101 MASS TRANSFER - II

Module I:
Liquid-liquid operations: Extraction: Introduction, liquid-liquid equilibrium, analytical and
graphical solutions for single and multistage operations, continuous counter-current
operation without and with reflux, fractional extraction, equipment for liquid contacting
operations, single stage, multistage and continuous contacting equipments.

Module II:
Leaching: Steady and unsteady state operations, equipments, analytical methods for single
and multistage operations.

Adsorption: Theory of adsorption, Industrial adsorbents, adsorption equilibrium –

isotherms and isobars, Freundlichisotherm, single and multistage operations, Ion-Exchange.

Module III:
Drying: Equilibrium, drying rate curve, batch and continuous drying,time of drying and
calculations, mechanism of batch drying, equipments for batch and continuous drying
operations, design of dryers.

Reference Books:

1. Mass Transfer Operations by R E Treybal, McGraw Hill.

2. Unit Operations of Chemical Engineering, 7th ed. by W L McCabe, J C Smith, and P
Harriott, McGraw-Hill.
3. Design of Equilibrium Stage Processes by B D Smith, McGraw-Hill.
4. Principles of Mass Transfer and Separation Processes by B K Dutta, PHI.
5. Mass Transfer Operations by ASuryanarayana, New Age International.

MASS TRANSFER - II LAB

1. To draw the ternary diagram for a system of water – acetone – chlorobenzene.
2. Extraction of oil from a sample of mustard cake.
3. Drying of solids in a tray dryer under forced draft condition.
4. Drying of solids in a rotary dryer.
5. To study the performance of a Swenson-Walker crystallizer and to determine
the crystal yield and the efficiency of crystallizer.
6. To determine that mass transfer coefficients for the given system using the
experimental setup.
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 4th Semester

PCE4I102 HEAT TRANSFER

Module I:
Introduction: Modes of heat transfer, basic laws of heat transfer, analogy between heat
flow andelectrical flow.Conduction: The Fourier heat conduction equation, Steady-state
one dimensional heat conduction through plane wall, cylindrical wall, spherical wall and
composite structures. Heat transfer from extended surfaces, unsteady state heat
conduction through a semi-infinite slab, critical insulation of thickness.

Module II:
Convection: Introduction to convection: Natural and forced convection, Natural
Convection: Grashoff number, natural convection from vertical and horizontal surfaces.
Forced convection, The convective heat transfer coefficient, introduction to thermal
boundary layer,Dimensionless numbers in heat transfer and their significance,
Dimensional analysis, Analogy between heat and momentum transfer,Reynold’sPrandtl
and Colburn analogies. Heat transfer to liquid metals,heat transfer for tubes in cross
flow.

Heat exchangers: Types of heat exchangers, log-mean temperature difference,energy

balances, overall heat transfer coefficients,heat exchanger effectiveness, Fouling factors,
design and description of heat transfer equipment.

Module III:
Evaporation: Types of evaporators, capacity and economy of evaporators,boiling point
elevation and Duhring’s rule,material and energy balance for evaporators, methods of
feeding, capacity and economy of multiple effect evaporators.

Heat Transfer with phase change: Heat transfer from condensing vapours: film and
drop-wise condensation, derivation and practical use of Nusselt equation, condensation
of superheated vapours, effect of non-condensable gases on ratio of condensation. Heat
transfer to boiling liquids. Boiling of a saturated liquids. Maximum heat flux and critical
temperature, minimum flux and film boiling, sub cooled boiling.

Module IV:
Heat transfer by radiation: Thermal radiation, black body radiation, Kirchhoff’s law,
emissivity, grey body, laws of black body radiation, geometric factor, radiation in
enclosures with black surfaces and grey surfaces. Large parallel plates, concentric,
cylindrical, spheres. Combined heat transfer by conduction, convection, and radiation.

Text Book:

1. Unit Operations of Chemical Engineering, 7th ed. by W L McCabe, J C Smith, and P

Harriott, McGraw-Hill.

Reference Books:
1. Process Heat Transfer by D Q Kern, McGraw-Hill.
5

2. Heat Transfer: A Practical Approach, 2nd ed. by Y A Cengel, McGraw-Hill.

Page

3. Heat Transfer, 10th ed. by J Holman and SBhattacharyya, McGraw-Hill.

B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 4th Semester

HEAT TRANSFER LAB

1. To find the overall heat transfer coefficient in parallel and counter-
current heat exchanger.
2. To determine the overall heat transfer coefficient of shell and tube heat
exchanger.
3. To study and operate single effect evaporator and to find its steam economy.
4. To calculate the overall heat transfer coefficient in vertical and
horizontal condenser.
5. To find the thermal conductivity of composite walls.
6. To find the overall heat transfer coefficient, fin effectiveness, and fin
efficiency for finned tube heat exchanger.
7. Determination of heat transfer coefficient for film wise and drop wise
condensation.
8. To determine the emissivity of the non–black surface and compare with
the black body.
9. Determination of thermal conductivity of liquid.
10. To determine the Stefan Boltzmann’s constant.

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 4th Semester

PCE4I103 CHEMICAL ENGINEERING THERMODYNAMICS

Module I:
The first law of thermodynamics, the thermodynamic state and state function, constant
volume and constant pressure processes.
Properties of pure fluids: PVT behavior of pure substances, virial equations of state, the
ideal gas, applications of virial equations, cubic equation of state, theorem of
corresponding states.
Second Law: Entropy, work function, phase rule, introduction to third law.

Module II:
Criteria of phase equilibrium, ideal solutions (use of Raoult’s) law, generation of Pxy and
Txy diagram for ideal solution.
Non-ideal behavior, partial properties, Gibbs-Duhem equation, calculation of fugacity
coefficient using generalized correlation, excess Gibbs energy, Lewis-Randall rule,
activity coefficient for VLE data.

Module III:
Solution thermodynamics: Thermodynamic properties and VLE from equation of state,
properties of fluid mixtures using Redlich-Kwong equation of states.
Chemical reaction equilibrium: Criteria to chemical reactions, Gibbs energy change
equilibrium constant, effect of temperature, calculation for single reaction in
homogeneous and heterogeneous systems.

