ISSN 2347 - 3983

Arlene G. Estacio et al., International Journal of Volume

Emerging7,Trends
No. 10in October 2019
Engineering Research, 7(10), October 2019, 388 - 392
International Journal of Emerging Trends in Engineering Research
Available Online at http://www.warse.org/IJETER/static/pdf/file/ijeter047102019.pdf
https://doi.org/10.30534/ijeter/2019/047102019

Characterization of High Temperature Calibration Bath through Stability and

Uniformity Tests with Data Acquisition using Standard Platinum Resistance
Thermometer and Precision Multimeter

Arlene G. Estacio1, Vilma C. Pagtalunan2, Rio S. Pagtalunan3, Ira C. Valenzuela4, Lean Karlo S.
Tolentino5, and Jennifer C. Dela Cruz6
1,6
School of Electrical, Electronics, and Computer Engineering, Mapúa University, Philippines,
jennycdc69@gmail.com
1,6
School of Graduate Studies, Mapúa University, Philippines
1
Metals Industry Research and Development Center, Department of Science and Technology, Philippines,
agestacio@mirdc.dost.gov.ph
2
Department of Electrical Engineering, Technological University of the Philippines, Philippines,
vcpagtalunan@yahoo.com
3
Metals Industry Research and Development Center, Department of Science and Technology, Philippines,
rspagtalunan@mirdc.dost.gov.ph
4,5
Department of Electronics Engineering, Technological University of the Philippines, Philippines
4
University Research and Development Services Office, Technological University of the Philippines,
ira_valenzuela@tup.edu.ph
5
University Extension Services Office, Technological University of the Philippines, Philippines,
leankarlo_tolentino@tup.edu.ph

 The liquid bath was further unvarying at lesser temperatures.

ABSTRACT The variances found were insignificantly distributed since the
Standard Deviation ranged only from 0.005 to 0.013. It
Calibration is one area in measurement where our country is indicates that the local calibration laboratories can also
still in the process of improvement. The absence of confirmed perform the tests for stability and uniformity on a calibration
approaches and actions for identifying the features of bath at an accuracy level comparable to national laboratories
calibration baths by numerous laboratories disallowed them to since the measured values obtained were within the values
assess more the finest measurement ability and develop their obtained in similar tests conducted in a national laboratory
accurateness. In recent advances in technology, there is now a abroad and have very small standard deviations.
way of providing the best measurement capability in
temperature calibration by providing validated methods in Key words : characterization, liquid calibration bath,
characterizing calibration baths that contributes to the measurement, stability, uniformity
uncertainty of measurement of the calibrated thermometer and
is therefore important to measure the extent of its contribution 1. INTRODUCTION
to the final uncertainty. This study adapted the process from
obtainable and current methods. Platinum Resistance Different setups were established for some calibration
Thermometer (PRT-Isotech) and Standard Platinum services outside the Philippines. These were not easily
Resistance Thermometer (SPRT-Hart) which are interfaced to replicated by almost all calibration labs since the at one time
Precision Digital Multimeters were used for measurements. comprehensive approaches and actions in facilitating the tests
Quite a few measurements were made at varying time for calibration enclosures/bath in terms of their stability and
durations implemented on several known positions in an uniformity were not provided. The absence of tested
orderly measurement form which enclosed the whole approaches and actions in identifying the faces of calibration
workspace. The uniformities and stabilities of the calibration baths by almost all home-grown calibration labs disallowed
bath were computed by getting the range of the Minimum them to assess more their finest measurement ability and
Difference with the Maximum Difference taken at every develop their accurateness [1-3].
established temperature point. Outcomes of measurements
exhibited that the calibration bath stability at every This paper aims to identify the characteristics of this Liquid
temperature setting are steadier at lesser temperatures and Calibration Bath at higher ambient temperatures by means of
have a tendency to rise as the temperature approaches 250ºC. validated technique and process of the Metals Industry
Research and Development Center (MIRDC) for measuring
stability and uniformity. This objective was achieved, by (1)
carrying out stability test by identifying the highest difference
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in temperature at a specified temperature set point and period,

(2) handling uniformity test by identifying the highest Internati
variation in temperature among stated locations in the Liquid onal
Calibration Bath, and (3) establishing a preliminary curve traceabi
fitting model stating the performance of stability of Liquid lity of
Calibration Bath. The results of this study offer assistance to measur
the home-grown facilities to accomplish at equivalence with ement
labs outside the country offering comparable calibration standar
services. This provided more responsiveness to the students ds
of the significance of calibration in this area of measurement, Calibration
and finally, future endeavors in this field of metrology [1] can Laboratories
be explored by a university for a possible specialization in the
undergraduate and graduate programs in the field of
engineering and technology.

