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Post Lab Expt 11 15

This experiment involves the preparation and properties of alkynes and acetylides. Calcium carbide reacts with water to produce acetylene gas. Terminal alkynes undergo reactions to form acetylides, such as reacting with cuprous chloride to form a blue-colored compound or reacting with silver nitrate to form a yellow or white precipitate. The volume of acetylene gas produced from a given amount of calcium carbide is calculated.

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82 views

Post Lab Expt 11 15

This experiment involves the preparation and properties of alkynes and acetylides. Calcium carbide reacts with water to produce acetylene gas. Terminal alkynes undergo reactions to form acetylides, such as reacting with cuprous chloride to form a blue-colored compound or reacting with silver nitrate to form a yellow or white precipitate. The volume of acetylene gas produced from a given amount of calcium carbide is calculated.

Uploaded by

Ryle Aquino
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
Available Formats
Download as PDF, TXT or read online on Scribd
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Experiment No.

11
Alkynes

Preparation of Acetylene Gas


CaC2 + 2 H2O HC CH + Ca (OH)2

HC CH + KMnO4 + H2O CH2 CHO + MnO2 + KOH


OH

5. Formation of Acetylides
a. Reaction with Cuprous Chloride
Blue color

HC CH + 2NH4OH +2 CuCl -> CuC CCu + 2NH4Cl +2H2O


C2H2 + 2 Br 2 C2H2Br4
tetrabromoethane b. Reaction with Silver Nitrate
Yellow or white ppt.
HC CH + 2NH4OH + 2 AgNO3 AgC CAg + 2NH4NO3 + 2
H2O

Answers to Questions Answers to Questions


1.

4. Sol’n:
Mw CaC2 = 64 g/mol Molar Vol:
2. Terminal Alkynes
1 mole of any gas= 22.4 li
3. Acetylide formation is used to terminate or
remove terminal protons in organic chemical Vol C2H2= 10g CaC2 x 1 mol CaC2 x 1mole C2H2 x 22.4 li
production & polymerization rxns 64 g/mol CaC2 1 mole CaC2 1 mole C2H2
Vol = 3.5 li C2H2
Answers to Questions
Experiment No.12
Aromatic Hydrocarbons
REVIEW OF NAMING AROMATIC
HYDROCARBONS
Experimental Results
Experimental Results
Answers to Questions
Answers to Questions
Answers to Questions
Answers to Questions
Answers to Questions
Answers to Questions
Answers to Questions
Answers to Questions
Experiment No.13
Hydrocarbons in Petroleum Products
Experimental Results

/yellow brown to colorless


Experimental Results
B. Gasoline

Ideal
Result
Experimental Results
Experimental Results

Ideal Result
Experimental Results

Br Test: No decolorization
Baeyer’s Test: No brown ppt
*Saturated HC are present
Answers to Questions
Experiment No.14
Properties of Halogen Compounds
Experimental Results
A. Physical Properties
1. Odor: Irritating
2. Solubility

Solutes:
Halogen
Containing
Compounds

Ethyl Iodide Iodoform Chloroform

Solvents:
1) Water 2) Ethyl Alcohol 3) Ether
Experimental Results
A. Physical Properties
Solubility
Halogen Compound Water Ethyl Alcohol Ether

Ethyl Iodide Immiscible Miscible Miscible


Chloroform Immiscible Miscible Miscible
Iodoform/ Insoluble Insoluble Insoluble
Methyltriiodide
Experimental Results
Experimental Results
Answers to Questions
Answers to Questions
Experiment No.15
Preparation of Iodoform
Experimental Results
Wt of iodoform crystals (actual yield) = 1 gram
Calculations

19.35%
Answers to Questions

assess

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