Bellingham Stanley Refractometer Adp 440 Plus Manual 001

ADP440+
Polarimeter
User Guide
ADP440+ User Guide (Eng)
Code 37-278
Issue 01
Revision A
Date January 2010
Bellingham and Stanley Ltd. has been manufacturing high quality optical instruments in the
UK since 1914 and is a leading manufacturer of refractometers and polarimeters. The current
range of products includes optical and digital hand refractometers as well as a full range of
laboratory refractometers and polarimeters available through a network of trained distributors
throughout the world. Process refractometers are also available through specialist outlets.
Our main website gives full details about Bellingham and Stanley Ltd. and our products.
Foreign language brochures in PDF format may be downloaded from this section of the site
by clicking the flag. We apologise if the foreign language brochure of your choice is not
available.
Contact Sales at Bellingham and Stanley Ltd. to discuss a particular application or to receive
details of your local distributor.
Bellingham + Stanley Ltd. recognise all trademarks
© Copyright Bellingham + Stanley Ltd. 2010
Every effort has been made to ensure the accuracy of the contents of the manual. However,
Bellingham + Stanley Ltd. can assume no responsibility for errors contained in the manual or their
consequences.
Printed in UK
Bellingham + Stanley Ltd. Bellingham + Stanley Inc.

Longfield Road, 1000 Hurricane Shoals Road,
Tunbridge Wells, Kent TN2 3EY Building D, Suite 300,
United Kingdom Lawrenceville, USA GA30043
Tel: +44 (0) 1892 500400 Tel: 770 822 6898
Fax: +44 (0) 1892 543115 Fax: 770 822 9165
DECLARATION OF CONFORMITY
According to ISO/IEC 17050-1 & 2 : 2004
Manufacturer's Name Bellingham & Stanley Limited
Manufacturer's Address Longfield Road,

Tunbridge Wells,
Kent TN2 3EY
United Kingdom
declares that the product
Product Name ADP440+ Polarimeter
Model Number All
Is designed to conform to the following Product Specifications:
Safety BS EN 60950-1:2002
EMC Emissions
• BS EN 55022:2006 Radiated Emissions Class A
• BS EN 55022:2006 Conducted Emissions Class A
Immunity
• BS EN 61000-3-2:2006 Harmonics
• BS EN 61000-3-11:2001 Flicker
• BS EN 61000-4-2:1995 ESD 8kV contact
• BS EN 61000-4-3:2006 EMS 3V/m
• BS EN 61000-4-5:2006 Surges 0.5kV (line to line)
1.0kV (line to earth)
• BS EN 61000-4-11:2004 Power outages 1 cycle/100%
Supplementary The product herewith is designed to comply with the requirements

of the EMC Directive 89/336/EEC and the Low Voltage Directive
73/23/EEC.
This symbol is an internationally agreed indicator that the product bearing it

should not be disposed of as general waste or garbage which might end up in
landfill sites, but should instead be sent for special processing and/or recycling in
those countries where appropriate legislation and facilities are in place.
This symbol indicates a caution or warning, please refer to the manual.
contents
Installing the instrument ............................................. 1
Instrument description................................................ 2
Instrument overview ............................................ 2-1
Basic operation ................................................... 2-4
Display screen information .................................. 2-9
The instrument logs............................................. 2-14
Measurement settings ......................................... 2-15
Sampling techniques ........................................... 2-20
Flow-through and water-jacketed tubes .............. 2-22
Setting up the system ................................................ 3
Menu flow chart................................................... 3-1
Shortcut keys ...................................................... 3-3
Calibration ........................................................... 3-5
Measurement settings ......................................... 3-8
Methods .............................................................. 3-9
User accessibility ................................................ 3-13
21 CFR Part 11 ................................................... 3-19
System settings................................................... 3-20
Customising the instrument................................. 3-23
Measurement traceability .................................... 3-25
Adding extra scales............................................. 3-27
Special library scales .......................................... 3-29
Setting the default values .................................... 3-40
Displaying the software / hardware details .......... 3-40
Specification............................................................... 4
Spares and accessories............................................. 5
Contents 37-278’01 Rev. A January 2010

section 1
Installing the instrument
Unpacking the instrument.................................... 1-1
Contents list ........................................................ 1-1
Part numbers....................................................... 1-1
Positioning the system ........................................ 1-2
Mains connection ................................................ 1-2
Power requirements ............................................ 1-2
Power supply adapter ......................................... 1-2
Installing the instrument 37-278’01 Rev. A January 2010 Section 1