Text Books:
1. Introduction to Chemical Engineering Thermodynamics, 7th ed. by J M Smith, H C
Van Ness, and M M Abbott, McGraw-Hill.
2. Textbook of Chemical Engineering Thermodynamics, 2nd ed. by K V Narayanan,
PHI, 2013.
Reference Books:
1. Chemical, Biochemical, and Engineering Thermodynamics, 4th ed. by S I Sandler,
Wiley.
2. Engineering and Chemical Thermodynamics, 2nd ed. by M D Koretsky, Wiley.
3. Introductory Chemical Engineering Thermodynamics, 2nd ed. by J R Elliott and C T
Lira, PHI.
4. Fundamentals of Chemical Engineering Thermodynamics, 1st ed. by T Matsoukas,
PHI.
5. Chemical Engineering Thermodynamics by Y V C Rao,Orient Blackswan.
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 4th Semester

PCE4I104 FUEL AND ENERGY TECHNOLOGY

Module I:
Fuels: Solid Fuels: Coal - Origin, chemical composition, calorific value, classifications,
Characteristics& distribution of Indian coals, storage and spontaneous combustion ofcoal,
coal washing and blending, petrographic constituents of coal, carbonization of
coal,manufacture and properties of metallurgical coke, recovery of by-products.

Module II:
Liquid Fuels: Origin and composition of crude oil, crude oil distillation and its products with
special reference to gasoline, kerosene and diesel oil, cracking and reforming, coaltar
distillation products,Shale oil.
Gaseous Fuels: Natural gas, coal gas,coke oven and blast furnace gas, manufacture of water
gas and producer gas, carbureted water gas.

Module III:
Synthetic Fuels: Hydrogenation of coal, Fischer–Tropsch synthesis.
Nuclear Fuels: Introduction, nuclear fuels and nuclear reactors, moderators and structural
materials.Introduction to renewable energy sources.

Module IV:
Combustion: Combustion of solids fuels, calculation of volumes and weights of air necessary
for combustion of fuels, gas analysis.

Text Books:
1. Fuels and Combustion, 3rd ed. by S Sarkar, Universities Press.
2. Elements of Fuels, Furnaces & Refractories by O P Gupta, Khanna.

Reference Books:
1. The Elements of Fuel Technology, 2nd ed. by G W Himus, L Hill.
2. Fuel Solid, Liquid and Gaseous, 4th ed. by J S SBrame and J G King, Edward Arnold.

FUEL TECHNOLOGY LAB

1. Determination of moisture content, volatile matter, carbon, and ash by
Proximate Analysis method.
2. Determination of Cloud & Pour Point of an oil sample.
3. Determination of Flash &Fire Point of an oil sample.
4. Determination of Moisture Content of an oil sample by Dean & Stark Apparatus.
5. Determination of Carbon Residue of an oil sample by Conradson’s Apparatus.
6. Determination of Aniline Point of an oil sample.
7. Determination of Viscosity of an oil sample by open cup apparatus.
8. Determination of Viscosity of an oil sample by closed cup apparatus.
9. Determination of Calorific Value of a fuel sample by Bomb Calorimeter.
10. Determination of washability characteristics of the supplied sample of Coal
using Float and Sink test.
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 4th Semester

PCE4D001 ADVANCED MASS TRANSFER (Major)

Module I:
Characteristic of equilibrium stage and flash calculations. Study of different types of
equilibrium cascadeconfigurations and its degrees of freedom analysis. Algebraic
method to determine the number of equilibriumstages. Calculation of stage
efficiency,tray diameter, pressure drop, and mass transferrate based method todesign a
packed column.
Module II:
Scale up of a column from laboratory data. Estimation of distillation column
efficiencyusing performance data and to develop its empirical correlation.Scale up of
distillation column. Rate basedmethod for packed distillation column.
Module III:
Approximate methods for multicomponent, multistage separations. Useof residue curve
for the conceptual design of distillation columns. Pressure swing and azeotropic
distillation.Rate based models for distillation. Modeling of batch distillation. Modeling
and simulation of absorption andleaching processes.
Module IV:
Diffusion in non-ideal system and development of generalized Maxwell-Stefan
formulation,Study of generalized Fick’s law, Estimation of binary and multicomponent
Diffusion Coefficients, Study ofinterphase mass and energy transfer.
Reference Books:
1. Separation Processes and Principles, 3rd ed. by JD Seader, E J Henley, and
D K Roper, John Willey& Sons.
2. Multicomponent Mass Transfer by R Taylor and R Krishna, Wiley-Interscience.
3. Principles and Modern Applications of Mass Transfer Operations, 2nd ed.
by J. Benitez, Willey-Interscience.
4. Design of Equilibrium Stage Processes by B D Smith, McGraw-Hill.

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 4th Semester

SEPARATION PROCESSES (Minor)

Module I:
An overview of separation methods, separation from liquids, gasses and vapors, solids.
Separation methods in bioprocessing: aqueous two-phase separation, Reverse micelle
extraction.

Module II:
Membraneseparations: Definition of a membrane and membrane processes such as:
microfiltration, reverse osmosis, ultrafiltration,dialysis, electrodialysis, gas permeation,
andpervaporation. Characterization of membrane such as colloidal
morphology,permeability and permeselectivity. Membrane modules such as plate and
frame device, spiral wound, tubular, andhollow-fiber. Membrane technology in gas
separation, biotechnology, and in food and biochemical industry.

Module III:
Ion-Exchange: Mechanism, ion-exchange media, equilibrium. Equipment and design
procedure and industrial applications. Adsorption as a separation process.
Thermodynamics of adsorption: basic relationship, representation, correlation and
prediction of single component adsorption equilibrium data and extension to multi-
componentadsorption. Equilibrium calculations. Isotherm expression of gas adsorption.

Module IV:
Chromatography separation: Fundamentals of HPLC, Chromatographic column,
Development of gradient-elution separations. Basic principles of capillary electro
chromatography, mobile phase composition, Stationery phases used in CEC; Solid
separation processes: Physical properties of solids, classification of powders, particle
size distributions, particle density, bulk density and porosity, forces of adhesion.
Separation of particulates and powders.

Reference Books:
1. Separation Processes and Principles, 3rd ed. by JD Seader, E J Henley, and D K
Roper, John Willey& Sons.
2. Principles of Mass Transfer and Separation Processes by B K Dutta, PHI.
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 4th Semester

PROCESS INSTRUMENTATION LAB

1. Study the operation of conductivity meter, measuring specific conductance of solutions
& determining the compositions of unknown solution from calibrated plot.

2. Study of the characteristics of different thermocouples & RTD sensors.

3. Determination of transient response of a vapor pressure & bimetallic thermocouple.

4. Determination of dissolved oxygen using DO meter.

5. Determination of gas-fraction in gas-liquid mixture using conducting probe.

6. Concentration analysis of hydrogen using gas-liquid chromatograph.

7. Concentration analysis using U-V-visible spectrophotometer & to study its principle of

operation.

