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    Experiment 1 - ATQ

    Uploaded by

    Andrea Nicole Rocafort
    The document summarizes the solubility results of various organic compounds in different solvent systems. It discusses the intermolecular forces involved when compounds dissolve in solvents such as hydrogen bonding, dipole-dipole interactions, and London dispersion forces. Specific examples provided are acetone and ethanol dissolving in water and diethyl ether. It also gives balanced chemical equations to show reaction of solvents like NaOH and H2SO4 with soluble compounds like benzoic acid, phenol, aniline, benzyl alcohol, and benzaldehyde. Finally, it asks to determine the best solvent to differentiate pairs of compounds based on their solubility behavior.

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    Experiment 1 - ATQ

    Uploaded by

    Andrea Nicole Rocafort
    250 views2 pages
    The document summarizes the solubility results of various organic compounds in different solvent systems. It discusses the intermolecular forces involved when compounds dissolve in solvents such as hydrogen bonding, dipole-dipole interactions, and London dispersion forces. Specific examples provided are acetone and ethanol dissolving in water and diethyl ether. It also gives balanced chemical equations to show reaction of solvents like NaOH and H2SO4 with soluble compounds like benzoic acid, phenol, aniline, benzyl alcohol, and benzaldehyde. Finally, it asks to determine the best solvent to differentiate pairs of compounds based on their solubility behavior.

    Original Description:

    Chem 31.1

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    The document summarizes the solubility results of various organic compounds in different solvent systems. It discusses the intermolecular forces involved when compounds dissolve in solvents such as hydrogen bonding, dipole-dipole interactions, and London dispersion forces. Specific examples provided are acetone and ethanol dissolving in water and diethyl ether. It also gives balanced chemical equations to show reaction of solvents like NaOH and H2SO4 with soluble compounds like benzoic acid, phenol, aniline, benzyl alcohol, and benzaldehyde. Finally, it asks to determine the best solvent to differentiate pairs of compounds based on their solubility behavior.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    250 views2 pages

    Experiment 1 - ATQ

    Uploaded by

    Andrea Nicole Rocafort
    The document summarizes the solubility results of various organic compounds in different solvent systems. It discusses the intermolecular forces involved when compounds dissolve in solvents such as hydrogen bonding, dipole-dipole interactions, and London dispersion forces. Specific examples provided are acetone and ethanol dissolving in water and diethyl ether. It also gives balanced chemical equations to show reaction of solvents like NaOH and H2SO4 with soluble compounds like benzoic acid, phenol, aniline, benzyl alcohol, and benzaldehyde. Finally, it asks to determine the best solvent to differentiate pairs of compounds based on their solubility behavior.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    of 2

    ROCAFORT, Andrea Nicole Z.

    2013-14862
    Experiment 1
    Solubility of Organic Compounds
    Results:
    TEST COMPOUND
    A
    B
    C
    D
    E
    F
    G
    H
    I
    J
    K
    L

    CHEMICAL NAME
    Benzoic acid
    Tert-butyl
    chloride/Toluene/Hexane
    Tert-butyl
    chloride/Toluene/Hexane
    Benzyl alcohol
    Benzaldehyde
    Acetone/Ethanol
    Phenol
    Aniline
    Tert-butyl
    chloride/Toluene/Hexane
    Sucrose
    Benzamide
    Acetone/Ethanol

    1. For solutes that are dissolved because of intermolecular attractions with the solvent,
    state the intermolecular forces of attraction involved.
    Sucrose- It is considered polar because of the hydrogen bonding between the
    OH group and water.
    Ethanol- It is soluble in water due to the OH group which allows hydrogen
    bonding but insoluble to diethyl ether because of the London dispersion forces
    present.
    Acetone- The carboxyl group is partially positive, allowing interactions to occur.
    Summary:
    Acetone + water: H-bonding, dipole-dipole, London dispersion forces
    Acetone + diethyl ether: London dispersion forces
    Ethanol + water: H-bonding, dipole-dipole, London dispersion forces
    Ethanol + diethyl ether: dipole-dipole, London dispersion forces
    Sucrose + water: dipole-dipole, London dispersion forces, H-bonding

    2.) For solutes that are dissolved because of reaction with the solvent, write the
    balanced equation involved:
    Benzoic acid + NaOH:
    C6H5COOH(s) + OH-(aq) -> C6H5COO-(aq) + H2O(l)
    Benzoic acid + NaHCO3:
    C6H5COOH(s) + HCO3(aq) -> C6H5COO-(aq) + H2O(l) + CO2(g)
    Phenol + NaOH:
    C6H5OH(aq) + OH-(aq) -> C6H5O-(aq) + H2O(l)
    Aniline + HCl:
    C6H5NH2(aq) + H+(aq) -> C6H5NH3+(aq)
    Benzyl Alcohol + H2SO4
    C6H5CH2OH(aq) + 2H2SO4(aq) -> C6H5COSO3H(s) + HSO4-(aq) + H3O+(aq)
    Benzaldehyde + H2SO4
    C6H5COH(aq) + 2H2SO4(aq) -> C6H5COSO3(s) + HSO4-(aq) + H3O+(aq)
    3. On the basis of solubility behavior, determine the best solvent to differentiate the
    following pairs of compounds:
    a. CH3COOH and CH3(CH2)5COOHNaHCO3
    b. CH3CH2OCH2CH3 and CH3CH2OH Dimethyl sulfoxide or water
    c. toluene and benzaldehyde - H2SO4
    d. tert-butyl chloride and tert-butanol - Water

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