Notes On Sample Examination
Notes On Sample Examination
There is a universal format for the description of rock cutting. It is recommended that all cutting
descriptions must adhere to this format.
1. Rock Name
2. Colour(s)
3. Hardness / fissility
4. Elements or grains
Clastic Carbonates
a. grain size a. ‘grain’ nature
b. roundness b. ‘grain’ size
c. sphericity
d. sorting
5. Cement / Matrix
a. abundance a. abundance
b. nature b. crystallinity
Example:
1030-1060 CLAYSTONE: dark grey, occasionally dark green/grey, firm to hard, slightly fissile
trace calcareous, rare glauconitic, slight earthy texture.
Cutting Descriptions / Rock Identification
This section contains useful information that will add in sample descriptions and the identification
of rock types.
Rock Types
Argillaceous Rocks:
- shale
- clay
- claystone
- marl
Carbonate Rocks
- Limestone
- Dolomite / Dolostone
- Chalk
Siliceous Rocks
- Siltstone
- Sand
- Sandstone
- Chert
- Breccia / Conglomerate
Evaporites
- Gypsum
- Anhydrite
- Halite
Organic Materials
- Coal
- Lignite
- Bituminous Minerals
ABUNDANT 15-20%
MODERATELY
10-15%
ABUNDANT
MINOR 5-10%
RARE 1-5%
TRACE <1%
Classification of Carbonate Rocks According to Depositional Texture
Durham’s Classification
MUDSTONE
Original Components Not Bound Less than 10%
Together During Deposition grains
Contains Mud
Depositional Texture Recognisable
CRYSTALLINE CARBONATE
Recognisable
Texture Not
Depositional
The following lists for each rock type contain standard terms that are used when describing
sedimentary rocks.
Argillaceous
1) Rock Type – Shale, Clay, Marl
2) Colour
Black Olive White Dark
Blue Orange Yellow Varicoloured
Brown Pink Pale Mottled
Grey Purple Light Dusky
Green Red Medium
3) Hardness
Plastic Brittle
Soft Poorly Compacted
Firm Moderately Compacted
Hard Well Compacted
4) Texture
Amorphous Micro Blocky Sub Fissile
Blocky Fisslie Splintery
Dispersive Sub Blocky Papery
5) Major Characteristics
Calcareous Sandy
Carbonaceous Pyritic
Dolomitic Silty
Fossiliferous Sulfureous
Glauconitic Micaceous
6) Sedimentary Features
Waxy Rough
Earthy Gritty
Laminated Smooth
Banded
4) Crystal Size
1.000 – 2.000 mm Very Coarse
Crystalline
0.500 – 1.00 mm Coarse Crystalline
0.250 – 0.500 mm Medium Crystalline
0.125 – 0.250 mm Fine Crystalline
0.063 – 0.125 mm Very Fine Crystalline
0.004 – 0.063 mm Microcrystalline
< 0.004 mm Cryptocrystalline
5) Crystal Shape
Euhedral
Sub Euhedral
Anhedral
Fibrous
Scaly
6) Hardness
Soft Firm
Friable Hard
Indurable Brittle
7) Fossil and Accessories
Siliceous
1) Rock Type – Siltstone, Sandstone, Sand, Chert
2) Colour
Amber Milky Clear
Black Pink Light
Blue Red Transparent
Brown Smokey Translucent
Grey White
Green Yellow
3) Texture
1.000 – 2.000 mm Very Coarse
0.500 – 1.00 mm Coarse
0.250 – 0.500 mm Medium
0.125 – 0.250 mm Fine
0.063 – 0.125 mm Very Fine
0.002 – 0.063 mm Silt
< 0.002 mm Shale-clay
Microcrystalline Chert
Roundness
Sorting
5) Induration - Hardness
Poorly Indurated Loose
Moderately Indurated Friable
Well Indurated Moderately Hard
Hard
Very Hard
6) Accessories
Biotite Glauconite Olivine Siderite
Chert Lignite Pyrite Shale
Feldspar Muscovite Sulphur Fossils
7) Porosity
None – Grains packed tightly together
Poor Intergranular Porosity – pores are not connected
Fair Intragranular Porosity – Pores present within grains
Good Intergranular Porosity – Some pores between grains are connected
Excellent Intergranular Porosity – All pores are connected
Sulplates
5) Transparency
Transparent
Translucent
Opaque
6) Hardness
Gypsum Anhydrite
Soft Poorly Indurated
Moderatley Indurated
Well Indurated
7) Porosity
Gypsum – None Anhydrite – Fractures (secondary porosity)
Oil Shows – Procedure and Description
Evaluation of oil shows in cuttings includes the description of odour, staining, bleeding,
fluorescence, leach tests and residues.