8. Composition analysis using digital refractometer& to study the principle of operation.

9. Measurement of Humidity using hair hygrometer & to study its principle.

10. Pressure measurement using different pressure gauges, U-tube manometer, pressure
transducer and study their characteristics.

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 5th Semester
Fifth Semester
Theory Practical
Code Course Name Hours/ Credit University Internal Hours/ Credit Marks
week Theory Marks Evaluation week Practical
L/T L/T
PC Transport Phenomena 3-0 3 100 50 2 1 50
PC Process Equipment 3-0 3 100 50 2 1 50
Design
PC Chemical Reaction 3-0 3 100 50 2 1 50
Engineering
PE Process 3-1 4 100 50
Instrumentation/Process
Simulation & Modelling
OE Biotechnology/Food 3-1 4 100 50
Biotechnology
PC Advance Lab-I 8 4 200
Total 17 17 500 250 14 7 350
Total Marks: 1100
Total Credits: 24
Honours Advance Heat 4 4 100 50
Transfer
Minor Batteries and
Fuel Cells

Laboratories :

1. Biotechnology Lab 2.Process Equipment Design Lab

3. Chemical Reaction Engineering Lab 4. Advanced Chemical Engg. Lab-I

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 5th Semester
Semester : 5th
--------------
1. PCE5D001 Honours(CP) 4-0-0 4
2. PCE5H001 OE(O2) Biotechnology 4-0-0 4
3. PCE5H002 OE(O2) Food Biotechnology 4-0-0 4
4. PCE5I101 PC(CP) Transport Phenomena 3-0-1 4
5. PCE5I102 PC(CP) Process Equipment Design 3-0-1 4
6. PCE5I103 PC(CP) Chemical Reaction Engineering 3-0-1 4
7. PCE5I201 PC(CP) Advance Lab - I 0-0-4 4
8. PCE5J001 PE(O3) Process Instrumentation 4-0-0 4
9. PCE5J002 PE(O3) Process Simulation & Modeling 4-0-0 4
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24
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 5th Semester

PCE5I101 TRANSPORT PHENOMENA

Module I:
Momentum Transport: Viscosity and the mechanism of momentum transport, Shell
momentum balances and Velocity distributions in laminar flow. The equation of changes for
Isothermal systems. Velocity distributions with more than one independent variable. Inter
phase transport in isothermal systems.

Module II:
Energy Transport: Thermal conductivity and mechanism of energy transport, shell energy
balances and temperature distributions in solids and laminar flow, the equations of change
for non - isothermal systems, temperature distribution with more than one independent
variable, Inter phase transport in non-isothermal systems.

Module III:
Mass Transport: Diffusivity and the mechanism of mass transport, concentration
distributions in solids and laminar flow, the equations of change for multi component
systems. concentration distributions with more than one independent variable, inter phase
transport in non-isothermal mixtures.

Text Book:
1. Transport Phenomena, 2nd ed. by R B Bird, W E Stewart, and E N Lightfoot, John Wiley
& Sons.

Reference Books:
1. Fundamentals of Momentum, Heat, and Mass Transfer, 5th ed. by J Welty, C E Wicks,
and R E Wilson, and G L Rorrer, Wiley.
2. Introduction to Transport Phenomena: Momentum, Heat, and Mass by B Raj, PHI.

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 5th Semester

PCE5I102 PROCESS EQUIPMENT DESIGN

Following books are allowed in the examination:
1. Joshi's Process Equipment Design, 5th ed. by V VMahajani and S B Umarji, Trinity Press.
2. Coulson and Richardson's Chemical Engineering: Chemical Engineering Design, Vol. 6,
2nd ed. by J M Coulson and J F Richardson, Editor – R K Sinnott, Butterworth-
Heinemann.

Module I:
Design of pressure vessels and storage tanks, rotary dryers, isothermal reactors.

Module II:
Detailed process design of Heat Exchangers:Concentric tube, Shell and tube types,
Condensers: Condenser coolers and desuperheater condensers for single vapour only.
Evaporators: Single and multieffects.

Module III:
Packed towers: For binary systems without reactions.
Distillation columns: For binary mixtures along with tray hydraulics.

Text Books:
1. Process Heat Transfer by D Q Kern, McGraw-Hill.
2. Mass Transfer Operations by R E Treybal, McGraw Hill.

Reference Books:
1. Perry's Chemical Engineers' Handbook, 8th ed. by D W Green and R H Perry, McGraw-
Hill.
2. Unit Operations of Chemical Engineering, 7th ed. by W L McCabe, J C Smith, and P
Harriott, McGraw-Hill.

PROCESS EQUIPMENT DESIGN LAB

Detailed process design of the following:
1. Design of shell and tube heat exchangers
2. Design of concentric tubes
3. Design of single effect evaporators
4. Design of multiple effect evaporators
5. Design of absorption column (packed tower)
6. Design of distillation column (plate tower)
7. Design of rotary drier
8. Design of storage tanks
9. Design of supports like leg, skirt, and saddle support
10. Design of flanges as per ASME and ISI specification
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 5th Semester

PCE5I103 CHEMICAL REACTION ENGINEERING

Module I:
Introduction and overview of the subject, kinetics of homogeneous reactions, elementary
and non-elementary reactions, concentration and temperature dependent term of a rate
equation, collision theory, transition - state theory and Arrhenius theory. Interpretation of
batch reactor data for both reversible and irreversible reactions. Various methods of
analysis of batch reactor data (including variable volume and variable pressure (data).
Isothermal batch reactor design.

Module II:
Homogeneous flow reactors: Design equations for steady state plug flow reactor (PFR) and
steady state continuous stirred tank reactor (CSTR), data analysis in flow reactors, mean
residence time, space time, space velocity. Combined reactors, reactors in parallel and in
series, size comparison of single reactors, recycle reactors.

Module III:
Design for parallel reactions, product distributions, contacting patterns for reactions in
parallel, quantitative treatment of product distribution, selectivity, multiple reactions, and
qualitative treatment of batch, PFR, and mixed reactors.
Basics of non-ideal flow, RTD, age distribution of fluid, pulse experiment, relationship
between F and E curves.

Text and Reference Books:

1. Chemical Reaction Engineering, 3rd ed. by O Levenspiel, Wiley.
2. Elements of Chemical Reaction Engineering, 4th ed. by H S Fogler, PHI.
3. Chemical Reactor Analysis and Design, 3rd ed. by G F Froment, K B Bischoff, and J De
Wilde, Wiley.
4. Chemical Engineering Kinetics, 3rd ed. by J M Smith, McGraw-Hill.

