BULLETIN 3050-TE

2001, by AMETEK, Inc. All rights reserved.

#3050-TE(05/04/01)
One of a family of innovative process analyzer solutions fromAMETEK Process Instruments.
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PRELIMINARY LITERATURE
PRELIMINARY LITERATURE
Model 3050-TE for Cryo-Recovery Plants
A TOTAL SOLUTION
PROVIDES ASSURANCE
At AMETEK Process Instruments, we know how difficult it is
to perform part per billion moisture (PPBv) analysis. After all,
we manufacture analyzers that are accurate, sensitive, and
responsive at a single PPBv moisture. With this knowledge
and ability, we have adapted our PPBv Quartz Crystal
Microbalance technology into a Zone 1 / Division 1 industrial
package suited for natural gas processing.
The Model 3050-TE solution is specifically designed to
monitor the PPBv moisture content of the natural gas feeding
turbo-expanders and other cryogenic processes. The Model
3050-TE measures moisture concentration directly, in PPBv
because at these concentrations and process pressures, it is
physically impossible to have or to calculate a moisture dew
point. (How is it possible to have a moisture dew point not
only far below the freezing point of water but also below the
temperature at which the natural gas will liquefy? Because of
this physical reality, the only meaningful term is the true
moisture concentration.)
When attempting PPBv moisture analysis, proper
selection of sample wetted components and their use is ultra
critical. If you use the wrong sample tubing, or if it is too long,
or if it is not properly heat traced, the minute changes in
process moisture concentration will never reach the analyzer
for measurement.
To ensure a successful and easy installation, the 3050-TE
is an integrated solution package for your turbo-expander
process. It includes all of the sample-handling components
from the sample tap to the analyzer. We provide this total
package because we know what to do, and more importantly
what not to do, in order to achieve high-performance, PPBv
moisture analysis.
While proper selection and use of sample handling
components is crucial for PPBv analysis, it is useless if the
analyzer they connect with cannot provide the sensitivity,
accuracy, and speed of response necessary for this
application. This is why 3050-TE is based upon Quartz
Crystal Microbalance (QCM) technology.
Quartz Crystal Microbalance Technology Quartz Crystal Microbalance Technology Quartz Crystal Microbalance Technology Quartz Crystal Microbalance Technology Quartz Crystal Microbalance Technology: Accurate. Reliable. Verifiable. Responsive. : Accurate. Reliable. Verifiable. Responsive. : Accurate. Reliable. Verifiable. Responsive. : Accurate. Reliable. Verifiable. Responsive. : Accurate. Reliable. Verifiable. Responsive.
INCREASE RECOVERY EFFICIENCY AND MINIMIZE DOWNTIME THROUGH BETTER INCREASE RECOVERY EFFICIENCY AND MINIMIZE DOWNTIME THROUGH BETTER INCREASE RECOVERY EFFICIENCY AND MINIMIZE DOWNTIME THROUGH BETTER INCREASE RECOVERY EFFICIENCY AND MINIMIZE DOWNTIME THROUGH BETTER INCREASE RECOVERY EFFICIENCY AND MINIMIZE DOWNTIME THROUGH BETTER
DRYER OUTLET MONITORING DRYER OUTLET MONITORING DRYER OUTLET MONITORING DRYER OUTLET MONITORING DRYER OUTLET MONITORING
A TOTAL SOLUTION FOR INDUSTRIAL PPBv MOISTURE ANALYSIS A TOTAL SOLUTION FOR INDUSTRIAL PPBv MOISTURE ANALYSIS A TOTAL SOLUTION FOR INDUSTRIAL PPBv MOISTURE ANALYSIS A TOTAL SOLUTION FOR INDUSTRIAL PPBv MOISTURE ANALYSIS A TOTAL SOLUTION FOR INDUSTRIAL PPBv MOISTURE ANALYSIS
QUARTZ CRYSTAL
MICROBALANCE - THE SAFEST
CHOICE
DRAMATICALLY BETTER ACCURACY
Consider the basic accuracy specification of the 3050-TE:
10ppb or 10% of reading (whichever is greater), from 20 to
10,000 ppb by volume. In the table on the right, weve
compared this to the accuracy of a humidity analyzer that is
typically listed as dew point. The typical specification is 3C
dew point for gases drier than -65C dew point. The data for
THE QUARTZ CRYSTAL
SENSOR
The heart of the 3050-TE analyzer is a quartz-crystal
microbalance (QCM) sensor and sampling system developed by
AMETEK specifically for
highly accurate moisture
measurements. The
sensor consists of a pair
of electrodes that
support the QCM sensor.
When voltage is applied
to the sensor, a very
stable oscillation occurs.
The faces of the
oscillator are covered
with a hygroscopic
polymer. As the amount
of moisture sorbed onto
the polymer varies, the mass of the QCM changes, producing a
corresponding change in the frequency of oscillation. This
change is directly related to the moisture concentration of the
surrounding gas.
PRELIMINARY LITERATURE PRELIMINARY LITERATURE
NON-EQUILIBRIUM OPERATING THEORY OF QCM
The analyzer systematically cycles between the actual process gas and a dried reference gas. During the process gas cycle
(above left), moisture molecules accumulate on the surface of the QCM sensor. During the reference gas cycle (above right),
these water molecules are swept off the surface of the sensor by the dry gas flow. Since there is no waiting for equilibrium, the
system proides a measurement of moisture concentration every cycle.
