Reaktor

Chapter 2 Stirred Reactors
Inside this chapter you will nd: REACTOR SELECTION GUIDE 4520 BENCH TOP, 1000 & 2000 mL 4520 HP BENCH TOP, 970 & 1900 mL 4530 MOVEABLE CART OR FLOOR STAND, 1000 & 2000 mL 4530 HP MOVEABLE CART OR FLOOR STAND, 970 & 1900 mL 4540 MOVEABLE CART OR FLOOR STAND, HIGH PRESSURE, 600 & 1200 mL 4550 GENERAL PURPOSE, CART OR FLOOR STAND, 1 & 2 GALLON (3.75 & 7.5 L) 4555 GENERAL PURPOSE, CART OR FLOOR STAND, 2.6 & 5 GALLON (10 & 18.75 L) 4560 MINI, BENCH TOP, 100-600 mL 4560 HT MINI, BENCH TOP, 300-600 mL 4570 HP/HT, BENCH TOP, CART, OR FLOOR STAND, 250-1800 mL 4580 HP/HT, CART OR FLOOR STAND, 1 & 1.5 GALLON (3.75 & 5.5 L) 4590 MICRO, BENCH TOP, 25-100 mL 4590 HP MICRO, BENCH TOP, 25-100 mL 4590 HP/HT MICRO, BENCH TOP, 25-100 mL 5100 LOW PRESSURE GLASS & METAL, 160-1500 mL 5500 COMPACT HIGH PRESSURE REACTORS, 25-600 mL
Reactor Selection Procedure
It is possible to convert most of these reactors from one size to another within the same series. This is done by substituting a longer or shorter cylinder with corresponding internal ttings including the stirrer shaft, thermowell or thermocouple, dip tube and cooling coil (if installed). In some cases, the heater will also need to be changed. The Parr Technical Service department will be happy to provide a list of the appropriate conversion parts for any contemplated conversion.
he selection process starts with establishing the Four Basic Specications discussed below. Having set these requirements, the user can then identify a suitable series group from the
Guide to Parr Stirred Reactors. The user should then review the standard ttings. Finally, a list of Secondary Specications should determine some of the ner details of the system.
Establish 4 Basic Specications

3. Vessel Size Parr stirred reactors are offered in many sizes ranging from 25mL to 18.75 liters (5-gallon). It should be noted that these volumes refer to the free space in the vessel, and for safe operation the maximum liquid charge held in the vessel should not exceed two-thirds of the available free space in sealed batch operations. Generally, several vessel volumes are offered within most series, and reactor sizes can be recongured with conversion parts. 4. Material of Construction Parr reactors are normally made of Type 316 Stainless Steel, but they can be made of other alloys as well. The list of available construction materials includes: Type 316/316L Stainless Steel Alloy 20 Alloy 400 Alloy 600 Nickel 200 Titanium Alloy B-2 Alloy C-276 Zirconium Grades 702 & 705 Other materials may be available upon request. The majority of organic reactions can be handled in a standard T316 Stainless Steel vessel, but other corrosion resistant alloys are available to provide vessels suitable for use with a wide range of corrosive acids, bases, salts and gases. Special alloy construction can be provided for both the internal parts of the vessel and the external valves and ttings. However, there are considerable cost savings if the user can accept standard external parts made of stainless steel instead of a special alloy. There is more detailed information on special materials in the Materials of Construction section of Chapter 1 on pages 10-11 of this catalog.
1. Maximum Operating Pressure Parr offers a number of operating pressures. Vessels 600mL and under in volume are typically rated for 3000 psi, and vessels 1L or larger are typically rated for 1900 psi. We also offer 5000 psi versions of these sizes for those who need this combination of smaller size and higher pressure. Some pressure limits can be increased with custom designs. However, higher pressure vessels generally require thicker walls, which can make temperature control more difcult, and larger volume, high pressure vessels are heavier and more difcult to handle. We also have a line of 5100 Series Glass Reactors which can handle up to 150 psi with a glass cylinder or up to 1000 psi with a metal cylinder. 2. Maximum Operating Temperature Traditionally, the choices here have been up to 350 C for vessels with PTFE gaskets and up to 500 C for exible graphite (previously metal gaskets). Parr added the option of a self-sealing O-ring closure for general purpose vessels over a full range of volumes. These quick closing designs are limited to 225 C, although this can be raised to 275 C with special O-ring materials.
Moveable and Fixed Head Designs
A moveable head is best for when you need to remove the entire reactor in one piece after running your operation.
A xed head allows you to remove the cylinder and leave the head and all of its attachments mounted to the stand.
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4520
Select Appropriate Series

Reactor Type Mid-Size, Bench Top Mid-Size, Bench Top, High Pressure Mid-Size, Moveable Cart or Floor Stand Mid-Size, Moveable Cart or Floor Stand, High Pressure Mid-Size, Moveable Cart or Floor Stand, High Pressure General Purpose, Cart or Floor Stand General Purpose, Floor Stand Mini, Bench Top Mini, Bench Top, High Temperature High Pressure/High Temperature, Cart or Floor Stand High Pressure/High Temperature, Bench Top High Press./High Temp., Cart or Floor Stand Micro, Bench Top Micro, Bench Top, High Pressure Micro, Bench Top, High Pressure, High Temperature (Fixed Head Only) Low Pressure Glass or Metal Reactors Mini or Micro, Bench Top, Compact Stand Nominal Size 1000 and 2000 mL 970 and 1900 mL 1000 and 2000 mL 970 and 1900 mL 600 and 1200 mL 1 and 2 gallon (3.75 and 7.5 L) 5 and 2.6 gallon (18.75 and 10 L) 100-600 mL 300-600 mL 1000 and 1800 mL 250 and 500 mL 1 and 1.5 gallon (3.75 L and 5.5 L) 25-100 mL 25-100 mL 25-100 mL 160 mL-1.5 L 25-600 mL Maximum Pressure psi (bar) 1900 (131) 2900 (200) 1900 (131) 2900 (200) 5000 (345) 1900 (131) 1900 (131) 3000 (200) 2000 (138) 5000 (345) 5000 (345) 3000 (200) 3000 (200) 5000 (345) 5000 (345) 150 (10.3) Glass 1000 (69) Metal 3000 (200) Maximum Temperature C 225-350 350 225-350 350 350 225-350 225-350 225-350 500 500 500 500 225-350 350 500 225 225-350
Series No.
4520 HP 4530 4530 HP 4540 4550 4555 4560 4560 HT 4571-4572 4577-4578 4575A-4576A 4575B-4576B 4581-4584 4590 4590 HP 4590 HP/HT 5100 5500
Size
25 mL 18.75 L Parr Instrument Company offers laboratory reactors and pressure vessels in sizes from 25 mL to 18.75 L. Generally it is best to select a size that will allow for 1/3 free space. This allows for some liquid expansion during the heating phase of a reaction.
Pressures (psi)
1900 3000 5000 Maximum Allowable Working Pressures (MAWP) are determined by adherence to the ASME pressure vessel design criteria. There are three ranges; up to 1900 psi, up to 5000 psi, and in most cases reactors in the 25 mL to 600 mL range can be rated to 3000 psi. Parr Instrument Company recommends research be restricted to 90% of any vessels MAWP rating. A vessels pressure capacity is directly tied to the temperature the vessel will be operating.
Temperatures
225 C 500 C Operating Temperatures have traditionally been up to 350 C using a at PTFE gasket. Flexible graphite gaskets have now extended the range to 500 C. New quick opening designs have been added to the Parr product line that use O-rings for the seal and normally limit the temperature to 225 C (Viton) or 275 C (Kalrez).
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Reactor Selection Guide

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Conrm Standard Fittings
Thermocouple or Thermowell Liquid Sampling Valve for Pressure Gage, analog type,
which shows the pressure within the vessel at all times.
withdrawing liquid samples through the dip tube shared with the gas inlet valve. Incoming gas can be used to clear the dip tube between liquid samples.
for measuring the temperature within the vessel. In small reactors, a thermocouple encased in a metal sheath extends directly into the vessel. In larger reactors, and in vessels constructed of special alloys, the control thermocouple is inserted into a thermowell which extends to a point near the bottom of the vessel. Internal Stirring System consists of a motor drive magnetically coupled to an internal stirrer shaft with attached turbine-type impeller(s). Dip Tube
Gas Release Valve to release
gas from the reactor during or at the completion of a run.
Cooling Coil
Safety Rupture Disc to
protect the vessel and the operator from dangerous pressures beyond the rated limit for the vessel.
Gas Inlet Valve for charging gas into the reactor. This valve and the liquid sampling valve are connected to a dip tube which extends to the bottom of the vessel.
Guide or Foot Bearing with a PTFE bushing to support and stabilize lower stirrer shaft. (Not required with footless magnetic drive)
Specify Detailed Options

removed from the heater for charging, product recovery, and vessel cleaning. In the xed head style the head remains in the mounting and the reactor heater then cylinder drop away to open the vessel. This is useful for users who wish to leave inlet and feed lines, discharge and vent lines, condensers, and similar head connections undisturbed between runs. The head is easily removable if desired by sliding the head out of its slot on the stand. 3. Support Stand Parr stirred reactors are most commonly mounted on a bench top stand for sizes of 2 liter or smaller. Vessels 1 liter or larger may be mounted on either moveable carts or xed oor stands. Care should be taken to check stand dimensions with the available space at the users facility. 4. Stirrer Type Parr reactors have a magnetic drive equipped for most low viscosity uids and light slurries. Drives with
here are a number of options to be considered and selections to be made in order to complete the specications for a reactor. You will need to choose from the following: 1. Sealing Style Parr reactors may be provided with a at gasket seal or an O-ring seal. Most commonly, a at PTFE gasket is used. These are generally good for temperatures up to 350 C. A graphite seal for temperatures up to 500 C is used for high temperature systems. O-ring seals allow for a convenient, boltless closure, but the material must be checked carefully against the intended process as there are many solvents and gases which attack O-rings. 2. Mounting Style Parr reactors may be provided with a moveable vessel mounting or xed head mounting. In the moveable vessel style the complete vessel assembly (only the head in the one gallon or larger) is
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higher coupling torque and more powerful motors are available for higher viscosity applications. Also, many reactors require a lower support bracket to stabilize the stirring shaft. In applications with abrasive particles or heavy mixing, a footless magnetic drive with a larger diameter shaft may be provided. 5. Cooling Coil An internal cooling coil can be installed in all reactors (except the Micro sizes) to remove the heat of a reaction and/or to cool the vessel at the end of a run. In some reactors a cooling coil is furnished as a standard tting. In others, a coil can be added as an option in either serpentine style or alternately in a spiral style for selected models. For the micro sizes, with their limited dimensions, a cold nger may be added as an option 6. Gage and Rupture Disc Ranges The pressure gage range must be selected to provide the resolution desired, while having a range high enough to handle the maximum pressure the reactor will undergo. One would be tempted to simply get a gage with the largest range possible, but this can reduce the resolution to unacceptable levels. One good rule of thumb for good resolution is to operate with the gage at half of its maximum range. The rupture disc is most commonly matched to the Maximum Allowable Working Pressure of the vessel, ensuring the disc will burst before reaching a pressure beyond the MAWP range. Care must be taken not to
take the vessel above 90% of its burst pressure under normal operation. This will help protect the disc from the effects of repeated pressure cycles. 7. Controller Options Parr controllers are typically set up to control temperature, but may also be set up with digital pressure displays, stirring speed, secondary temperature, and other displays and controls. These may be set up with data logging via PC as well. For more information on these options, see the Controller Section of this catalog. 8. Certication ASME, CE, CHINA, and Parr Certications are available for users who require these recognized quality assurance certications. 9. Custom Options A wide range of custom options such as special openings in the head or cylinder, high viscosity stirrers, windows, special valves, heaters or jackets, explosion proof wiring, and volume modications are available. Various accessories, such as glass or PTFE liners, condensers, catalyst holders, and alternate stirrers are available to further adapt these reactors to the individual users applications. Detailed information for these and other options are in Optional Fittings, Chapter 5, starting on page 101 of this catalog.
How to use the Ordering Guide: T
he last page of each Reactor Series in this chapter is an Ordering Guide. A composite identication/ order number can be generated by combining the individual symbols from the separate sections. In the following example: Using the Ordering Guide from the Series 4560 Stirred Reactors for our sample order, we have chosen to order a 600 mL xed head reactor, FKM O-ring, the vessel manufactured out of T316 Stainless Steel, a general purpose magnetic drive also made of T316SS, 115V power supply, 1/4 hp explosion-proof motor, 3000 psi pressure gage, no bottom drain valve, and a 4848 controller. The order number for that particular conguration would appear as follows:
No. 4568 - OV-SS-GP-115-XP.25-3000-4848

