Comparison of gas sensing properties of zinc oxide (metal oxide) nano Structures the

effect of morphology and temperature

Sidra Arshad *1; Sammia Shahid1,
1.
Department of Chemistry, School of Science, University of Management and Technology Lahore Pakistan
*Corresponding auther: S2016140024@umt.edu.pk
Introduction:
ZnO is a material which is of great interest for a variety of applications due to its unique
properties and the availability of a variety of growth methods resulting in a number of
different morphologies and a wide range of material properties of
synthesized nanostructures ZnO nano structures synthesis and impact of their
morphologies and temperature on ZnO nano structure and their gas sensing properties
are disused in following 6 papers.
Material: Material: Material :
Material;: Material:
1. Zinc shoot, argon, Material : Zinc
oxygen, Alumina and hexamethylenetetramine BRUKER D8 focus solvents, Silicon wafers , wiresf gold
zinc nitrate hexahydrate aluminium alloy, stainless
silicon substrate was
and hexamethylene (HMTA) diffractometer , ionophore steel chamber , gold
used. sodium hydroxide metallic Zn target , 90 L membrane, SEM,
2. water ,ethanol , HCl tetramine , N2 gun ,SEM catalyst.
sputtering Chamber, Seed solution,
Procedure: Procedure: Procedure:
1g zinc shoots place in Procedure : Zinc nitrate and HTMA ZnO on rotating surface in Procedure :
furnace Si and alumina slide was cleaned Then 25 mL solution of presence of oxygen . Zinc nanorods thin Procedure:
Experimental device was 9L
substrate were placed in immersed into sodium hydroxide and
sputtering chamber.The gas flow
film was prepared by Thin film deposit on
transferred into a sol gel method in two silicon wafer at 1 torr and
cold zone. O2 and Ar solution of zinc nitrate stainless-steel autoclave
rate control by brooks flow

mixture was introduce to

meters Structural stages Cleaning of the 650 degree for 30 sec
hexahydrate sample with the characterization of the coatings
the reactor at ratio 1: 8. capacity of 100 ml. and was performed by Bragg substrate, Cover ZnO deposition time. Gas
is dried with N2 gun cool white powder Brentano configuration X-ray with iono phores pressure controlled by
gas sensing and observe under collected washed out to diffraction (XRD) using a membrane. mass flow controller.
measurement were BRUKER D8
SEM. remove impurities.
performed. focus diffractometer
Result and discussion :
Method 1 :SEM images conformed the formation of Zno nano wire at different morphologies and 1D nanorods similar to coral colonies and XRD pattern of typical ZnO sample.
Method 2: The adsorption process of oxygen and the electron-hole pair generation have been discuss.
Method 3:SEM images of ZnO nanorods treated by different annealing temperature
It morphologies.Annealing treatment can improve the crystal quality and result in enhanced gas sensing properties.
Method 4: ZnO nano particles was deposited by magnetron sputtering ,XRD analysis and morphology of film changes with increases in temperature.
Method 5: XRD analysis used to identify the crystalline structure and deposit material was amorphous in naturemax crystallinity was observed at 700 degree centigrade.
Method 6: annealing effect the morphologies of temperature and size of ZnO nanorods with increase in temperature.
Morphology Target gas temperture
comparison
Here I use different gases to determine the effect of Nano rod H2S 27

annealing treatment on morphologies on different type gas Nano wire Ethanol 300
sensing properties.
Nano tube H2 200

1. References:
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