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12 Practical Notes

This document describes an experiment to detect acid and basic radicals in a given salt through a series of chemical tests. The experiment involves treating the salt with reagents like dilute and concentrated sulfuric acid, nitric acid, hydrochloric acid, ammonium chloride, and ammonium hydroxide to observe any reactions like gas evolution or precipitate formation. Based on the observations, inferences are made about which acid or basic radicals may be present in the original salt sample.

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1K views2 pages

12 Practical Notes

This document describes an experiment to detect acid and basic radicals in a given salt through a series of chemical tests. The experiment involves treating the salt with reagents like dilute and concentrated sulfuric acid, nitric acid, hydrochloric acid, ammonium chloride, and ammonium hydroxide to observe any reactions like gas evolution or precipitate formation. Based on the observations, inferences are made about which acid or basic radicals may be present in the original salt sample.

Uploaded by

krish
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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EXPERIMENT NO - 2

❖ AIM : To detect one acid and basic radicals from the given salt .
❖ APPARATUS REQUIRED :
i) Test tube
ii) Test tube holder
iii) burner
iv) Pt - wire
v) Beaker
vi) Glass rod
vii) Dropper
❖ MATERIALS REQUIRED :
Given salt and required reagents .
❖ PHYSICAL SATE :
i) Odour : No specific odour.
ii) Colour : White crystalline solid .
iii) Solubility : Soluble in water .
❖ DRY TEST :
Experiment Observation Inference
01. Dry heating test Write your observation ............
02. Flame test Write you observation ............

❖ TEST FOR ACIDIC RADICALS :


Experiment Observation Inference
1. Salt + dil. H2SO4 No gas evolved CO32-, S2- , NO2- , SO32- may be
absent.
2. Salt + conc. H2SO4 Colourless, pungent smelling gas
giving dense white fumes when a Cl- may be present .
rod dipped in NH4OH is brought
near the mouth of the test tube
3. Salt solution + conc. HNO3 + A white precipitate is formed
AgNO3 solution which is soluble in ammonium Cl- confirmed
hydroxide solution .

❖ TEST FOR BASIC RADICALS :

Experiment Observation Inference


1. Salt solution + dil. HCl No ppt. formed Group - I absent
2. Salt solution + dil. HCl + H2S No ppt. formed Group - II absent
gas
3. To the salt solution added a
pinch of solid NH4Cl. Boiled the No ppt. formed Group - III absent
solution, cooled it and added
excess of NH4OH solution .
4. Through a part of this solution, No ppt. formed Group IV absent
passed H2S gas .
5. salt solution + NH4Cl + NH4OH White ppt. formed Group V present
+ (NH4)2CO3 ( Ca2+ , Ba2+ , Sr2+ may be present )
❖ CONFIMATORY TEST FOR BASIC RADICALS :
Write only confirmatory test for the particular basic radical present .

❖ RESULT :
1. Acid radicals :
2. Basic radical :

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