A. Model No. 4568 B. C. D. E. F. G. H. I. Gasket Material Stirrer Drive MOC Voltage Motor Gage BDV -OV -SS -GP -No Symbol -115 -XP.25 -3000 -No Symbol J. Controller -4848
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Series 4520 1 & 2 Liter General Purpose Reactor Systems

Series Number:
4520
Type:
General Purpose
Stand:
Bench Top
Vessel Mounting:
Moveable or Fixed Head

Vessel Sizes, mL:
1000-2000 970-1900 HP
Standard Pressure MAWP Rating, psi (bar):
1900 (131)
Standard Maximum Operating Temp., C: 225 w/ FKM O-ring 275 w/ FFKM O-ring 350 w/ PTFE Flat Gasket
High Pressure (HP) MAWP Rating, psi (bar):
2900 (200)
Model 4523 Fixed Head Reactor open to show Internal Fittings, and a 4848 Controller shown with optional Expansion Modules.
Maximum Operating Temperature, C, at High Pressure (HP): 350 @ 2900 psi
hese are the largest of the Parr Reactors that can be handled on a bench top. They can be furnished with either a self-sealing, O-ring closure for working temperatures up to 225 C or with a at, PTFE gasket for higher temperatures to 350 C. An optional HP (High Pressure) at gasket version has been added for maximum allowable working pressure of 2900 psi (200 bar) at 350 C. Both xed head and moveable vessel designs are available.
An optional pneumatic lift is available for the heavier 2 liter cylinder and heater. It should be noted, however, that the 2 liter, xed head model is tall and may not be convenient to operate on a standard height bench top. We recommend using a oor stand. (See Series 4530) With their larger diameter, these mid-size reactors have sufcient space for special modications, such as: an internal cooling coil, bottom drain valve (not on 2 liter bench top), ball valve for a solids charging
port, catalyst addition devices, condensers, electrical feedthroughs and more. Details are provided in the Chapter 5 of this catalog, starting on page 101. The standard magnetic stirrer drive on these 4520 Models works well for reaction mixtures with viscosities up to 25,000 centipoise. For heavier stirring loads, these reactors can be equipped with larger magnetic drives, more powerful motors, and drive trains capable of delivering additional stirring torque.
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Series 4520 Pressure Reactor System Specications Shaded bar indicates specications that change within series. Model Number Sizes, mL Sizes for HP Models, mL Maximum Pressure (MAWP) HP Maximum Pressure (MAWP) Maximum Temperature with FKM O-ring with FFKM O-ring with PTFE Flat Gasket Fixed Head Bench Top Split-Ring (6 Cap Screws) Split-Ring (12 Cap Screws) 1/8" Male NPT A1120HC6 16 Inch-Pounds 2 (2.28" dia.) 4.5 inches 0-2000 psi (140 bar) Thermowell Optional Serpentine or Spiral Optional 1000 NA Calrod 1500 1/8 hp variable speed 115 or 230 14 / 7 4.00 3.75 5.4 28 10.5 32 17 24 38* 125 48 130 4509M * Stand height is 48-inches with Bottom Drain Valve option. Other options available. See Ordering Guide, visit www.parrinst.com, or call for more information. 38* 120 48 125 5.4 32 10.5 36 1000 1500 Optional NA Reactor Mounting High Pressure Closure 225 C 275 C 350 C Moveable
4523
1000 970
4524
2000 1900 1900 psi (131 bar) 2900 psi (200 bar)
4525
1000 970
4526
2000 1900
Vessel Style Closure Valve Connections Magnetic Stirrer, Model No. Impeller(s), 6 blades
Maximum Torque Pressure Gage, Size Temperature Measurement Cooling Coil Bottom Drain Valve Heater Style Heater Power, Watts Stirrer Motor Volts, AC Maximum Load, amps, 115 / 230 Inside Diameter, inches High Pressure Inside Diameter, inches Inside Depth, inches Weight of Vessel, pounds
Range
Style
Electrical Supply
Vessel Dimensions
Reactor Dimensions Width, inches w/o Controller Depth, inches Height, inches Weight, pounds
Spare Parts Kit
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Series 4520 1 & 2 Liter General Purpose Reactor Systems

INDEX TO OPTIONS
OPTIONS PAGE Certication 9 Materials of Construction 10 Magnetic Drive 14 Gaskets & Seals 18 Stirrer Motor 104 Rupture Disc 110 Pressure Gage 111 Cooling Coil 115 Bottom Drain Valve 116 4848 Reactor Control 91 4838 Temperature Control 94 4871 Process Control 95 CUSTOM OPTIONS Stirrers 106 Heaters 102 External Valves and Fittings 117 Solids Charging Ports 114 Condensers 109 Electrical Glands 122 Catalyst Addition Device 114 Catalyst Baskets 108 Relief Valves 111 Windows 121 Gear Drives 104 Explosion Proof Options 119 Sample Collection Device 116
Model 4525 Reactor, 1000 mL, Moveable Vessel, and a 4848 Controller shown with optional Expansion Modules.

ACCESSORIES Liners 115 Spare Parts Kits 122 Pressure Hoses 118 Check Valves 117 Liquid Pipettes 113 Gas Burettes 113
Model 4523 Bench Top Reactor, 1000 mL, Fixed Head Style.
4526 Moveable Vessel, 2000 mL
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Series 4520 Ordering Guide

The Order No. for the Base System is: 452__-T-SS-M-115-VS.12-2000-4848 A composite identication number to be used when ordering a 4520 Series Reactor can be developed by combining individual symbols from the separate sections below. For more information on how to use this ordering guide, please see page 27.
A Base Model Model No. Size 4523 1000 mL 4524 2000 mL 4525 1000 mL 4526 2000 mL B High Pressure Option -No Symbol Standard Conguration -HP 2900 psi (200 bar) C Gasket / Maximum Temperature -OV FKM O-ring / 225 C -OK FFKM O-ring / 275 C -T PTFE Flat Compression Gasket / 350 C D Materials of Construction -SS T316 Stainless Steel -MO Alloy 400 -IN Alloy 600 -HB Alloy B-2 -HC Alloy C-276 -CS Alloy 20 -TI2 Titanium Grade 2 -TI4 Titanium Grade 4 -NI Nickel 200 -ZR Zirconium Grade 702 or 705 E Magnetic Stirrer Drive -M General Purpose, 16 in-lb -HD Heavy Duty, 60 in-lb -FMD1 Footless, General Purpose, 16 in-lb -FMD2 Footless, Heavy Duty, 60 in-lb F Mag. Drive Material of Construction -No Symbol Same Material As Vessel -MOC Symbol Indicate Material of Construction G Electrical Supply -115 115 VAC -230 230 VAC H Motor Option -VS .12 Variable Speed, 1/8 hp -VS .25 Variable Speed, 1/4 hp -VS .50* Variable Speed, 1/2 hp -XP .25 Explosion Proof, Variable Speed, 1/4 hp -XP .50* Explosion Proof, Variable Speed, 1/2 hp -AM .25 Air Motor, 1/4 hp -AM .50 Air Motor, 1/2 hp * 230V Systems Only I Pressure -3000 -2000 -1000 Gage 3000 psi / 200 bar 2000 psi / 137 bar 1000 psi / 70 bar Vessel Style Fixed Fixed Moveable Moveable -600 -200 -100 600 psi / 40 bar 200 psi / 14 bar 100 psi / 7 bar
J Internal Cooling Coil -No Symbol No Coil -CC Spiral Coil -SC Serpentine Coil K Bottom Drain Valve -No Symbol No Bottom Drain Valve -BDV L Bottom Drain Valve, 3/8" NPT, for 4523 and 4525 Vessels Only
Controller PID Control, Ramp & Soak Programming, Motor Speed Control, and Data logging with Software Optional RS485 to USB Cable for 4848 Controller Process Controller
-4848 -A1925E4 -4871
M 4848 Expansion Modules -TDM Tachometer Display Module -MCM Tachometer w/Motor Control Module -PDM Pressure Display Module -HTM High Temperature Cut Off Module -ETLM External Temperature Limit Module -MTM Motor Torque Module N 4848 Cooling Control: Solenoid Valve Module -SVM1 115 VAC -SVM2 230 VAC O Custom Options (List All Desired) -AS Anchor Stirrer -SB Static Catalyst Basket -DB Dynamic Catalyst Basket -CAD Catalyst Addition Device -BF Bafes -GE Gas Entrainment Stirrer -RC Reux Condenser -RTC Reux Take-off Condenser -ABH Aluminum Block Heater -WJ Welded Jacket -SCP Solids Charging Port -SA Spiral Stirrer -PS Paddle Stirrer P Certications -No Symbol No Certication -ASME ASME Certication -CE/PED European Community Certication/Pressure -CH China Certication -P Parr Certication Q Spare Parts Kit -4509M Spare Parts Kit for 4520 Series
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Series 4530 1 & 2 L General Purpose Reactor Systems

Series Number:
4530
Type:
his series of reactors will appeal to users who have any of the following needs: Reactors Congured for Polymer Studies. The reactors in this series are mounted on a sturdy oor stand which will accommodate larger stirrer drive motors and stronger power trains than are generally not available for the bench top models. With these options it is possible to provide the high torque and low stirring speeds required for work with polymers and other mixtures with viscosity of 1 million centipoise and more. These mountings are also better suited for the installation of a drain valve in the cylinder bottom for convenient removal of the reaction mixture while it is still hot. Reactors Requiring Extensive Modications. Floor stand mountings provide a good base for reactor modications and for the addition of accessories, such as: condensers, packed columns, special motors, special heaters, jacketed vessels, automatic valves or regulators, and many other ttings. Both xed head and moveable vessel designs are available. Reactors that Need to be Moved. These reactors are designed for use in an area where a bench top is not available. Users who wish to move the reactor to storage when not in use, will appreciate the movable cart design of the Series 4531 and 4532. All of the 1 and 2 liter reactors in this series can be furnished with either a self-sealing, O-ring closure for working temperatures up to 225 C, or with a at, PTFE gasket for higher temperatures to 350 C. HP versions. These reactors are now available in an HP (High Pressure) version up to 2900 psi (200 bar) at 350 C.
General Purpose
Stand:
Floor Stand
Vessel Mounting:

Vessel Sizes, mL:
1000-2000 970-1900 HP
1900 (131)
2900 (200)
4534 Floor Stand Reactor, 2000 mL, Fixed Head, with Spiral Cooling Coil and Liquid Charging Pipette, in the open position, and a 4848 Controller with optional Expansion Modules.
Maximum Operating Temperature, C, at High Pressure (HP): 350 @ 2900 psi
4534 Reactor, assembled with heater raised.
4534 Reactor, assembled with heater down.

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Series 4530 Pressure Reactor System Specications Shaded bar indicates specications that change within series. Model Number Sizes, mL Sizes for HP Models, mL Maximum Pressure (MAWP) HP Maximum Pressure (MAWP) Maximum Temperature with FKM O-ring with FFKM O-ring with PTFE Flat Gasket Moveable Cart Reactor Mounting High Pressure Closure 225 C 275 C 350 C Fixed Head Floor Stand Split-Ring (6 Cap Screws) Split-Ring (12 Cap Screws) 1/8" Male NPT A1120HC 16 Inch-Pounds 2 (2.28" dia.) 4.5 inches 0-2000 psi (140 bar) Thermowell Optional Serpentine or Spiral 3/8 NPT (1900 psi / 350 C) Calrod 1000 1500 1000 1500 1000 1500 1/4 hp Variable Speed 115 or 230 14 / 7 4.0 3.75 5.4 28 35 18 50 200 215 225 10.5 32 5.4 32 21 28 62 240 225 4539M (General Purpose) or 4539MA (Heavy Duty) Other options available. See Ordering Guide, visit www.parrinst.com, or call for more information. 10.5 36 5.4 28 21 28 62 240 10.5 32 1/4 NPT (2900 psi / 350 C) Moveable Floor Stand
4531
1000 970
4532
2000 1900
4533
1000 970
4534
2000 1900
4535
1000 970
4536
2000 1900
1900 psi (131 bar) 2900 psi (200 bar)
Vessel Style Closure Valve Connections Magnetic Stirrer, Model No.
Maximum Torque Impeller(s), 6-Blade Pressure Gage, Size Temperature Measurement Cooling Coil Bottom Drain Valve (Optional) Heater Style Heater Power, Watts Stirrer Motor Volts, AC Maximum Load, amps, 115 / 230 Inside Diameter, inches High Pressure Inside Diameter, inches Inside Depth, inches Weight of Vessel, pounds Width, inches w/o Controller Depth, inches Height, inches Weight, pounds Range
Style
Electrical Supply
Vessel Dimensions
Reactor Dimensions
Spare Parts Kit
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Series 4530 1 & 2 L General Purpose Reactor Systems

INDEX TO OPTIONS
4532 Floor Stand Reactor, 2000 mL, Moveable Vessel on Cart, and a 4848 Temperature Controller with optional Expansion Modules.

