xi yi ei ei/var(ei) resumen estadístico

9.8 0.1742 0.264926519 1.352343372 N= 15

9.8 0.1740 0.264692866 1.351150666 Intercepto -0.4288
9.8 0.1751 0.265780336 1.356701763 sa = 0.0850645727044148
49.8 1.0033 -0.28579067 -1.45884649 pendiente (m) = 0.0345
49.8 1.0068 -0.28230525 -1.44105482 sm = 0.0005626201540874
49.8 1.0054 -0.28370861 -1.44821841 sy/x = 0.195901813763674
99.9 2.9306 -0.08672468 -0.4426946 r= 0.9983
99.9 2.9445 -0.07274431 -0.37133044 r= 2
0.9966
99.9 2.9432 -0.07412117 -0.3783588 LOD (estimado) = 17.0374
199.1 6.5538 0.114626328 0.585121322
199.1 6.5295 0.090369838 0.46130169 Señal media, y0 = 0.158935382590158
199.1 6.5197 0.080555575 0.411203824 No réplicas = 1
249.2 8.1671 -0.00024243 -0.00123751 Concentración, x = 17.0374343387944
249.2 8.1650 -0.00235148 -0.01200338 sC = 6.10812239796128
249.2 8.1744 0.007037147 0.035921808
xmedia = 121.56
ymedia = 3.76443603223406
Sxx 121240.116
Syy 144.762710673236
Sxy 4182.17170843087

Nivel de prob. (P%) = 95

t(P%)*sa 0.183770836646018
probabilidad (a) 0.0002261916056504
lím. sup. a = -0.244999222054844
lím. inf. a = -0.61254089534688
t(P%)*sm 0.0012154669463846
probabilidad (m) 2.1386389444385E-17
lím. sup. m = 0.0357104166908312
lím. inf. m = 0.0332794827980619
t(P%)*sC 13.1957961783939
lím. sup. C = 30.2332305171883
lím. inf. C = 3.84163816040051
#REF!
1823.4 56.46654048
sumatorios=
xi - xmedia yi - ymedia (xi - xmedia)2 (yi - ymedia)(x
2
i-xmedia)·(yi-ymedia) xi2 residual, ei xj
10 -3.59022906
-111.76 12490.2976 12.88974473 401.2440002 96.04 0.264926519 9.8
-111.76 -3.59046272 12490.2976 12.89142252 401.2701133 96.04 0.264692866 21.77
-111.76 -3.58937525 12490.2976 12.88361467 401.1485776 96.04 0.265780336 33.74
-71.768 -2.76114827 5149.4976 7.623939748 198.1399996 2480.04 -0.28579067 45.71
-71.76 -2.75766285 5149.4976 7.604704378 197.8898859 2480.04 -0.28230525 57.68
-71.76 -2.75906621 5149.4976 7.612446336 197.990591 2480.04 -0.28370861 69.65
-21.666 -0.83388529 469.1556 0.695364673 18.06195533 9980.01 -0.08672468 81.62
-21.66 -0.81990492 469.1556 0.672244074 17.75914052 9980.01 -0.07274431 93.59
-21.66 -0.82128179 469.1556 0.674503772 17.78896349 9980.01 -0.07412117 105.56
77.544 2.789364731 6012.4516 7.780555605 216.2873413 39640.81 0.114626328 117.53
77.54 2.765108241 6012.4516 7.645823584 214.406493 39640.81 0.090369838 129.5
77.54 2.755293978 6012.4516 7.591644906 213.6454951 39640.81 0.080555575 141.47
127.642 4.402692955 16291.9696 19.38370526 561.9597288 62100.64 -0.00024243 153.44
127.64 4.400583902 16291.9696 19.36513868 561.6905292 62100.64 -0.00235148 165.41
127.64 4.409972533 16291.9696 19.44785774 562.8888941 62100.64 0.007037147 177.38
00 0 0 0 0 0 #N/A 189.35
00 0 50 0 0 100 0 150 0 #N/A 200 201.32 250
0 0 0 0 0 0 #N/A 213.29
-20 0 0 0 0 0 #N/A 225.26
0 0 0 0 0 0 #N/A 249.2
0 0 0 0 0 0 #N/A
0 50 100 150 200 250
0.3
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0.2
0 0 0 0 0 0 #N/A
0.1 0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0
0 0 0 0 0 0 #N/A
-0.1 0 0 0 0 0 0 #N/A
-0.2 0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
-0.3
0 0 0 0 0 0 #N/A
-0.4 0 0 0 0 0 0 #N/A
residuales
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
 0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
0 0 0 0 0 0 #N/A
-1.1369E-13 0 121240.116 144.7627107 4182.171708 342892.62 #N/A
 yj yi+t·syj yi-t·syj
-0.09071955 0.36700195 -0.54844105 CONCENT SEÑAL SEÑAL Y RELACIÓN
0.322185 0.77580149 -0.13143149 9.8 100.5 576.9 0.17420697
0.73508955 1.18503424 0.28514486 9.8 100.4 577.1 0.17397331
1.14799409 1.59471088 0.70127731 9.8 100.8 575.8 0.17506078
1.56089864 2.00484109 1.11695619 49.8 579.8 577.9 1.00328777
1.97380319 2.41543343 1.53217295 49.8 579.7 575.8 1.00677319
2.38670774 2.82649518 1.9469203 49.8 580.4 577.3 1.00536983
2.79961229 3.23803226 2.36119231 99.9 1692.1 577.4 2.93055074
3.21251684 3.65004913 2.77498454 99.9 1698.7 576.9 2.94453111
3.62542138 4.06254871 3.18829406 99.9 1698.2 577 2.94315425
4.03832593 4.47553234 3.60111953 199.1 3776.3 576.2 6.55380076
4.45123048 4.88899976 4.0134612 199.1 3768.2 577.1 6.52954427
4.86413503 5.30294911 4.42532095 199.1 3767.1 577.8 6.51973001
5.27703958 5.71737696 4.8367022 249.2 4710.8 576.8 8.16712899
5.68994413 6.13227836 5.2476099 249.2 4710.4 576.9 8.16501993
6.10284868 6.54764693 5.65805042 249.2 4733.8 579.1 8.17440857
00 6.51575322
250 6.96347497 6.06803148
300
6.92865777 7.37975354 6.47756201
7.34156232 7.79647261 6.88665203
8.16737142 8.63118755 7.70355528

