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Certificate of Analysis: Gravimetric

The document provides a Certificate of Analysis for a Diolein Standard (Catalog No. 33022, Lot No. A0207353) intended for laboratory use, with a concentration of 5000 µg/mL in pyridine. It includes details on purity, storage conditions, expiration date (February 28, 2026), and manufacturing notes under ISO 9001:2015 standards. Additional notes on handling, uncertainty values, and purity determination methods are also included.

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Mauricio Cruz
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21 views2 pages

Certificate of Analysis: Gravimetric

The document provides a Certificate of Analysis for a Diolein Standard (Catalog No. 33022, Lot No. A0207353) intended for laboratory use, with a concentration of 5000 µg/mL in pyridine. It includes details on purity, storage conditions, expiration date (February 28, 2026), and manufacturing notes under ISO 9001:2015 standards. Additional notes on handling, uncertainty values, and purity determination methods are also included.

Uploaded by

Mauricio Cruz
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as PDF, TXT or read online on Scribd
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110 Benner Circle

Bellefonte, PA 16823-8812
Tel: 1-814-353-1300 Certificate of Analysis
Fax: 1-814-353-1309 gravimetric
www.restek.com

FOR LABORATORY USE ONLY-READ SDS PRIOR TO USE.


This Reference Material is intended for Laboratory Use Only as a standard for
the qualitative and/or quantitative determination of the analyte(s) listed.

Catalog No. : 33022 Lot No.: A0207353


Description : Diolein Standard

Diolein Std 5000µg/mL, Pyridine, 1mL/ampul

Container Size : 2 mL Pkg Amt: > 1 mL


Expiration Date : February 28, 2026 Storage: 10°C or colder
Ship: Ambient

Percent Grav. Conc. Expanded Uncertainty


Component # Compound CAS #
Purity (weight/volume) (95% C.L.; K=2)

1 1,3-Diolein 2465-32-9 99% 5,020.0 µg/mL +/- 29.4602 µg/mL

Solvent: Pyridine 110-86-1 99%

Date Mixed: 02-Feb-2024 Balance: 1128360905

Manufactured under Restek's ISO 9001:2015


Registered Quality System
Certificate #FM 80397
By Marlina Cowan at 3:42 pm, Feb 02, 2024

01-Nov-2022 rev. Page 1 of 2


General Reference Material Notes

Expiration Notes:
· Expiration date valid for unopened ampul stored in compliance with the recommended conditions.
· Uncertainty, concentration, and expiration of the RM are based on the unopened product being stored according to the
recommended condition found in the storage field.
Purity Notes:
· Purity and/or chemical identity are determined by one or more of the following techniques: GC/FID, HPLC, GC/µECD,
GC/MS, LC/MS, RI, and/or melting point.
· Compounds with a listed purity of less than 99% have been weight corrected to compensate for impurities and/or salts.
A correction factor is used to calculate the amount of compound necessary to achieve the desired concentration of the
parent compound in solution.
· Purity of isomeric compounds is reported as the sum of the isomers.
· Purity values are rounded to the nearest whole number.
Uncertainty Value Notes:
· Uncertainties are determined using data from balances and glassware, raw material purity, and, when significant,
equipment tolerances or calibration results.
Manufacturing Notes:
· Concentration is based upon gravimetric preparation using either a balance whose calibration has been verified daily
using NIST traceable weights, and/or dilutions with Class A glassware.
Handling Notes:
· Stability of the unopened product, when stored in compliance with the recommended conditions, is guaranteed through
the expiration displayed on the product label and certificate. Contact Restek for additional opened product stability
information, with the knowledge/understanding that open product stability is subject to the specific handling and
environmental conditions to which the product is exposed. For your convenience Restek supplies deactivated vials with
most standards packed in 2mL ampules. Larger volume deactivated vials are available through Restek as a custom
ordered item. Additionally, Restek sells DMDCS for the purpose of glassware deactivation as catalog number 31861,
which includes complete instructions.

01-Nov-2022 rev. Page 2 of 2

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