4533 Reactor, 1000 mL Vessel with Gear Drive, Dual Condenser and Spiral Stirrer.
2000 mL Stirred Moveable Vessel
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A Base Model Model No. Size 4531 1000 mL 4532 2000 mL 4533 1000 mL 4534 2000 mL 4535 1000 mL 4536 2000 mL Vessel Style Moveable, Cart Moveable, Cart Fixed Head, Floor Stand Fixed Head, Floor Stand Moveable, Floor Stand Moveable, Floor Stand I Pressure Gage -3000 3000 psi / 200 bar -2000 2000 psi / 137 bar -1000 1000 psi / 70 bar -600 600 psi / 40 bar -200 200 psi / 14 bar -100 100 psi / 7 bar J Internal Cooling Coil -No Symbol No Coil -CC Spiral Coil -SC Serpentine Coil K Bottom Drain Valve -No Symbol No Bottom Drain Valve -BDV Bottom Drain Valve L Controller PID Control, Ramp & Soak Programming, Motor Speed Control, and Data logging with Software Optional RS485 to USB Cable for 4848 Controller Process Controller
B High Pressure Option -No Symbol Standard Conguration -HP 2900 psi (200 bar) C Gasket / Maximum Temperature -OV FKM O-ring / 225 C -OK FFKM O-ring / 275 C -T PTFE Compression Gasket / 350 C D Material -SS -MO -IN -HB -HC -CS -TI2 -TI4 -NI -ZR of Construction T316 Stainless Steel Alloy 400 Alloy 600 Alloy B-2 Alloy C-276 Alloy 20 Titanium Grade 2 Titanium Grade 4 Nickel 200 Zirconium Grade 702 or 705
-4848 -A1925E4 -4871
M 4848 Expansion Modules -TDM Tachometer Display Module -MCM Tachometer w/Motor Control Module -PDM Pressure Display Module -HTM High Temperature Cut Off Module -ETLM External Temperature Limit Module -MTM Motor Torque Module N 4848 Cooling Control: Solenoid Valve Module -SVM1 115 VAC -SVM2 230 VAC O Custom Options (List All Desired) -AS Anchor Stirrer -SB Static Catalyst Basket -DB Dynamic Catalyst Basket -CAD Catalyst Addition Device -BF Bafes -GE Gas Entrainment Stirrer -RC Reux Condenser -RTC Reux Take-off Condenser -ABH Aluminum Block Heater -WJ Welded Jacket -SCP Solids Charging Port -SA Spiral Stirrer -PS Paddle Stirrer P Certications -No Symbol No Certication -ASME ASME Certication -CE/PED European Community Certication -CH China Certication -P Parr Certication Q Spare Parts Kit -4539M General Purpose Spare Parts Kit for 4530 Series -4539MA Heavy Duty Spare Parts Kit for 4530 Series
E Magnetic Stirrer Drive -M General Purpose, 16 in-lb -HD Heavy Duty, 60 in-lb -XHD Extra Heavy Duty, 120 in-lb -FMD1 Footless, General Purpose, 16 in-lb -FMD2 Footless, Heavy Duty, 60 in-lb -FMD3 Footless, Extra Heavy Duty, 120 in-lb F Mag. Drive Material of Construction -No Symbol Same Material As Vessel -MOC Symbol Indicate Material of Construction G Electrical Supply -115 115 VAC -230 230 VAC H Motor Option -VS .25 Variable Speed, 1/4 hp -VS .50 Variable Speed, 1/2 hp (230V Only) -XP .25 Explosion Proof, Variable Speed, 1/4 hp -XP .50 Explosion Proof, Var. Speed, 1/2 hp (230V Only) -AM .25 Air Motor, 1/4 hp -AM .50 Air Motor, 1/2 hp -GDD Geared Direct Drive (Fixed Head Units Only)
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Series 4540 600-1200 mL High Pressure Reactor Systems

Series Number:
4540
Type:
High Pressure
Stand:
Floor Stand or Bench Top

Vessel Mounting:

Vessel Sizes, mL:
600 and 1200

High Pressure MAWP Rating, psi (bar):
5000 (345)
Standard Maximum Operating Temp., C: 350 w/ PTFE Flat Gasket
his series of stirred reactors has been designed for users who need higher operating pressures than the 2000 to 3000 psi offered by the General Purpose Reactors, but do not require the high operating temperatures provided by the Series 4570 High Pressure, High Temperature Reactors. These reactors offer working pressures to 5000 psi (345 bar) at temperatures to 350 C. These vessels have been designed with outside dimensions comparable to the Series 4520 and 4530 Reactors so that they can use the same support system, stirrer drive and heater as these popular general purpose models. This provides not only an attractively priced high pressure/moderate temperature system, but also reactors that can be interchanged with the 1 and 2 liter sizes. The thicker walls required for higher oper ating pressures reduce the volumes of these reactors to 600 and 1200 mL. These reactors can be used in either the bench top or oor stand mountings. While the 1200 mL reactor is offered as a bench top model, it is too tall and too heavy to be handled comfortably on a standard height bench top. It is recommended that the oor stand support option should be selected unless the user has an adjustable bench top which will accommodate the overall height of the 1200 mL systems.
Model 4544 High Pressure Reactor, 600 mL, Moveable Style Vessel, with heater lowered, and a 4848 Controller shown with optional Expansion Modules.
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Series 4540 Pressure Reactor System Specications Shaded bar indicates specications that change within series. Model No. - Moveable Vessel Model No. - Fixed Head Sizes, mL Maximum Pressure (MAWP) Maximum Temperature with PTFE Flat Gasket Reactor Mounting Valve Connections Magnetic Stirrer, Model No. Bench Top 350 C Floor Stand Split-Ring (8 Cap Screws) 1/4" Male NPT A1120HC6 16 Inch-Pounds 2 (1.75" dia.) 4.5 inches 5,000 psi (345 bar) Thermowell Optional Serpentine 1" NPS (Floor Stand Supports Only) Calrod 1000 1/8 1500 1/8 1000 1/8 115 or 230 14 / 7 3.25 4.7 51 17 24 38 125 4549MA 48 135 175 4549MB 9.8 57 4.7 51 21 28 63 185 175 4549MB 9.8 57 4.7 51 35 18 50 185 9.8 57 1500 1/8 1000 1/4 1500 1/4 Moveable Cart Vessel Details Closure
4544 4545
600
4546 4547
1200
4544A 4545A
600
4546A 4547A
1200
4544C
600
4546C
1200
5000 psi (345 bar)
Maximum Torque Impeller(s), 6-Blade Pressure Gage, Size Temperature Measurement Cooling Coil Bottom Drain Valve (Optional) Heater Style Heater Power, Watts Stirrer Motor, hp Volts, AC Maximum Load, amps, 115 / 230 Inside Diameter, inches Inside Depth, inches Weight of Vessel, pounds Width, inches Depth, inches Height, inches Weight, pounds Range
Style
Electrical Supply
Vessel Dimensions
Reactor Dimensions
Spare Parts Kit
Other options available. See Ordering Guide, visit www.parrinst.com, or call for more information.
1 - 8 0 0 - 8 7 2 - 7 7 2 0
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Series 4540 600-1200 mL High Pressure Reactor Systems

INDEX TO OPTIONS

Model 4546C Reactor, 1200 mL, Moveable Head Style, on a Moveable Cart, and a 4848 Reactor Controller shown with optional Expansion Modules.
1200 mL Fixed Head, and 600 mL Moveable Reaction Vessels.
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A Base Model Model No. Size 4544 600 mL 4544A 600 mL 4544C 600 mL 4545 600 mL 4545A 600 mL 4546 1200 mL 4546A 1200 mL 4546C 1200 mL 4547 1200 mL 4547A 1200 mL Vessel Style Moveable Bench Top Moveable Floor Stand Moveable Cart Fixed Head Bench Top Fixed Head Floor Stand Moveable Bench Top Moveable Floor Stand Moveable Cart Fixed Head Bench Top Fixed Head Floor Stand H Pressure Gage -3000 3000 psi / 200 bar -5000 5000 psi / 345 bar I Internal Cooling Coil -No Symbol No Coil -SC Serpentine Coil J Bottom Drain Valve -No Symbol No Bottom Drain Valve -BDV Bottom Drain Valve, 1" NPS K Controller B Gasket / Maximum Temperature -T PTFE Compression Gasket / 350 C C Materials of Construction -SS T316 Stainless Steel -MO Alloy 400 -IN Alloy 600 -HB Alloy B-2 -HC Alloy C-276 -CS Alloy 20 -TI2 Titanium Grade 2 -TI4 Titanium Grade 4 -NI Nickel 200 -ZR Zirconium Grade 702 or 705 D Magnetic Stirrer Drive -M General Purpose, 16 in-lb -FMD1 Footless, General Purpose, 16 in.-lb, E Mag. Drive Material of Construction -No Symbol Same Material As Vessel -MOC Symbol Indicate Material of Construction F Electrical Supply -115 115 VAC -230 230 VAC G Motor Option -VS .12 Variable Speed, 1/8 hp -VS .25 Variable Speed, 1/4 hp -XP .25 Explosion Proof, Variable Speed, 1/4 hp -AM .25 Air Motor, 1/4 hp -4848 -A1925E4 -4871 PID Control, Ramp & Soak Programming, Motor Speed Control, and Data logging with Software Optional RS485 to USB Cable for 4848 Controller Process Controller
L 4848 Expansion Modules -TDM Tachometer Display Module -MCM Tachometer w/Motor Control Module -PDM Pressure Display Module -HTM High Temperature Cut Off Module -ETLM External Temperature Limit Module -MTM Motor Torque Module M 4848 Cooling Control: Solenoid Valve Module -SVM1 115 VAC -SVM2 230 VAC N Custom Options (List All Desired) -AS Anchor Stirrer -SB Static Catalyst Basket -CAD Catalyst Addition Device -BF Bafes -GE Gas Entrainment Stirrer -RC Reux Condenser -RTC Reux Take-off Condenser -ABH Aluminum Block Heater -WJ Welded Jacket -SCP Solids Charging Port O Certications -No Symbol No Certication -ASME ASME Certication -CE/PED European Community Certication -CH China Certication -P Parr Certication P Spare Parts Kit -4549MA Spare Parts Kit for 4544-4547 -4549MB Spare Parts Kit for 4544A-4547A, 4544C, 4546C
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Series 4550 1 & 2 Gallon Reactor Systems

