2430 & TB2448 Comarision

Report No.
2413-021
Messrs.
Report
Comparative testing of ThreeBond 2448
and ThreeBond 2430
Date of issue: May. 30, 2013
Product Development Division

R&D Group Three Bond Co., Ltd.
Office in charge
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Report No.
2413-021
Page 1/5
Date of issue: May. 30, 2013

Messrs.
Product Development Division
R&D Group
Request No. Three Bond Co., Ltd.
Report
Report No. 2413-021
Title Comparative testing of ThreeBond 2448 and ThreeBond 2430
Purpose
Comparative testing of aqueous epoxy MEC ThreeBond 2448 and solvent-based epoxy
MEC ThreeBond 2430 was conducted.
Hereinafter, ThreeBond is abbreviated to TB.
[Properties and characteristics]
Item TB2448 TB2430
Main component Epoxy resin Epoxy resin
Appearance Blue Blue
Breakloose torque *1 Unit: N・m 65.7 to 75.9 65.2 to 76.6
Allowable temperature Sealing 170°C 170°C
limit Locking *2 150°C 120°C
Time to practical
Curing rate 30 min to 1 hr 30 min to 1 hr
strength
(at 20 to 25℃)
Time to final strength 24 hrs 24 hrs
Applicable minimum
M2 M2
screw diameter
*1 JIS Class 2, M10×P1.5, zinc plating chromate treatment bolt/nut, tightening torque : 30 N・m,
curing conditions: 25°C ×24 hrs
*2 Temperature at which return torque higher than tightening torque can be obtained
[Breakloose torque at each size]

Breakloose torque Tightening
Bolt size Pitch (N・m) torque
TB2448 TB2430 (N・m)
M2 0.25 0.36 0.32 0.30
M4 0.70 3.3 3.5 2.0
M6 1.00 13.4 13.3 8.0
M8 1.25 26.3 26.3 15
M10 1.50 70.3 70.6 30
M12 1.50 101.0 102.0 50
M14 2.00 168.0 164.0 90
<Test method>
Bolts of each size processed are tightened, and the breakloose torque is measured after the
agent is cured at 25°C for 24 hours.
<Test conditions>
* Bolt and nut: Zinc plating chromate treatment
*Treatment: Treated with TB2448 and TB2430
* Number of test pieces: n = 5
* Measuring conditions: 3TS-4150-005 (bolt M10), 3TS-4150-002 (other than bolt M10)

Report No.
2413-021
Page 2/5
[Sealing test (oil-tightness)]

Sealing Test Pressure (MPa)
test block temperature
material (°C) 2.0 4.0 6.0 8.0 10.0
25 0/10 0/10 0/10 0/10 0/10
Iron
170 0/10 0/10 0/10 0/10 0/10
TB2448
25 0/10 0/10 0/10 0/10 0/10
Aluminum
170 0/10 0/10 0/10 0/10 0/10
25 0/10 0/10 0/10 0/10 0/10
Iron
170 0/10 0/10 0/10 0/10 0/10
TB2430
25 0/10 0/10 0/10 0/10 0/10
Aluminum
170 0/10 0/10 0/10 0/10 0/10
<Test method>
Bolt processed are tightened on a sealing test block at each tightening torque, and the agent is
cured at 25 ℃ for 24 hours. Then, the block is mounted on sealing testing equipment.
Immediately the hydraulic pressure is increased to 2.0 MPa, and the block is kept at the pressure
for 5 minutes, for which the bolts are checked for leak. Then, the pressure is increased by 2.0
MPa up to 10 MPa. The block is kept at each pressure for 2 minutes. The bolts are visually
checked for leak at each pressure using a developer.
<Test conditions>
* Bolt: JIS, Class 2, zinc plating chromate treatment M10×P1.5
* Treatment: Treated with TB2448 and TB2430
* Sealing test block: Iron and aluminum
* Tightening torque: 30 N・m
* Test temperature: 25°C and 170°C
* Test medium: Turbine oil

Report No.
2413-021
Page 3/5
[Chemical resistance test]
<Test method>
After bolts processed are tightened, and the agent is cured at 25°C for 24 hours. Then, the bolts
are immersed in each immersion liquid. After a lapse of the specified time, the bolts are taken out
from the immersion liquid, and the breakloose torque is measured.
<Test conditions>
* Bolt and nut: JIS Class 2, zinc plating chromate treatment, M10×P1.5
* Tightening torque: 30 N・m
* Immersion conditions: 10% sodium hydroxide solution, gas oil, gasoline (regular), n-hexane and
methanol, at 40°C for 7 days
Other solvents: at 100°C for 7 days
* Measuring conditions: 3TS-4150-005

Report No.
2413-021
Page 4/5
[Breakloose torque to each material]
<Test method>
After blots processed are tightened and the agent is cured at 25°C for 24 hours, the breakloose
torque is measured.
<Test conditions>
* Bolt and nut: JIS Class 2, M10×P1.5
* Tightening torque: 30 N・m (Brass, and aluminum bolts: 15 N・m)
* Measuring conditions: 3TS-4150-005

Report No.
2413-021
Page 5/5
[Axial tension at each tightening torque]

Tightening Axial tension (kN)
torque
TB2448 TB2430 No coating
（N・m）
20 5.7 5.5 4.1
30 9.2 9.1 6.2
40 11.1 11.1 8.4
50 13.6 14.1 10.6
60 17.5 17.8 12.8
<Test method>
Bolts processed are set on tightening testing equipment, and the axial tension at each tightening
torque is measured.
<Test conditions>
* Bolt: JIS, Class 2, M10×P1.5, zinc plating chromate treatment,
hexagon headed bolt, property class10.9
* Nut: ISO Class 1, zinc plating chromate treatment, hexagon nut
* Test equipment: Tightening test equipment NST-500NM made
by Japan Instrumentation System Co., Ltd.

2430 & TB2448 Comarision

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Report No.

Date of issue: May. 30, 2013

Product Development Division

PDF created with pdfFactory Pro trial version www.pdffactory.com

Date of issue: May. 30, 2013

Title Comparative testing of ThreeBond 2448 and ThreeBond 2430

[Breakloose torque at each size]

PDF created with pdfFactory Pro trial version www.pdffactory.com

[Sealing test (oil-tightness)]

PDF created with pdfFactory Pro trial version www.pdffactory.com

[Chemical resistance test]

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[Breakloose torque to each material]

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[Axial tension at each tightening torque]

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