ODOUR
The smell should be described in the range of faint, fair to strong, as this will normally
distinguish between condensates, light oils and heavy oils.
Typically, if bleeding is seen in drilled cuttings it is an indication of a tight formation since the
hydrocarbons have been retained. Good permeability would result in most hydrocarbons being
flushed.
Oil staining is more representative of porosity and oil distribution. Descriptions of the staining
should include colour and distribution.
Heavier oil stains tend to be dark brown, while lighter oil stains are typically light to colourless.
Live, volatile oil will smoke and smell when held in a flame; the flame will usually turn blue.
The amount of oil staining should be characterised in terms of none, rare, common, abundant
etc and the distribution should be described as spotty, patchy, streaky or uniform.
FLUORESENCE
Crude oils under ultra-violet light will produce a fluorescence glow. The fluorescence can be
assessed in terms of concentration, colour and intensity, which can be used to evaluate oil type
and production potential. However, there are limitations to this process due to colour
perception of the geologists, other materials also fluoresce, and only a small proportion of the
fluorescence produced my the UV light is seen by the naked eye.
1. Check sample staining while still wet under a microscope. Stain will range from light brown
through to dark brown and black for asphaltic residue. Describe the distribution of the
stain, spotty, streaky, patchy or uniform and the amount of the staining.
2. Next observe the FLUORESCENCE, noting the intensity and brightness. Always keep the
previous sample for comparison. As the logging unit is hot/dry, hydrocarbons quickly
evaporate so check for fluorescence as soon as possible. The depth of colour and its
intensity/brightness should be note – dull yellow, bright yellow etc…
3. Next the sample is cut with a strong solvent i.e. trichloroethane or Propanol. This solvent
will leach out any hydrocarbons in the rock. The cut is an indication of the permeability of
the rock.
Cuts can be DIFFUSE or STREAMING depending on porosity and permeability. The speed
of the cut is also noted as well as the colour of the cut. Colour will range as follows:
PALE BLUE
BLUE/WHITE TO PALE WHITE
MILKY WHITE
YELLOW WHITE
If there is little or no cut then a crush cut can be performed. This is when a sample is
crushed slight before adding the solvent. A crush cut will indicate a rock with low
permeability.
A crush cut is described as a normal cut but it must be noted that a crush cut was
performed.
NB. If performing a cut on chalk, the sample must be DRY before attempting the cut, as
wet chalk will always produce a weak cut due to poor permeability and surface tension.
4. A Natural cut is the colour of the solvent (in natural light) immediately after cutting. This
colour will range from slight discolouration to dark brown.
5. After the solvent has evaporated a residual ring is left. The fluorescence of the residue is
noted plus its colour in natural light.
HCl Effervescence
A quick test can be made with 10% hydrochloric acid to distinguish between calcite and dolomite.
Separate the cuttings from the sample tray and place in a porcelain spot tray. Add a few drops of
acid to the sample and view the results: -
If oil is present, large bubbles will form on a cutting when it is immersed in dilute HCl.
Swelling
Swelling clays will also tend to be soft and sticky (although oil-based and inhibitive mud systems
will prevent swelling) making sample washing and sample description very difficult.
If a white precipitate forms, then the sample is indeed a sulphate – either gypsum or anhydrite.
To distinguish between the two, it should be noted that gypsum is not so common in the
subsurface, therefore, the sample will typically be anhydrite. Also anhydrite is commonly
associated with dolomite.
However, to confirm the distinction use the following procedure:
Chloride Test
To confirm the presence of salt or Halite (NaCl) the following test can be used:
Alizarin Red
This can simply be dropped on to the cuttings – if calcite is present it will turn a deep red colour
while everything else remains uncoloured.
Cement Test
After drilling through casing shoes at the start of a new hole section, it is useful to confirm the
presence of cement.
As it is alkaline, this can be done by adding phenolphthalein (pH indicator) after washing the
sample. If the “cuttings” turn bright purple then they are cement.
Standard Abbreviations