Is 1489 (Part-2) Portland-Pozzolana Cement Specification (CA
Is 1489 (Part-2) Portland-Pozzolana Cement Specification (CA
Is 1489 (Part-2) Portland-Pozzolana Cement Specification (CA
Titr~ATJr)
Indian Standard
PORTLAND-POZZOLANA CEMENT -
T
SPECIFICATIOh
PART 2 CALCINED CLAY BASED
( Third Revision )
First Reprint MARCH 1993
UDC 621*944+1*046
9 BIS 1991
FOREWORD
This Indian Standard ( Part 2 ) ( Third Revision ) was adopted by the Bureau of Indian Standards
after the draft finalized by the Cement and Concrete Sectional Committee had been approved by the
Civil Engineering Division Council.
Portland-pozzolana cement can be produced either by grinding together Portland cement clinker
and pozzolana with addition of gypsum or calcium sulphate, or by intimately and uniformly blending
Portland cement and fine pozzolana. While grinding of the two materials together presents no difficulty,
the mixing of dry powders uniformly is extremely difficult. The blending method should, therefore, be
resorted to only when the grinding method is impossible or proves uneconomical in a particular case.
Where blending method is adopted, every care should be taken to see that the blending is as intimate
as possible. Generally, if the blending is not uniform, it is reflected in the performance tests. The
Sectional Committee responsible for the preparation of this specification is of the opinion that the
blending method should be confined to factories and such other works where intimate and uniform
blending is feasible with the employment of requisite machinery so as to ensure uniformity of produc-
tion and guaranteed performance.
Portland-pozzolana cement produces less heat of hydration and offers greater resistance to the
attack of aggressive waters than normal Portland cement. Moreover, it reduces the leaching of
calcium hydroxide liberated during the setting and hydration of cement. It is particularly useful in
marine and hydraulic construction and other mass concrete structures. Portland-pozzolana cement can
generally be used wherever 33 grade ordinary Portland cement is usable under normal conditions.
However, it should be appreciated that all pozzolanas need not necessarily contribute to strength at
early ages. In view of this fact, this present specification has been prepared to enable manufacturers to
produce Portland-pozzolana cement equivalent to 33 grade ordinary Portland cement on the basis of
3, 7 and 28-days compressive strength.
For construction of structures using rapid construction methocls like slipform construction, Portland-
pozzolana cemcnl shall bc used with caution since 4 to 6 h strength of concrete is significant in such
construction.
This standard was first published in 1962 and subsequently revised in 1967 and 1976. In this revision
the standard has been split into two parts based on the pozzolana used in the manufacture of such
cements in view of the special needs of some hydraulic structures which require pozzolana cement
manufactured only with fly ash pozzolana and for easy identification of pozzolana used in the manu-
facture of Portland-pozzolana cement in the interest of consumers. Part 1 of this standard covers
pozzolana cement manufactured by using only fly ash pozzolana and Part 2 covers pozzolana cement
manufactured by using either calcined clay or a mixture of calcined clay and fly ash as pozzolana. In
this revision both chemical and physical requirements have been kept the same as was given in 1976
version of this standard as amended from time to time. Various requirements of Portland-pozzolana
cement given in 1976 version of this standard had been modified from time to time by issuing amend-
ments based on the experience gained with the use of the standard and the requirements of the users
and also keeping in view the raw materials and fuel available in the country for manufacture of cement
The important amendments include lowering the value of compressive strength in lime reactivity
test from 5 MPa to 4 MPa, incorporating a value of 3 day compressive strength as 16 MPa, modifying
the requirement of sulphuric anhydride ( SOs ) and insoluble residue, deleting the requirement of
pozzolanicity test, increasing the value of 28 days compressive atrenth from 31 MPa to 33 MPa, making
autoclave soundness test compulsory irrespcctivc of the magnesia content in cement, incorporating
a provision for retest in respect of autoclave soundness test after aeration of the cement, incorporting
a clause on false set of cement and permitting packaging of cement in 25 kg bag\. All thc\c an~encl-
ments have been taken care of in this revision.