This study, though, is restricted on the usage of overflowing Figure 1: Traceability of measurements standards through
and stirred-liquid calibration bath. Different stirred-liquid laboratories [4]
baths’ calibration chamber can put up several temperatures
extending from -50°C to +600°C with regards to the kind of Most of the calibration labs practice variable-temperature
enclosure form since thermometers are adjusted by
liquid utilized. Earlier test method initially was on low
comparison scheme [4], as shown in Figure 2. For the said
temperature range, yet, because of increasing temperature
setup, thermometers are calibrated against with the other
differences when one increased the temperature settings, it
calibrated thermometer. The other calibrated thermometer
was noted that there were changes in the behavior of the liquid
was compared with one more adjusted thermometer of better
used such as bubbles created in the calibration bath, therefore,
accurateness in a calibrations chain that should eventually be
fixed points of test were done at its highest temperature of 250
traceable prior to a main standard thermometer [2], [5].
°C.

It limited the settings in temperature during test from 150oC to

250oC and applied one kind of liquid all over the measurement
process and at minimum 23 ± 3 ° C and 55 ± 15%RH. The
calibration bath utilized silicone oil. Measurements were
made on several determined locations in an organized
measurement form that consists of the whole workspace of the
Liquid Calibration Bath [2]. The experimentation proper was
performed in Instrumentation Laboratory of MIRDC located
at Bicutan, Taguig City, Philippines.

The results of this paper align with the notion of traceability in

measurement in which devices for measurement are adjusted
Figure 2: Comparison Method of Thermometers’ Calibration Set-up
by means of advanced accurateness standards which are
noticeable to every country’s National Laboratories [1], [4] as
2. MATERIALS AND METHODS
shown in Figure 1 below. Illustrating the behavior of
calibration bath’s uniformity and stability supports to
The measurement methods took the procedure from
intensify accurateness in calibration that improved
accessible and current methods, e.g. MIRDC, [6-24] but
uncertainty of measurement.
generally, they were implemented by SPRT-Hart and
PRT–Isotech thermometers which are interfaced to the
precision Digital Multimeter. The said two thermometers
were both submerged at the middle location for the testing of
stability. Test of uniformity, instead, was executed at varying
submersion lengths of 75mm, 150mm, 200mm, and 250mm
while the temperature test points were secured at 150°C, 175°
C, 200°C, 225°C, and 250°C. The SPRT was utilized to create
the point of reference by submerging it at a depth of 200mm.
It is made fixed at the calibration bath’s halfway point. The
PRT was utilized for temperature measurement at varying test
points. Careful attention during setup were done to guarantee
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that the liquid bath is occupied with silicone oil up to a level The noted temperatures for analyzing stability were observed
that will run-off from the calibration chamber’s inner tubing at a height of 200mm from the calibration bath surface. It is
[6]. The whole setup could warmup for 30 minutes before test still uniform inside the uniformity test’s results range for both
point setting. After it was warmed and set up, the 1st test point, horizontal and vertical analyses. Refer also to 3.2.
150°C, was set on the calibration bath. Its stabilization period
was observed. Several calibration bath models have
dissimilar period of stabilization from ambient temperature to
the “set point” temperature. In this paper, the used bath
observed the requirement from the manual of the
manufacturer. After the stabilization period, it was stabilized
for 5 additional minutes before the 1st recorded digital
multimeter reading. Measurements were made at varying
periods.

The instruments as listed in Tables 1 and 2 below are the

equipment utilized through the test.

Table 1: List of instrument used

Description Code Brand/Model
No.
Calibration T049 ASL CB15-45e Calibration
Enclosure Liquid Bath
SPRT1 T038 Hart 5699 SPRT
(Reference,
Fixed)
SPRT2 (Test, T033 Isotech 670SH PRT
Movable)

Table 2: List of equipment used

Indicator Used Code No. Setting
Agilent 34401A E050 4-wire, 100W
DMM
Fluke 8842A DMM T038 4-wire, 100W

A comprehensive procedural guide on the gathering of data

was observed as specified in [4] (pp. 44-50).

