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A Practical Guide To Microstructural Analysis of Cementitious Materials

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A Practical Guide to

Microstructural Analysis of
Cementitious Materials

Edited by
Karen Scrivener
Ecole Polytechnique Federale de Lausanne, Switzerland

Ruben Snellings
VITO, Mol, Belgium

Barbara Lothenbach
EMPA, Dübendorf, Switzerland

~CRC Press
~ Taylor&. Francis Group
Boc• Raton London New Yortc

CRC Preu ls an lmprfnt of the


Tl)ltor &: Fnmcls Group, an lnfonn• buslness
A SPON PRESS BOOK
Contents

List of abbreviations vii


Preface XI
Editors XV
Contributors xvii

1 Sample preparation 1
FRANK WINNEFELD, AXEL SCHÖLER AND BARBARA LOTHENBACH

2 Calorimetry 37
LARS WADSÖ, FRANK WINNEFELD, KYLE RIDING AND PAUL SANDBERG

3 Characterisation of development of cement hydration


using chemical shrinkage 75
METTE GEIKER

4 X-ray powder diffractioµ applied to cement 107


RUBEN SNELLINGS

5 Thermogravimetric analysis 177


BARBARA LOTHENBACH, PAWEt DURDZINSKI AND KLAARTJE DE WEERDT

6 High-resolution solid-state nuclear magnetic resonance


spectroscopy of portland cement-based systems 213
J0RGEN SKIBSTED

7 Proton nuclear magnetic resonance relaxometry 287


ARNAUD C. A. MULLER, JONATHAN MITCHELL AND PETER J. MCDONALD

y
vl Contents

8 Electron microscopy 351


KAREN SCRIVENER, AMELIE BAZZONI, BERTA MOTA AND JOHN E. ROSSEN

9 Mercury intrusion porosimetry 419


ELISE BERODIER, JULIEN BIZZOZERO AND ARNAUD C. A. MULLER

10 Laser diffraction and gas adsorption techniques 445


MARTA PALACIOS, HADI KAZEMI-KAMYAB, SARA MANTELLATO
AND PAUL BOWEN

11 Ternary phase diagrams applied to hydrated cement 485


DUNCAN HERFORT AND BARBARA LOTHENBACH

Glossary 503
Index 509

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