Mass of cement packed in bags and the tolerance requirements for the masq of cement packed in bags
shall be in accordance with the relevant provisions of the S/n~&cl CJ~‘B’~@/rts ~/id ,tlk~~.~r~.v ( ~~c~ngcd
C‘ot77777ot/i~i~s ) Rules. 1077 and B-I.2 ( see Annex B ). Any modification in thcsc rules in rcspcct of
tolerance on mass of cement would apply automatically to this standard.
IS I489 ( Part 2 ) : 1991
lndian Standard
PORTLAND-POZZOLANACEMENT-
SPECIFICATION
PART 2 CALCINED CLAY BASED
( Third Revision J
1 SCOPE shall be either Lalcined clay pozzolana confor-
ming to IS 1344 : 1981 or a mixture of calcined
This standard ( Part 2 ) ( Third Revision) clay pozzolana conforming to IS 1344 :1981 and
covers the manufacture, physical and chemical fly ash conforming to 1s 3812 : 1981 subject to
requirements of Portland-pozzolana cement the requirements of 4.1.2 and 4.1.3.
manufactured by using calcined clay pozzolana
or a mixture of calcined clay and fly ash 4.1.2 Fineness and average compressive strength
pozzolana. in lime reactivity of pozzolana that is to be
blended with finished Portland cement to pro.
2 REFERENCES duce Portland-pozzolana cement, when testec!
The Indian Standards listed in Annex A are in accordance with the procedure specified in
necessary adjuncts to this standard. IS 1727 : 1967, shall not be less than 320 ms/kg
and 4-O MPa respectively. Average compressive
3 TERMINOLOGY strength in lime reactivity test of such pozzo-
lana shall be carried out at the fineness at
3.0 For the purpose of this standard, the defi- which pozzolana has been ground for blending.
nitions given in IS 4845 : 1968 and the following
shall apply. 4.1.3 Average compressive strength in lime
reactivity of pozzolana that is to be interground
3.1 Pozzolana with Portland cement clinker for manufacture
An essentially silicious material which while in of Portland-pozzolana cement shall not be less
itself possessing little or no cementitious pro- than 4.0 MPa when tested at the fineness of
perties will, in finely divided form and in the POI tland-pozzolana cement manufactured out
presence of water, react with calcium hydroxide of it or at the fineness in ‘as received’ condition,
whichever is greater, in accordance with proce-
at ambient temperature to form compounds
possessing cementitious properties. The term dure specified in IS 1727 : 1967.
includes natural volcanic material having pozzo- 4.1.4 The purchaser shall have the right, if he
lanic properties as also other natural and so desires to obtain samples of pozzolana used
artificial materials, such as diatomaceous earth, in the manufacture of Portland-pozzolana
calcined clay and fly ash. cement for purposes of checking its conformity
3.2 Portland Clinker to the requirements specified in 4.1.1 to 4.1.3.
I
IS 1489( Part 2 ) : 1991
3
IS 1489 ( Part 2 ) : 1991
shall be equal to or more than the quantity However, the actual temperature during the
in 10.2.2. testing shall be recorded.
10.3 Supplies of cement in bulk may be made 12.3 Consistency of Standard Cement Paste
by arrangement between the purchaser and the
supplier ( manufacturer or stockist ). The quantity of water required to produce a
paste of standard consistency to be used for
NOTE - A single bag Or conta”‘er ‘Ontaining determination of the water content of mortar
1 000 kg or more net mass of cement shall be consi-
dered as bulk supply of cement. Supplies of cement for the compressive strength test and for the
may also be made in intermediate containers, for determination of soundness and setting time,
example, drums of 200 kg, by agreement between the shall be obtained by the method described in
purchaser and the manufacturer.
JS 4031 ( Part 4 ) : 1988.
