Chapter 3 Smart Sensor Fabrication Technology
Chapter 3 Smart Sensor Fabrication Technology
SYSTEMS
( MEMS )
Fabrication
(Manufacture)
Packaging
Manufacturing
MEMS STEPS Testing
•The MEMS materials:
• Primarily silicon its compounds
• Other materials are quartz crystal, glass, metals
such as aluminum, titanium, tungsten and copper
• Polymers such as photo resist.
•What is Micromachining ?
• Micromachining is a parallel (batch) process in
which dozens to tens of thousands of identical
elements are fabricated simultaneously on the
same wafer.
• Divided into three major categories: basic,
advanced, and nonlithographic processes.
MEMS and sensors technology
Recent development of MEMS and sensors technology is essentially based on
micromachining. This technology consists of specific design and fabrication
processes, many of which are borrowed from the integrated circuit industry.
The PECVD process can operate at lower temperatures (down to 300° C) thanks to
the extra energy supplied to the gas molecules by the plasma in the reactor.
However, the quality of the films tend to be inferior to processes running at higher
temperatures. The material is deposited on one side of the wafers.
High temperature
Oxide Doped Semiconductor
Impurity
P2O5
Deposition of Silicon Nitrides
However, the quality of the films tend to be inferior to processes running at higher
temperatures. The material is deposited on one side of the wafers.
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Add material: Plasma Enhanced CVD (PECVD)
Vapor Phase Epitaxy (VPE) is the most important process in which the conditions
are created to support epitaxial growth.
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8
BASIC PROCESS TOOLS
Deposition Process
Epitaxy: Epitaxy is a deposition method to grow a crystalline silicon layer over a
silicon wafer, but with a differing dopant type and concentration
Impurity dopants
Silicon Contain source gas High Temperature
[AsH3 ; PH3]
[SiH4/SiCl4/SiH2Cl2] ( 800 C )
(Controlled) [Controlled]
800C
Wafer Scale p-n junction for
Controlled electrochemical etching
Epitaxial growth
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One of the methods of manufacturing SOI (silicon-on-insulator) substrates
0
Thermal oxidation
The substrate can be oxidized in an oxygen rich atmosphere.
In the case of silicon the temperature is raised to 800° C - 1100° which gives high
quality amorphous silicon dioxide.
The final oxide thickness can be controlled by selecting the temperature and
oxidizing conditions.
Thermal oxidation of silicon generates compressive stress in the silicon dioxide
film,as SiO2 molecules take more volume than Si atoms, and there is also a
mismatch between the coefficients of thermal expansion of Si and SiO2 .
As a result, thermally grown oxide films cause bowing of the underlying substrate.
850C 1150C
Si + O2/ Steam SiO2
Evaporation
Condenses on a substrate
to form a film
Evaporation
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Add material and pattern at once: lift-off
sample
sample
sample
sample
Resist dissolution
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Requirements of Deposition
• Advantages
• Uniformly covers substrate
• Simple process without chemicals or gases
• Disadvantages
• Alloys are difficult to deposit
• Different metals have different vapor pressures
• High aspect ratio features are difficult to cover
• Trajectory of evaporated particles tends to be vertical, which may not pattern sidewalls
evenly
Sputtering
In sputtering, a target made of a material to be deposited is physically
bombarded by a flux of inert-gas ions (usually argon) in a vacuum chamber at a
pressure of 0.1–10 Pa.
Atoms or molecules from the target are ejected and deposited onto the substrate.
There are several kinds of sputtering differing by the ion excitation mechanism.
Atoms or molecules from the target are ejected and deposited onto the substrate.
There are several kinds of sputtering differing by the ion excitation mechanism.
Applying external magnetic field increases the ion density near the target,
thus raising the deposition rates (magnetron sputtering).
Construction of the
magnetron cathode
RF and Ion Beam
In RF (radio frequency), the target and Sputtering
the
wafer form two parallel plates with RF
excitation applied to the target.
In ion-beam deposition ions are
generated in a remote plasma, then
accelerated at the target
• Advantages
• Low temperature process
• Good Conformal Coating
• Good Step Coverage
• Disadvantages
• Dielectrics require RF Source
• RF environment may affect other depositions
Casting
In casting the material to be deposited is dissolved in a solvent and then applied
to the substrate by spraying or spinning.
This is particularly useful for polymer materials, which may be easily dissolved in
organic solvents, and it is the common method used to apply photoresist to
substrates (in photolithography).
The thicknesses obtained range from a single monolayer of molecules (adhesion
promotion) to tens of micrometers. In recent years, the casting technology has also
been applied to form films of glass (SOG) materials on substrates.
Thick (5–100 μm) SOG has the ability to uniformly coat surfaces and smooth out
underlying topographical variations, effectively planarizing surface features.
The mask itself consists of a patterned opaque chromium (the most common),
emulsion, or iron oxide layer on a transparent fused-quartz or soda-lime glass
substrate.
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Lithography – positive and negative resist
When resist is exposed to a
radiation source of a specific
wavelength (from UV to blue),
the chemical resistance of the
resist to developer solution
changes.
Photoresist may also be used as a template for patterning material deposited after
lithography. The resist is subsequently etched away, and the material deposited on
the resist is "lifted off".
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Lithography - alignment
• Wet Etch
Masking material
• Chemical solution
• Usually Isotropic (can be
anisotropic in crystals)
• Very selective: resist etch rate Etching
vs. material etch rate
• High etch rate
• Difficult to control precisely
• Resolution limitation
• Batch processing
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Etching: In etching, the objective is to selectively remove material
using imaged photoresist as a masking template.