CHEMICAL REACTION ENGINEERING LAB

1. To determine the order and value of the rate constant for the liquid reaction of caustic
soda and ethyl acetate in a batch reactor.
2. To determine the rate constant for a reaction of ethyl acetate with sodium hydroxide in
a PFR.
3. To determine the residence time distribution in the given configuration for pulse and
step inputs.
4. To evaluate the performance of a series of mixed reactors for the given system of NaOH
and CH3COOC2H5.
5. To perform the kinetic studies to establish the rate constant using CSTR.
6. To study the performance of an isothermal batch reactor.
7. To study the reaction kinetics in a fluidized/packed bed reactor.
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 5th Semester

PCE5J001 PROCESS INSTRUMENTATION

Module I:
Basic concepts and qualities of measurement, Level measurement: Methods of liquid level
measurement, Direct methods, Hook-type level indicator, sight glass, Float-type level
indicator, Displacer level detectors, Indirect methods, Hydrostatic pressure type, Pressure
gauge method, Air bellows, Air purge system, Liquid purge system, Electrical methods.

Module II:
Flow Measurement: Methods of flow measurement, Inferential flow measurement, Quantity
flowmeters, Mass flowmeters, Calibration of flowmeters, Selection of flowmeters.
Pressure measurement: Pressure, Methods of pressure measurement, Manometers, Elastic
pressure transducers, Measurement of vacuum, Force-balance pressure gauges, Electrical
pressure transducers, Pressure switches, Calibration of pressure measuring instruments,
Maintenance and repair of pressure measuring instruments, Troubleshooting.

Module III:
Temperature measurement: Temperature, Temperature scales, Methods of temperature
measurement, Expansion temperature, Filled-system thermometers, Electrical temperature
instruments. Pyrometers: Radiation and optical.
Methods of composition analysis: Absorption spectroscopy, Emission spectroscopy, Mass
spectroscopy.

Text and Reference Books:

1. Industrial Instrumentation by D P Eckman, CBS.
2. Instrumentation: Devices and Systems, 2nd ed. by C Rangan, G Sarma, and V S V Mani,
McGraw-Hill.
3. Principles of Measurement Systems, 3rd ed. by J P Bentley, PHI.
4. Industrial Instrumentation and Control, 3rd ed. by S K Singh, McGraw-Hill.

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 5th Semester

PCE5J002 PROCESS SIMULATION AND MODELLING

Module I:
Modeling: Fundamentals of mathematical models and formulation – Continuity equation,
Equation of motion, Transport equations, Energy equation, Equations of state, Equilibrium,
Chemical kinetics and their applications; Lumped and distributed parameter models – Fluid
systems, C.S.T.R. (single, series, isothermal, constant hold up, variable hold up, gas phase
pressurized and non-isothermal), Single component vaporizer, Multi-component flash
drum, Batch reactor, Reactor with mass transfer, Ideal binary distillation column, Batch
distillation, Heat exchanger, etc.

Module II:
Optimization: Single variable optimization (analytical, dichotomous search, fibonacci,
golden section, regulafalsi), Multivariable optimization (analytical, geometric programming,
linear programming), Convergence methods (Newton’s methods, direct substitution,
Wegstein’s method).

Module III:
Simulation: Techniques of digital simulation – Information flow, from process to
information flow diagram, From information flow diagram to numerical form, Recycles,
Calculation of a recycle set, etc.

Text Books:
1. Process Modeling, Simulation, and Control for Chemical Engineers, 2nd ed. by W L
Luyben, McGraw-Hill.

Reference Books:
1. Process Plant Simulation by B V Babu, Oxford University Press.
2. Engineering Optimization: Theory and Practice by S S Rao, New Age.
3. Process Control: Modeling, Design and Simulation, 1st ed. by B W Bequette, PHI.
4. System Modeling and Simulation: An Introduction by FLSeverance, Wiley.

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 5th Semester

PCE5H001 BIOTECHNOLOGY
Module I:
Introduction and application of microbiology, Structure and functioning of bacterial cell,
Classification and Identification criteria for bacteria. Nutritional requirements and
nutritional types of bacteria.

Module II:
Isolation of micro-organisms, pure culture techniques and cultural characteristics. Bacterial
growth, measurements and reproduction.

Module III:
Fundamentals of microbiology ecology and ecosystems, microbial associations and
interactions. Applications of microbiology.

Module IV:
Types of bacteria in water, sanitary examination of water, water purification, average
disposal and sewage purification.

Text and Reference Books:

1. Microbiology, 4th ed. by MJPelczar, RDReid, and ECSChan, McGraw-Hill.
2. Microbial Ecology: Fundamentals and Applications, 4th ed. by R M Atlas and R Bartha,
Benjamin Cummings.

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 5th Semester

PCE5H002 FOOD BIOTECHNOLOGY

Module I:
Food quality and Production technology: Analysis of food, major ingredients present in
different product, Food additives: colour, flavour, vitamins, Single cell protein, mushroom,
Fermentative production of food, Pickling and alcoholic beverages, genetically manipulated
crops based food, oriental foods, probiotics, prebiotics, and synbiotics in food products.

Module II:
Technology for improved process: Enzyme in bakery, fermented cereal products, Enzymes
in fat/oil industries, Protease in cheese making, enzymes in beverage production,
Utilization of food waste for production of value added products, enzymes in sugar syrup,
genetically modified food.

Module III:
Food spoilage and control: Spoilage of food, Microbiology of water, meat, milk, vegetables,
Microbial safety of food products, Chemical safety of food products, heavy metal, fungal
toxins, pesticide and herbicide contamination, Food preservatives and additives, Post-
harvest technology for food preservation. Technology – canning, dehydration,
ultrafiltration, sterilization, irradiation etc.

Text and Reference Books:

1. Modern Food Microbiology, 7th ed. by J M Jay, M J Loessner, and D A Golden, Springer.
2. Food Microbiology, 5th ed. by W C Frazier and D C Westhoff, McGraw-Hill.
3. Prescott & Dunn's Industrial Microbiology by G Reed, CBS.
4. Technology of Food Preservation, 4th ed. by N W Desrosier and J N Desrosier, Avi
Publishing Co Inc.
5. Introduction to Food Engineering, 5th ed. by R P Singh and D R Heldman, Academic
Press.

