International Journal of Chemical Engineering and Applications, Vol. 3, No.

6, December 2012

Design of Gas-Liquid Separator for Complete Degasing

Tamagna Uki, Subhash T. Sarda, and Thomas Mathew

 available pressure drop (15 Bar). The GLS design is divided

Abstract—Entrapment of Gas in Liquid flow stream can into three sections;
cause substantial problems in process plant operations. Release A. Design of the Main Vessel and Gas Outlet Nozzle
of gas slug can possibly lead to unwanted release of Chemicals
into the environment. Hence, design of Gas-Liquid Separator The sizing main vessel of the GLS is based on the design
(GLS) becomes very important in a process plant. The GLS procedure stated in GPSA Data book [1]. The vessel is
should be properly sized to discretely separate gas and liquid designed with an assumption that, the drum designed will
phases. The paper discusses a Case study of a problem faced not allow liquid droplets of size greater than 100 microns
by the authors in one of their operating plants and the remedy
(Dp) and spherical in shape, to entrain into the vapor space
for it. It outlines the sizing procedure used for design of GLS
for industrial application and its impact on the process. of the vessel.
The gas space of the GLS is designed first. This
determines the diameter of the vessel and the height of the
Index Terms—Gas-liquid separator, design, case study.
gas space to obtain optimum separation of the gas and liquid.
Liquid droplets in a vessel separate under the influence of
gravity, which has to be more than the drag force acting on
I. INTRODUCTION the droplet. The coefficient of drag (C’) is determined using
One of our Process Plants had gone through several the following equation:
stages of modifications for capacity enhancement and cost
1.31𝑋10 7 𝜌 𝑔 𝐷𝑝 (𝜌 𝐿 −𝜌 𝑔 )
reduction. The plant was commissioned in 1980s and is 𝐶′(𝑁𝑅𝑒 )2 = (1)
𝜇2
currently operating at 190% of its initial designed capacity.
Duringimplementation of one such scheme we faced a
 Design of the main vessel and Gas outlet nozzle.
problem of entrapment of inert gas in a liquid stream that
 Design of the feed inlet deflector
prevented the new scheme to perform as designed.
Investigations revealed limitation in one of the old  Design of the Liquid outlet nozzle and the Vortex
equipment. Subsequent sections discuss the problem, Breaker.
solution implemented and benefits realized.
𝜌𝐿 = 𝐷𝑒𝑛𝑠𝑖𝑡𝑦 𝑜𝑓 𝑙𝑖𝑞𝑢𝑖𝑑

𝜌𝑔 = 𝐷𝑒𝑛𝑠𝑖𝑡𝑦 𝑜𝑓 𝑔𝑎𝑠
II. PROBLEM ROOT CAUSE IDENTIFICATION
The affected unit (Fig. 1) has a Reactor whose Vent Gas 𝜇 = 𝑉𝑖𝑠𝑐𝑜𝑠𝑖𝑡𝑦 𝑜𝑓 𝑔𝑎𝑠
goes to Heat Recovery Unit (HRU). Part of the liquid
condensate from HRU is circulated back to the reactor; the Corresponding Reynold’s Number (NRe) for the system
rest is processed in a distillation column. Uncondensed inert can be obtained from GPSA Data book [1] Fig. 7-3. Since
gases are sent to a separate Gas Handling Unit (GHU). NRe for this case lies between 2 and 500, Terminal settling
Dynamic Simulationofthe system predicted 12 % velocity (Vt) is determined using Intermediate Law equation:
entrapment of inert gases inthe liquid leg due to limitation in
Vent Gas Condenser Separator (VGCS). It disturbed the 2.94𝑔 0.71 𝐷𝑝1.14 (𝜌 𝐿 −𝜌 𝑔 )0.71
𝑉𝑡 = (2)
column and Low Boiling Chemical Processing (LBCP) unit. 𝜌 𝑔0.29 𝜇 0.43

Replacing VGCS was not economically feasible. Hence, it 𝑔 = 𝐴𝑐𝑐𝑒𝑙𝑒𝑟𝑎𝑡𝑖𝑜𝑛 𝑑𝑢𝑒 𝑡𝑜 𝑔𝑟𝑎𝑣𝑖𝑡𝑦
was decided to install a GLS in the affected stream to de-gas
the liquid. The velocity of the gas (Vg) separating in the GLS should
be less than Vt.For a conservative approach,Vg is kept33%
less than Vt i.e.
III. DESIGNING OF THE GAS-LIQUID SEPARATOR
2
The main challenge in the design of GLS was that, the 𝑉𝑔 = 𝑉𝑡 (3)
3
available pressure drop between the gas outlet of the GLS
and the operating pressure of the gas-handling system was This velocity along with the volumetric flow rate of the
only 0.1 Bar. However, the liquid outlet of the GLS and the gas (Qg) can be used to determine the diameter of the vessel.
downstream liquid processing system had adequate (Dv) by using the following equation:

 4𝑄𝑔
Manuscript received September 10, 2012; revised November 15, 2012. 𝐷𝑣 = (4)
𝜋𝑉𝑔
The authors are with Reliance Industries Limited, Mumbai, India (e-mai:
amagna.ukil@ril.com)

DOI: 10.7763/IJCEA.2012.V3.247 477

 International Journal of Chemical Engineering and Applications, Vol. 3, No. 6, December 2012

TO GAS HANDLING UNIT

HEAT RECOVERY UNIT
VENT GAS CONDENSER
VENT
TO ATMOSPHERE
VENT GAS

SEPARATED INERTS

VENT GAS LOW

CONDENSER BOILING
SEPARATOR CHEMICAL

LOW BOILING
CHEMICAL
PROCESSING UNIT

GAS LIQUID
LIQUID RECYCLE SEPARATOR
FEED
TO REACTOR 2-PHASE STREAM
DISTILLATION
COLUMN

DEGASSED LIQUID
REACTOR

PRODUCT CONC. LIQUID

Fig. 1. Affected unit of the plant and location of GLS Subsequent sections outline the steps followed to size the GLS and its internals.

Height of vapor Space(L) can be determined by assuming performance has been identified recently, through the use of
that the time taken by the gas to travel from the feed inlet to Computational Fluid Dynamics (CFD) modeling. Main
the gas outlet nozzle is same as the time taken by the liquid functions of inlet device are:
droplets to settle from the gas phase to liquid.L can be  Reduce the momentum of the inlet stream and enhance
determined by: flow distribution of the gas and liquid.
4𝑄𝑔  Efficient separation of the bulk liquid phase from the
𝐿= (5) gas.
𝜋𝑉𝑔 𝐷𝑣
 Prevent droplet shattering and re-entrainment of bulk
Velocity of the outgoing gas (Vgo) is kept at 0.3 m/s liquid phase.
(minimum allowable velocity for gas pipelines) considering GPSA Data book [1] discusses various types of inlet
minimum pressure drop across the gas outlet nozzle. The devices. In this case, we have selected Half-Pipe inlet
diameter of the outlet nozzle (Do) can be determined by the device (after evaluating various options, viz. Cyclonic feed
following equation: entry, diverter plate etc. on the basis of aforesaid parameters)
4𝑄𝑔 to distribute the flow across the circumference of the vessel.
𝐷𝑜 = (6) Sizing of the inlet device is based on the convention that;
𝜋𝑉𝑔𝑜
diameter of inlet device (𝐷𝑑 ) is twice the diameter of inlet
Simulations show a pressure drop of only 0.004 bar nozzle (𝐷𝑖 ).
across the gas outlet nozzle.
Sizing the liquid space of the GLS, involves assumption 𝐷𝑑 = 2  𝐷𝑖 (8)
of residence time (tr) of the liquid in the vessel. As per
GPSA [1], the trfor a vessel for Gas-Condensate separation CFD model of the Half-Pipe inlet (Figure-2) for the GLS
should be within 120 to 240 seconds. We consider a trof 120 shows the flow pattern inside the vessel
seconds. The height of vessel (Ll) required for holding the
liquid for specified trcan be determined by the following
equation:
4𝑄𝑙
𝐿𝑙 =
𝜋𝐷𝑉2
 𝑡𝑟 (7)

𝑄𝑙 = 𝑉𝑜𝑙𝑢𝑚𝑒𝑡𝑟𝑖𝑐 𝐹𝑙𝑜𝑤 𝑜𝑓 𝑙𝑖𝑞𝑢𝑖𝑑

In addition to Ll, some extra height must be provided to
the GLS forlevel controllability. GPSA [1] states that:
 The distance between center line of the feed inlet
nozzle and the maximum allowable liquid level should
be twice the diameter of the feed nozzle.
 The distance between lowest allowable level of the
liquid and the Bottom Tan Line of the vessel must be
apart by a distance of 0.17 times the diameter of the
GLS.
Following the above steps, the GLS that was designed
had diameter (Dv) of 1300 mm and Tan-to-Tan height of
2000 mm. 2:1 ellipsoidal Dish-ends are provided at the
bottom and top of the vessel.
B. Design of the Feed Inlet Deflector
The importance of inlet device with respect to separation Fig. 2. Influence of inlet distributor on Flow Pattern of feed inside the GLS

