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    Citrate Bitartrate Iodide Identification Tests

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    Patricia Anne
    The document summarizes laboratory reports from a pharmaceutical chemistry class on the identification and preparation of various salts. It includes laboratory reports from a student group on potassium iodide, potassium bitartrate, and sodium citrate. For each salt, the group describes preparation methods and provides results from various identification tests, including reactions with reagents like silver nitrate and tests for characteristic ions. Photos document the results obtained for samples prepared by the group versus commercial standards.

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    © All Rights Reserved
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    Citrate Bitartrate Iodide Identification Tests

    Uploaded by

    Patricia Anne
    168 views7 pages
    The document summarizes laboratory reports from a pharmaceutical chemistry class on the identification and preparation of various salts. It includes laboratory reports from a student group on potassium iodide, potassium bitartrate, and sodium citrate. For each salt, the group describes preparation methods and provides results from various identification tests, including reactions with reagents like silver nitrate and tests for characteristic ions. Photos document the results obtained for samples prepared by the group versus commercial standards.

    Original Description:

    Sodium Citrate, Potassium Bitartrate, and Potassium Iodide Identification Tests

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    © © All Rights Reserved

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    The document summarizes laboratory reports from a pharmaceutical chemistry class on the identification and preparation of various salts. It includes laboratory reports from a student group on potassium iodide, potassium bitartrate, and sodium citrate. For each salt, the group describes preparation methods and provides results from various identification tests, including reactions with reagents like silver nitrate and tests for characteristic ions. Photos document the results obtained for samples prepared by the group versus commercial standards.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    168 views7 pages

    Citrate Bitartrate Iodide Identification Tests

    Uploaded by

    Patricia Anne
    The document summarizes laboratory reports from a pharmaceutical chemistry class on the identification and preparation of various salts. It includes laboratory reports from a student group on potassium iodide, potassium bitartrate, and sodium citrate. For each salt, the group describes preparation methods and provides results from various identification tests, including reactions with reagents like silver nitrate and tests for characteristic ions. Photos document the results obtained for samples prepared by the group versus commercial standards.

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    © All Rights Reserved
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    POTASSIUM IODIDE

    TITLE

    A laboratory group report for Pharmaceutical Chemistry 1

    Class Schedule: PHARM 114L 3:30-5:30 MWF

    Prepared by Group 3

    *Group Members Contribution Signature


    1. ALIM, Mia Franz Preparation and Identification of Potassium iodide
    2. ANCERO, Angelica L. Preparation of Potassium iodide
    3. BALNEG, Joyce R. Preparation of Potassium iodide
    4. BALUYOT, Leianne Wichelle Labelled the Potassium iodide product
    5. BAUZON, Raechell Anne Preparation of Potassium iodide
    6. BILLEDO, Monica Lai Identification of Potassium iodide
    7. BOADO, Patricia Anne L. Preparation and identification of potassium iodide;
    prepared the group report for identification tests.

    Excellent(25pts) Good(20pts) Satisfactory(15pts) Needs Improvement


    (10pts)
    Analytical Results □ □ □ □
    Questions for □ □ □ □
    Research

    Comments, Suggestions, Deductions:

    Total Deductions:

    Total Score:
    Identification Test for Potassium iodide (photo documentation)

    1. Add a pinch of the salt in water and stir.


    Result: The salt was dissolved, thus, making it soluble in water.

    Prepared Potassium iodide by the group Commercial Potassium iodide

    2. To the above solution, add silver nitrate T.S.


    Result: Formation of yellow precipitate of AgI

    Prepared Potassium iodide by the group Commercial Potassium iodide

    3. To another solution of the salt, add hydrochloric acid or sulfuric acid.


    Result: Formation of white precipitate.
    Rationale: The reagents used was concentrated Hydrochloric acid and Sulfuric acid, thus, no formation of white
    precipitate formed. The reagents that was supposed to be used is diluted HCl and sulfuric dioxide gas.
    Reference: http://ncert.nic.in/ncerts/l/kelm207.pdf
    Prepared Potassium iodide by the group Commercial Potassium iodide
    Hydrochloric acid Hydrochloric acid