Series Number:
4550
Type:
General Purpose
Stand:
Floor Stand
Vessel Mounting:
Vessel Sizes, Gallons:
1 and 2
1900 (131)
hese 4550 Reactors extend the size range of the 4530 Series to 1 and 2 gallon (3.75 and 7.5 liter) sizes, providing excellent facilities for pilot plant studies. They can be furnished with either a self-sealing O-ring closure for working temperatures up to 225 C, or with a at, PTFE gasket for higher temperatures to 350 C. Both xed head and moveable head designs are available. The moveable head, Model 4551 and 4552, reactors are designed so that they can be opened or closed conveniently without removing the cylinder from the heater and without auxiliary handling equipment. The split-ring cover clamp sections can be moved into place from the sides, and the cap screws can be tightened with the vessel in place in its heater. The xed head versions, Model 4553 and 4554, allow the head (and the connections made to it) to remain in place while the cylinder and heater are lowered with the aid of the included pneumatic lift system. The 1 gallon size is usually recommended for high viscosity polymer studies. An optional bottom drain valve may be added for convenient product recovery. As with the smaller oor stand models, these larger, self- contained systems can be equipped with a variety of attachments, such as: condensers, solids charging port, bottom drain, special motors, special heaters, jacketed vessels and automatic valves and regulators. Because of the higher wattage heaters for these reactors, all models in the 4550 Series require a 230 volt power supply.
Model 4554 Reactor Fixed Head, Two Gallon Vessel, Pneumatic Lift, Hinged Split Rings, opened to show Internal Fittings and Serpentine Cooling Coil, with 4848 Reactor Controller shown with optional Expansion Modules.
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Series 4550 Pressure Reactor System Specications Shaded bar indicates specications that change within series. Model Number Sizes, Gallon (Liter) Maximum Pressure (MAWP) Maximum Temperature with FKM O-ring with FFKM O-ring with PTFE Flat Gasket Vessel Style Reactor Mounting Valve Connections Magnetic Stirrer, Model No. Closure Moveable Cart Split-Ring (10 Cap Screws) 1/4" NPT Male A1180HC 60 Inch-Pounds 2 (3.85" dia.) 4.5 inches 0-2000 psi (140 bar) Thermowell Optional Serpentine or Spiral 3/8" NPT Calrod 2250 2700 1/2 hp variable speed Pneumatic Lift 230 13 15 6.0 8.6 95 35 18 50 265 295 4559M Other options available. See Ordering Guide, visit www.parrinst.com, or call for more information. 315 17.2 120 8.6 115 20 31 75 345 17.2 140 13 15 2250 2700 225 C 275 C 350 C Fixed Head Floor Stand
4551
1 (3.75)
4552
2 (7.50) 1900 psi (131 bar)
4553
1 (3.75)
4554
2 (7.50)
Maximum Torque Impeller(s), 6-Blades Pressure Gage, Size Temperature Measurement Cooling Coil Bottom Drain Valve (Optional) Heater Style Heater Power, Watts Stirrer Motor Lift Mechanism Electrical Supply Volts, AC Maximum Load, amps Vessel Dimensions Inside Diameter, inches Inside Depth, inches Weight of Vessel, pounds Reactor Dimensions Width, inches w/o Controller Depth, inches Height, inches Weight, pounds Spare Parts Kit Range
Style
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Series 4550 1 & 2 Gallon Reactor Systems

INDEX TO OPTIONS
The innovative Parr Hinged Split-Rings on the 4553 and 4554 add to a safe vessel removal routine. Simply loosen the compression bolts, unlatch the split-ring closures, and pivot the split-rings out of the way.

4551 Floor Stand Reactor, 1 Gallon, with Bottom Drain Valve, and a 4848 Temperature Controller shown with optional Expansion Modules.
4553 Floor Stand Reactor with Gear Drive, Hinged Split Rings, and heater attached.
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The Order No. for the Base System is: 455__-T-SS-HD-230-VS.50-2000-4848 A composite identication number to be used when ordering a 4550 Series Reactor can be developed by combining individual symbols from the separate sections below. For more information on how to use this ordering guide, please see page 27.
A Base Model Model No. Size 4551 1 Gallon 4552 2 Gallon 4553 1 Gallon 4554 2 Gallon Vessel Style Moveable, Cart Moveable, Cart Fixed Head, Floor Stand Fixed Head, Floor Stand I Internal Cooling Coil -No Symbol No Coil -CC Spiral Coil -SC Serpentine Coil J Bottom Drain Valve -No Symbol No Bottom Drain Valve -BDV Bottom Drain Valve 3/8" NPT K Controller -4848 -A1925E4 -4871 PID Control, Ramp & Soak Programming, Motor Speed Control, and Data logging with Software Optional RS485 to USB Cable for 4848 Controller Process Controller
B Gasket / Maximum Temperature -OV FKM O-ring / 225 C -OK FFKM O-ring / 275 C -T PTFE Compression Gasket / 350 C C Materials of Construction -SS T316 Stainless Steel -MO Alloy 400 -IN Alloy 600 -HB Alloy B-2 -HC Alloy C-276 -CS Alloy 20 -TI2 Titanium Grade 2 -TI4 Titanium Grade 4 -NI Nickel 200 -ZR Zirconium Grade 702 or 705 D Magnetic Stirrer Drive -HD Heavy Duty, 60 in-lb -XHD Extra Heavy Duty, 120 in-lb -FMD2 Footless, Heavy Duty, 60 in-lb -FMD3 Footless, Extra Heavy Duty, 120 in-lb E Mag. Drive Material of Construction -No Symbol Same Material As Vessel -MOC Symbol Indicate Material of Construction F Electrical Supply -230 230 VAC G Motor Option -VS .50 Variable Speed, 1/2 hp -XP .50 Explosion Proof Variable Speed, 1/2 hp -AM .50 Air Motor, 1/2 hp -GDD Geared Direct Drive (Fixed Head Units Only) H Pressure -2000 -1000 -600 -200 -100 Gage 2000 psi / 137 bar 1000 psi / 70 bar 600 psi / 40 bar 200 psi / 14 bar 100 psi / 7 bar
L 4848 Expansion Modules -TDM Tachometer Display Module -MCM Tachometer w/Motor Control Module -PDM Pressure Display Module -HTM High Temperature Cut Off Module -ETLM External Temperature Limit Module -MTM Motor Torque Module M 4848 Cooling Control: Solenoid Valve Module -SVM1 Not Available -SVM2 230 VAC N Custom Options (List All Desired) -AS Anchor Stirrer -BF Bafes -GE Gas Entrainment Stirrer -RC Reux Condenser -RTC Reux Take-off Condenser -ABH Aluminum Block Heater -WJ Welded Jacket -SCP Solids Charging Port -SA Spiral Agitator O Certications -No Symbol No Certication -ASME ASME Certication -CE/PED European Community Certication -CH China Cerication -P Parr Certication P Spare Parts Kit -4559M Spare Parts Kit for 4550 Series
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Series 4555 10 & 20 Liter Reactor Systems

Series Number:
4555
Type:
General Purpose
Stand:
Floor Stand
Vessel Mounting:
Vessel Sizes, Liters:
10 and 20
1900 (131)
Maximum Operating Temperature, C: 225 w/ FKM O-ring 275 w/ FFKM O-ring 350 w/ PTFE Flat Gasket
he Model 4555 and 4557 Reactors with their 5 gallon (18.75 L) capacity are the largest stirred reactors offered by Parr. The 4556 and 4558 Models are similar units with a 10 liter (2.6 gal) volume which falls between the larger 5 gallon design and the smaller 1 and 2 gallon models in the 4550 Series. Vessel styles are offered in a moveable head or xed head design. These reactors are available with an FKM O-ring seal for operating temperatures to 225 C, and FFKM O-ring for temperatures to 275 C, or with a at, PTFE gasket for operating temperatures up to 350 C maximum. In the moveable head design, the vessel is held in a support system which minimizes the physical effort required to handle these heavy components. The hoist is attached to a support column which provides a convenient means for lifting the head and cylinder out of the stand. These components may be transferred to the holding position on the right side of the stand. Vessels equipped with a bottom drain valve will probably remain in the heater most of the time, but can be lifted out when necessary. The xed head support stand features hinged split-rings that 4557 Floor Stand Reactor, Flexible Mantle Heater, with Split Rings and Pneumatic Lift. swing to either side allowing Below: Hinged Split Rings open revealing Serpentine Cooling Coil, with Heater and the head to remain xed to Vessel lowered via Pneumatic Lift. the stand while a pneumatic lift allows the cylinder to be raised and lowered. When lowered, the cylinder can be slid forward for cleaning and servicing. These reactors are generally used for pilot plant or for custom chemical production purposes, usually with a variety of attachments added to the basic units. Various heaters, larger motors, heavier stirrer drives and remote controls appropriate to the size of these reactors have been designed and are available. Modied versions of these units are available with higher working pressures and temperatures.
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Series 4555 Pressure Reactor System Specications Shaded bar indicates specications that change within series. Model Number Sizes, Gallon (Liter) Maximum Pressure (MAWP) Maximum Temperature with FKM O-ring with FFKM O-ring with PTFE Flat Gasket Vessel Style Reactor Mounting Valve Connections Magnetic Stirrer, Model No. 2 (5.25" dia.) 2 (3.85" dia.) 4.5 inches 0-2000 psi (140 bar) Thermowell Standard Serpentine 1.0" NPT Ceramic, 3-Zone 4500 4250 3/4 hp variable speed 230-1P or 400-415V 3-Phase Y 1P-40 amps, 3P-15 amps/leg 9.5 16.25 375 63 25 91 1000 4559PCM Other options available. See Ordering Guide, visit www.parrinst.com, or call for more information. Because of considerable power requirements for a unit this size, 3-phase power is typical. Single phase 230 VAC is also possible, but requires a power source capable of supplying over 40 amps, well beyond the limits of most laboratory power supplies. Users are advised to have a qualied electrician install a suitable 3-phase Y power supply. Parr Technical Support will be happy to assist with electrical specications. Systems with lower electrical requirements such as jacketed systems or lower wattage mantle heaters may be able to use single phase effectively. 900 95 1000 4559PDM 7.75 12.2 250 9.5 16.25 375 31 43 87 900 7.75 12.2 250 6000 Band Heater, 3-Zone 3600 Closure Moveable Head Cart Split-Ring (12 Cap Screws) 3/8" NPT Male A1750HC 60 Inch-Pounds 2 (5.25" dia.) 2 (3.85" dia.) 225 C 275 C 350 C Fixed Head Floor Stand
4555
5 (18.75)
4556
2.6 (10) 1900 psi (131 bar)
4557
5 (18.75)
4558
2.6 (10)
Maximum Torque Impeller(s), 6-Blades Pressure Gage, Size Temperature Measurement Cooling Coil Bottom Drain Valve (Optional) Heater Style Heater Power, Watts Stirrer Motor Electrical Supply Volts, AC Maximum Load Vessel Dimensions Inside Diameter, inches Inside Depth, inches Weight of Vessel, pounds Reactor Dimensions Width, inches w/o Controller Depth, inches Height, inches Weight, pounds Spare Parts Kit Range
Style
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Series 4555 10 & 20 Liter Reactor Systems

INDEX TO OPTIONS

4556 Floor Stand Reactor on a Cart, 10 Liter Moveable Vessel, Electric Hoist, and a 4848 Controller shown with optional Expansion Modules.
10 Liter Stirred Vessel removed from heater.
Model 4556 Reactor, 10 Liter Vessel, with head removed.
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The Order No. for the Base System is: 455__-T-SS-HD-230-VS.75-2000-SC-C3-4848-ASME A composite identication number to be used when ordering a 4555 Series Reactor can be developed by combining individual symbols from the separate sections below. For more information on how to use this ordering guide, please see page 27.
A Base Model Model No. Size 4555 5 Gallon 4556 10 Liter 4557 5 Gallon 4558 10 Liter Vessel Style Moveable Moveable Fixed Head Fixed Head K Heater -C3 -CA3 -BH1 -BH2 -WJ -MHTR Options Ceramic, 3-Zone (4555/4556) Cast Aluminum, 3-Zone (4555/4556) Band Heater Band Heater (High Temperature) Welded Jacket Flexible Mantle Heater, 1-zone
B Gasket / Maximum Temperature -OV FKM O-ring / 225 C -T PTFE Compression Gasket / 350 C C Materials of Construction -SS T316 Stainless Steel -MO Alloy 400 -IN Alloy 600 -HB Alloy B-2 -HC Alloy C-276 -CS Alloy 20 -TI2 Titanium Grade 2 -TI4 Titanium Grade 4 -NI Nickel 200 -ZR Zirconium Grade 702 or 705 D Magnetic Stirrer Drive -HD Heavy Duty, 60 in-lb -XHD Extra Heavy Duty, 120 in-lb -FMD2 Footless Magnetic Drive, 60 in-lb -FMD3 Footless Magnetic Drive, 120 in-lb E Mag. Drive Material of Construction -No Symbol Same Material As Vessel -MOC Symbol Indicate Material of Construction F Electrical Supply -230 230 VAC, Single Phase -400 400-480V 3-Phase Y G Motor Option -VS .75 Variable Speed, 3/4 hp -XP .75 Explosion Proof Variable Speed, 3/4 hp -AM .100 Air Motor, 1 hp H Pressure -2000 -1000 -600 -200 -100 Gage 2000 psi / 137 bar 1000 psi / 70 bar 600 psi / 40 bar 200 psi / 14 bar 100 psi / 7 bar
L Head Lift Mechanism (Cart only) -EH Electric Hoist (115 VAC) -MH Manual Hoist M Stirrer Drive Gear Ratios DD Direct Drive 3D 3:1, 0-600 rpm 5D 5:1, 0-360 rpm 10D 10:1, 0-180 rpm N Controller -4848 -A1925E4 -4871 PID Control, Ramp & Soak Programming, Motor Speed Control, and Data logging with Software Optional RS485 to USB Cable for 4848 Controller Process Controller
O 4848 Expansion Modules -TDM Tachometer Display Module -MCM Tachometer w/Motor Control Module -PDM Pressure Display Module -HTM High Temperature Cut Off Module -ETLM External Temperature Limit Module -MTM Motor Torque Module P 4848 Cooling Control: Solenoid Valve Module -SVM1 Not Available -SVM2 230 VAC Q Custom Options (List All Desired) -AS Anchor Stirrer -SA Spiral Stirrer -BF Bafes -GE Gas Entrainment Stirrer -RC Reux Condenser -RTC Reux Take-off Condenser -SCP Solids Charging Port R Certications -No Symbol No Certication -ASME ASME Certication -CE/PED European Community Certication -CH China Certication -P Parr Certication S Spare Parts Kit -4559PCM Spare Parts Kit for 4555 and 4557 -4559PDM Spare Parts Kit for 4556 and 4558
I Internal Cooling Coil -No Symbol No Coil -SC Serpentine Coil J Bottom -No Symbol -BDV1 -ABDV Drain Valve No Bottom Drain Valve Bottom Drain Valve, 1" NPT Air Actuated Bottom Drain Valve
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Series 4560 Mini Reactor Systems