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 5th Semester

PCE5D001 ADVANCED HEAT TRANSFER (Major)

Module I:
Conduction: Steady and unsteady state heat conduction. Unsteady state heating and cooling
of solid objects. Transient heat conduction in bodies with finite internal and surface
resistance, Transient heat conduction charts,Insulation design and selection.

Module II:
Convection: Heat transfer coefficient, Dimensional analysis in convective heattransfer, Heat
transfer during laminar and turbulent flow in closed conduits, empirical correlation, Heat
transfer inlaminar and turbulent flow over a flat plate, Heat transfer in liquid metals,
Analogy between momentum and heattransfer, Heat transfer with phase change: Boiling
and condensation heat transfer.

Module III:
Recent developments in heatexchangers: Heat Transfer Augmentation, Recent
developments in the design of compact heat exchangers: Featuresof Plat Fin and Tube Fin
heat exchangers, Construction, Heat transfer and pressure drop, Analysis of plate fin
andtube fin heat exchangers.

Reference Books:
1. Heat Transfer: Principles and Applications by B K Dutta, PHI.
2. Heat Transfer, 8th ed. by JP Holman, McGraw-Hill.

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 5th Semester

BATTERIES & FUEL CELLS (Minor)

Module I:
Storage Cell Technologies: Storage cell fundamentals, Characteristics. Emerging trends in
batteries. Specifications, Storage cell definitions & specifications, Carbon-zinc & alkaline
cells, Mercury, zinc-air, and silver oxide button cells, Lead-acid, Edison, NiCad&NiMH cells,
Lithium technology, Applications of storage cell.

Module II:
Industrial Fuel cell fundamentals.Alkaline fuel cell, Acidic fuel cells, SOFC. Emerging areas in
Fuel cells. Fuel cell outlook, Sources, comments, & revision history, Applications: Industrial
and commercial.

Reference Books:
1. Linden’s Handbook of Batteries, 4th ed. by T B Reddy, McGraw-Hill.
2. Principles of Fuel Cells by XLi, CRC Press.
3. Fuel Cells: Principles and Applications by B Viswanathan and M A Scibioh, CRC Press

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 5th Semester

BIOTECHNOLOGY LAB
1. Different sterilization and inoculation techniques.
2. Preparation of various types of media.
3. Effect of pH, substrate concentration, and temperature on cell growth.
4. Determination of volumetric mass transfer co-efficient.
5. Determination of mixing time and size and density of the microbial cells.
6. Determination of thermal death rate constant.
7. Preparation of immobilized whole cell system.
8. Substrate degradation, cell growth, and product formation kinetics using free cells and
whole cell immobilization.
9. Treatment of sample waste water in a bioreactor.
10. Production of acetic acid using fermentor.

ADVANCED CHEMICAL ENGINEERING LAB - I

1. Hydrodynamic studies of inverse fluidized bed.
2. Determination of surface area using BET apparatus.
3. Determination of BOD and COD in the water sample.
4. Determination of concentration of dyes using spectrophotometric analysis.
5. Determination of the composition of the gas using gas chromatograph.
6. Optimization of shell & tube and double pipe heat exchanger using ASPEN PLUS.
7. Determination of viscosity of slurry using Brook-field viscometer & to study its
principle of operation.
8. Particle-size analysis using Particle size analyzer & to study its principle of operation.
9. Study and operation of a magnetic separator and thereby finding its efficiency of
separation.
10. Study and operation of Emulsion polymerization reactor.

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 6th Semester
Sixth Semester
Theory Practical
Code Course Name Hours/ Credit University Internal Hours/ Credit Marks
Week Theory Marks Evaluation Week Practical
L/T L/T
PC Numerical Methods & 3-0 3 100 50 2 1 50
MATLAB
PC Process Dynamics & 3-0 3 100 50 2 1 50
Control
PE Fundamentals of 3-1 4 100 50
Biochemical
Engineering/Fluidization
Engineering
PE Polymer 3-1 4 100 50
Technology/separation
Technology
MC & Environmental Science & 3-0 3 100 50
GS Engineering
OE Industrial Lecture # 3 1 50
HS Business Communication 2-0 1 50 4 2 100
& Skill for Interview # #
MC Yoga 2 1 50
Total 19 18 500 300 13 6 300
Total Marks: 1100
Total Credits: 24
Honours Advance Chemical 4 4 100 50
Reaction
Engineering
Minor Computational Fluid
Dynamics

# To be conducted by the Training & Placement department by inviting experts from the industry. No academician to be
called. Record may be asked by the University for verification. Evaluation to be done by the TPO.

# # To be conducted by the Training & Placement department of the College.

Laboratories :

1. CAD Lab 2. Project on Internet

3. Process Control Lab
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 6th Semester
Semester : 6th
--------------
1. PCE6D001 Honours(CP) 4-0-0 4
2. PCE6E101 HS(CP) Business Communication & Skill for 1-0-2 3
Interview
3. PCE6H301 OE(CP) Industrial Lecture # 0-0-1 1
4. PCE6I101 PC(CP) Numerical Methods & MATLAB 3-0-1 4
5. PCE6I102 PC(CP) Process Dynamics & Control 3-0-1 4
6. PCE6J001 PE(O1) Fundamentals of Biochemical Engineering 4-0-0 4
7. PCE6J002 PE(O1) Fluidization Engineering 4-0-0 4
8. PCE6J003 PE(O2) Polymer Technogy 4-0-0 4
9. PCE6J004 PE(O2) Separation Technology 4-0-0 4
10. PCE6L101 ^SE(CP) Industrial Safety 3-0-1 4
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 6th Semester

PCE6I101 NUMERICAL METHODS& MATLAB

Module I:
Interpolation: Piecewise Linear Interpolation, Piecewise Quadratic Interpolation, Piecewise
Cubic Hermite Interpolation, Piecewise Spline Interpolation.
Numerical Differentiation: First Derivative, Higher Derivatives, Partial Derivative,
Richardson’s Extrapolation. Romberg algorithm for numerical integration.

Module II:
Eigen values and Eigen Vectors: Basic power method, Rayleigh Quotient, Shifted power
method, Accelerating convergence, Inverse power method, Basic QR method, Better QR
method, Findingeigen vectors, Accelerating convergence.
Fourier methods: Discrete Fourier Transforms, Fast Fourier Transforms, Matrix form of
FFT, Algebraic form of FFT, Mixed-Radix FFT.

Module III:
Ordinary Differential Equations: Adams-Bashforth Methods, Adams-Moulton Methods,
Adams Predictor-Corrector methods, Other Predictor-Corrector methods (Simpson’s
method and Milne’s method).