Unpacking the instrument
Carefully remove all of the packing material. It is recommended that the box
and other packing materials are retained so that, should the need arise, the
polarimeter can be safely returned to the manufacturer.
Check that all parts listed below are present and that no transit damage has
occurred. If any are damaged or missing, contact the supplier immediately.
Contents list
1 ADP440+ Polarimeter module, see table below for part number
1 Power supply, 55-105
1 Mains lead, see below for part number
1 Polarimeter tube, 35-47
1 Operating Instructions, 37-256
1 Instruction manual CD-ROM, 55-300
1 Key-fob type ID tags (pack of 3), 22-071
Part numbers
ADP440+ polarimeter part numbers
Installation
Complete polarimeter
Model Polarimeter module only
including power supply
ADP440+ 37-40 37-440
Mains lead part numbers (for use with Power supply 55-105)
Mains cord wire colours

Code
Moulded plug type for Voltage
Line Neutral Earth no.
(Phase) (Return) (Ground)
Switzerland 230V - - - 61-181

Denmark 230V - - - 61-182
India / South Africa 230V - - - 61-188
Australia 230V - - - 61-189
Green /
No plug – open lead - Brown Blue 61-190
Yellow
UK 13 Amp square pin
230V - - - 61-191
to BS1363/A
United States (3 pin) 110V - - - 61-192
Europe (Schuko) 230V - - - 61-193
Installing the instrument 37-278’01 Rev. A January 2010 Page 1-1

Positioning the system
Place the instrument on a flat and stable bench that is:
• dry and indoors

• away from draughty or hot equipment like fans or heaters
• out of direct sunlight or strong ambient light
• away from potential sources of interference, such as RFI generating
equipment
• within reach of a power point
• not using a power circuit that also has large motors or noise generating
equipment connected to it
Mains connection
The power supply adapter is supplied with a moulded mains cord and plug,
to suit one of several socket types. For UK lead, replace fuse only with the
type indicated on the plug.
Power requirements
Voltage 110 to 230 V~ ±10%
Frequency 50 to 60 Hz
Installation
Maximum current 200 mA
Power supply adapter 55-105

RISK OF ELECTRIC SHOCK:
• For electrical safety information, read the label on the power supply.
• For indoor use only.
• Must be kept dry.
• Disconnect the equipment from the mains supply before unplugging the
mains lead from the power supply unit.
• Do not open the power supply adapter. No user serviceable parts
inside.
WARNING:
• Do not cover, designed to operate with free air convection.
• No cleaning required.
Note: A waterproof power supply adaptor, code no. 55-250, which can be
used in damp environments, is available as an optional extra.
Page 1-2 37-278’01 Rev. A January 2010 Installing the instrument

section 2
Instrument description
Instrument overview................................................... 2-1
The polarimeter ................................................... 2-1
The services panel .............................................. 2-2
The display panel ................................................ 2-3
Basic operation .......................................................... 2-4
Switching on........................................................ 2-4
Switching off........................................................ 2-4
Switching on for the first time .............................. 2-4
Initial operation after switching on ....................... 2-5
Manoeuvring through the menus......................... 2-6
Keying in letters, numbers and other characters . 2-7
Keying in numerical values.................................. 2-8
Display screen information......................................... 2-9
Taking a reading ................................................. 2-10
Blocked light path................................................ 2-10
Grey result display .............................................. 2-10
Zeroing the reading ............................................. 2-11
Optical density..................................................... 2-12
Temperature sensor............................................ 2-12
Printing the readings ........................................... 2-13
24 column print format ........................................ 2-13
Printer options ..................................................... 2-13
The instrument logs ................................................... 2-14
The System log ................................................... 2-14
The Reading log.................................................. 2-14
ADP Log Acquisition Program............................. 2-14
Measurement settings................................................ 2-15
Mode menu ......................................................... 2-15
Measurement settings in detail............................ 2-16
Remote operation................................................ 2-18
RS232 serial port ................................................ 2-19
Sampling techniques.................................................. 2-20
Cleaning .............................................................. 2-20
Filling the tube..................................................... 2-20
Cover glass stress............................................... 2-21
Temperature compensation ................................ 2-21
Flow-through and water-jacketed tubes ..................... 2-22
Instrument description 37-278’01 Rev. A January 2010 Section 2

