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    This Study Resource Was: Data Sheet Experiment 3 Synthesis of Potassium Tris (Oxalato) Ferrate (III) Trihydrate

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    Solutions Master
    This document summarizes an experiment on the synthesis of potassium tris(oxalato)ferrate(III) trihydrate. The student used 5.0144 grams of Fe(NH4)2(SO4)2.6H2O and obtained 4.9632 grams of K3[Fe(C2O4)3].3H2O. Calculations show the theoretical yield was 6.2879 grams. The percent yield was determined to be 78.93%.

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    This Study Resource Was: Data Sheet Experiment 3 Synthesis of Potassium Tris (Oxalato) Ferrate (III) Trihydrate

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    Solutions Master
    538 views3 pages
    This document summarizes an experiment on the synthesis of potassium tris(oxalato)ferrate(III) trihydrate. The student used 5.0144 grams of Fe(NH4)2(SO4)2.6H2O and obtained 4.9632 grams of K3[Fe(C2O4)3].3H2O. Calculations show the theoretical yield was 6.2879 grams. The percent yield was determined to be 78.93%.

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    Original Title

    Data Sheet Exp 3.6.PDF

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    This document summarizes an experiment on the synthesis of potassium tris(oxalato)ferrate(III) trihydrate. The student used 5.0144 grams of Fe(NH4)2(SO4)2.6H2O and obtained 4.9632 grams of K3[Fe(C2O4)3].3H2O. Calculations show the theoretical yield was 6.2879 grams. The percent yield was determined to be 78.93%.

    Copyright:

    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    538 views3 pages

    This Study Resource Was: Data Sheet Experiment 3 Synthesis of Potassium Tris (Oxalato) Ferrate (III) Trihydrate

    Uploaded by

    Solutions Master
    This document summarizes an experiment on the synthesis of potassium tris(oxalato)ferrate(III) trihydrate. The student used 5.0144 grams of Fe(NH4)2(SO4)2.6H2O and obtained 4.9632 grams of K3[Fe(C2O4)3].3H2O. Calculations show the theoretical yield was 6.2879 grams. The percent yield was determined to be 78.93%.

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    DATA SHEET

    EXPERIMENT 3

    Synthesis of Potassium tris(oxalato)ferrate(III) trihydrate

    Name : KHAIRIN NABILAH BINTI MOHAMAD


    YELSOP
    Student ID : 2017404078
    Date of Experiment : 8/6/2020

    RESULTS

    m
    e r as
    co
    1. Mass of Fe(NH4)2(SO4)2.6H2O used = 5.0144 g

    eH w
    o.
    2. Moles of Fe(NH4)2(SO4)2.6H2O used = 0.0128 mol
    rs e
    3. Mass of K3[Fe(C2O4)3].3H2O obtained = 4.9632 g
    ou urc
    4. Theoretical yield of K3[Fe(C2O4)3].3H2O (moles) =0.0128 𝑚𝑜𝑙𝑒
    o

    5. Theoretical yield of K3[Fe(C2O4)3].3H2O (mass) =6.2879 g


    aC s
    v i y re

    6. Percent yield of K3[Fe(C2O4)3].3H2O =78.93%


    ed d
    ar stu

    Calculations

    Show all your calculations.


    sh is

    2. Moles of Fe(NH4)2(SO4)2.6H2O used =


    Th

    mass
    NO. OF MOLES =
    RMM
    5.0144
    =
    392.13

    = 0.0128 g/mol

    https://www.coursehero.com/file/67865065/DATA-SHEET-EXP-36pdf/
    4. Mole Fe(NH4)2(SO4)2.6H2O = Fe(OH)3
    Mole of Fe(OH)3 =0.0128 g/mol

    Mass of K2C2O4=
    1 × 1000
    = 50 𝑔
    20
    Mole K2C2O4=
    50
    = 0.3008 𝑚𝑜𝑙
    166.22
    Mass of H2C2O4=

    m
    e r as
    0.5 × 1000
    = 10 𝑔

    co
    50

    eH w
    Mole of H2C2O4=

    o.
    rs e 10
    ou urc
    = 0.1111 𝑚𝑜𝑙
    90
    From the overall equation:
    o
    aC s

    3 mole of K2C2O4≡ 2 mole K3[Fe(C2O4)3].3H2O


    v i y re

    0.3008
    × 2 = 0.2005 𝑚𝑜𝑙𝑒
    3
    ed d
    ar stu

    3 mole H2C2O4 ≡ 2 mole K3[Fe(C2O4)3].3H2O


    0.1111
    sh is

    × 2 = 0.0741 𝑚𝑜𝑙𝑒
    3
    Th

    2 mol of Fe(OH)3 ≡ 2 mole K3[Fe(C2O4)3].3H2O


    0.0128
    × 2 = 0.0128 𝑚𝑜𝑙𝑒
    2

    The limiting reactant is Fe(OH)3


    Therefore, the theoretical mole of K3[Fe(C2O4)3].3H2O = 0.0128 𝑚𝑜𝑙𝑒

    https://www.coursehero.com/file/67865065/DATA-SHEET-EXP-36pdf/
    5. The theoretical yield of K3[Fe(C2O4)3].3H2O (mass)
    0.0128 𝑚𝑜𝑙𝑒 × 491.24 𝑔/𝑚𝑜𝑙 =6.2879 g
    6. Percent yield of K3[Fe(C2O4)3].3H2O =

    4.9632
    × 100% = 78.93%
    6.2879

    m
    e r as
    co
    eH w
    o.
    rs e
    ou urc
    o
    aC s
    v i y re
    ed d
    ar stu
    sh is
    Th

    https://www.coursehero.com/file/67865065/DATA-SHEET-EXP-36pdf/

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