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    CL-452 Process Design Project: Group 23

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    Rajnayan Datta
    This document provides a summary of a process design project presentation by Group 23. It includes: - Process flow diagrams for converting n-butane to maleic acid and then to tetrahydrofuran. - Stoichiometric equations and input/output streams for key reactors and distillation columns. - References cited for separation of products.

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    CL-452 Process Design Project: Group 23

    Uploaded by

    Rajnayan Datta
    85 views10 pages
    This document provides a summary of a process design project presentation by Group 23. It includes: - Process flow diagrams for converting n-butane to maleic acid and then to tetrahydrofuran. - Stoichiometric equations and input/output streams for key reactors and distillation columns. - References cited for separation of products.

    Original Description:

    IIT Bombay Chemical Engineering BTech degree completion requirement

    Original Title

    Design Project

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    This document provides a summary of a process design project presentation by Group 23. It includes: - Process flow diagrams for converting n-butane to maleic acid and then to tetrahydrofuran. - Stoichiometric equations and input/output streams for key reactors and distillation columns. - References cited for separation of products.

    Copyright:

    © All Rights Reserved
    Download as PPTX, PDF, TXT or read online from Scribd
    Download as pptx, pdf, or txt
    85 views10 pages

    CL-452 Process Design Project: Group 23

    Uploaded by

    Rajnayan Datta
    This document provides a summary of a process design project presentation by Group 23. It includes: - Process flow diagrams for converting n-butane to maleic acid and then to tetrahydrofuran. - Stoichiometric equations and input/output streams for key reactors and distillation columns. - References cited for separation of products.

    Copyright:

    © All Rights Reserved
    Download as PPTX, PDF, TXT or read online from Scribd
    Download as pptx, pdf, or txt
    of 10

    CL-452

    Process Design Project


    Week 4 Presentation
    Date: 16 February 2017

    GROUP 23
    Raj Nayan Datta - 131030020
    Shivam Jindal - 130020123
    G.V. N Reddy - 130020110
    Shrey Nagori - 130020002
    Shanti Priya - 130020115
    PFD (n-butane to Maleic Acid)
    Stoichiometric Equations
    C4H10 + 7/2O C4O3H2 + 4H2O

    C4O3H2+ H2O C4O4H4

    C4O4H4 + 5H2 0.9 [C4H8O + 3H2O]

    0.1 [C4H10O2 + 2H2O]


    Riser Reactor

    Input kmol/hr kg/hr Output kmol/hr kg/hr

    n.butane 53.58 3107.64 Maleic


    Anhydride 53.58 5250.84
    Air 893 25897
    n-butane
    0
    O2 187.53 6000.96
    N2+ other
    gases 705.47 19896.04
    N2+ other 705.47 19896.04
    gases Water
    214.32 3857.76
    Absorber

    Input kmol/hr kg/hr Output kmol/hr kg/hr

    Maleic Maleic Acid


    Anhydride 53.58 5250.84 53.58 6215.28

    Water (vapour) Water


    267.9 4822.2 214.32 3857.76
    PFD (Maleic Acid to THF)
    Bubble Reactor

    Input kmol/hr kg/hr Output kmol/hr kg/hr

    Maleic Acid Tetrahydrofuran


    53.58 6215.28 48.222 3471.984

    Water 1,4 butanediol


    214.32 3857.76 5.358 482.22

    H2 Water
    267.9 535.8 369.702 6654.636
    Distillation Column 1

    Overhead kmol/hr kg/hr Bottoms kmol/hr kg/hr

    Tetrahydrofuran Tetrahydrofuran
    47.967495 3453.65964 0.254505 18.32436

    1,4 butanediol 1,4 butanediol


    0 0 5.358 482.22

    Water Water
    367.7433533 6619.38036 1.958646667 35.25564
    Distillation Column 2

    Overhead kmol/hr kg/hr Bottoms kmol/hr kg/hr

    Tetrahydrofuran Tetrahydrofuran
    47.967495 3453.65964 0

    Water Water
    0.09593499 1.72682982 367.6474183 6617.65353
    References
    1. Hans-Juergen Gosch, H. Rust, R. Fischer, C. Hechler and R. Pinkos. “Separation of 1,4-butanediol from
    hydrogenation mixtures”. US 5342488 A. issued on 30 Aug 1994

    2. J. K. Kouba and R. B. Snyder. “Coproduction of butanediol and tetrahydrofuran and their subsequent
    separation from the reaction product mixture”. US 4656297 A. issued on Apr 7, 1987

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