Series Number:
4560
Type:
Mini
Stand:
Bench Top
Vessel Mounting: Moveable or
Fixed Head
Sizes, mL:
100 - 600
Standard Temperature MAWP Rating, psi (bar):
3000 (200)
High Temperature (HT) MAWP Rating psi (bar):
2000 (138)
High Temperature (HT) Maximum Operating Temperature, C: 500 w/ FG Flat Gasket
hese are the most popular of all Parr Stirred Reactors. Although they are called Mini reactors, they offer a range of sizes large enough to work with signicant sample sizes, yet small enough to be handled with ease by all operators. They are made in both xed head and moveable vessel styles, with a choice of either a self sealing O-ring closure with no cap screws for working temperatures up to 225 C, or with a at, PTFE gasket for higher temperatures up to 350 C sealed with six cap screws in a split-ring cover clamp. Choosing the high tempera ture option (HT) boosts the maximum temperature to 500 C, but de-rates the MAWP to 2000 psi (138 bar). Standard Mini reactors can be converted to high temperature reactors (500 C max temperature and 2000 psi MAWP) by changing the head openings to cone connections, replacing the valves with high temperature valves, replacing the gasket with a graphoil Flat Gasket, replacing the heater with a ceramic ber heater, and replacing the split ring. Contact Parr for details. Although internal and external space is limited in these small vessels, gas entrainment impellers, catalyst baskets, condensers and other options are available. All reactors in this series can also be easily converted from one size to another by simply substituting a longer or shorter cylinder with the corresponding internal ttings and heaters. The support system for these Mini Reactors is designed specically to provide stability at stirring speeds up to 1700 rpm, in a compact mounting small enough to t into a laboratory hood. The support system can also be adapted to accept any of the smaller vessels from the 4590 Micro Reactor Series.
4566 Mini Reactor, 300 mL, Fixed Head, Quick-release Split Ring, and a 4848 Controller shown with optional Expansion Modules.
4566 with Aluminum Block Heater, Bottom Drain Valve, and a 4848 Controller shown with optional Expansion Modules.
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Series 4560 Pressure Reactor System Specications Shaded bar indicates specications that change within series. Model Number Sizes, mL Maximum Pressure (MAWP) HT Max. Pressure (MAWP) Maximum Temperature with FKM O-ring with FFKM O-ring with PTFE Flat Gasket with FG Flat Gasket (HT) Reactor Mounting Valve Connections Magnetic Stirrer, Model No. Impeller(s), 4-Blade, 1.38" dia. Range, Standard Pressure Range, High Pressure Included 1 1 2 1 1 3.5 inches 0-2000 psi (140 bar) 0-3000 psi (200 bar) Fixed Thermocouple (Thermowell for special alloys) Not Included Single Loop 1/4" NPT (Not available on HT Models.) Mantle 510 800 590 Ceramic Fiber 800 1100 780 Clamp-on 500 N/A 800 1/8 hp variable speed 115 or 230 10 / 5 (14 / 7 High Temperature) 2.5 4 10 2.5 6 13 2.5 8 16 2.5 2 8 2 2 9 12 18 28 60 32 63 36 66 28 60 28 60 4569M * Height increases 4-inches with the Bottom Drain Valve option. Other options available. See Ordering Guide, visit www.parrinst.com, or call for more information. 28 62 32 65 36 68 28 60 28 60 2.5 4 12 2.5 6 15 2.5 8 18 2.5 2 8 2 2 9 510 Mantle 590 Ceramic Fiber 1000 1200 780 Clamp-on 500 N/A Included Not Included 500 C Moveable Bench Top Split-Ring (6 Cap Screws) 1/8" NPT Male A1120HC6 16 Inch-Pounds 1 1 2 1 1 NA 225 C 275 C 350 C 500 C Fixed Head NA
4561
300
4562
450
4563
600
4564
160
4565
100
4566
300
4567
450
4568 4566B 4566C

600 160 100
3000 psi (200 bar) 2000 psi (138 bar)
Vessel Style Closure
Maximum Torque Pressure Gage, Size
Temperature Measurement Cooling Coil Bottom Drain Valve Heater Style Heater Power, Watts Heater Power, Watts Heater Style w/ HT Option Stirrer Motor Volts, AC Maximum Load, amps, 115 / 230 Inside Diameter, inches Inside Depth, inches Weight of Vessel, pounds
Style
Electrical Supply
Vessel Dimensions
Reactor Dimensions Width, inches w/o Controller Depth, inches Height, inches* Weight, pounds w/ Controller
Spare Parts Kit
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Series 4560 Mini Reactor Systems

INDEX TO OPTIONS
Model 4563 Mini Reactor, 600 mL, Moveable Vessel, PTFE Flat Gasket Seal, with vessel disassembled, and a 4848 Controller shown with optional Expansion Modules.

4560 Reactor Vessels from left to right, 300 mL, 100 mL, 450 mL, 160 mL, and 600 mL.
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A Base Model Model No. Size 4561 300 mL 4562 450 mL 4563 600 mL 4564 160 mL* 4565 100 mL * 4566 300 mL 4567 450 mL 4568 600 mL 4566B 160 mL* 4566C 100 mL* * High temperature option not available. Vessel Style Moveable Moveable Moveable Moveable Moveable Fixed Head Fixed Head Fixed Head Fixed Head Fixed Head I Pressure Gage -3000 3000 psi / 200 bar -2000 2000 psi / 137 bar -1000 1000 psi / 70 bar -600 600 psi / 40 bar -200 200 psi / 14 bar -100 100 psi / 7 bar J Bottom Drain Valve -No Symbol No Bottom Drain Valve -BDV K Bottom Drain Valve Installed (Not Available on High Temperature Vessels)
B High Temperature Option -No Symbol Standard Conguration -HT High Temperature / 500 C C Gasket / Maximum Temperature -OV FKM O-ring / 225 C -OK FFKM O-ring / 275 C -T PTFE Flat Compression Gasket / 350 C -FG Flexible Graphite Gasket / 500 C D Material of Construction -SS T316 Stainless Steel -MO Alloy 400* -IN Alloy 600 -HB Alloy B-2* -HC Alloy C-276 -CS Alloy 20* -TI2 Titanium Grade 2* -TI4 Titanium Grade 4* -NI Nickel 200* -ZR Zirconium Grade 702 or 705* * Not available for HT option E Magnetic Stirrer Drive -M General Purpose, 16 in-lb -FMD1 Footless, 16 in-lb F Stirrer Drive Material of Construction -No Symbol Same Material As Vessel -MOC Symbol Indicate Material of Construction G Electrical Supply -115 115 VAC -230 230 VAC H Motor Option -VS .12 Variable Speed, 1/8 hp -VS .25 Variable Speed, 1/4 hp -XP .25 Explosion Proof Variable Speed, 1/4 hp -AM .25 Air Motor, 1/4 hp
Controller PID Control, Ramp & Soak Programming, Motor Speed Control, and Data logging with Software Optional RS485 to USB Cable for 4848 Controller Process Controller
-4848 -A1925E4 -4871
L 4848 Expansion Modules -TDM Tachometer Display Module -MCM Tachometer w/Motor Control Module -PDM Pressure Display Module -HTM High Temperature Cut Off Module -ETLM External Temperature Limit Module -MTM Motor Torque Module M 4848 Cooling Control: Solenoid Valve Module -SVM1 115 VAC -SVM2 230 VAC N Custom Options (List All Desired) -AS Anchor Stirrer -SB* Static Catalyst Basket -CAD* Catalyst Addition Device -BF* Bafes -GE Gas Entrainment Stirrer -RC Reux Condenser -RTC Reux Take-off Condenser -SCP Solids Charging Port -ABH* Aluminum Block Heater -WJ Welded Jacket * 300 mL vessels and larger only O Certications -No Symbol No Certication -ASME ASME Certication -CE/PED European Community Certication/Pressure -CH China Certication -P Parr Certication P Spare Parts Kit -4569M Spare Parts Kit for 4560 Series
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Series 4570/80 High Temperature/High Pressure Reactor Systems

Series Number:
4570/80
Type:
arr offers a number of different reactors in the 4570 and 4580 Series in a variety of sizes and with different mountings for operating pressures to 5000 psi (345 bar) and temperatures to 500 C. 4571 - 4572 Reactors These are 1000 and 1800 mL moveable head reactors mounted in movable carts. 4577 - 4578 Reactors These are 1000 and 1800 mL xed head reactors mounted on a oor stand with pneumatic lift. 4575 - 4576A Reactors These are 500 and 250 mL bench top reactors with 5000 psi (345 bar) and 500 C ratings. They are available as either moveable or xed head vessels. 4581 - 4582 Reactors These 1 gallon (3.75 L) and 1.5 gallon (5.5 L) reactors are designed for 3000 psi (200 bar) maximum pressure with a 500 C maximum working temperature and mounted on movable carts. 4583 - 4584 Reactors These are 1 gallon (3.75 L) and 1.5 gallon (5.5 L) xed head reactors mounted on oor stands with pneumatic lift. All of these reactors have been designed with suitable valves, ttings and modications to the vessel itself to operate at the higher temperature and pressure ratings. Flat, exible graphite (FG) gaskets are used for temperatures in the higher range to 500 C. These can be replaced with PTFE gaskets for procedures in which the temperature will not exceed 350 C. All cart and oor stand models use ceramic ber heaters to achieve the higher operating temperatures.
Model 4577 High Temperature/High Pressure Reactor, Floor Stand, Fixed Head 1000 mL with Heater and Pneumatic Lift.
High Temperature High Pressure

Stand:
Bench Top, Floor Stand or Cart

Vessel Mounting:

Vessel Sizes, mL:
250-5500
Standard Pressure MAWP Rating, psi (bar): 3000 (200) 4580 5000 (345) 4570
Maximum Operating Temperature, C: 500 w/ FG Flat Gasket
The Series 4570/80 High Temperature/High Pressure Reactors come in three congurations, from left to right: Bench Top (250 & 500 mL Only), Floor Stand, and Cart.
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Series 4570/80 Pressure Reactor System Specications Shaded bar indicates specications that change within series. Model No. Moveable Vessel Model No. Fixed Head Reactor Mounting Sizes, mL Maximum Pressure, MAWP Maximum Temperature with FG Flat Gasket Closure (Cap Screws) Valves Mounted Valve Connections Magnetic Stirrer, Model No. Impeller(s), 6-Blade (4-blade) A1120HC 16 Inch-Pounds 2 (2" dia.) Split Ring (12) 500 C Split Ring (16) Head 1/4" NPT Female A1180HC 60 Inch-Pounds 2 (3.5" dia.) 4.5 inches 0-5000 psi (345 bar) Thermowell Included Serpentine Serpentine 1" NPS (Floor stand supports only) Ceramic 2800 1/4 hp 230 13 3.75 6.2 70 85 10.5 85 100 9.7 100 120 14 2800 2800 1/2 hp 230 15 5.5 15 130 160 6.6 35 37 1000 1/8 hp 115 or 230 12 / 6 2.5 3.2 29 31 Single Loop A1120HC 16 Inch-Pounds 2 (1.38" dia.) Split Ring (8) Vessel Details
4571 4577
1000
4572 4578
1800
4581 4583
3750
4582 4584
5500
4575B 4575A
500
4576B 4576A
250
Cart / Floor Stand 5000 psi (345 bar)
Cart / Floor Stand 3000 psi (200 bar)
Bench Top 5000 psi (345 bar)
Maximum Torque Pressure Gage, Size Temperature Measurement Cooling Coil Bottom Drain Valve Heater Style Heater Power, Watts Stirrer Motor, Variable Speed Volts, AC Maximum Load, amps, 115 / 230 Inside Diameter, inches Inside Depth, inches Weight of Moveable Vessel, pounds Weight of Fixed Vessel, pounds Moveable Width x Depth x Height, in. Fixed Width x Depth x Height, in. Moveable Weight w/Controller, pounds Fixed Weight w/Controller, pounds
Range
Style
Electrical Supply
Vessel Dimensions
Reactor Dimensions Cart: 35 x 18 x 50 Floor Stand: 20 x 31 x 75 245 265 4579B 265 285 Cart: 35 x 18 x 50 Floor Stand: 20 x 31 x 75 325 345 4589B 355 375 Bench Top: 17 x 24 x 42 125 127 4579D 120 122
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Series 4570/80 High Temperature/High Pressure Reactor Systems

INDEX TO OPTIONS
Model 4581 High Temperature/High Pressure Reactor, with One Gallon Moveable Vessel, and a 4848 Reactor Controller with optional Expansion Modules.

Model 4575B High Pressure/High Temperature 500 mL Moveable Vessel Assembly.
Model 4576A HT/HP Reactor, Fixed Head Bench Top, with 250 mL Vessel.
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Series 4570/80 Ordering Guide

The Order No. for the Base System is: 457__ or 458__-FG-M or HD-SS-115 or 230-VS.__-5000-4848 A composite identication number to be used when ordering a 4570 or 4580 Series Reactor can be developed by combining individual symbols from the separate sections below. For more information on how to use this ordering guide, please see page 27.
A Base Model Model Size 4571 1000 mL 4572 1800 mL 4575B 500 mL 4576B 250 mL 4575A 500 mL 4576A 250 mL 4577 1000 mL 4578 1800 mL 4581 4582 4583 4584 1.0 Gallon 1.5 Gallon 1.0 Gallon 1.5 Gallon Vessel Style Moveable Head, Cart Moveable Head, Cart Moveable Head, Bench Top Moveable Head, Bench Top Fixed Head, Bench Top Fixed Head, Bench Top Fixed Head, Floor Stand Fixed Head, Floor Stand Moveable Head, Cart Moveable Head, Cart Fixed Head, Floor Stand Fixed Head, Floor Stand -XP .50* -AM .25 -AM .50* -GDD Explosion Proof Variable Speed, 1/2 hp Air Motor, 1/4 hp (4575-4576 Only) Air Motor, 1/2 hp Geared Direct Drive (Fixed Head Unit Only)
* For use with Heavy Duty (HD) Magnetic Stirrer Drive. Only available on 230V systems. I Pressure Gage -2000 2000 psi / 137 bar -3000 3000 psi / 200 bar -5000 5000 psi / 345 bar J Bottom Drain Valve -No Symbol No Bottom Drain Valve -BDV Bottom Drain Valve (Not available on 250 mL or Bench Top Systems.)
B Gasket / Maximum Temperature -FG Flexible Graphite Gasket, 500 C -T PTFE Compression Gasket, 350 C C Materials of Construction -SS T316 Stainless Steel -MO Alloy 400* -IN Alloy 600 -HB Alloy B-2* -HC Alloy C-276 -CS Alloy 20* -TI2 Titanium Grade 2* -TI4 Titanium Grade 4* -ZR Zirconium Grade 702* or 705* * Maximum temperature limited. D Magnetic Stirrer Drive for 4575-76 Only -M General Purpose, 16 in-lb -FMD Footless, General Purpose, 16 in-lb E Magnetic Stirrer Drive for 4571-4584 Only -M General Purpose , 16 in-lb -HD Heavy Duty, 60 in-lb -XHD Extra Heavy Duty, 120 in-lb -FMD1 Footless, 16 in-lb. -FMD2 Footless, Heavy Duty, 60 in-lb -FMD3 Footless, Extra Heavy Duty, 120 in-lb F Mag. Drive Material of Construction -No Symbol Same Material As Vessel -MOC Symbol Indicate Material of Construction G Electrical Supply -115 115 VAC (4575-4576 Only) -230 230 VAC H Motor Option -VS .12 Variable Speed, 1/8 hp (4575-4576 Only) -VS .25 Variable Speed, 1/4 hp -VS .50* Variable Speed, 1/2 hp -XP .25 Explosion Proof Variable Speed, 1/4 hp
K Controller -4848 -A1925E4 -4871 PID Control, Ramp & Soak Programming, Motor Speed Control, and Data logging with Software Optional RS485 to USB Cable for 4848 Controller Process Controller
L 4848 Expansion Modules -TDM Tachometer Display Module -MCM Tachometer w/Motor Control Module -PDM Pressure Display Module -HTM High Temperature Cut Off Module -ETLM External Temperature Limit Module -MTM Motor Torque Module M 4848 Cooling Control: Solenoid Valve Module -SVM1 115 VAC -SVM2 230 VAC N Custom Options (List All Desired) -AS Anchor Stirrer -SB* Static Catalyst Basket -GE Gas Entrainment Stirrer -RC Reux Condenser -RTC Reux Take-off Condenser -BF Bafes * Not available on 250 mL vessels O Certications -No Symbol No Certication -ASME ASME Certication -CE/PED European Community Certication -CH China Certication -P Parr Certication P Spare Parts Kit -4579B Spare Parts Kit for 4571, 4572, 4577, 4578 -4589B Spare Parts Kit for 4581, 4582, 4583, 4584 -4579D Spare Parts Kit for 4575B, 4576B, 4575A, 4576A
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Series 4590 Micro Reactor Systems

Series Number:
4590
Type:
Micro
Stand:
Bench Top
Vessel Mounting: Moveable or
Fixed Head
Sizes, mL:
25, 50, 100

3000 (200)
5000 (345)
4597 Micro Reactor, Fixed Head, 50 mL, and a 4848 Reactor Controller with optional Expansion Modules.
High Temperature (HT) / High Pressure (HP) Maximum Operating Temperature, C: 500 w/ FG Flat Gasket (Fixed Head Only)
hese are the smallest of all Parr Stirred Reactors. They will be a good choice for chemists working with very expensive materials or materials only available in small amounts. They will also appeal to users who wish to minimize the risks associated with hazardous materials or reactions by restricting the reactants or products to a minimum. Use of the Series 4590 Reactors also helps minimize the quantities of waste products which may require special disposal procedures. The 4590 systems are now available in high pressure (5000 psi) or high pressure/high temperature (500 C) versions. These micro reactors have been designed to provide as many of the features of the larger vessels as possible in the limited space available. All of the standard head ttings are provided, with optional cooling now available with aluminum block heaters with cooling capability, welded jackets or Cold Fingers.
These systems are offered in both xed head and moveable head vessel styles with choices of a self sealing O-ring for temperatures up to 225 C or with FFKM O-ring for temperatures to 275 C or with a at PTFE gasket for temperatures to 350 C, or with a Flexible Graphite gasket for temperatures to 500 C with the HP/HT option (for xed head versions only). A split ring closure is standard. All three volumes use the same ceramic ber heater. These micro reactors can be easily converted from one size to another by simply substituting a larger or smaller cylinder and the corresponding internal ttings. The support system can also be readily adapted to accept any of the vessels from the 4560 Mini Reactor Series. The opportunity to modify these small reactors is restricted because of the limited head space available.
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Series 4590 Pressure Reactor System Specications Shaded bar indicates specications that change within series. Model Number Sizes, mL Maximum Pressure (MAWP) HP Maximum Pressure (MAWP) Maximum Temperature with FKM O-ring with FFKM O-ring with PTFE Compression Gasket with FG Flexible Graphite Reactor Mounting Valve Connections Magnetic Stirrer, Model No. NA Moveable Bench Top Split-Ring (6 Cap Screws) 1/8" NPT Male (1/4" NPT Male required for HP/HT) A1120HC6 16 Inch-Pounds 1 (.81" dia.) 3.5 inches 0-3000 psi (200 bar) N/A Optional 1/4" NPT (Not Available on HP/HT) Ceramic Fiber Heater 700 1/8 hp Variable Speed 115 or 230 6/3 NA 1.0 2.0 7 1.3 2.3 7 1.3 4.6 8 12 18 28 55 55 36 56 4599M * Add 4" to height with Bottom Drain Valve option. Other options available. See Ordering Guide, visit www.parrinst.com, or call for more information. 56 28 56 36 57 1.0 2.0 7 5/2 6/3 8/5 1.3 2.3 7 1.3 4.6 8 5/2 0-5000 psi (345 bar) Fixed Thermocouple (Thermowell for special alloys) 225 C Split Rings with Latches 275 C Split Rings with Latches 350 C Split Rings (6 Cap Screws) 500 C Split Rings Fixed Head
4591
25
4592
50
4593
100
4596
25
4597
50
4598
100
3000 psi (200 bar) 5000 psi (345 bar)
Vessel Style Closure
Maximum Torque Impeller, 4-Blade Pressure Gage, Size Range w/ HP/HT Option Range Temperature Measurement Cooling Coil Bottom Drain Valve (Optional) Heater Style Heater Power, Watts Stirrer Motor Volts, AC Maximum Load, amps, 115 / 230 Maximum Load, amps, HP/HT, 115 / 230 Inside Diameter, inches Inside Depth, inches Weight of Vessel, pounds
Electrical Supply
Vessel Dimensions
Reactor Dimensions Width, inches w/o Controller Depth, inches Height, inches* Weight, pounds
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Series 4590 Micro Reactor Systems

INDEX TO OPTIONS

Model 4593 Reactor, 100 mL Moveable Vessel, with PTFE Compression Gasket, and Split Ring Closure, Mantle Heater, shown with a 4848 Reactor Controller with optional Expansion Modules.
Model 4593 100 ml stirred vessel.
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A Base Model Model Size 4591 25 mL 4592 50 mL 4593 100 mL 4596 25 mL 4597 50 mL 4598 100 mL Vessel Style Moveable Moveable Moveable Fixed Head Fixed Head Fixed Head H Motor -VS .12 -VS .25 -XP .25 -AM .25 Option Variable Speed, 1/8 hp Variable Speed, 1/4 hp Explosion Proof Variable Speed, 1/4 hp Air Motor, 1/4 hp
B Moveable Head Options Standard Conguration -No Symbol -HP 5,000 psi (345 bar) @ 350 C Fixed Head Options -No Symbol Standard Conguration -HP 5,000 psi (345 bar) @ 350 C -HP/HT 5,000 psi (345 bar) @ 500 C C Gasket / Maximum Temperature -OV FKM O-ring / 225 C -OK FFKM O-ring / 275 C -T PTFE Compression Gasket / 350 C -FG Flexible Graphite / 500 C (HP/HT option only) D Material of Construction -SS T316 Stainless Steel -MO Alloy 400* -IN Alloy 600 -HB Alloy B-2* -HC Alloy C-276 -CS Alloy 20* -TI2 Titanium Grade 2* -TI4 Titanium Grade 4* -NI Nickel 200 -ZR Zirconium Grade 702* or 705* * Maximum temperature limited. E Stirrer Drive -M General Purpose Magnetic F Mag. Drive Material of Construction -No Symbol Same Material As Vessel -MOC Symbol Indicate Material of Construction G Electrical Supply -115 115 VAC -230 230 VAC
I Pressure Gage -5000 5000 pis / 345 bar -3000 3000 psi / 200 bar -2000 2000 psi / 137 bar -1000 1000 psi / 70 bar -600 600 psi / 40 bar -200 200 psi / 14 bar -100 100 psi / 7 bar J Controller PID Control, Ramp & Soak Programming, Motor Speed Control, and Data logging with Software Optional RS485 to USB Cable for 4848 Controller Process Controller
-4848 -A1925E4 -4871
K 4848 Expansion Modules -TDM Tachometer Display Module -MCM Tachometer w/Motor Control Module -PDM Pressure Display Module -HTM High Temperature Cut Off Module -ETLM External Temperature Limit Module -MTM Motor Torque Module L 4848 Cooling Control: Solenoid Valve Module -SVM1 115 VAC -SVM2 230 VAC M Custom Options (List All Desired) -RC Reux Condenser -RTC Reux Take-off Condenser -GE Gas Entrainment Stirrer -ABH Aluminum Block Heater -WJ Welded Jacket N Certications -No Symbol No Certication -ASME ASME Certication -CE/PED European Community Certication/Pressure -CH China Certication -P Parr Certication O Spare Parts Kit -4599 Spare Parts Kit for 4590 Series -4599HT Spare Parts Kit for 4590HT Series
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Series 5100 Low Pressure Reactors

