Behr Labor Technik Kjeldahl N Stand en
Behr Labor Technik Kjeldahl N Stand en
Behr Labor Technik Kjeldahl N Stand en
Labor-Technik
EN
Contents
Kjeldahl method for determining nitrogen
The behr program for determination of nitrogen using
the Kjeldahl method______________________________________ 4
behrosog 3 scrubber_____________________________________ 20
The behr program for the determination of nitrogen using the Kjeldahl method provides
the user individually configurable complete solutions for the laboratory.
Digestion units
Kjeldahl block digestion systems
Block digestion systems with high-quality corrosion-resistant block housing made of
stainless steel. Manual or with automatic lift.
n High-efficiency heating and extraction hood with exhaust collector
n behr single-knob control for particularly easy and fast programming
n Menu navigation in national language
n 25 freely configurable programs for block temperature and digestion time
n Applications can be saved
Standard systems
n Digestion vessels with 250 ml volume (8, 12 or 20 sample slots)
Micro-Kjeldahl systems
n Digestion vessels with 100 ml volume (16, 24 or 40 sample slots)
Infrared digestion systems
The digestion units of the behrotest® InKjel series are equipped with efficient quartz
glass infrared heating. Apart from the traditional series with energy control, there is a
fully equipped series of appliances for temperature-controlled digestion.
The quality and positioning of the behr infrared heaters guarantees the user identical
heating phases and digestion temperatures on all sample slots. This also applies to
double-rowed arrangement in insert racks for 12 samples.
Direct sample heating by the infrared heaters prevents the agonisingly long heating and
cooling times of conventional heating block systems.
The behrotest ® InKjel is therefore the ideal rapid digestion system for the determination
of nitrogen using the Kjeldahl method and other high-temperature digestion tests.
Scrubber
The two-stage behrosog scrubber – pre-separator plus safety stage – prevents any acid
fumes whatsoever from reaching the environment.
Titration stations
The behrotest® STI manual titration station or an automatic titrator ensure reliable, safe
and fast titration for completion of the nitrogen determination.
4
Areas of application
Meat/sausages
Biogas plants
Spirits
Delicatessen
Coffee
Nuts
Wastewater
Feedstuffs
5
Block digestion systems
behr Kjeldahl block digestion systems
6
Block digestion systems
Frequency 50/60 Hz
Current consumption 5A 8A 8A 10 A
7
behr Kjeldahl block digestion systems with fully automatic lift
behr’s L series Kjeldahl block digestion systems are equipped with a fully automatic
lift. This enables the user to avoid handling the heavy samples unit and the hot chemi-
cals. The software not only controls the sample lift but also the behrosog 3 and therefore
enables largely automatic digestion.
At the end of the digestion the lift moves the complete unit upwards, including the rack
and extraction hood. Following a freely programmable cooling/ extraction time, it raises
the extraction hood and moves it into the end position.
n Temperature profiles and the starting time of the digestion are freely programmable.
behr single-knob control for particularly easy and fast programming.
n
n USB interface.
n The Windows software supplied enables the user to bidirectionally transfer
application-specific time/temperature profiles via the interface between one or several
units and a PC.
n The removable inspection door on the insertion rack enables the progress of the
digestion to be observed.
Available with 230 V~/50-60 Hz.
Fully automatic
boil cool finished
8
Block digestion systems
Good to know:
behrotest® standard digestion vessels have standard dimensions. That means
they fit into digestion and distillation units of most brands. Of course, it also
means that standard digestion vessels of most brands can be used with
behr distillation units.
SR 3i SR 4 SR 5
SIST 100
9
Infrared rapid detection units
behrotest ® InKjel
Infrared rapid detection units
Quartz heaters:
n uniform effect along the entire length
n insulated from the housing, no energy loss through heat transfer
n full heat output within 1 minute, no preheating required
11
Digestion units
The digestion units of the behrotest ® InKjel series are equipped with efficient infrared
heating. The quality and positioning of the behr infrared heaters guarantees the user
identical heating phases and digestion temperatures on all sample slots. This also ap-
plies to double-rowed arrangement in insert racks for 12 samples. The digestion tubes
hang in the rack and do not touch the bottom of the digester. As a result, the digestion
vessels are at less risk of breakage than in an aluminium heating block.
n Direct sample heating by the infrared heaters prevents the agonisingly long
heating times of conventional heating block systems.
n You can reach a radiation temperature of 830 °C within one minute and heat up the
samples in 10 minutes to their boiling temperature of 410°C.
