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    Certificate of Analysis: Brammer Standard Company, Inc

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    Ali Mohsin
    This document is a certificate of analysis for a reference material called BS 64C used for high carbon steel. It provides the certified chemical composition values and associated uncertainties for elements like carbon, manganese, phosphorus, and others. The values are based on an interlaboratory testing program and various analytical methods like ASTM standards and spectroscopy. Certified reference materials were used to validate the analytical data.

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    © All Rights Reserved
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    Certificate of Analysis: Brammer Standard Company, Inc

    Uploaded by

    Ali Mohsin
    245 views4 pages
    This document is a certificate of analysis for a reference material called BS 64C used for high carbon steel. It provides the certified chemical composition values and associated uncertainties for elements like carbon, manganese, phosphorus, and others. The values are based on an interlaboratory testing program and various analytical methods like ASTM standards and spectroscopy. Certified reference materials were used to validate the analytical data.

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    Brammer standard BS 64C

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    bs64c

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    This document is a certificate of analysis for a reference material called BS 64C used for high carbon steel. It provides the certified chemical composition values and associated uncertainties for elements like carbon, manganese, phosphorus, and others. The values are based on an interlaboratory testing program and various analytical methods like ASTM standards and spectroscopy. Certified reference materials were used to validate the analytical data.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    245 views4 pages

    Certificate of Analysis: Brammer Standard Company, Inc

    Uploaded by

    Ali Mohsin
    This document is a certificate of analysis for a reference material called BS 64C used for high carbon steel. It provides the certified chemical composition values and associated uncertainties for elements like carbon, manganese, phosphorus, and others. The values are based on an interlaboratory testing program and various analytical methods like ASTM standards and spectroscopy. Certified reference materials were used to validate the analytical data.

    Copyright:

    © All Rights Reserved
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    of 4

    Brammer Standard Company, Inc.

    Certificate of Analysis
    B.S. 64C
    Reference Material for High Carbon Steel

    Certified Estimate of Certified Estimate of


    Value1 Uncertainty2 Value1 Uncertainty2

    Analysis listed as percent by weight

    C 0.920 0.007 Co 0.004 0.002

    Mn 0.22 0.01 N 0.0084 0.0003

    P 0.015 0.001 V 0.005 0.001

    S 0.0024 0.0005

    Si 0.22 0.01 Information Values3

    Cu 0.016 0.002 Al (0.005)

    Ni 0.038 0.003 Nb (<0.003)

    Cr 0.261 0.008 Sn (0.001)

    Mo 0.008 0.001 Ti (0.002)

    1
    The certified value listed is the present best estimate of the true value based on the results of an
    interlaboratory testing program.
    2
    The uncertainties listed are based on value judgments of the material inhomogeneity and possible bias in
    the determined analytical values. No attempt is made to derive exact statistical measurements of
    imprecision because several methods were used in the determination of most constituents.
    3
    Values in parentheses are not certified and are provided for information only.

    See the following pages for more information. Replaces Certificate Number REV64C-040892
    New Certificate Number REV2-64C-012710

    New Certificate Number REV2-64C-012710 was Revised to show uncertainty values on January 27, 2010