Wet Etching :-
Anisotropic Wet Etching:
Dipped into Removal of material
Depending on the
Substrate Crystallographic orientation
KOH Solution
Anisotropic etching
• Dry Etch
• Gas phase
• Sputter + chemical etch
• Anisotropic
• Less selective
• High resolution
• Excellent control
• Single wafer processing
Gas available @ McGill:
• Oxides/Nitrides: CF4, CHF3,
O2, Ar
• Silicon: HBr, Cl2, Ar
• Metals: HBr, Cl2, Ar, N2, NF3
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Deep Reactive Ion (DRIE) etching
In this process, etch depths of hundreds of microns can be achieved with almost
vertical sidewalls.
The primary technology is based on the so-called "Bosch process", where two
different gas compositions are alternated in the reactor.
The first gas composition creates a polymer on the surface of the substrate, and the
second gas composition etches the substrate. The polymer is immediately
sputtered away by ion bombardment, but only on the horizontal surfaces and not
the sidewalls. Since the polymer only dissolves very slowly in the chemical part of
the etching, it builds up on the sidewalls and protects them from etching.
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Remove silicon: Deep Reactive Ion Etching
• DRIE
• We need 2 gases, one for etching
and another one to deposit a
protective polymer.
• We need to alternate etching and
deposition then we pulse the gas
injection
• We need energetic ions to remove
the polymer on the feature bottom
to allow Si etching during SF6 cycle.
C4F8 deposition
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Pattern material: Mask design
CleWin LASI
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Pattern material: Electrolithography E-beam
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To the outside world: Dicing
• Dicing:
• Precision diamond saw to cut out wafer in small dies
• Blade thicknesses from 100 to 250µm
• Accurate alignment (~ 50µm)
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To the outside world: wire bonding
• WireBonder
• Connect microelectrodes to the outside world
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Screen printing
A wide variety of materials, including metals, chemical compopunds and ceramics,
can be applied using screen printing (e.g. in sensor technology).
Screen printing begins with the production of a stencil, which is a flat, flexible
plate with solid and open areas.
The stencil has a fine-mesh screen as a bottom layer.
Separately, a paste is made of fine particles of the material of interest, along with
an organic binder and a solvent. A mass of paste is applied to the stencil, then
smeared along with a squeegee. A layer of paste is forced though the openings in
the stencil, leaving a pattern on the underlying substrate.
Drying evaporates the solvent. Firing burns off the organic binder and sinters the
remaining metal or ceramic into a solid.
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Screen printing
Image reproduction
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New Methods for
Nanomanufacturing
• Thinner layers are necessary for higher speed transistors in IC design
• Gate oxide thickness < 50 A
• Approaches atomic layer dimensions
• Atomic Layer Deposition
• A 2 step process of deposition and re-layering
• SiOH* + SiCl4 →Si –O-SiCl3 + HCl
• SiCl* + H2O → SiOH* + HCl
New Methods for
Nanomanufacturing
• Molecular vapor deposition
• Anti-stiction layers in MEMS are needed to avoid structures fusing to
substrates
• Vapor deposition of compounds avoids contamination found in liquid
processes
• Oxygen plasma clean operation precedes deposition process
LIGA Process
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Achievable machining accuracies
Levels of precision required
Level Tolerance Mechanical Electronic Optical Surface finish
(µm)
Normal 200 µm Normal domestic General purpose Camera, telescope and Shaping 12.5–16
appliances and electrical parts, e.g., binocular bodies Milling 6.3–0.8
automotive fittings, switches, motors, and Reaming 3.2–0.8
etc connectors Turning 6.3–0.4
Drilling 6.3–0.8
50 µm General purpose Transistors, diodes, Camera shutters, lens
mechanical parts for magnetic heads for holders for cameras
typewriters, engines, tape recorders and
etc microscopes
Precision 5 µm Mechanical watch Electrical relays, Lenses, prisms, optical Boring 6.3–0.4
parts, resistors, condensers, fiber and connectors Laser 6.3–0.8
machine tool silicon wafers, TV (multi mode) ECM 3.2–0.2
bearings, color masks Grinding 3.2–0.1
gears, ballscrews,
rotary
compressor parts
0.5 µm Ball and roller Magnetic scales, CCD, Precision lenses, ELID 0.6–0.2
bearings, quartz oscillators, optical Honing 0.8–0.1
precision drawn wire, magnetic memory scales, IC exposure
hydraulic servo- bubbles, magnetron, masks (photo x-ray),
valves, IC line width, thin film laser polygon mirrors,
aerostatic bearings, pressure transducers, x-ray mirrors, elastic
ink-jet nozzles, thermal printer deflection mirrors,
aerodynamic gyro heads, monomode optical
bearings. thin film head discs. fiber
and connectors.
Levels of precision required
turbulence
Micro
projection
array
Milling Turning
In situ
Scribing
measurement
Microgrinding
Microdrilling applications
• Coarse microdrilling machines drill holes from 0.03 mm in diameter to
0.50 mm in diameter, with increments of 0.01 mm
• Air bearings and bushings
• EDM (Electrochemical Discharge Machining) tooling
• Electronic components
• Gas and liquid flow
• Microwave components
• Nozzles
• Optical components
• Laser is a good option
Laser drilling
• Application of lasers to micromanufacturing has several advantages
• Noncontact processing
• Capability of remote processing
• Automation
• No tool wear
• Possibility of machining hard and brittle materials
Stimulated emission
Pumping and cavity
Properties of laser light
• Monochromaticity
• Directionality → 1 mrad (0.06°)
• Brightness → 3 mW HeNe laser @ 1 mm beam diameter = 240
brighter than the Sun
• Coherence → coherence length = 3.105 m against 3 µm for white light
• Spatial profile → Gaussian beam most studied
• Temporal profile → continuous or pulsed
Gas lasers
200 µm
100 µm
100 µm
1 µm
100 µm 200 µm