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    Observation For Missed Practical Sessions-CH2303

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    Suleka Ranasinghe
    The document contains observations from multiple practical sessions in chemistry that were missed due to student union actions. It includes data from experiments determining softening point, kinematic viscosity, aniline point of fuels, flash point and fire point of solvents, viscosity of liquids, water content in crude oil, ASTM distillation of fuels, proximate analysis of coal, and determination of melting point. Groups observed properties such as temperature, time, volume, and weight at different steps of the experiments.

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    Observation For Missed Practical Sessions-CH2303

    Uploaded by

    Suleka Ranasinghe
    28 views5 pages
    The document contains observations from multiple practical sessions in chemistry that were missed due to student union actions. It includes data from experiments determining softening point, kinematic viscosity, aniline point of fuels, flash point and fire point of solvents, viscosity of liquids, water content in crude oil, ASTM distillation of fuels, proximate analysis of coal, and determination of melting point. Groups observed properties such as temperature, time, volume, and weight at different steps of the experiments.

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    The document contains observations from multiple practical sessions in chemistry that were missed due to student union actions. It includes data from experiments determining softening point, kinematic viscosity, aniline point of fuels, flash point and fire point of solvents, viscosity of liquids, water content in crude oil, ASTM distillation of fuels, proximate analysis of coal, and determination of melting point. Groups observed properties such as temperature, time, volume, and weight at different steps of the experiments.

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    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    28 views5 pages

    Observation For Missed Practical Sessions-CH2303

    Uploaded by

    Suleka Ranasinghe
    The document contains observations from multiple practical sessions in chemistry that were missed due to student union actions. It includes data from experiments determining softening point, kinematic viscosity, aniline point of fuels, flash point and fire point of solvents, viscosity of liquids, water content in crude oil, ASTM distillation of fuels, proximate analysis of coal, and determination of melting point. Groups observed properties such as temperature, time, volume, and weight at different steps of the experiments.

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    Observation for Missed Practical Sessions- CH2303

    (Cancelled Due to Student’s Union Actions)

    Observations for Group 05 (21.09.2020)

    Experiment: Determination of softening point of resin tar or similar material using the Ring and
    Ball Apparatus

    Temperature when ball touches the bottom plate

    Sample 01 (T1) : 43 ᵒC

    Sample 02 (T2) : 43 ᵒC

    Experiment: Determination of kinematic viscosity by Saybolt and Engler viscometers

    Saybolt Viscometer

    Sample Sample Required time (seconds) for


    Temperature (oC)
    No. filling 60 ml volume
    1 727
    2 Room Temperature (30 oC) 736
    3
    SAE 40
    4 382

    5 40 oC 598
    6

    Engler Viscometer

    Sample Sample Efflux Time (seconds) for


    Temperature (oC)
    No. filling 100 ml volume
    1 905
    2 Room Temperature (32 oC) 942
    3
    SAE 40
    4 387

    5 40 oC 341
    6

    Observations for Group 01 (21.09.2020)


    Experiment: Determination of the Aniline point of a petroleum fraction

    Aniline Point of Kerosene (Heating) : 62 oC

    Aniline Point of Kerosene (Cooling) : 58 oC

    Aniline Point of Diesel (Heating) : 76 oC

    Aniline Point of Diesel (Cooling) : 75 oC

    Experiment: Determination of the flash point and the fire point of Solvents

    Pensky Martens closed cup tester

    Kerosene Diesel

    Sample 01 Sample 02 Sample 01 Sample 02

    Flash point (0C) 41.5 67

    Cleveland open cup tester

    Kerosene Diesel

    Sample 01 Sample 02 Sample 01 Sample 02

    Flash point (0C) 33 35 42 42

    Fire point (0C) 35 36 55 53

    Observations for Group 02 (21.09.2020)


    Experiment: Determination of the viscosity of very viscous liquid

    I. . Universal Torsion Viscometer:-

    Measurement No Angle
    1 347
    2 321

    II. Universal Penetrometer:-

    Measurement No Depth (mm)


    1 14.24
    2 14.06
    3 14.82

    III. Rotary Viscometer:-

    Measurement No Viscosity (mPaS)


    1 218
    2 -

    Experiment: Determination of the water and sediment content of crude oil

    Sample No Volume of Water and Sediment (ml)


    1 2.2

    2 3.1

    Observations for Group 05 (23.09.2020)


    Experiment: ASTM Distillation
    SI No Volume of distillate collected(ml) Temperature (oC) Temperature (ºF)

    01 0 121
    02 10 160
    03 20 169.5
    04 30 176
    05 40 183
    06 50 189
    07 60 196
    08 70 206
    09 80 215
    10 90 227
    11 95 235

    12 97 242

    EXPERIMENT: Proximate analysis of coal

    Determination of inherent moisture


    Weight of watch glass (W1) = 35.64 g
    Weight of watch glass + 5g of coal (W 2) = 40.64 g
    Weight of watch glass + coal (after drying at 110 °C for 1 hr) (W 3) = 40.56 g

    Determination of volatile matter


    Weight of silica crucible +lid (W4) = 15.38 g
    Weight of silica crucible +lid + 1g of coal (W5) = 16.38 g
    Weight of silica crucible +lid + coal (after drying at 680 °C for 7 min) (W 6) = 16.11 g

    Determination of ash

    Weight of silica crucible +lid (W7) = 16.17 g


    Weight of silica crucible +lid + 1g of coal (W8) = 17.17 g
    Weight of silica crucible +lid + coal (after drying at 680 °C for 1 hr) (W 9) = 16.77 g
    Observations for Group 06 (23.09.2020)
    Experiment: Viscosity Index

    Time taken to flow at 100 ᵒF :- 26 min 10 sec

    Time taken to flow at 210 ᵒF :- 2 min 25 sec

    Viscometer constant :- 0.10276

    Experiment: Determination of Melting Point

    Temperature at solid begins to melt (T1) - 80.5 °C

    Temperature at melting is complete (T2) – 82 °C

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