High-quality quartz heaters instead of the usual steel tubular heating elements en-
n
sure particularly uniform heating of all sample slots.
behr single-knob control for particularly easy and fast programming.
n
n Menu navigation in national language.
The behrotest ® InKjel is therefore the ideal digestion system for the determination of
nitrogen using the Kjeldahl method and other high-temperature digestion tests. With
the Kjeldahl digestion method, the temperature is set by the boiling temperature of the
sulphuric acid.
Complete system with tiered rack, fume removal unit, insert rack and glass digestion tubes.
Type Product description Art. No.
InKjel 625 M
InKjel 625 P rapid digestion system with 25 freely configurable programs for energy
and digestion time for 6 sample slots, 250 ml
Rapid digestion system with 25 freely configurable programs for energy and digestion time
and direct heating of the samples using high-quality quartz infrared heaters (1500 W).
n 6 glass digestion tubes of 250 ml
n Constant heating of all samples to 410 °C in approx. 10 minutes
n Uniform heating of all sample slots
n Windows software enables the user to bidirectionally transfer application-specific
time/temperature profiles between one or several units and a PC via the USB inter-
face.
n Energy savings compared to aluminium block
Complete system with tiered rack, fume removal unit, insert rack and glass digestion tubes.
Type Product description Art. No.
InKjel 625 P
12
Infrared rapid detection units
InKjel 1210 M
InKjel 1210 P rapid digestion system with 25 freely configurable programs for energy
and digestion time for 12 sample slots, 100 ml
Rapid digestion system with 25 freely configurable programs for energy and digestion time
and direct heating of the samples using high-quality quartz infrared heaters (1500 W).
n 12 glass digestion tubes of 100 ml
n Constant heating of all samples to 410 °C in approx. 10 minutes
n Uniform heating of all sample slots
n Windows software enables the user to bidirectionally transfer application-specific
time/temperature profiles between one or several units and a PC via the USB interface.
n Energy savings compared to aluminium block
Complete system with tiered rack, fume removal unit, insert rack and glass digestion tubes.
Type Product description Art. No.
InKjel 1210 P
InKjel 1225 M rapid digestion system with manual energy control
for 12 sample slots, 250 ml
Rapid digestion system with manual energy control and direct heating of the samples
using high-quality quartz infrared heaters (1500 W).
n 12 glass digestion tubes of 250 ml
n Constant heating of all samples to 410 °C in approx. 10 minutes
n Uniform heating of all sample slots
n Energy savings compared to aluminium block
Complete system with tiered rack, fume removal unit, insert rack and glass digestion tubes.
Type Product description Art. No.
InKjel 1225 M
13
InKjel 1225 P rapid digestion system with 25 freely configurable programs for energy
and digestion time for 12 sample slots, 250 ml
Rapid digestion system with 25 freely configurable programs for energy and digestion time
and direct heating of the samples using high-quality quartz infrared heaters (1500 W).
n 12 glass digestion tubes of 250 ml
n Constant heating of all samples to 410 °C in approx. 10 minutes
n Uniform heating of all sample slots
n Windows software enables the user to bidirectionally transfer application-specific time/
temperature profiles between one or several units and a PC via the USB interface.
n Energy savings compared to aluminium block
Complete system with tiered rack, fume removal unit, insert rack and glass digestion tubes.
Type Product description Art. No.
InKjel 450 P rapid digestion system with 25 freely configurable programs for
InKjel 450 M
energy and digestion time for 4 sample slots, 500 ml
Rapid digestion system with 25 freely configurable programs for energy and digestion time
and direct heating of the samples using high-quality quartz infrared heaters (1500 W).
n 4 glass digestion tubes of 500 ml
n Constant heating of all samples to 410 °C in approx. 10 minutes
n Uniform heating of all sample slots
n Windows software enables the user to bidirectionally transfer application-specific time/
temperature profiles between one or several units and a PC via the USB interface.
n Energy savings compared to aluminium block
Complete system with tiered rack, fume removal unit, insert rack and glass digestion tubes.
Type Product description Art. No.
InKjel 450 P
14
Infrared rapid detection units
InKjel 475 P rapid digestion system with 25 freely configurable programs for energy InKjel 475 M
and digestion time for 4 sample slots, 750 ml
Rapid digestion system with 25 freely configurable programs for energy and digestion time and
direct heating of the samples using high-quality quartz infrared heaters (1500 W).
n 4 glass digestion tubes of 750 ml
n Constant heating of all samples to 410 °C in approx. 10 minutes
n Uniform heating of all sample slots
n Windows software enables the user to bidirectionally transfer application-specific time/
temperature profiles between one or several units and a PC via the USB interface.
n Energy savings compared to aluminium block
Complete system with tiered rack, fume removal unit, insert rack and glass digestion tubes.