Module IV:
Parabolic Partial Differential Equation: Explicit Method, Implicit method, Crank-Nicolson
method. Hyperbolic Partial Differential Equation: Explicit Method, Implicit method. Elliptic
Partial Differential Equation: Finite-difference method.

Text Books:
1. Applied Numerical Analysis Using MATLAB, 2nd ed. by L V Fausett, Pearson.

Reference Books:
1. Numerical Mathematics and Computing, 7th ed. by E W Cheney and D R Kincaid,
Brooks Cole.
2. Applied Numerical Methods with MATLAB: for Engineers & Scientists, 3rd ed. by S C
Chapra, McGraw-Hill.
3. Applied Numerical Methods for Engineers Using MATLAB and C by R J Schilling and S L
Harris, S Chand. 3
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 6th Semester

PCE6I102 PROCESS DYNAMICS AND CONTROL

Module I:
Response of first order systems, Physical examples of first order systems Response of first
order systems in series, Response of Second order systems, Transportation lag. Control
System, controllers and final control elements, Block diagram of a Chemical Reactor Control
system, Closed loop transfer functions, Transient response of simple control systems.

Module II:
Stability, Root locus, Frequency response, Control system design by frequency response.

Module III:
Cascade control, feed forward control, ratio control, Dead time compensation, internal
model control, controller tuning and process identification, control valves.

Module IV:
Introduction to sampled data controllers, sampled data control of a first order process with
transportation lag, Design of sampled data controllers, Digital computer simulation of
control systems.

Text Books and Reference Books:

1. Process Systems Analysis and Control, 3rd ed. by D R Coughanowr and S E LeBlanc,
McGraw-Hill.
2. Chemical Process Control: An Introduction to Theory and Practice by G
Stephanopoulos, PHI.
3. Process Dynamics & Control by J M Douglas, PHI.
4. Computer Aided Process Control by S K Singh, PHI.
5. Outlines of Chemical Instrumentation Process Control, 3rd ed. by ASuryanarayana,
Khanna Publishers.

PROCESS CONTROL LAB

1. To study the response of a single tank with step change in inlet flow and to find out
time constant graphically.
2. To study the transient response of two interacting tanks with step change in inlet flow
rate and to find out the time constant graphically.
3. To study the transient response of two non-interacting tanks with step change in inlet
flow rate and to find out the time constant graphically.
4. To study the open loop response and the operation of ON-off electronic temperature
controller and determination of its performance to control the temperature of a system
having capacity to store thermal energy.
5. To study the open loop response and the operation of ON-OFF electronic pressure
controller and determination of its performance to control the pressure of a pressure
vessel.
6. To study of effect of PD, PI and PID controller on a temperature control trainer.
7. To study of effect of PD, PI and PID controller on a pressure control trainer.
8. To study the stability of a temperature control trainer.
9. To study the stability of a pressure control trainer.
10. To study the dynamic characteristics of a mercury in glass thermometer.
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 6th Semester

PCE6J001 FUNDAMENTALS OF BIOCHEMICAL ENGINEERING

Module I:
Overview of microbiology, aerobic &anaerobic fermentation processes, fermenter design,
sterilization of microbial medium, kinetics of microbial growth, enzymes and its kinetics,
immobilization of enzymes, chemostats.

Module II:
Transport phenomena in biochemical engineering, heat and mass transfer in bioprocessing,
oxygen transfer in fermenter, monitoring and control of fermentation process.

Module III:
Downstream processing: Recovery and purification of products, allied unit operation for
product recovery, production of biogas and ethanol, effluent treatment by biological
methods.

Text and Reference Books:

1. Biochemical Engineering Fundamentals, 2nd ed. by J E Bailey and D F Ollis, McGraw-
Hill.
2. Biochemical Engineering: Principles and Concepts, 3rd ed. by S T Ahmed Inamdar, PHI.
3. Introduction to Biochemical Engineering, 2nd ed. by D G Rao, McGraw-Hill.
4. Bioprocess Engineering: Basic Concepts, 2nd ed. by M L Shuler and F Kargi, PHI.
5. Biochemical Engineering: A Textbook for Engineers, Chemists and Biologists, 1st ed. by
S Katoh, J Horiuchi, and F Yoshida, Wiley-VCH.

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 6th Semester

PCE6J002 FLUIDIZATION ENGINEERING

Module I:
Introduction to fluidization, types of fluidization, gross behavior of fluidized beds, minimum
fluidization velocity, pressure drops in fluidized beds, bed voidage, TDH, viscosity and
fluidity of beds, bubble behavior, bed expansion, distributor design.

Module II:
Simple mathematical treatment, Solid transport: flow and fluidized solids, solids transfer,
terminal velocity, particle entrainment and elutriation, simple calculations.

Module III:
Heat and mass transfer in fluidized beds: Heat transfer mechanism, principles of gas-solid
and bed surface transfer, heat transfer to liquid fluidized systems, generalized correlation
for fluidized bed mass transfer and its limitations.

Module IV:
Semi-fluidization: principles, productionof various bed parameters, Industrial applications;
Design of fluidized bed reactors: Concept of RTD, basic designprinciples for fluidized bed.

Text Books:
1. Fluidization Engineering, 2nd ed. by D Kunii and O Levenspiel, Butterworth-
Heinemann.

Reference Books:
1. Handbook of Fluidization and Fluid-Particle Systems by W C Yang, CRC Press.
2. Fluidization by M Leva, McGraw-Hill.
3. Fluidization by J F Davidson and D Harrison, Academic Press.

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 6th Semester

PCE6J003 POLYMER TECHNOLOGY

Module I:
History of polymers, classification and types of polymers,chemistry, kinetics, and methods
of polymerization. Introduction to reactor design for polymerization.

Module II:
Properties of plastics and macromolecular structure. Polymer degradation. Molecular
weight of polymers and its determination by viscometry, light-scattering, and osmotic
pressure methods.

Module III:
Monomers and their manufacture. Manufacture and uses of important polymers:
polyethylene, polypropylene, polystyrene, polyvinyl chloride, nylons, polyesters, polyvinyl
alcohol, polyvinyl acetate, polymethyl-methacrylate, polyacrylic acid, polylactic acid, phenol
formaldehyde, urea formaldehyde,polycarbonate, and Teflon.

Module IV:
Polymer additives, compounding of plastics. Casting and mouldingof plastics, equipments,
design of moulds. Plastic materials and elastomers as materials of construction in chemical
equipments.