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 International Journal of Chemical Engineering and Applications, Vol. 3, No. 6, December 2012

C. Design of the Liquid Outlet Nozzle and Vortex- 2) Sizing the vortex-breaker
Breaker When the flow inside the vessel is rotational, there are
The liquid outlet for this GLS is designed with the chances that the liquid phase inside the vessel can develop a
objective to prevent any entrainment of the incoming gas Vortex flow pattern similar to a whirlpool. This can lead to
with the liquid. In-order to ensure that no gas escape with sucking of the gas in to the liquid phase. A properly sized
the liquid phase, the following measures were taken; Vortex-Breaker can prevent such a phenomenon.
1) Sizing the liquid outlet nozzle Borghei et al. [4] state that Vortex Breaker should be a
Ukil et al. [2] states that diameter of the liquid outlet(D”) cross (+) formed by welding two metallic plates. The
for Gas-Liquid Separators should be sized using the dimension of the cross should be typically twice the
diameter of the outlet nozzle. This provides best
Froude’s Number ( 𝑁𝐹𝑟 )analysis. This helps in providing
performance in terms of preventing vortex formation. But,
Self-Venting capability to the outlet Nozzle. Self-Venting
the CFD simulations (Fig. 2) show that the Half-Pipe liquid
nature of the nozzle enables it to automatically vent any
inlet distributor used in the vessel has high potential to
entrained gas from the liquid stream. 𝑁𝐹𝑟 for the liquid outlet
induce vortices in the liquid space of GLS. Hence, to further
can be calculated by the following equation:
reduce the chance of vortex formation, a circular disc of
𝑉𝑜
𝑁𝐹𝑟 = (9) diameter twice that of the liquid outlet nozzle is welded on
𝑔𝐷"
the top of the crossed plates of the Vortex Breaker (Fig. 3).
𝑉𝑜 = 𝑉𝑒𝑙𝑜𝑐𝑖𝑡𝑦 𝑜𝑓 𝐿𝑖𝑞𝑢𝑖𝑑 𝑎𝑐𝑟𝑜𝑠𝑠 𝑡𝑕𝑒 𝑜𝑢𝑡𝑙𝑒𝑡 𝑛𝑜𝑧𝑧𝑙𝑒 The figure below represents the schematic of the designed
GLS with the notations used in this paper
Estimate of Voare mentioned in the article published by
Ukil et al. [2]. Simpson et al. [3] State that nozzle with
𝑁𝐹𝑟 <0.31 is inherently capable of self-venting any
entrapped gas.
Ukil et al. [2]state that if the height of the liquid inside
the vessel (h) is less than a conservative estimate, then there
are chances that the gas will get entrapped into the liquid
that leaves the vessel, due to the swirling flow patterns of
Gas and liquid inside the vessel. h can be determined by
using Harleman’s Equation, which is;
𝑉0 𝑕
= 3.24  (10)
𝑔𝐷” 𝐷”

h can be considered as the lowest allowable liquid level in

the GLS.

Fig. 4. GLS as designed

Fig. 3. Schematic of the Vortex-breaker installed in the GLS Fig. 5. Trend of Liquid Feed to the Distillation Column

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 International Journal of Chemical Engineering and Applications, Vol. 3, No. 6, December 2012

IV. CONCLUSION stabilizing the downstream LBCP unit.

The GLS aswas commissioned in our manufacturing  Created avenue for energy saving of0.7 Million USD
plant in June, 2012. Benefits experienced since then are; by reducing steam usage in distillation column.
 Decrease in flow fluctuations (Fig – 5) in the feed to
Distillation Column at the downstream of GLS. REFERENCES
 Stoppage of Volatile Organic Compound(VOC) [1] GPSA Engineering Data Book, 12th Edition, Chapter 7, pp 1-18
[2] T. Ukil and M. Thomas, “Reduce Gas entrainment in Liquid lines,”
emission to atmosphere from distillation column top Chemical Engineering, June-2011.pp 42-44
vent. [3] L. L. Simpson, Chemical Engineering, 1960, pp 191
 Benefit realized amounts to 0.54 Million USD by [4] S. M. Borghei, “Partial Reduction of Vortex in vertical intake pipe,”
Scientiairanica, vol. 17, issue 2.

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