    Brammer Standard Company, Inc., 14603 Benfer Road, Houston, TX 77069-2895


    Telephone (281) 440-9396 Fax (281) 440-4432
    BS 64C analysis listed as percent concentration Certificate Number REV2-64C-012710
    -----------------------------------------------------------------------------------------------------------------------------------------------------
    Analysis C Mn P S Si Cu Ni Cr Mo
    -----------------------------------------------------------------------------------------------------------------------------------------------------
    1 0.913 0.205 0.014 0.0018 0.21 0.014 0.034 0.25 0.0064
    2 0.918 0.213 0.0149 0.0021 0.22 0.015 0.036 0.257 0.007
    3 0.92 0.22 0.015 0.0021 0.22 0.016 0.038 0.26 0.007
    4 0.92 0.22 0.015 0.0022 0.230 0.016 0.038 0.261 0.008
    5 0.920 0.22 0.015 0.0025 0.23 0.0165 0.039 0.261 0.008
    6 0.9237 0.23 0.015 0.0025 0.23 0.017 0.040 0.263 0.009
    7 0.927 0.23 0.016 0.0030 0.018 0.040 0.264 0.009
    8 0.233 0.016 0.0030 0.018 0.040 0.266 0.0092
    9 0.243 0.040 0.27
    -----------------------------------------------------------------------------------------------------------------------------------------------------
    Average 0.9202 0.2238 0.01511 0.00240 0.2233 0.0163 0.0383 0.2613 0.00795
    -----------------------------------------------------------------------------------------------------------------------------------------------------
    Std Dev 0.0044 0.0114 0.00064 0.00043 0.0082 0.0014 0.0021 0.0057 0.00107
    -----------------------------------------------------------------------------------------------------------------------------------------------------
    Certified 0.920 0.22 0.015 0.0024 0.22 0.016 0.038 0.261 0.008
    -----------------------------------------------------------------------------------------------------------------------------------------------------
    t 2.45 2.31 2.36 2.36 2.57 2.36 2.31 2.31 2.36
    -----------------------------------------------------------------------------------------------------------------------------------------------------
    C(95%) 0.0041 0.0088 0.00054 0.00036 0.0086 0.0012 0.0016 0.0043 0.00089
    -----------------------------------------------------------------------------------------------------------------------------------------------------

    continued from above


    ------------------------------------------------------------------------------------------------------------------
    Analysis Co N V Al Nb Sn Ti
    -------------------------------------------------------------------------------------------------------------------
    1 0.003 0.0081 0.004 0.002 0.001 0.0004 0.001
    2 0.003 0.0083 0.005 0.002 <0.001 0.0006 0.0012
    3 0.003 0.0083 0.005 0.004 <0.003 0.00079 0.0013
    4 0.0035 0.0085 0.0053 0.005 0.001 0.002
    5 0.0044 0.0086 0.0056 0.005 0.001 0.002
    6 0.0058 0.0058 0.0051 0.0011 0.002
    7 0.006 0.0057 0.0016 0.002
    8 0.006 0.006 0.0022
    9 0.0064
    10 0.008
    -------------------------------------------------------------------------------------------------------------------
    Average 0.0043 0.00836 0.0051 0.0049 0.0009 0.0017
    -------------------------------------------------------------------------------------------------------------------
    Std Dev 0.0014 0.00019 0.0006 0.0019 0.0004 0.0005
    -------------------------------------------------------------------------------------------------------------------
    Certified 0.004 0.0084 0.005 (0.005) (<0.003) (0.001) (0.002)
    -------------------------------------------------------------------------------------------------------------------
    t 2.36 2.78 2.57 2.26 2.45 2.36
    -------------------------------------------------------------------------------------------------------------------
    C(95%) 0.0012 0.00024 0.0007 0.0013 0.0004 0.0004
    -------------------------------------------------------------------------------------------------------------------
    C(95%) = (t x sd)//n The half-width confidence interval, where t is the appropriate Student's t value, sd is the interlaboratory standard
    deviation, and n is the number of acceptable mean values. For further information regarding the confidence interval for the certified value see
    ISO Guide 35:2006 section 6.

    Values in parentheses are not certified and are provided for information only.

    Some of the co-operating laboratories were:


    Allegheny Ludlum Steel Corporation, Brackenridge, PA
    Allegheny Ludlum Steel Corporation, Lockport, NY
    Alpha Research Laboratories, Stevensville, MI
    Anderson Laboratories, Greenville, WI
    Brammer Standard Co., Inc., Houston, TX
    Crucible Specialty Metals, Syracuse, NY
    Hoesch Stahl AG, Dormund, Germany
    Jessop Steel Company, Washington, PA
    J. Dirats and Co., Inc., Westfield, MA
    VHG Laboratories, Inc., Manchester, NH
    Analysis: Chemical analyses were made on millings from cross-sections of the bars. The individual values listed
    above are the average of each analyst's results.