    Sulfuric acid Sulfuric acid


    POTASSIUM BITARTRATE
    TITLE

    A laboratory group report for Pharmaceutical Chemistry 1

    Class Schedule: PHARM 114L 3:30-5:30 MWF

    Prepared by Group 3

    *Group Members Contribution Signature


    8. ALIM, Mia Franz Preparation and Identification of Potassium bitartrate
    9. ANCERO, Angelica L. Preparation of Potassium bitartrate
    10. BALNEG, Joyce R. Preparation of Potassium bitartrate
    11. BALUYOT, Leianne Wichelle Preparation of Potassium bitartrate
    12. BAUZON, Raechell Anne Preparation of Potassium bitartrate
    13. BILLEDO, Monica Lai Labelled the Potassium bitartrate product and prepared the
    group report
    14. BOADO, Patricia Anne L. Labelled the Potassium bitartrate product and prepared the
    group report

    Excellent(25pts) Good(20pts) Satisfactory(15pts) Needs Improvement


    (10pts)
    Analytical Results □ □ □ □
    Questions for □ □ □ □
    Research

    Comments, Suggestions, Deductions:

    Total Deductions:

    Total Score:
    Identification Test for Potassium bitartrate (photo documentation)

    1. Heat the crystals at high temperature.


    Result: Ash-like forming chars

    Prepared Potassium bitartrate by the group Commercial Potassium bitartrate

    2. Dissolve the residue in water and perform the Beilstein’s test.


    Result: Negative result for Beilstein’s test.

    Prepared Potassium bitartrate by the group Commercial Potassium bitartrate

    3. Prepare a saturated aqueous solution of potassium bitartrate, neutralized with sodium hydroxide, add silver
    nitrate T.S.
    To the precipitated formed, dissolve it with ammonia T.S. and the solution warmed.
    Result: Silver mirror/metallic silver is deposited along the inner walls of the test tube.

    Prepared Potassium bitartrate by the group Commercial Potassium bitartrate


    4. Prepare a 1% resorcinol solution in a hydrochloric acid. Add a few drops of this solution to a dry salt of potassium
    bitartrate. Then add 3 mL of sulfuric acid and slowly heat the solution.
    Result: Rose-red color is formed; after heating, it becomes colorless.

    Prepared Potassium bitartrate by the group Commercial Potassium bitartrate

    4. Acidify a tartarate solution with acetic acid. Add a few drops of ferrous sulfate T.S. and hydrogen peroxide T.S.,
    then add an excess of sodium hydroxide T.S.
    Result: Purple/violet color of solution.

    Prepared Potassium bitartrate by the group Commercial Potassium bitartrate


    SODIUM CITRATE
    TITLE

    A laboratory group report for Pharmaceutical Chemistry 1

    Class Schedule: PHARM 114L 3:30-5:30 MWF

    Prepared by Group 3

    *Group Members Contribution Signature


    15. ALIM, Mia Franz Preparation of Sodium citrate
    16. ANCERO, Angelica L. Preparation of Sodium citrate
    17. BALNEG, Joyce R. Preparation of Sodium citrate
    18. BALUYOT, Leianne Wichelle Identification Test for Sodium citrate
    19. BAUZON, Raechell Anne Identification of Sodium citrate
    20. BILLEDO, Monica Lai Labelled the Sodium citrate and prepared the group report
    21. BOADO, Patricia Anne L. Labelled the Sodium citrate and prepared the group report
    for the identification tests.

    Excellent(25pts) Good(20pts) Satisfactory(15pts) Needs Improvement


    (10pts)
    Analytical Results □ □ □ □
    Questions for □ □ □ □
    Research

    Comments, Suggestions, Deductions:

    Total Deductions:

    Total Score:
    Identification Test for Sodium Citrate (photo documentation)

    1. Perform Belstein’s Test.


    Result: Negative result for Belstein’s test.

    Prepared Sodium Citrate by the group Commercial Sodium Citrate

    2. Test for citrate ion


    2a. Prepare 1:10 solution of the compound; add excess calcium chloride T.S. and heat.
    Result: white granular precipitate of calcium citrate settles out
    Chemical Reaction: Na3C6H5O7 + CaCl2 —> Ca(CH3COO)3 + NaCl

    Prepared Sodium Citrate by the group Commercial Sodium Citrate

    2b. Prepare 5 ml of sodium citrate solution and add 0.5 ml mercuric sulfate T.S. Heat the solution and add
    dropwise Potassium permanganate T.S.
    Result: formation of white precipitate

    Prepared Sodium Citrate by the group Commercial Sodium Citrate

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