Text and Reference Books:

1. Polymer Science and Technology, 3rd ed. by J R Fried, PHI.
2. Textbook of Polymer Science by F W Billmeyer, Wiley.
3. Principles of Polymerization, 4th ed. by G Odian, Wiley.
4. Polymer Science, 2nd ed. by VRGowarikar, JSreedhar, and NVViswanathan, New Age.
5. Contemporary Polymer Chemistry, 3rd ed. by HAllcock, FLDeceased, and JMark, PHI.
6. Introduction to Polymer Science and Technology by N B Singh and S SDas, New Age.

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 6th Semester

PCE6J004 SEPARATION TECHNOLOGY

Module I:
Rate governed processes, definitions and terminologies.
Membranes: Types and modules, classification of membrane processes, membrane
materials, advantages and disadvantages of membrane processes, major areas of
application, preparation and characterization of membranes.

Module II:
Principles, advantages, disadvantages, and applications of reverse osmosis, nano-filtration,
ultra-filtration, and micro-filtration.

Module III:
Principles, advantages, disadvantages, and applications of dialysis, gas separation,
pervaporation, electrodialysis, and liquid membranes.

Module IV:
Facilitated transport, recent advances in membrane processes, and biomedical applications
of membranes.

Text and Reference Books:

1. Perry's Chemical Engineers' Handbook, 8th ed. by D W Green and R H Perry, McGraw-
Hill.
2. Separation Processes, 2nd ed. by C J King, Dover Publications.
3. Handbook of Separation Process by R W Rousseau, Wiley.
4. Principles of Mass Transfer and Separation Processes by B K Dutta, PHI.
5. Membrane Separation Processes by K Nath, PHI.
6. Transport Processes and Separation Process Principles, 4th ed. by C J Geankoplis,
Pearson.
7. Separation Process Principles, 2nd ed. by J D Seader and E J Henley, Wiley.

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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 6th Semester

PMG6M001 ENVIRONMENTAL SCIENCE AND ENGINEERING

Module I
Multidisciplinary nature of environmental studies
Definition, scope and importance, Need for public awareness.
Natural Resources:
Renewable and non-renewable resources:
Natural resources and associated problems.
a) Forest resources: Use and over-exploitation, deforestation, case studies. Timber extraction,
mining, dams and their effects on forest and tribal people.
b) Water resources: Use and over-utilization of surface and ground water, floods, drought, conflicts
over water, dams-benefits and problems.
c) Mineral resources: Use and exploitation, environmental effects of extracting and using mineral
resources, case studies.
d) Food resources: World food problems, changes caused by agriculture and overgrazing, effects of
modern agriculture, fertilizer-pesticide problems, water logging, salinity, case studies.
e) Energy resources: Growing energy needs, renewable and non renewable energy sources, use of
alternate energy sources. Case studies.
f) Land resources: Land as a resource, land degradation, man induced landslides, soil erosion and
desertification.
 Role of an individual in conservation of natural resources.
 Equitable use of resoureces for sustainable lifestyles.

Module II
Ecosystems
Concept of an ecosystem.
 Structure and function of an ecosystem.
 Producers, consumers and decomposers.
 Energy flow in the ecosystem.
 Ecological succession.
 Food chains, food webs and ecological pyramids.
 Introduction, types, characteristic features, structure and function of the following ecosystem :-
a) Forest ecosystem
b) Grassland ecosystem
c) Desert ecosystem
d) Aquatic ecosystems (ponds, streams, lakes, rivers, oceans, estuaries)
Environmental Pollution Definition
 Cause, effects and control measures of :-
a) Air pollution
b) Water pollution
c) Soil pollution
d) Marine pollution
e) Noise pollution
f) Thermal pollution
g) Nuclear hazards
 Solid waste Management: Causes, effects and control measures of urban and industrial wastes.
 Role of an individual in prevention of pollution.
 Pollution case studies.
 Disaster management: floods, earthquake, cyclone and landslides.

Module III
Social Issues and the Environment
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 From Unsustainable to Sustainable development

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 Urban problems related to energy

B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 6th Semester
 Water conservation, rain water harvesting, watershed management
 Resettlement and rahabilitation of people; its problems and concerns. Case Studies
 Environmental ethics : Issues and possible solutions.
 Climate change, global warming, acid rain, ozone layer depletion, nuclear accidents and
holocaust. Case Studies.
 Wasteland reclamation.
 Consumerism and waste products.
 Environment Protection Act.
 Air (Prevention and Control of Pollution) Act.
 Water (Prevention and control of Pollution) Act
 Wildlife Protection Act
 Forest Conservation Act
 Issues involved in enforcement of environmental legislation.
 Public awareness.

Module IV
Human Population and the Environment
 Population growth, variation among nations.
 Population explosion – Family Welfare Programme.
 Environment and human health.
 Human Rights.
 Value Education.
 HIV/AIDS.
 Women and Child Welfare.
 Role of Information Technology in Environment and human health.
 Case Studies.

References
1. Agarwal, K.C. 2001 Environmental Biology, Nidi Publ. Ltd. Bikaner.
2. R. Rajagopalan, Environmental Studies, Oxford University Press
3. Ajith Sankar, Environmental Mangement, Oxford University Press
4. Bharucha Erach, The Biodiversity of India, Mapin Publishing Pvt. Ltd., Ahmedabad – 380 013,
India, Email:mapin@icenet.net (R)
5. Brunner R.C., 1989, Hazardous Waste Incineration, McGraw Hill Inc. 480p
6. Clark R.S., Marine Pollution, Clanderson Press Oxford (TB)
7. Cunningham, W.P. Cooper, T.H. Gorhani, E & Hepworth, M.T. 2001, Environmental Encyclopedia,
Jaico Publ. House, Mumabai, 1196p
8. De A.K., Environmental Chemistry, Wiley Eastern Ltd.
9. Down to Earth, Centre for Science and Environment (R)
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 6th Semester

PEN6E101 BUSINESS COMMUNICATION AND SKILL FOR INTERVIEW

Course Objectives
 To develop communication competence in prospective engineers.
 To enable them to convey thoughts and ideas with clarity and focus.
 To develop report writing skills.
 To equip them to face interview & Group Discussion.
 To inculcate critical thinking process.
 To prepare them on problem solving skills.
 To provide symbolic, verbal, and graphical interpretations of statements in a problem
description.
 To understand team dynamics & effectiveness.
 To create an awareness on Engineering Ethics and Human Values.
 To install Moral and Social Values, Loyalty and also to learn to appreciate the rights of others.
 To learn leadership qualities and practice them.