11 SAMPLING
12.4 Independent Testing
11.1 Samples for Testing and by Whom to be
Taken 12.4.1 If the purchaser or his represen!ative
requires independent tests, the samples shall be
A sample or samples for testing may be taken taken before or immediately after delivery at
by the purchaser or his representative, or by the option of the purchaser or his representa-
any person appointed to superintend the works tive, and the tests shall be carried out in accor-
for the purpose of which the cement is required, dance with this standard on the written instruc-
or by the latter’s representative. tions of the purchaser or his representative.
11.1.1 The samples shall be taken within three 12.4.2 Cost of Testing
weeks of the delivery and all the tests shall be
commenced within one week of sampling. The manufacturer shall supply, free of charge,
the cement required for testing. Unless other-
11.1.2 When it is not possible to test the wise specified in the enquiry and order, the cost
samples within one week, the samples shall be of the tests shall be borne as follows:
packed and stored in air-tight containers till
such time they are tested. a> By the manufacturer if the results show
that the cement does not comply with
11.2 In addition to the requirements of 11.1, this standard. and
the methods and procedure or sampling shall
be in accordance with IS 3535 : 1986. b) By the purchaser if the results show that
the cement complies with this standard.
11.3 Facilities for Sampling and Identifying
The manufacturer or supplier shall afford every 13 REJECTION
facility, including labour and materials for 13.1 Cement may be rejected if it does not
taking and packing the samples for testing the comply with any of the requirements of this
cement and for subsequent identification of the specification.
cement sampled.
13.2 Cement remaining in bulk storage at the
12 TESTS mill, prior to shipment, for more than six
months, or cement in bags in local storage in
12.1 The sample or samples of pozzolana the hands of a vendor for more than 3 months
cement drawn as described in 11 shall be tested after completion of tests, may be retested
as per methods referred to in relevant clauses. before use and may be rejected if it fails to
12.2 The temperature for carrying out physical conform to any of the requriements in this
tests shall, as far as possible, be 27 f. 2°C. specification.
IS 1489( Part 2 ) : 1991
ANNEX A
( Clause 2 )
ANNEX B
( Clause 10.2 )
B-l The average net mass of cement packed in than 5 percent of the bags in the sample and
bags at the plant in a sample shall be equal to the minus error in none of such bags in the
o’r more than 50 kg, The number of bags in sample shall exceed 4 percent of the specified
a sample shall be as given below: net mass of cement in the bag.
Butch Size Sample Size NOTE - The matter given in B-1 and B-l.1 is extra-
cts based on the Standards of Weights and Measures
100 to 150 20 ( Packaged Commodities ) Rules, 1977 to which
reference shall be made for full details. Any modi-
151 ,, 280 32 fication made in these Rules and other related Acts
and Rules would apply automatically.
281 ,, 500 50
501 ,, I 200 80 B-1.2 In case of a wagon/truck load of 20 to 25
tonnes, the overall tolerance on net mass of
I 201 ,, 3 200 125 cement shall be 0 to + O-5 percent.
3 201 and above 200
NOTE -The mass of jute sacking bag conforming to
The bags in a sample shall be selected at ran- 1s 2580 : 1982 to hold 50 kg of cement is 531 g, the
mass of a double hessian bituminized (CR1 type 1
dom ( see IS 4905 : 1968 ). bag to hold 50 kg of cement is 630 g, the mass of a
&ply paper bag to hold 50 kg of cement is approxl-
B-l.1 The number of bags in a sample showing mutely 400 g and the mass of a polyethylene lined
a minus error greater than 2 percent of the ( CR1 type ) jute bag to hold SO kg of cement !P
specified net mass ( 50 kg ) shall be not mole approximately 480 g.