The number of water molecules that accumulate on the surface of the sensor is a function of the difference in moisture
between the process gas and reference gas. The analyzer compares the process gas with the known, dry reference as opposed
to trying to measure an absolute value that only occurs once equilibrium has been achieved. When a high moisture event
occurs, the 3050-TE responds quickly to alert you to the problem. After the high moisture event passes, the non-equilibrium
nature of the 3050-TE means that no long dry down period is ever needed before you will get accurate low ppbv measurements.
the aluminum oxide analyzer is based upon the specifications
of a newly calibrated probe. The aluminum oxides calibration
drift, temperature instability and other sources of error are not
typically taken into account by the probe manufacturers
accuracy specification. The aluminum oxides slow speed of
response is another issue.
LONG TERM STABILITY
REDUCES MAINTENANCE COSTS
The 3050-TE analyzer is inherently more stable due to its
quartz crystal microbalance technology. The stability of the
vibrating quartz crystal means that you never need to send the
analyzer out for re-calibration. This means that you will
forever eliminate those costly, routine maintenance projects
that are associated with aluminum oxide humidity sensors.
But dont take our word about the analyzers stability; ask the
analyzer itself! Every 3050-TE comes equipped with an
internal, verification system that consists of both zero and
span challenges, which are created from
the actual sample gas.
BUILT-IN VERIFICATION CAPABILITY
With the built-in zero module and the
internal moisture generator, the 3050-TE
gives you data you can have confidence
in. On a programmed schedule, or
whenever you feel its necessary, you can
route your process gas through the 3050-
TEs internal zero gas generator and its
internal moisture generator, giving you a
zero reference and a span calibration
standard based upon the actual process gas. The 3050-TE
automatically zeroes itself and compares its moisture
measurement with the NIST-traceable known value of the
internal moisture generator. If necessary, the analyzer can
make small corrections to its calibration automatically. If a
Actual PPBv
Moisture
3050-TE
Accuracy
Aluminum Oxide
(1)
Accuracy
50 10 PPBv +38 PPBv / -22.2 PPBv
100 10% of reading +71.8%/-42.9% of reading
500 10% of reading +62.7%/-39.5% of reading
1,000 10% of reading +59.6%/-38.2% of reading
10,000 10% of reading +30.9%/-24.0% of reading
(1)
Based upon accuracy of 3 degrees C below 65C dew point. Dew Point
conversions referenced to 14.7 psia.
System Components: 3050-TE analyzer, Heated sample probe
(pipe thread or flange), 3 meters of special, heat-traced sample
line
Technology: Quartz Crystal Microbalance
Range: Calibrated from 0.01 to 100 parts per million by
volume (ppmv)
Accuracy: +10 ppbv or +10% of the reading, whichever is
greater, from 10-10,000 ppbv
Reproducibility: +5 ppbv or +5% of the reading, whichever is
greater
Limits of Detection: 0.01 ppmv (10 ppbv)
Moisture Generator: 1000 ppbv nominal; calibration is NIST-
traceable
QCM Response Time: 80% of a step change in either
direction in less than 10 minutes
Sensitivity: 5 ppb or 1% of reading, whichever is greater
Allowable Inlet Pressure: 7 to 200 Barg (100 to 3000 psig)
(with pressure-reducing sample probe providing 3.45 Barg (50
psig) maximum pressure to the analyzer))
Exhaust Pressure: 0 to 1 Barg (0 to 15 psig)
Sample Gas Temperature: 0 to 100
O
C (32 to 212
O
F);
analyzer performance is immune to changes in sample gas
temperature
Gas Flow Requirements: Approximately 1.0 slpm
Outputs: Isolated 4 to 20 mA analog signal, keyboard
selectable; 12 bit (0.025%) resolution, RS-232 and RS-485
serial communication ports
Alarms: Two contact closures; system and data invalid alarm
Ambient Temperature Limits:
- 40 to +60
O
C (-40 to 140
O
F)
Voltage / Power requirements:
115 +10% VAC, 50/60 Hz, 400W max
230 +10% VAC, 50/60 Hz, 400W max
Approvals and Certifications:
UL/CSA/CE Class I, Division 1, Groups B,C,D, T6
CENELEC Zone 1 IIC T6
PERFORMANCE SPECIFICATIONS*
Reference Gas
severe calibration problem exists, the analyzer will provide an
alarm. With the 3050-TE, you will always be confident that the
analyzer is responsive to the moisture present in the sample
gas.
GAIN PEACE OF MIND THROUGH ACTIVE FEEDBACK
The Model 3050-TE is an active device. It is constantly
monitoring itself for its frequency of oscillation, sample flow,
sample pressure, operating temperature, ambient
temperature, and other telling parameters. In addition, the
QCM sensor is continually challenged with increasing and
decreasing moisture levels due to the non-equilibrium nature
of its operation. Through this continuous system of active
feedback, the 3050-TE keeps you confident in its
performance. Remember if at any time you doubt the
analyzers readings you can use the built-in verification
function.
The 3050-TE is simply the best analyzer available for
your cryogenic turbo-expander process. Make the decision to
protect your process, your revenue, and your peace of mind
today.
*Specifications are preliminary and subject to change.