Series Number:
5100
Type:
Glass or Metal
Bench Top
Vessel:
Fixed Head
Sizes, mL:
The split ring for the glass vessel is padded with high temperature plastic cushions so the glass vessel does not come in direct contact with the metal split ring. Six sealing screws are tightened only nger tight to develop the seal on the O-ring. The split ring snaps together with latches to provide a secure and positive closure. The alternate metal cylinders use a different split ring designed to handle the higher working pressure of the metal vessels. Positive Agitation by High Torque Magnetic Drives These reactors are equipped with Parr magnetic drives to provide a trouble free internal stirrer. These drives have been designed and tested to routinely deliver 2000 hours of operation without service.
160 mL - 1.5 L
Maximum Operating Pressure, psi (bar): Glass: Metal:
150 psi (10 bar) 1000 psi (69 bar)
5111 Bench Top Reactor, 1000 mL, Fixed Head, Glass Jacketed Vessel.
Maximum Operating Temperature, C:
225
he Parr series 5100 Low Pressure Reactors are offered in response to users requests for: 1. A system for running reactions similar to those that have been conducted for many years in the Parr shaker, but which offer stirring for better scalability, higher operating temperatures and pressures, and more extensive reactor controls and instrumentation. 2. Reactors for elevated pressures with glass vessels that permit direct observation of mixing action, color changes, or changes of state. 3. Reactors designed for convenient operation at moderate pressure and/or for corrosion resistance. Convenient and Easy Sealing with O-rings and Split Ring Closures Parr has developed a new O-ring and closure system to accommodate the requirements of this unique glass-to-metal seal and support, which is convenient to use. A face seal-type O-ring design is used with the proven and popular Parr split ring closure. For this application a special gasket groove was designed to retain the O-ring on the head of the reactor when it is opened. A full range of O-ring materials is available for chemical compatibility with reactants, products and solvents.
Internal Stirrers The standard internal stirrer for these vessels is a turbine type impeller. These impellers have been designed to provide good axial mixing to keep any solid particles up in suspension and to provide good gas distribution through the liquid phase. A gas entrainment impeller is available as an alternate agitator for those users whose primary need is gas re-circulation from the head space of the reactor through the liquid phase. Standard Reactor Fittings The head of each glass reactor is equipped with: Pressure gage, 3-1/2 inch diameter, calibrated 0-200 psi and 0-14 bar Gas release valve Gas inlet valve Liquid sampling valve Internal thermocouple Internal cooling loop standard 300 mL to 1.5 L Internal stirrer with magnetic drive Heads intended for use with glass cylinders are equipped with spring-loaded relief valves adjustable between 50-150 psi. All heads are equipped with a rupture disc rated for 1000 psi. Internal ttings are T316 Stainless Steel with PTFE coating.
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Split Ring for Glass Reactors.
Split Ring for Metal Reactors.
Materials of Construction These reactors are a combination of a glass reaction vessel with a metal head, internal stirrer, dip tube, thermowell, cooling loop, and external valves and ttings, or alternately an all metal system. The standard material of construction for the head is Type 316 Stainless Steel with PTFE coated T316SS internals. As an alternative the head and internal wetted parts can be provided in any of the standard Parr materials of construction. See the 5100 Ordering Guide. Size Series 5100 Reactors can be easily converted between the 160, 300, 450, and 600 mL sizes by simply changing the cylinders and internal parts. In a similar manner, 1 L and 1.5 L are interchangeable. While the 160-600 mL stand cannot be converted to hold 1 and 1.5 L vessels, the larger stand can be converted to accommodate the 160-600 mL vessels. If you plan to convert at a later time, be sure to order the stand for the largest size you plan to use so the shield and supports will not have to be replaced. Heating and Temperature Control These reactors are available with either jacketed or non-jacketed glass cylinders allowing for heating by either a user supplied circulator or with a removable heating mantle respectively. While we would normally expect glass vessels to be equipped with circulating jackets to maintain their transparent feature, some users may not need to heat their reactions or may prefer to use removable heating mantles when they need to work at elevated temperatures. Although transparency is not an issue with metal vessels, users will generally want to select the same heating method for metal vessels as they use for glass vessels so they can utilize the same heating and control system for both. Users who are using a circulating bath that has its own temperature control for use with these reactors will want to order the reactor without a heating mantle and may only need a
motor controller for stirring speed to complete the system. Most laboratory circulators should be adequate for these small vessels. Moveable electric heating mantles are available for vessels that do not have attached circulating jackets. These mantles are for use with 115 or 230 VAC. 4848 Controller The Parr 4848 Controller provides PC communications to all of the functions housed in the controller. The 4848 Controller offers PID Control with auto tune, Ramp and Soak Programming, Separate Heating and Cooling Control Loops, Stirrer Motor Speed Control, Full or Half Power Heater Option, Lockout Relay and Reset for Over Temperature Protection, Expansion Modules for Tachometer, Pressure, and High Temperature Alarm. Users who wish to program their reactor to automatically step through a pre-set temperature prole will want to select the 4848 Controller with this feature. These controllers will control the electric heating mantle but not a user supplied circulator. A2110E Motor Controller For those who supply their own circulator for use with glass jacketed versions of the 5100, Parr offers The A2110E Motor Controller for setting and controlling the speed of the stirrer motor. Stirrer Motors Series 5100 Reactors are provided with a choice of three motors. The standard motor is a 1/8 hp variable speed motor. The standard stirring speed is from 0-1700 rpm. A dual pulley can be inverted to double the torque and halve the speed. An explosion proof motor (1/4 hp) is available. This motor is also variable speed and offers the same stirrer speed ranges as the standard motor. An air motor is available for users who prefer the added safety of motors that are not electrical and have available a variable compressed air source.
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Series 5100 Low Pressure Reactors

5110 Conversion Sets: Glass to Metal or Metal to Glass Series 5100 Reactors can be easily converted between glass and metal cylinders. The conversion sets include the cylinder, closure, gage and safety relief devices for the converted to system. Sets do not include heater.
Series 5100 Pressure Reactor System Specications Shaded bar indicates specications that change within series. Model Number Sizes, mL Maximum Pressure, Glass Maximum Pressure, Metal Maximum Temperature with FKM O-ring Reactor Mounting Closure (Cap Screws) Valve Connections Magnetic Stirrer, Model No. 1 2 2 3.5 inches 0-200 psi (0-14 bar) 0-1000 psi (0-65 bar) Fixed, Type J, Thermocouple Included None Single Loop Mantle 510 510 590 590 780 780 400 400 400 450 550 650 Included 225 C Fixed Head Bench Top Split-Rings (6) 1/8" Male NPT A1120HC9 16 Inch-Pounds 1 2 2 Vessel Style
5101
300
5102
450
5103
600
5104
160
5111
1000
5112
1500
150 psi (10 bar) 1000 psi (69 bar)
Glass Under Pressure

In the seventy years Parr has been offering apparatus incorporating glass vessels and bottles to be used under pressure, we have learned the following important lessons. 1. Reactions at elevated pressures and temperatures can be conducted safely only if the user takes into consideration all of the potential hazards that may occur if the glass vessel should break under pressure. 2. Vessel design is important. Glass vessels must have rounded sections, proper annealing, cushioning supports, and provisions for dealing with differential thermal expansion as well as adequate thicknesses, careful construction, inspection and testing. All of the glass vessels used in these reactors are tested to a minimum of 225 psi (15 bar). 3. Careful maintenance is also critical to safe operation of glass vessels. Scratches on metal vessels which are highly ductile are cosmetic. Scratches on brittle glass vessels create enormous stress risers which can completely destroy the structural integrity of the vessel. Great care must be employed in handling and washing these vessels to maintain the strength designed into them and conrmed by their original hydrostatic testing. 4. Finally, operators must be trained to recognize the potential hazards and ensure that adequate safety provisions are in place and operational at all times.
Maximum Torque Impeller(s), 4-blade Pressure Gage, Size Range, Glass Range, Metal Temperature Measurement Cooling Coil Heater Style Heater Power Glass, Watts Heater Power Metal, Watts
Style
Stirrer Motor Volts, AC Maximum Load, amps, 115 / 230 Inside Diameter, inches Inside Depth, inches Weight of Cylinder, Glass, pounds Weight of Cylinder, Metal, pounds 4.0 0.75 3 6.0 1.1 5
1/8 hp Variable Speed 115 or 230 8.5 / 5.2 2.5 8.0 1.25 7 17 24 30 60 63 5109M 66 60 109 5119M 2.0 0.75 3 4 6.0 3 9 21 26 33 113 4 8.0 5 13
Electrical Supply
Vessel Dimensions
Spare Parts Kit
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The Order No. for the Base System is: 51___-G-SS-4B-115-VS.12-200 A composite identication number to be used when ordering a 5100 Series Reactor can be developed by combining individual symbols from the separate sections below. For more information on how to use this ordering guide, please see page 27.
A Base Model Model No. Size 5101 300 mL 5102 450 mL 5103 600 mL 5104 160 mL (215 mL Glass Jacketed) 5111 1000 mL 5112 1500 mL B Cylinder Type -GJ Glass Jacketed -G Glass -MJ Metal Jacketed -M Metal C Materials of Construction* -SS T316 Stainless Steel -HB Alloy B-2 -HC Alloy C-276 -TI Titanium * Other Alloys Available on Request D Stirrer Options -4B 4-Bladed Stirrer Impeller, 160-600 mL -6B 6-Bladed Stirrer Impeller, 1000 & 1500 mL -GE Gas Entrainment Stirrer Impeller E Electrical Supply -115 115 VAC -230 230 VAC F Motor Option -VS .12 Variable Speed, 1/8 hp -VS .25 Variable Speed, 1/4 hp -XP .25 Explosion Proof Variable Speed, 1/4 hp -AM .25 Air Motor, 1/4 hp G Pressure Gage -200 200 psi / 14 bar -100 100 psi / 7 bar -1000 1000 psi / 70 bar (Metal Vessels Only) H Heater -MH Mantle (Non-Jacketed Vessels Only) -NH No Heater I Controller PID Control, Ramp & Soak Programming, Motor Speed Control, and Data logging with Software Optional RS485 to USB Cable for 4848 Controller Speed Controller No Controller J 4848 -TDM -MCM -PDM -HTM -ETLM -MTM Expansion Modules Tachometer Display Module Tachometer w/Motor Control Module Pressure Display Module High Temperature Cut Off Module External Temperature Limit Module Motor Torque Module
K 4848 Cooling Control: Solenoid Valve Module -SVM1 115 VAC -SVM2 230 VAC L Certication -ASME ASME Certication (Metal Vessels Only) -PED PED Certication (Metal Vessels Only) -CE European Community Standard (for EMC Compliance)
M 5110 & 5120 Conversion Sets Glass to Metal
Catalog Number
5110A 5110B 5110C 5110D 5110E 5110F 5110M 5110N 5120A 5120B 5120C 5120D
Size mL
300 300 450 450 600 600 215 160 1000 1000 1500 1500
Converts From
Glass Jacketed Glass Glass Jacketed Glass Glass Jacketed Glass Glass Jacketed Glass Glass Jacketed Glass Glass Jacketed Glass
Converts To
Metal Jacketed Metal Metal Jacketed Metal Metal Jacketed Metal Metal Jacketed Metal Metal Jacketed Metal Metal Jacketed Metal
Metal to Glass
Catalog Number
5110G 5110H 5110I 5110J 5110K 5110L 5110P 5110Q 5120E 5120F 5120G 5120H
Size mL
300 300 450 450 600 600 215 160 1000 1000 1500 1500
Converts From
Metal Jacketed Metal Metal Jacketed Metal Metal Jacketed Metal Metal Jacketed Metal Metal Jacketed Metal Metal Jacketed Metal
Converts To
Glass Jacketed Glass Glass Jacketed Glass Glass Jacketed Glass Glass Jacketed Glass Glass Jacketed Glass Glass Jacketed Glass
-4848 -A1925E4 -A2110E -NC
N Spare Parts Kit -5109M Spare Parts Kit for Models 5101, 5102, 5103, 5104 -5119M Spare Parts Kit for Models 5111 and 5112
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Series 5500 High Pressure Compact Laboratory Reactors

