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    Tugas II Fenomena Transport Lanjut

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    زينل الغزالي
    1) This document describes an experiment to determine the rate-controlling step of the reduction of NiO. Rate data was collected at various time points and fitted to kinetic models for reaction control, diffusion control, and combined control. 2) By determining the rate constants from the linear fits, diffusion through the product layer was found to have the best fit rate equation, indicating it is the rate-controlling step. 3) The regression value of 1 for the diffusion model line confirms that diffusion through the product layer controls the overall reaction rate.

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    Tugas II Fenomena Transport Lanjut

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    زينل الغزالي
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    1) This document describes an experiment to determine the rate-controlling step of the reduction of NiO. Rate data was collected at various time points and fitted to kinetic models for reaction control, diffusion control, and combined control. 2) By determining the rate constants from the linear fits, diffusion through the product layer was found to have the best fit rate equation, indicating it is the rate-controlling step. 3) The regression value of 1 for the diffusion model line confirms that diffusion through the product layer controls the overall reaction rate.

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    1) This document describes an experiment to determine the rate-controlling step of the reduction of NiO. Rate data was collected at various time points and fitted to kinetic models for reaction control, diffusion control, and combined control. 2) By determining the rate constants from the linear fits, diffusion through the product layer was found to have the best fit rate equation, indicating it is the rate-controlling step. 3) The regression value of 1 for the diffusion model line confirms that diffusion through the product layer controls the overall reaction rate.

    Copyright:

    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    31 views3 pages

    Tugas II Fenomena Transport Lanjut

    Uploaded by

    زينل الغزالي
    1) This document describes an experiment to determine the rate-controlling step of the reduction of NiO. Rate data was collected at various time points and fitted to kinetic models for reaction control, diffusion control, and combined control. 2) By determining the rate constants from the linear fits, diffusion through the product layer was found to have the best fit rate equation, indicating it is the rate-controlling step. 3) The regression value of 1 for the diffusion model line confirms that diffusion through the product layer controls the overall reaction rate.

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    © All Rights Reserved
    Download as DOCX, PDF, TXT or read online from Scribd
    Download as docx, pdf, or txt
    of 3

    TUGAS II FENOMENA TRANSPORT LANJUT

    Diketahui :
    8,134 673 C AB
    T : 673 K PH O =
    2
    V solid
    8,134 673 0,003271
    rp : 0,5 cm = 0,06542
    B : 0,1 gmol/cm3 = 279,7661

    [NiO] : 0,05 gmol/cm3


    V solid : 0,06542 cm3
    C NiO : 0,003271 gmol
    b :1
    PH : 1 2

    Kendali Reaksi
    Kendali Difusi Gabungan
    kimia

    1/3 k rp
    t X 1-(1-X) + 1-3(1-X)2/3 + 2(1-X)]
    1 /3 6 De
    1(1X ) 2/3
    1-3(1-X) + 2(1-X)
    kX
    + 3 km

    0 0 0 0 0
    3 0,1 0,03451062 0,003490745 0,038003546
    41,8 0,35 0,13376089 0,048889437 0,182657981
    81,4 0,47 0,19073277 0,095259635 0,286002673
    159 0,62 0,27568436 0,186100542 0,461798448
    332 0,81 0,42511029 0,388505471 0,813633466
    Kendali laju reaksi
    0.9
    Reaksi Kimia Linear (Reaksi Kimia) Linear (Reaksi Kimia)
    0.8
    f(x) = 0x + 0.07
    0.7 R = 0.99
    0.6

    0.5
    Difusi lapisan produk Linear (Difusi lapisan produk) Kendali gabungan
    Y 0.4 f(x) = 0x + 0.07
    f(x)==0.96
    R 0x - 0
    0.3 R = 1
    0.2

    0.1
    Linear (Kendali gabungan)
    0
    0 50 100 150 200 250 300 350

    waktu (detk)

    Menentukan nilai k dengan menggunakan pers. garis dari laju reaksi yang dikendalikan oleh
    reaksi kimia
    y = 0,0011x + 0,0745
    R = 0,9584
    0,0011 B r p
    k = =0,084072149
    b C AB

    Menentukan nilai De dengan menggunakan pers. garis dari laju reaksi yang dikendalikan oleh
    Difusi melalui lapisan produk
    y = 0,0012x - 1E-05
    R = 1

    0,0023 B r p
    De= = 0,007642923
    6 bC AB

    Menentukan nilai k m untuk kendali gabungan dengan menggunakan perbandingan pH2O dan
    pH2
    PH O
    km =
    2
    =279,7661
    PH 2
    No Pengendali reaksi Persamaan garis Regresi

    1 Reaksi kimia y = 0,0011x + 0,0745 R = 0,9584

    2 Difusi melalui lapisan Produk y = 0,0012x - 1E-05 R = 1

    3 Kendali gabungan y = 0,0022x + 0,0745 R = 0,9889

    Berdasarkan hasil yang diperoleh, laju reaksi proses reduksi NiO dikendalikan oleh difusi
    melalui lapisan produk. Hal ini ditunjukkan pada kurva kendali laju reaksi bahwa regresi pada
    persamaan garis difusi melalui lapisan produk adalah 1.

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