5
IS 1489 ( Part 2 ) : 1991
ANNEX C
( Foreword )
COMPOSITION OF THE TECHNICAL COMMITTEE
Chairman Representing
( Continurd on page 7 )
6
IS 1489 ( Part 2 ) : 1991
Mombars
RQPRmJEwfATIV~ Builders Agociation of India, Bombay
SHIU A. u. RlJ3isIW3~A~I Cement Corporation of India Limited, New Delhi
SHRI C. 5. SHABMA ( AUnncllr)
SERI J. SEX GUPTA National Buildings Organization, New Delhi
Ssar A. K. LAL ( Allwnai~ )
SARI T. N. SUBBA RAO Gammon India Limited, Bombay
SERI S. A. REDDI ( Alternat 1
S~JPERINTENDENTENGINEER ( DEEI~NS ) Public Works Department, Government of Tamil Nadu
EXECWTIVEE~CUNEE~, S. M. R. DIVISION
( Alternate )
SBRI S. B. SURI Central Soil and Materials Research Station, New Delhi
SBRI N. CHANDBASEKARAN ( Ahrnatr )
DR H. C. VISVEBVARAYA The Institution of Engineers ( India ), Calcutta
SARI D. C. CHA~TURVE~I ( Ahsrnate )
Sam G. R AXAN, Director General, BIS ( Ex-o&o Msmbsr )
Director ( Civ Engg )
Sscvtar~
SHRI N. C. BANDYOPADHYAY
Joint Director ( Civ Engg ), BIS
( Confinud on pngs 8 )
IS 1489 ( Part 2 ) : 1991
This standard contains clauses 4.1.4, 4.2 and 12.4.1 which permit the purchaser to use his option
and clauses 10.2.1 and 10.3 call for agreement between the purchaser and the manufacturer.
The composition of the technical committee responsible for the formulation of this standard is given
in Annex C.
For the purpose of deciding whether a particular requirement of this standard is complied with, the
final value, observed or calculated, expressing the result of a test, shall be rounded off in accor-
dance with IS 2 : 1960 ‘Rules for rounding off numerical values ( revised )‘. The number of significant
places retained in the rounded off value should be the same as that of the specified value in this
standard. .
The use of the Standard Mark is governed by the provisions of the Bureau of Indian Standards
Act, 1986 and the Rules and Regulations made thereunder. The Standard Mark on products
covered by an Indian Standard conveys the assurance that they have been produced to comply
with the requirements of that standard under a well defined system of inspection, testing and
quality control which is devised and supervised by BIS and operated by the producer. Standard
marked products are also continuously checked by BIS for conformity to that standard as a
further safeguard. Details of conditions under which a licence for the use of the Standard Mark
may he granted to manufacturers or producers may be obtaiued from the Bureau of
Indian Standards.
Bureau of Indian Standards
BIS is a statutory institution established under the Bureau of Indian Standards Act, 7986 to promote
harmonious development of the activities of standardization, marking and quality certification of
goods and attending to connected matters in the country.
Copyright
BIS has the copyright of all its publications. No part of these publications may be reproduced in
any form without the prior permission in writing of BIS. This does not preclude the free use, in the
course of implementing the standard, of necessary details, such as symbols and sizes, type or grade
aesignations. Enquiries relating to copyright be addressed to the Director (Publications), BIS.
Indian Standards are reviewed periodically and revised, when necessary and amendments, if any, are
issued from time to time. Users of Indian Standards should ascertain that they are in possession of
the latest amendments or edition. Comments on this Indian Standard may be sent to BIS giving the
following reference:
Headquarters :
Manak Bhavan, 9 Bahadur Shah Zafar Marg, New Delhi 110002
Telephones : 331 01 31,331 13 75 Telegrams : Manaksanstha
( Common to all Offices )
( Third Revision )
(CED2)
Printed at t%meo Printing Press Delhi, India
AMENDMENT NO.2 JUNE 1993
TO
IS 1489 ( Part 2 ) : 1991 PORTLAND-POZZOLANA
CEMENT-SPECIFICATION
PART2 CALCINED CLAY BASED
( Third Revision)
(CED2)
Reprography Unit, BIS, New Delhi, India
AMENDMENT NO. 3 MAY 2000
TO
IS 1489 ( Part 2 ) : 1991 PORTLAND-POZZOLANA
CEMENT - SPECIFICATION
PART 2 CALCINED CLAY BASED
(Third Revision)
Substitute ‘net mass’ for ‘nominal average net mass’ and ‘average net mass’
wherever these appear in the stmdard.
(CED2)
ReprographyUnit, BIS, New Delhi, India