Series Number:
5500
Type:
High Pressure Compact

Stand:
Bench Top
Vessel Mounting:
Moveable
Sizes, mL:
25-600
Standard Pressure MAWP, psi (bar):
3000 (200)
Maximum Operating Temperature, C: 225 w/ FKM O-ring 275 w/ FFKM O-ring 350 w/ PTFE Flat Gasket Parr Series 5500 HPCL Reactor and a 4848 Reactor Controller shown with optional Expansion Modules.
Familiar Parr Designs ll of the safety, convenience and reliability features which have been the hallmark of Parr pressure reaction equipment for more than 50 years have been incorporated into a new line of high pressure, compact laboratory reactors. (HPCL Reactors.) The Series 5500 HPCL Reactors are based upon our popular micro and mini, Series 4590 & 4560 Reactors. There are several differences between these new reactors and their original counterparts. Primarily, these are: 1. A smaller, more compact magnetic drive is installed. 2. A smaller, more compact variable speed stirrer motor. 3. The larger support stand, overarm and motor have been eliminated. 4. An Aluminum Block Heater also serves as the support stand.
As a result of these changes, we are now able to offer these new reactors to users who do not require the wide variety of options and expandability provided by our Series 4500 Reactors at a signicantly lower cost. These new designs will be welcomed by not only investigators with limited space or budgets, but also by investigators building multiple reactor installations for combinatorial chemistry or high throughput investigations. The reaction vessels used in these new HPCL reactors are identical to the ones furnished in the Series 4590 Micro and Series 4560 Mini Reactors. HPCL Reactors use the popular Parr split ring closure. These vessels are rated for a maximum working pressure of 3000 psi. The maximum operating temperature is de pendent upon the seal selected, PTFE gasket for up to 350 C; with FKM O-ring to 225 C or FFKM O-ring to 275 C.
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Series 5500 Pressure Reactor System Specications Shaded bar indicates specications that change within series. Model Number Sizes, mL Maximum Pressure Maximum Temperature with FKM O-ring with FFKM O-ring with PTFE Flat Gasket 225 C 275 C 350 C Moveable Compact Bench Top Split Ring (6 Cap Screws for Flat Gasket) (0 Cap Screws for Quick Close) 1/8" Male NPT 2.5 (0.28 Nm) 1 (0.81" dia.) 1 (0.81" dia.) 3.5 inches 0-3000 psi (200 bar) Fixed Thermocouple NA Coldnger NA Aluminum Block (External Cooling Optional) 700 1000 700 1/17 hp 115 or 230 8/4 1 2 12 1.3 2.25 12 10 / 5 1.3 4.5 12 8/4 2.5 4 13 8.3 9.5 23 25 23 25 25 25 23 26 5529SPK Other options available. See Ordering Guide, visit www.parrinst.com, or call for more information. 25 28 27 30 23 25 23 25 2.5 6 15 10 / 5 2.5 8 17 2.5 2 12 8/4 2 2 12 1000 700 Standard Single Loop NA NA Spiral 2 (1.38" dia.) 1 (0.81" dia.)
5511
25
5512
50
5513
100
5521
300
5522
450
5523
600
5524
160
5525
100
3000 psi (200 bar)
Vessel Style Reactor Mounting Closure Valve Connections Maximum Torque, Inch-Pounds Impeller(s), 4-blade Pressure Gage, Size Range Temperature Measurement Cooling Coil Optional Cooling Coil
Bottom Drain Valve Heater Style Heater Power, Watts Stirrer Motor, Variable Speed Electrical Supply Volts, AC Maximum Load, amps, 115 / 230 Inside Diameter, inches Inside Depth, inches Weight of Vessel, pounds
Vessel Dimensions
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Series 5500 High Pressure Compact Laboratory Reactors

The 25, 50, and 100 mL reactors are equipped with gas inlet and outlet valves, a liquid sampling valve, pressure gage, safety rupture disc, and internal thermocouple in addition to the internal stirrer. The 300, 450, and 600 mL reactors include an internal cooling loop in addition to these ttings. New Magnetic Drive To take advantage of the new technology available in magnets today, Parr has designed a new compact, magnetically-coupled stirrer drive especially for these smaller vessels. Tests show that this new drive is sufcient to stir reaction mixtures with viscosities up to 10,000 centipoise in a 600 mL reaction vessel. Variable Speed Motor A 1/17 hp variable speed motor provides stirring speeds adjustable from 0 to 1700 rpm. An optional tachometer pickup provides a signal to the optional tach ometer display module which can be installed in the 4848 Controller. Heater / Reactor Support A heater also serves as the vessel support for the HPCL Reactors. This is an aluminum block style heater for excellent thermal uniformity. The cartridge heaters used in this heating block are easily replaced if required. A stainless steel heat shield is provided around the heating block. This style of heater/reactor support provides a very small footprint, ideal for limited bench space. Model 4848 Temperature Controller The Series 4848 Controller used with the standard Parr line of medium and high pressure reactors is also furnished for use with these reactors. The 4848 offers the user options for redundant temperature sensor and alarm, digital pressure readout, stirring speed display or control, motor load, and bi-directional digital communication (RS-485). Alternate Controllers Available A single 4871 Process Controller can control up to eight High Pressure Compact Laboratory Reactors.
High Pressure Compact Reactor Vessel, 100 mL.
Options As shown in the ordering guide, a variety of options are available for these Series 5500 Reactors. In addition to the options described here, there are a number of additional accessories such as glass or PTFE liners, special stirrers, gages, gas and liquid feed systems, custom valves, etc., as described in the options section of this catalog. Please remember that the Series 5500 reactors have been designed and packaged to provide the basic functions of these small laboratory reactors and not all of the options available for the more versatile Series 4500 Reactors can be incorporated into these units. Investigators who need explosion proof operation, jacketed vessels, bottom drain valves, high torque stirrers, catalyst baskets, etc., will need to start with a Series 4590 Micro Reactor or a Series 4560 Mini Reactor.
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The Order No. for the Base System is: 55___-T-SS-115-VS-M-3000-4848 A composite identication number to be used when ordering a 5500 Series Reactor can be developed by combining individual symbols from the separate sections below. For more information on how to use this ordering guide, please see page 27.
A Base Model Model No. Size 5511 25 mL 5512 50 mL 5513 100 mL 5521 300 mL 5522 450 mL 5523 600 mL 5524 160 mL 5525 100 mL Cylinder, I.D. 1.0-inch 1.3-inch 1.3-inch 2.5-inch 2.5-inch 2.5-inch 2.5-inch 2.0-inch H Pressure Gage -3000 3000 psi / 200 bar -2000 2000 psi / 137 bar -1000 1000 psi / 70 bar -600 600 psi / 40 bar -200 200 psi / 14 bar -100 100 psi / 7 bar I Controller PID Control, Ramp & Soak Programming, Motor Speed Control, and Data logging with Software Optional RS485 to USB Cable for 4848 Controller Process Controller
-4848 -A1925E4 -4871
B Gasket / Maximum Temperature -OV O-ring 225 C -OK O-ring 275 C -T PTFE Compression Gasket, 350 C C Materials -SS -MO -IN -HB -HC -CS -TI2 -TI4 -NI -ZR of Construction (MOC) T316 Stainless Steel Alloy 400 Alloy 600 Alloy B-2 Alloy C-276 Alloy 20 Titanium Grade 2 Titanium Grade 4 Nickel 200 Zirconium Grade 702 or 705
J 4848 Expansion Modules -TDM Tachometer Display Module -MCM Tachometer w/Motor Control Module -PDM Pressure Display Module -HTM High Temperature Cut Off Module -ETLM External Temperature Limit Module -MTM Motor Torque Module K 4848 Cooling Control: Solenoid Valve Module -SVM1 115 VAC -SVM2 230 VAC L Custom Options (List All Desired) -GE Gas Entrainment Stirrer -BF Bafes -SCP Solids Charging Port -CAD Catalyst Addition Device (300 mL or larger only) -RC Reux Condenser -RTC Reux Take-off Condenser M Certications No Symbol No Certication -ASME ASME Certication -CE-PED European Community PED -CE European Community Standard (for EMC Compliance)
D Electrical Supply -115 115 VAC -230 230 VAC E Motor -VS
1/17 HP Variable Speed
F Magnetic Stirrer Drive -M General Purpose Magnetic G Mag. Drive Materials of Construction -No Symbol Same Material As Vessel -MOC Symbol Indicate Material of Construction
N Spare Parts Kit -5529SPK Spare Parts Kit for 5500 Series
1 - 8 0 0 - 8 7 2 - 7 7 2 0
P a r r
In s t r u m e n t
C om pany
67
Notes
68
Pa rr
Instrum e n t
Comp a n y

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Chapter 2 Stirred Reactors

Reactor Selection Procedure

Establish 4 Basic Specications

Moveable and Fixed Head Designs

Select Appropriate Series

Reactor Selection Guide

which shows the pressure within the vessel at all times.

Gas Release Valve to release

gas from the reactor during or at the completion of a run.

Specify Detailed Options

How to use the Ordering Guide: T

No. 4568 - OV-SS-GP-115-XP.25-3000-4848

Series 4520 1 & 2 Liter General Purpose Reactor Systems

Moveable or Fixed Head

Standard Pressure MAWP Rating, psi (bar):

High Pressure (HP) MAWP Rating, psi (bar):

Maximum Operating Temperature, C, at High Pressure (HP): 350 @ 2900 psi

Spare Parts Kit

Series 4520 1 & 2 Liter General Purpose Reactor Systems

4526 Moveable Vessel, 2000 mL

Series 4520 Ordering Guide

-4848 -A1925E4 -4871

Series 4530 1 & 2 L General Purpose Reactor Systems

Moveable or Fixed Head

Standard Pressure MAWP Rating, psi (bar):

High Pressure (HP) MAWP Rating, psi (bar):

Maximum Operating Temperature, C, at High Pressure (HP): 350 @ 2900 psi

4534 Reactor, assembled with heater raised.

4534 Reactor, assembled with heater down.

1900 psi (131 bar) 2900 psi (200 bar)

Vessel Style Closure Valve Connections Magnetic Stirrer, Model No.

Spare Parts Kit

Series 4530 1 & 2 L General Purpose Reactor Systems

2000 mL Stirred Moveable Vessel

Series 4530 Ordering Guide

-4848 -A1925E4 -4871

Series 4540 600-1200 mL High Pressure Reactor Systems

Floor Stand or Bench Top

Moveable or Fixed Head

600 and 1200

Standard Maximum Operating Temp., C: 350 w/ PTFE Flat Gasket

5000 psi (345 bar)

Spare Parts Kit

Series 4540 600-1200 mL High Pressure Reactor Systems

1200 mL Fixed Head, and 600 mL Moveable Reaction Vessels.

Series 4540 Ordering Guide

Series 4550 1 & 2 Gallon Reactor Systems

Moveable or Fixed Head

Vessel Sizes, Gallons:

Standard Pressure MAWP Rating, psi (bar):

Series 4550 1 & 2 Gallon Reactor Systems

Series 4550 Ordering Guide

Series 4555 10 & 20 Liter Reactor Systems

Moveable or Fixed Head

Vessel Sizes, Liters:

Standard Pressure MAWP Rating, psi (bar):

Series 4555 10 & 20 Liter Reactor Systems

10 Liter Stirred Vessel removed from heater.

Model 4556 Reactor, 10 Liter Vessel, with head removed.