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    Instrumental Methods For Chemical Analysis

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    Gerges Samir
    This document outlines the course code, objectives, outcomes and units of study for an instrumental methods for chemical analysis course. The course aims to help students understand advanced instrumentation for chemical analysis and be able to choose the appropriate instrument for different analyses. The course covers topics like absorption and emission spectroscopy, UV-visible spectrometry, flame emission and atomic absorption spectroscopy, infrared spectrometry, mass spectrometry, gas and liquid chromatography, and X-ray diffraction.

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    Instrumental Methods For Chemical Analysis

    Uploaded by

    Gerges Samir
    12K views3 pages
    This document outlines the course code, objectives, outcomes and units of study for an instrumental methods for chemical analysis course. The course aims to help students understand advanced instrumentation for chemical analysis and be able to choose the appropriate instrument for different analyses. The course covers topics like absorption and emission spectroscopy, UV-visible spectrometry, flame emission and atomic absorption spectroscopy, infrared spectrometry, mass spectrometry, gas and liquid chromatography, and X-ray diffraction.

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    Chemical analysis

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    Instrumental Methods for Chemical Analysis

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    This document outlines the course code, objectives, outcomes and units of study for an instrumental methods for chemical analysis course. The course aims to help students understand advanced instrumentation for chemical analysis and be able to choose the appropriate instrument for different analyses. The course covers topics like absorption and emission spectroscopy, UV-visible spectrometry, flame emission and atomic absorption spectroscopy, infrared spectrometry, mass spectrometry, gas and liquid chromatography, and X-ray diffraction.

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    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    12K views3 pages

    Instrumental Methods For Chemical Analysis

    Uploaded by

    Gerges Samir
    This document outlines the course code, objectives, outcomes and units of study for an instrumental methods for chemical analysis course. The course aims to help students understand advanced instrumentation for chemical analysis and be able to choose the appropriate instrument for different analyses. The course covers topics like absorption and emission spectroscopy, UV-visible spectrometry, flame emission and atomic absorption spectroscopy, infrared spectrometry, mass spectrometry, gas and liquid chromatography, and X-ray diffraction.

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    of 3

    176

    INSTRUMENTAL METHODS FOR


    CHEMICAL ANALYSIS

    Course Code: 13CH1145 L T P C


    4 0 0 3

    Course Educational Objectives:


    To make the student understand the advanced instrumentation available
    for chemical analysis.
    Course Outcomes:
    After studying this course the student would be able to choose the
    instrument needed for analysis.
    UNIT-I (12 Lectures)
    AN INTRODUCTION TO INSTRUMENTAL METHODS:
    Terms Associated With Chemical Analysis, Classification Of Instrumental
    Techniques, A Review Of The Important Considerations In Analytical
    Methods, Basic Functions of Instrumentation, Important Considerations
    in Evaluating an Instrumental Method.
    MEASUREMENTS, SIGNALS AND DATA:
    Introduction, Signal-to-Noise Ratio, Sensitivity and Detection Methods,
    Source of Noise, Hardware Techniques for Signal-to-Noise Enhancement,
    Software Techniques for Signal-to-Noise Enhancement, Evaluation of
    Results, Accuracy and Instrument Calibration, Chemometrics.
    UNIT-II (12 Lectures)
    AN INTRODUCTION TO ABSORPTION AND EMISSION
    SPECTROSCOPY:
    The Nature of Electromagnetic Radiation, The Electromagnetic Spectrum,
    Atomic Energy Levels, Molecular Electronic Energy Levels, Vibrational
    Energy Levels, Raman Effect, Lasers, Nuclear Spin Behaviour, Electron
    Spin Behaviour.
    G V P College of Engineering (Autonomous) 2013
    177

    ULTRAVIOLET AND VISIBLE SPECTROMETRY-INSTRUMENTATION:


    Radiation Sources, Wave Length Selection, Cells and Sampling Devices,
    Detectors, Instruments for Absorption Photometry.
    ULTRAVIOLET AND VISIBLE ABSORPTION METHODS:
    Fundamental Laws of Photometry, Spectrophotometric Accuracy,
    Photometric Precision, Quantitative Methodology, Differential or
    Expanded-Scale Spectroscopy.
    UNIT-III (12 Lectures)
    FLAME EMISSION AND ATOMIC ABSORPTION SPECTROSCOPY:
    Introduction, Instrumentation for Flame Spectrometric Methods, Flame
    Emission Spectrometry, Atomic Absorption Spectrometry, Interference
    Associated with Flame and Furnaces, Applications, Comparison of FES
    and AAS.
    INFRARED SPECTROMETRY:
    Correlation of Infrared Spectra with Molecular Structure, Instrumentation,
    Sample Handling.
    UNIT-IV (12 Lectures)
    MASS SPECTROMETRY:
    Sample Flow in a Mass Spectrometer, Inlet Sample System, Ionization
    Methods in Mass Spectrometry, Mass Analyzers, Ion-Collection System,
    Vacuum System, Isotope- Ratio Spectrometry, Correlation of Mass Spectra
    With Molecular Structure.
    GAS CHROMATOGRAPHY:
    Gas Chromatographs, Derivative Formation, Gas Chromatographic
    Columns, Liquid Phases and Column Selection, Detectors for Gas
    Chromatography.
    HIGH PERFORMANCE LIQUID CHROMATOGRAPHY:
    HPLC Instrumentation, Mobile-Phase Delivery System, Sample
    Introduction, Separation Columns, Detectors.
    X RAY DIFFRACTION:
    General Principles, Braggs equation, Laue photographic method, Rotating

    G V P College of Engineering (Autonomous) 2013


    178

    crystal method, Oscillating crystal method, Powder method, Interpretation


    of the Diffraction pattern, Applications of XRD.
    UNIT-V (12 Lectures)
    CHROMATOGRAPHY: GENERAL PRINCIPLES:
    Classification of Chromatographic Methods, Chromatographic Behaviour
    of Solutes, Column Efficiency and Resolution, Column Processes and
    Band Broadening, Time of Analysis and Resolution, Quantitative
    Determinations.
    TEXT BOOK:
    Willard,H.H, Merritt,L.L, Dean,J.A, and Settle, F.A, “Instrumental
    methods of analysis” CBS Publishers & Distributors, 7 Ed, 1986.
    REFERENCES:
    1. Srivastava. A.K. and. Jain, P.C, “Instrumental Approach to
    Chemical Analysis”, 4th Edition , S Chand and Company
    Ltd, New Delhi, 2012.
    2. Chatwal. G. R., Anand, Sham K., “Instrumental Methods of
    Chemical Analysis” 5th Edition, Himalaya Publishing House,
    2005.

    pqr

    G V P College of Engineering (Autonomous) 2013

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