MODULE I
Communication Skill: Introduction to Communication, The Process of Communication,
Barriers to Communication, Listening Skills, Writing Skills, Technical Writing, Letter
Writing, Job Application, Report Writing, Non-verbal Communication and Body
Language, Interview Skills, Group Discussion, Presentation Skills, Technology-based
Communication.

MODULE II
Critical Thinking & Problem Solving: Creativity, Lateral thinking, Critical thinking,
Multiple Intelligence, Problem Solving, Six thinking hats, Mind Mapping & Analytical
Thinking.
Teamwork: Groups, Teams, Group Vs Teams, Team formation process, Stages of Group,
Group Dynamics, Managing Team Performance & Team Conflicts.

MODULE III
Ethics, Moral & Professional Values: Human Values, Civic Rights, Engineering Ethics,
Engineering as Social Experimentation, Environmental Ethics, Global Issues, Code of
Ethics like ASME, ASCE, IEEE.

MODULE IV
Leadership Skills: Leadership, Levels of Leadership, Making of a leader, Types of
leadership, Transactions Vs Transformational Leadership, VUCA Leaders, DART
Leadership, Leadership Grid & leadership Formulation.

Expected outcome:
The students will be able to
 Communicate effectively.
 Make effective presentations.
 Write different types of reports.
 Face interview & group discussion.
 Critically think on a particular problem.
 Solve problems.
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 Work in Group & Teams

 Handle Engineering Ethics and Human Values.
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 Become an effective leader.

B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 6th Semester
References:
1. Barun K. Mitra; (2011), “Personality Development & Soft Skills”, First Edition; Oxford Publishers.
2. Kalyana; (2015) “Soft Skill for Managers”; First Edition; Wiley Publishing Ltd.
3. Larry James (2016); “The First Book of Life Skills”; First Edition; Embassy Books.
4. Shalini Verma (2014); “Development of Life Skills and Professional Practice”; First
Edition; Sultan Chand (G/L) & Company
5. John C. Maxwell (2014); “The 5 Levels of Leadership”, Centre Street, A division of
Hachette Book Group Inc.

PCE6D001 ADVANCED CHEMICAL REACTION ENGINEERING (Major)

Module I:
Homogeneous reactor design and analysis-I: Ideal reactors. Review of isothermal design for
batch, semi-batch,and flow reactors.Multiple reactions and reaction networks: Yield-
selectivity concepts, Wei-Prater analysis forfirst order networks, reaction networks of
general order. Reactor energy balance and its applications to reactordesign and analysis.

Module II:
Homogeneous reactor design and analysis-II: Non-ideal reactors. Review of the
basicconcepts of residence time distributions, single parameter models for real reactor
behavior, macromixing andmicromixing, segregated flow model and Zweitering's analysis
of maximum mixedness, IEM and other models formicromixing.

Module III:
Heterogeneous reactors-I: Gas-solid systems. Review of kinetics of gas-solid catalytic
reactionswith and without diffusion limitations. Reactor design for fixed and fluidized bed
reactors. Selected case studies,Non-catalytic gas-solid reactions: review of kinetics; reactor
design case studies.

Module IV:
Heterogeneous reactors-II:Gas-liquid systems. Basic theories of mass transfer with chemical
reaction model systems and model reactors,Reactor design for mechanically agitated and
bubble column reactors. Selected case studies.

Reference Books:
1. Chemical Reactor Analysis and Design, 3rd ed. by G F Froment, K B Bischoff, and J De
Wilde, Wiley.
2. Elements of Chemical Reaction Engineering, 4th ed. by H S Fogler, PHI.
3. Chemical Reaction Engineering, 3rd ed. by O Levenspiel, Wiley.
4. Chemical Reactor Analysis and Design Fundamentals by JBRawlings and J G E
kerdt,Nob Hill Publishing.
5. Chemical and Catalytic Reaction Engineering by J JCarberry, Dover Publications.
6. Heterogeneous Reactions, Vol. I and II by L K Doraiswamy and MMSharma, John
Wiley& Sons.
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B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 6th Semester

COMPUTATIONAL FLUID DYNAMICS (Minor)

Module I:
Governing equations of fluid flow. Finite difference, finite volume, and finite element
methods. Laplace equation. Diffusion equation or Wave Equation. Application of finite
volume method to fluid flow problems.

Module II:
Pressure correction techniques: Gauss Siedel and Gauss Jordan. Introduction to
multigridmethods. Boundary conditions, Structured and unstructured mesh. Introduction to
CAD systems and different standards used for DATA exchange.

Module III:
Governing equations for turbulent flow, Rotating machinery, Combusting flow, Multiphase
flow. Simple internal flows:T-Junction, Driven Cavity, Manifold, and Valves. External Flows:
Flow over Ahmed Body, Car-Reacting Flow in a Gas Burner, and Multiphase Flow in an Air
Lift Reactor.

Reference Books:
1. An Introduction to Computational Fluid Dynamics: The Finite Volume Method, 2nd ed.
by H Versteeg and W Malalasekra, Pearson.
2. Computational Fluid Dynamics: The Basics with Applications, J D Anderson, McGraw-
Hill.
3. Fundamentals of Computational Fluid Dynamics, T K Sengupta, University Press.
4. Introduction to Computational Fluid Dynamics, P Niyogi, S K Chakrabratty, and M K
Laha, Pearson.

COMPUTER AIDED DESIGN LAB

1. Finding out matrix addition, multiplication, inversion, rank, and Eigen values using
MATLAB simulator and plotting set ofdata using MATLAB.
2. Parameter estimation using least-square technique using MATLAB.
3. Writing ‘m’ files in MATLABplatform to solve coupled linear algebraic equations using
Gauss elimination method.
4. Writing ‘m’ files in MATLABplatform to solve non-linear algebraic equations using
Newton Raphsontechnique.
5. Writing ‘m’ files in MATLABplatform to control level in a tank using P/PI/PID
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controller.
6. Finding out response of a first and second order system(transfer function) using
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‘simulink’.
B.Tech (Chemical Engineering) Syllabus for Admission Batch 2015-16 6th Semester
7. Simulation of a stirred tank reactor (both open loop and closed loop) using‘simulink’.
8. Simulation of steady Flow of air through a cylindrical tube using GAMBIT and FLUENT.
9. Simulation of steadystate fluid flow and heat transfer processes using GAMBIT and
FLUENT when liquid water flows through a cylindricaltube.
10. Simulation of steady Flow of air through a ‘T’ joint using GAMBIT and FLUENT.

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