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    CHE 200 Week 12 - Batch Distillation

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    eastskykim1995

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    CHE 200 Week 12 - Batch Distillation

    Uploaded by

    eastskykim1995
    5 views6 pages

    Original Title

    CHE 200 Week 12 -Batch Distillation

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    © All Rights Reserved
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    Download as pdf or txt
    5 views6 pages

    CHE 200 Week 12 - Batch Distillation

    Uploaded by

    eastskykim1995

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    of 6

    Batch distillation

     How is the amount of material vaporized related to the composition


    still left in the still?
    Batch distillation: Rayleigh equation
    From (1) & (2):
    dW dx dW
    xi  W i  yi
    dt dt dt
    At t:
    dW dx
    (Wi)t ( yi  xi ) W i
    (xi)t dt dt
    dW dxi
    Initial

    W ( yi  xi )
    FdW ziF dxi
      
    W W xiW ( yi  xi )

    Total mass balance: F ziF dxi


    ln   (3)
    W xiW ( yi  xi )
     dW dD
     (1)
    dt dt W
    z AF  xA
    *
    ( y A ) ave  F w
    Component balance: W
    ( 4)
    1
     d ( xiW ) dD dW dx dD F
     yi   ( xi  W i )  yi (2) Rayleigh equation
    dt dt dt dt dt
    Numerical integration of Rayleigh’s equation

    x y* 1/(y*-x)
    Analytical Approach
    F z AF dx A  AB x A
    ln   and yA 
    W x AW ( y A  x A ) ( AB  1) x A  1

    W
    z AF  x Aw
    *
    ( y A ) ave  F
    W
    1
    F

    For multicomponent batch distillation:

    ∑xiw=1
    Batch distillation with reflux
    Tutorial #11
     Raw moonshine containing 20
    mole % ethanol (A) in water (B)
    is fed to a batch still and distilled
    until only the still residue
    contains just 2 mole % ethanol.
    What fraction of the charge
    remains in the still? What is the
    composition of the distillate
    “refined moonshine”. P= 1bar.

    11

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