Type Product description Art. No.
InKjel 475 P
Technical data for digestion systems
InKjel M InKjel P
Frequency 50/60 Hz
Current consumption 8A 8A
15
Rapid Infrared Digestion Systems
behrotest ® InKjel TC
behr InKjel TC rapid infrared devices with temperature control combine the advantages
of infrared digestion and block digestion in one unit: Their fast infrared digestion at
controlled temperatures enables an extremely high sample throughput.
With the programmable models of the InKjel TCP line the analyst has the choice from 25
individually configurable programs for temperature and digestion time.
You can reach a radiation temperature of 830 °C within one minute and heat up the
samples in 10 minutes to their boiling temperature of 410°C. High-quality quartz heaters
instead of the usual steel tubular heating elements ensure particularly uniform heating
of all sample slots.
InKjel Programmable rapid infrared digestion system for 6 reaction vessels B00636206
625 TCP with 250 ml volume. Temperature control.
InKjel Programmable rapid infrared digestion system for 4 reaction vessels B00636209
450 TCP with 500 ml volume. Temperature control.
InKjel Programmable rapid infrared digestion system for 4 reaction vessels B00636210
475 TCP with 750 ml volume. Temperature control.
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Infrared rapid detection units
AE 4 Fume removal equipment for InKjel 450 and InKjel 475 B00218088
(M and P)
AE 6 Fume removal equipment for InKjel 625 (M and P) B00218089
AE 6
AE 12/100 Fume removal equipment for InKjel 1210 (M and P) B00218070
AE 12 Fume removal equipment for InKjel 1225 (M and P) B00218090
EG 12/100 Insert rack for 12 digestion vessels of 100 ml B00218069
in the InKjel 1210 (M and P)
EG 6 Insert rack for 6 digestion vessels of 250 ml B00218086
in the InKjel 625 (M and P)
EG 12 Insert rack for 12 digestion vessels of 250 ml B00218087
in the InKjel 1225 (M and P)
EG 4/500 Insert rack for 4 digestion vessels of 500 ml B00218085
in the InKjel 450 (M and P)
EG 4/750 Insert rack for 4 digestion vessels of 750 ml B00218080
EG 6 in the InKjel 475 (M and P)
SR 3i SR 4 KJ 500 KJ 750
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behrotest ® fully equipped work stations
for nitrogen determination according to Kjeldahl
Based on our block or infrared digestion systems, we have put together various full configura-
tions for users with diverse requirements.
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fully equipped work stations
ASB-IR
ASM-IR
ASE-IR
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behrosog 3 Scrubber
Scrubber
n PTFE-coated
double-head
n Liquid is easy to
diaphragm pump
change by simply
draining the
glass bottles n Integrated
mist eliminator
n Continuously variable
control of the air
flow rate 16 ... 40 l/min
n Transparent
safety door
20
behrosog 3 Scrubber
Scrubber
The two-stage behrosog process extraction system (scrubber) – pre-separator plus safety
stage – prevents any acid fumes whatsoever from reaching the environment. Compact
process extraction system for extracting and neutralising aggressive acid fumes,
especially from the Kjeldahl digestion method for nitrogen determination. An upstream
two-stage pre-separator washes out the toxic substances. The process extraction system is
equipped with a vacuum pump 40 l/min. There is no need to connect to the water supply.
n Efficient running costs
n Continuously variable intake flow
Both cleaning stages (condensation and neutralisation stage) prevent the emission
n
of toxic substances into the environment
Optionally, the additional cooling system for the behrosog 3 ACS can be connected to the
system, consisting of stand, bottles and cooler.
behrosog 3
Scrubber
Type Product description Art. No.
behrosog 3 Scrubber with suction pump (40 l/min), cooling stage, B00217925
neutralisation stage and drip catcher
Frequency 50/60 Hz
Power consumption 80 W
Weight approx. 18 kg
Dimensions in cm (W x D x H) approx. 38 x 34 x 40
behrosog 3
Pump delivery rate max. 40 l/ min without backpressure with ACS
SIMVAC
Suction device with water jet pump and neutralisation bottle incl. hose and frame.
Without fittings!