0 250 300
xi yi ei ei/var(ei) resumen estadístico xi - xmedia
9.7 0.1839 -0.03816187 -0.38587092 N= 15 -112.133333 10
9.7 0.1811 -0.04099809 -0.41454915 Intercepto 0.1550 -112.133333
9.7 0.1832 -0.03885255 -0.39285469 sa = 0.04290532 -112.133333
49.9 0.5148 0.01456234 0.14724602 pendiente (m) = 8
0.0069 -71.9333333
49.9 0.4807 -0.01951014 -0.19727532 sm = 0.000283 -71.9333333
49.8 0.4611 -0.0384286 -0.38856802 sy/x = 0.09889801 -72.0333333
99.9 1.0171 0.17094715 1.72851958 r= 0.9893 -21.9333333 6
99.9 0.9537 0.10751947 1.08717525 r2= 0.9787 -21.9333333
99.9 0.9513 0.10510115 1.06272257 LOD (estimado) = 42.8791 -21.9333333
199.9 1.4006 -0.13757546 -1.39108417 78.0666667 4
199.8 1.4043 -0.13317619 -1.34660135 Señal media, y0 = 0.4516525 77.9666667
199.9 1.3988 -0.13937692 -1.40929959 No réplicas = 1 78.0666667
249.8 1.9348 0.0514078 0.51980624 Concentración, x = 42.8790648 127.966667 2
249.9 1.9690 0.0848752 0.85820941 sC = 15.1108547 128.066667
249.8 1.9351 0.05166671 0.52242412 127.966667
xmedia = 121.833333 00
ymedia = 0.99796246 00 5
Sxx 122122.093 0
5.97399113
Syy -20
Sxy 845.002014 0
0
0 50
Nivel de prob. (P%) = 95 0.3
0
t(P%)*sa 0.0926913 0
0.2
probabilidad (a) 0.00316073 0
lím. sup. a = 0.24764977 0.1 0
lím. inf. a = 0.06226717 0
0
t(P%)*sm 0.00061139 0
2.9718E-12 -0.1 0
probabilidad (m)
lím. sup. m = 0.00753071 -0.2 0
lím. inf. m = 0.00630793 0
-0.3
t(P%)*sC 32.6450168 0
lím. sup. C = 75.5240817 -0.4 0
lím. inf. C = 10.234048 0
#REF! 0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
 0
0
0
0
0
0
0
0
0
1827.5 14.9694369 3.2685E-13
sumatorios=
 yi - ymedia (xi - xmedia)2 (yi - ymedia)(x
2
i-xmedia)·(yi-ymedia) xi2 residual, ei xj yj
10 -0.81404844 12573.8844 0.66267486 91.2819649 94.09 -0.03816187 9.7 0.22207589
-0.81688466 12573.8844 0.66730055 91.5999998 94.09 -0.04099809 21.71 0.30517694
-0.81473912 12573.8844 0.66379983 91.3594134 94.09 -0.03885255 33.72 0.38827799
8 -0.48316751 5174.40444 0.23345085 34.7558499 2490.01 0.01456234 45.73 0.47137904
-0.51723999 5174.40444 0.26753721 37.2067965 2490.01 -0.01951014 57.74 0.55448009
-0.53685039 5188.80111 0.28820834 38.671123 2480.04 -0.0384286 69.75 0.63758114
6 0.01918336 481.071111 0.000368 -0.42075512 9980.01 0.17094715 81.76 0.72068219
-0.04424431 481.071111 0.00195756 0.97042527 9980.01 0.10751947 93.77 0.80378324
-0.04666264 481.071111 0.0021774 1.02346713 9980.01 0.10510115 105.78 0.88688429
4 0.4025929 6094.40444 0.16208104 31.4290858 39960.01 -0.13757546 117.79 0.96998534
0.40630023 6078.80111 0.16507988 31.6778747 39920.04 -0.13317619 129.8 1.05308639
