a at enjooing crow comes Cap COLUMN BINARY DISTILLATION IN A BuBBLE OsJecTive: To study the operation of ubble cap distillation column. Ai: 21 Toverify the rayleigh equation 92 Tocebtain the Tx data under ttl rex conden a steady state and compare with theoretical value. the minimum To operate the column under total reflux condition and calculate umber of theoretical stages using fenske's equation. n under any desired refx condition and calculate To operate the colurm McCabe Thiele’s method. theoretical number of stages using 25 To calaulate the overall efficiency of the bubble cap distilation column INTRODUCTION: rating the components of 2 saiuions whic depends ‘upon the distribution of the substanc’® petween a gas and liquid phases applied to cases were all components are present IT oth phases. Instead of introducing ° new e mixture in order to provide the ‘second phase, as is done in 925 phase is created from the original solution by Distillation Is the method of s8Pé substance into th absorption or desorption, the new vaporization or condensation: When cistittion is carried out In plate columns stage, The number of theoretical stages require pes of tray. The main requirement of the tray i are so many ty intimate mixing between the liquid and vapour streams. in which each plate constitutes 2 single 4 to effect a required separation. There is that it should provide widely used tray because of its rangh of the valve tray. ‘eded by newer types, such at or triangular slots cut -the bubble cap tray has been the most operation, butit is now tending to be supers ‘The individual caps are mounted on risers and have rectangular around their sides: usa CAP DISTILLATION COLUMN age a 1 of 17 (Rev. 1) Ko: Engineers Pt Limited, Amba4, THEORY: ube cap dtatin column are capable of dealing win very ow Hau re and are therefore useful for oparation at ow refx aos. riiany th ss filed wth F moles of feed with 37 For empl bate dilation process i the number of component. Let at any moment tion x of the more volatile component 1D. Concentration of the wid inthe si 4 fas the moo fraction of tho more volte mol offauid inthe stil bo B having a moe ra {ie A) and let the moles of accumulated condensate ba quium vapour sy. Over a small time, the change inthe amount of a eb andthe amount of vapour wihdrawn is dD. The folowing ferential mass balance equations may be writen Tota material balance ae 40 © Component A balan: =d(6)=y'ad @ Cn slving he above enustion: = Bde x68 = dD Put dB = dD from q(t = Bax = 7 dD x60 = Bebx=y" —2)60 Again pt aD = -o8 Boe =" = 1968 ° Byaranging the above equation Integrating Ea(@): Ke eye hat inte te Scanned with CamScannerno E100 08 mere Nats rumber of actual lies te cour 5, DESCRIPTION: even plates for mounting the Bubble caps, ‘The setup consists of a column with s w pubie cap. An elec peated rebollnsalag ah aps provid with eae ete cear comemronn foe ete egee pe enon See ee comer Se eee itera Aeron ore em & Eee et citer ern clot ren re iter neste eves ne rote ono, purpose. Urumes Require: 1. Electity Supt: Single Phase, 220 VAC, 80 2,32 Amp MCB wth car connection, 62 Water Supply: Continuous @ 2 LPM at bar 63 Flaor Drain Requires 64 Reractrometer for analysis P| 65 Chemicals. Water 15 Methanol 4 7. _ ExpERIMENTAL PROCEDURE: TA Staarine Proceoure: TAA. Prepare calibration char of refractive it ra scve index and liquid composition of 74.2 Prepare methanolwater solution by mixing known amount of aistled amount of distil water and mathanol (composition of estion of methanol in solution range of 15 to 25% by volume), ae Enon Lie Aaa ‘ube car osrecanow cout ‘agen bor Scanned with CamScanner% 1.124 Coot down the samples to room temperature & measure their refractive indices. “71:26 Repoat the experiment for diferent set point temperatures & reflux ratios 7.2. CLosine Proceoure: 7.241 When experiments over switch OFF the heater. 7.21. Switch OFF the main power supply fo the set-up. 7.22. After 10 min stop the water supoly. arta como creertetc vim ny ‘open the valve Vis ‘Osservarion & CALCULATION: 8.4.aDarat [Rolaivevolatity a ~S~C= SESS | Molecular weight of methanol My =S2gmole SSS | Molecular weight of Water My = 18 gimole “Actual numberof plates Ne [Enialpy offeed He a 8A.bDara:2. 136 5 —— Scanned with CamScanner