20 l/min 13 l/min
28 l/min 16 l/min
SIMVAC
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behr steam distillers S 1 to S 5
Customised features
Steam distillers
behr S series steam distillers are the optimum addition to the behr Kjeldahl digestion
system. Depending on the requirements, the user can choose between five automatic
steam distillers. These have identical basic designs, however, their ease of use and
degree of automation differ. The top of the range unit, the behr S 5, is prepared for work
with an external titrator.
The Windows software supplied enables the user to bidirectionally transfer application-
specific distillation parameters between one or several units and a PC via the USB inter-
face. The CD includes a library with common applications.
22
Steam distillers
which are prone to wear out during everyday use in the laboratory.
23
Steam distiller S 1 with automatic addition of NaOH
n Exemplary safety and reliability
n Robust and insensitive housing made of polyurethane
n Distillation time approx. 3 min per sample
n Detection limit 0.1 mg N
n Retrieval rate > 99.5%
n Reproducibility ± 1%
n Adjustable steam output (10% - 100%)
n Particularly easy, menu-driven operation using a single control
(behr single-knob control)
n Programmable reaction time
n Programmable distillation time
n USB interface
n Level monitoring for the canister set
n Practical quick-release clamping device, which the user can
also easily operate with their left hand
S1
Type Product description Art. No.
S1 S1 Steam distiller, semi-automated B00218025
KAS 20 Canister set for S 1 and S 2, consisting of 2 canisters à 20 l, B00218041
incl. float switches
S2
Type Product description Art. No.
24
Steam distillers
S3
Type Product description Art. No.
Steam distiller S 4 with automatic addition of NaOH, H2O and H3BO3 with automatic
extraction of the sample residues and with 99 programs
n Exemplary safety and reliability
n Robust and insensitive housing made of polyurethane
n Distillation time approx. 3 min per sample
n Detection limit 0.1 mg N
n Retrieval rate > 99.5%
n Reproducibility ± 1%
n Adjustable steam output (10% - 100%)
n Particularly easy, menu-driven operation using a single control (behr single-knob control)
n Programmable reaction time
n Programmable distillation time
n USB interface
n Level monitoring for the canister set
n Practical quick-release clamping device, which the user can
also easily operate with their left hand
S4
Type Product description Art. No.
25
Steam distiller S 5 with automatic addition of NaOH, H2O and H3BO3 with
automatic extraction of the sample residues, with 99 programs and a
connection option for external titrator
Exemplary safety and reliability
n
Robust and insensitive housing made of polyurethane
n
Distillation time approx. 3 min per sample
n
Detection limit 0.1 mg N
n
Retrieval rate > 99.5%
n
Reproducibility ± 1%
n
Adjustable steam output (10% - 100%)
n
Particularly easy, menu-driven operation using a single control (behr single-knob control)
n
Programmable reaction time
n
Programmable distillation time
n
USB interface
n
Level monitoring for the canister set
n
Practical quick-release clamping device, which the user can
n
also easily operate with their left hand
S5
Type Product description Art. No.
S5
S5 Steam distiller, fully automatic, prepared B00218034
for external titrator (e.g. TB 2)
Frequency 50/60 Hz
26
Steam distillers
S1 S2 S3 S4 S5
Number of programs 1 1 10 99 99
USB interface +
27
Adapter for the use of different digestion vessels
Adapter
Our practical adapter ensures that you can use digestion vessels by manufacturers, who deviate from standard sizes
in our behrotest® steam distillers.
28
Steam distillers
Canister sets
behr canister sets are based on hazardous goods canisters with UN approval.
The level sensors form a unit with the screw caps. If necessary, the user can therefore
also directly connect commercial chemical containers without any need for dangerous
refilling or transfer actions.
Canister sets
Type Product description Art. No.
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Simple and secure data collation
and result calculation with a PC
behrotest® HTI 3:
the integrated collection and evaluation solution for nitrogen determination according to Kjeldahl
The behrotest® HTI 3 consists of analytical scales, the behrotest® titration station STI 2 and collection and evaluation software
behrotest® KjelSoft. KjelSoft receives the data from the scales and titration station via USB-interface points, collates it and
automatically calculates the nitrogen and protein content of the samples. Precise sample classification and manipulation assurance
according to GLP are thus guaranteed.
Export of all data in Excel format facilitates the transfer to a LIMS. For documentation there is an additional option for export in
PDF format.
The behrotest® HTI 3 offers the user for the determination of nitrogen according to Kjeldahl:
Simple collation and evaluation
n
Manipulation assurance
n
Precise sample identification
n
Clear illustration of all values and results in the form of tables
n
Simple operation
n
User administration
n
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Kjeldahl software
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B00520182 EN - V3_1_009
Made
in
077109
Germany