0.40079143 6094.40444 0.16063377 31.2884511 39960.01 -0.13937692 141.81 1.13618744
2 0.9368503 16375.4678 0.87768848 119.88561 62400.04 0.0514078 153.82 1.21928849
0.97100963 16401.0711 0.9428597 124.353967 62450.01 0.0848752 165.83 1.30238954
0.9371092 16375.4678 0.87817365 119.918741 62400.04 0.05166671 177.84 1.38549059
0 0 0 0 0 0 #N/A 189.85 1.46859164
0 0 50 0 0 100 0 1500 #N/A 200 201.86 1.55169269
250 300
0 0 0 0 0 #N/A 213.87 1.63479374
0 0 0 0 0 #N/A 225.88 1.71789479
-2
0 0 0 0 0 #N/A 249.9 1.88409689
0 0 0 0 0 #N/A
0 50 100 150 200 250 300
0.3
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0.2
0 0 0 0 0 #N/A
0.1 0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0
0 0 0 0 0 #N/A
-0.1 0 0 0 0 0 #N/A
-0.2 0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
-0.3
0 0 0 0 0 #N/A
-0.4 0 0 0 0 0 #N/A
residuales
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 0 0 0 0 #N/A
0 122122.093 5.97399113 845.002014 344772.51 #N/A
 yi+t·syj yi-t·syj CONCEN SENAL CL SEÑAL N RELACION
0.45314365 -0.00899187 9.7 106.1 576.9 0.18391402
0.53417349 0.07618038 9.7 104.5 577.1 0.1810778
0.61542193 0.16113405 9.7 105.5 575.8 0.18322334
0.69689434 0.24586374 49.9 297.5 577.9 0.51479495
0.7785956 0.33036458 49.9 276.8 575.8 0.48072247
0.86053003 0.41463224 49.8 266.2 577.3 0.46111207
0.94270131 0.49866307 99.9 587.3 577.4 1.01714583
1.02511241 0.58245406 99.9 550.2 576.9 0.95371815
1.10776559 0.66600299 99.9 548.9 577 0.95129983
1.19066232 0.74930836 199.9 807 576.2 1.40055536
1.27380327 0.8323695 199.8 810.4 577.1 1.40426269
1.35718832 0.91518656 199.9 808.2 577.8 1.39875389
1.44081652 0.99776046 249.8 1116 576.8 1.93481276
1.52468615 1.08009293 249.9 1135.9 576.9 1.96897209
1.6087947 1.16218647 249.8 1120.6 579.1 1.93507166
1.69313898 1.2440443
250 1.77771508 1.3256703
300
1.8625185 1.40706898
1.94754418 1.4882454
2.1182398 1.64995398

250 300
Datos Muestra Datos Estándar
tab alpuri 20 tabletas Peso tomado alpuri
principio act. 100 mg %pureza
peso prom 175 mg matraz
Peso equivalente tomado 150 mg alicuota
matraz 100 mL matraz
alicuota 2 mL
matraz 50 mL
(A) UV-VIS

(A) 0.335

Conce de la sln estandar

49.698

Conce estandar
1.98792
0.1590336

Señales
0.0622386168224299

Análisis
3.1119308411215
155.596542056075

mg de alpurirol
103.731028037383

% según USP
103.7
Porcentaje aceptado por USP
 50.2 mg
0.99 % 0.99
25 mL
2 mL
25 mL

0.856

de la sln estandar Peso

mg 175 mg---------- 100
X mg---------- 150
nce estandar
mg/ml 262.5
mg/ml

Señales
mg/ml

Análisis
mg/ml
mg/ml

g de alpurirol
mg alpuriro por tableta

según USP
%
rcentaje aceptado por USP