3. RESULTS AND DISCUSSION

3.1 Result of Stability Test for 1500C to 2500C

Calibration bath stability at every temperature setting have a

tendency to rise as the temperature approaches 250ºC. As
shown in Figures 3(a) to (e) and Figure 4, the stabilities of the
calibration bath were computed by getting the Maximum
Difference to Minimum Difference range taken at every
temperature point, e.g. 150°C, 175°C. The variances found
were insignificantly distributed since the Standard Deviation Figure 3: (a) to (e) Calibration bath’s stability at various temperature
value is within 0.005 to 0.013. This specifies that the settings
determined values are lower than the suitable limit of 0.01 to
0.05 which was performed in Australia’s CSIRO where a 3.2 Result of Uniformity Test
similar study was performed [2].
Inside the calibration bath, he temperature’s uniformity is
Measured temperatures at lesser set point, e.g. -30ºC, -20°C, 0
largely caused by the liquid’s motion. Irregular temperature
°C are more stable than with greater set points which similarly
may occur in the circulating system at several points [2].
adapts to the measurement results done by [4] for setting
which are less than 30ºC. When the liquid flow rate is improved, the bath’s uniformity
may be increased. Though, it is not recommended because
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amount of stirring must be limited to avoid overheating.

Hence, the following part of this study is the assessment of the
calibration bath’s uniformity by means of horizontal and
vertical positions.
A. Uniformity test with regard to horizontal position
From the documented measurements gathered in the
measurements results, the deviation of reading at every
position, center, front, left, back, and right relative to the
designated reference position was determined. In this part,
the horizontal position illustrates the temperature uniformity
behavior at different temperature set points, i.e., 150°C, Figure 5: Result of Vertical Uniformity
175°C, 200°C, 275°C, and 250°C. The differences of
readings of the two SPRT’s were determined. Taking into
consideration that the Hart SPRT was fixed at the center 4. CONCLUSION AND RECOMMENDATION
position and Isotech PRT was placed at each designated It is possible to say that the local calibration laboratories can
positions. The differences were computed for each also perform the stability and uniformity tests on a calibration
temperature setting. Using the values of the difference of bath at an accuracy level comparable to national laboratories
readings with respect to horizontal position, i.e. center, front since the measured values obtained based on the procedure
left, back and right positions in the calibration bath, a graph outlined were within the values obtained in similar tests
was generated to show the calibration bath’s uniformity. conducted in a national laboratory abroad and have very small
Figure 4 shows the bath’s uniformity with respect to standard deviations. After series of measurements done on
horizontal position. the calibration bath’s stability and uniformity and the analyses
of gathered data, it is also concluded that the method and
procedure can establish the characterization of a calibration
bath controlled by temperature.

This further concludes that the method for testing

implemented in this paper matches the industry’s local
requirement for accuracy. When the test temperature setting
reaches 1750C, bubbles were observed to appear in the
calibration bath. Presence of bubbles affect the calibration
bath’s uniformity and stability as this influence the
homogeneity of the silicone oil.

Figure 4: Result of Horizontal Uniformity Future studies include calibration baths which will be
characterized using different liquids, e.g. ethyl alcohol and
distilled water and development and implementation of
B. Uniformity test with regard to vertical position
software for high temperature calibration bath testing [25].
From the noted measurements gathered in the measurements Likewise, further technique and process validation through
results, the deviation of readings at each length of immersion assessment of measurements’ uncertainty and En-value test
relative to the designated reference length of immersion was can be done to broaden the applicability of the said
determined. In this part, the vertical position illustrates the characterization technique. Since the said stability and
behavior at various immersion length, i.e. at 75, 150, 200, and uniformity determination method and procedure is suitable in
250mm in the bath for different locations, i.e. center, front, in terms of accuracy, the test setup performance is described
back, left, and right. This was computed for each temperature by the uncertainty of measurements where the testing
setting. The difference of readings of the two SPRT’s was conditions are affected by the given parameters: (1)
determined. Taking into consideration that the Hart SPRT environmental conditions of ambient temperature ranging
was fixed at the center position and Isotech PRT was from 20 to 26°C and relative humidity range of 40 to 55%
immersed at 75, 150, 200, and 250mm immersion lengths at R.H. , (2) a stirred-liquid and overflowing calibration liquid
each designated positions. This was computed for each bath functioning at 150°C to 250°C must be the enclosure
temperature setting. Using the values of the difference of used and silicone oil as the only liquid utilized during the test
readings with respect to various immersion lengths or vertical and (3) test thermometers’ accuracy of at least + 0.05°C.
position in the calibration bath, a graph was generated to show
the calibration bath’s uniformity. Figure 5 shows the
uniformity of the bath with respect to vertical position.

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