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    PEKA Experiment2

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    darkmaxk

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    PEKA Experiment2

    Uploaded by

    darkmaxk
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    1 views2 pages

    PEKA Experiment2

    Uploaded by

    darkmaxk

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    © All Rights Reserved
    Download as DOC, PDF, TXT or read online from Scribd
    Download as doc, pdf, or txt
    of 2

    PEKA Experiment

    Acids and Bases

    Title: Acid-base titration


    Aim: _________________

    Apparatus: 25.0 cm3 pipette, burette, 250 cm3 conical flask, retort stand with clamp,
    white tile
    Materials: 0.1 mol dm3 sulphuric acid, , approximately 0.2 mol dm-3
    potassium hydroxide, KOH solution, phenolphthalein
    Procedure:
    1. Rinse a clean burette with a small amount of 0.1 mol dm-3 sulphuric acid,
    .Clamp the burette on a retort stand
    2. Fill the burette with 0.1 mol dm-3 sulphuric acid, .Adjust the meniscus
    level of the acid to a reading at `0’ or slightly below the ‘0` mark.
    3. Record the initial burette reading.
    4. Pipette 25.0cm3 of potassium hydroxide, KOH solution into a conical flask
    5. Add two drops of phenolphthalein into the potassium hydroxide, KOH solution
    and shake it well. Observe the colour of the solution.
    6. Place the conical flask with its contents on a white tile below the burette as shown
    7. Add the sulphuric acid, carefully and slowly from the burette into the
    conical flask.Swirl the conical flask throughout the process of titration.
    8. When the colour of the mixture turn paler, add the sulphuric acid, a drop
    at a time while swirling the flask. Observe carefully the change in colour of the
    mixture.
    9. Stop adding the sulphuric acid, as soon as the solution in the conical flask
    turn colourless.(This is the end point)
    10. Record the final burette reading.
    11. Repeat steps 1 to 10 twice.Tabulate your readings.

    Method:
    1. …….
    2. ………..
    3. ……….
    .
    Result:
    Titration number 1 2 3
    Final burette reading cm3
    Initial burette reading, cm3
    Volume of sulphuric acid,
    cm3

    *Find average
    Calculation:
    1. What is the volume of 0.1 mol dm-3 sulphuric acid, required to exactly
    3
    neutralize 25.0 cm of potassium hydroxide, KOH solution?
    2. Calculate the concentration of potassium hydroxide, KOH solution, in g dm-3,
    based on the result obtained ( Relative atomic mass: H,1;O,16;K,39)

    Discussions:
    1. What is the colour of phenolphthalein in potassium hydroxide,KOH solution?
    2. Why do you need to rinse the burette with a small amount of sulphuric acid,
    in step 1?
    3. What is the use of the white tile in this activity?
    4. State the change in colour at the end point if methyl orange is used to replace
    phenolphthalein in this activity

    Conclusion:__________________________________

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