    Analytical Methods: Methods of analysis used were a combination of ASTM Standard Methods E 350, E 415,
    E 1019, plus additional ICP, and AA spectrometric methods.

    Traceability: The following Certified Reference Materials were used to validate the analytical data listed above:
    NIST SRM 32e, 125b, 361 to 365; BAM 039-2, 044-1; BCS 455/1, 456/1, 458/1; ECRM 085-1, 088-1, 096-1,
    184-1, 481-1; GBW 01402; IMZ 1.22, 1.74

    Homogeneity: This Reference Material was tested for homogeneity using ASTM Standard Method E 826 and found
    acceptable. It was also examined by spark atomic emission spectrometry and found to be compatible with the
    following NIST Certified Reference Materials: SRM 1222, 1224, 1225, 1261A to 1265A, 1761 to 1767

    Form: This Reference Material is machined in the form of a disc, approximately 44 mm diameter and 19 mm thick by
    Brammer Standard Company. The bar stock used for this material was produced by hot-rolling billets and annealing.

    Certified area: The entire depth of the disc may be used.

    Caution: As with any bar material, avoid spark atomic emission spectrometric burns in the center of the disc
    (5 mm radius), as some segregation may be present.

    Sample Preparation: For best analytical results, use the same method for preparing the analytical surface on all
    reference materials as you use for production specimens. Avoid overheating the disc during surface preparation.

    Certificate Number: The unique identification number for this certificate of analysis is REV2-64C-012710. This
    BS 64C Certificate of Analysis was revised to show the estimate of uncertainty for the certified values. After
    reviewing the analytical data, a third decimal place was certified for carbon and chromium, and the niobium, tin, and
    titanium values were changed to uncertified to conform to current versions of ISO Guides.

    This Reference Material was first revised on April 8, 1992, after testing by additional laboratories in 1991 and 1992
    The first Certificate of Analysis for BS 64C was certified on August 9, 1990.

    Refer to the “Certificates” section of the Brammer Standard Company website for any revision to this or other
    Brammer Standard Company’s Certificates of Analysis.

    Safety Notice: A Material Safety Data Sheet (MSDS) is not required for this material. This material will not release
    or otherwise result in exposure to a hazardous chemical, under normal conditions of use. Inquiries concerning this
    Reference Material should be directed to:

    Brammer Standard Co., Inc. Phone: (281) 440-9396 website: brammerstandard.com


    14603 Benfer Road
    Houston, Texas 77069-2895 USA Fax: (281) 440-4432 email: contact@brammerstandard.com

    Certified by: ____________________________ on January 27, 2010.


    Beau R. Brammer

    Certificate Number REV2-64C-012710


    Referenced Documents

    ASTM documents available from ASTM, 1916 Race Street, Philadelphia, PA, 19103.

    Versions available at the time of interlaboratory testing

    E 350 - 90 Standard Test Methods for Chemical Analysis of Carbon Steel, Low-Alloy Steel, Silicon Electrical Steel, Ingot Iron, and Wrought Iron

    E 415 - 85 (Reapproved 1989) Standard Test Method for Optical Emission Vacuum Spectrometric Analysis of Carbon and Low-Alloy Steel

    E 826 - 85 (Reapproved 1990) Standard Practice for Testing Homogeneity of Materials for the Development of Reference Materials

    E 1019-93 Standard Test Methods for Determination of Carbon, Sulfur, Nitrogen, and Oxygen in Steel and in Iron, Nickel, and Cobalt Alloys

    ISO Guides and Standards available from Global Engineering - www.global.ihs.com

    ISO Guide 35 Reference Materials - General and statistical principles for certification

    Certificate Number REV2-64C-012710

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