Instrument overview
The polarimeter
The ADP440+ polarimeter is a self-contained, easy-to-use instrument
suitable for measuring the rotation of optically active samples. The readings
are displayed in either ºAngular or ºZ (International Sugar Scale) on a backlit
widescreen LCD display. Other reading scales are available see page 3-27.
The instrument is housed in a rigid polyurethane foam moulded case which is
light in weight whilst being extremely rugged and has a high resistance to
chemical attack from the majority of commonly used samples.
Upper lid: Sample chamber: ID tag reader:

Can be replaced with optional Open the hinged lids and place This area of the
slotted lids to suit water- a polarimeter tube or Quartz housing is capable of
jacketed or flow through tubes Control Plate on the stainless reading ID tags
steel rails wirelessly using RFID.
Lower lid:
Open to insert a tube
Housing:
Low density expanded Display panel:
polyurethane foam. Lightweight see page 2-3
yet good mechanical strength
and stability
Instrument description 37-278’01 Rev. A January 2010 Page 2-1

The services panel
RS232 Serial port 1: RS232 Serial port 2:

For printing or remote For connecting either a
communication barcode scanner or
refractometer
Parallel Port
For connecting to a
Power connector:
parallel printer
24V dc from
power supply
Warning symbol:
See similarly
marked warnings in
this manual
Code number:
B+S code number for
the instrument
module.
CE mark:
Specifies the
Serial number:
instrument conforms to
Always specify this
relevant EU safety and
number in any
EMC regulations
communication with
B+S Ltd.
Page 2-2 37-278’01 Rev. A January 2010 Instrument description

The display panel
Operation status bar

Shows the details of the
current operation
Current time
Soft key functions

Power key:
Press to switch ON Softkeys
Press for 2 seconds to Functions change
switch to STANDBY with display
Power indicator
STANDBY — Red
ON - Green
Arrow keys Alpha-numeric keys

Forward/Back keys ‘Telephone style’ keys for
for negotiating entering letters and
through menus etc.. numbers

Basic operation
Switching on
Plug in the power supply and switch on the mains supply. The instrument
will display configuration data and then switch to standby mode with the
power indicator showing red.
To switch on, press the Power Key – the Power Indicator will show green.
Switching off
To switch to standby, press the Power Key and hold down until a
Basic operation
confirmation screen shows (approximately 2 seconds). Press Yes to switch

to standby – the Power Indicator will show red, or press No to continue
operating.
Note: It is preferable for the instrument to be left on continuously even if a

reading is to be taken only once per day.
Switching on for the first time

When the instrument is switched on for the first time after delivery, a ‘Setup
Wizard’ will step you through a number of questions so that the system can
be configured for your particular application.
Initially, it is a requirement to select the language.
Step 1 Setup the standard measurement conditions. These are the

settings which measurements are to be taken, the reading scale and
temperature compensation that should be used. When the correct
conditions are selected, press Quit.
Step 2 Set the clock. Adjust the instrument clock to local time.
Step 3 Set the printer options. Select whether readings are to be

printed, stored in memory or both. When the correct conditions are
selected, press Quit.
Step 4 Pair ID tag to administrator. The instrument is supplied with 3

ID tags, one of which can be paired to the administrator user.
When prompted place the desired ID tag onto the reader (see pages
2-1 and 3-15).
The Setup Wizard can be run at any time by selecting the Tools menu.

Initial operation after switching on
When the instrument is switched on, the reading mechanism will start-up.
The screen shown below will be displayed briefly.
After a few seconds the following will be displayed. It is important that the
chamber is empty whilst the instrument stabilises.
Basic operation
The instrument will now wait for reading mechanism to reach operating
speed, the vertical progress bar indicates how much longer this will take,
which should take less than one minute. When reached, it will automatically
carry out a zero, this is why the chamber must be empty.
If by accident a tube was in the chamber simply remove it and press ‘Zero’.
The polarimeter is now ready for use.
It is recommended that in order to take accurate readings, allow a further 30

minutes for the instrument to stabilise, as specified in ICUMSA procedures.

Manoeuvring through the menus
Menu items can be found and selected by either:
pressing the Up/Down softkeys and then pressing Select

or
pressing the item number key i.e. press 3 for Setup
Basic operation
If the menu item contains a list of options to choose from then either:
select the menu item and then choose the option from the displayed list
or
press the Forward/Back arrow keys to step through the options
Menu items that can be modified by using the arrow keys are identified by
arrows being displayed next to the menu items value (highlighted below).
Return to the Measurement display by repeatedly pressing Quit to step back

through the menus.

Keying in letters, numbers and other characters
When it is necessary to enter in text, such as a method name, the alpha-
numeric entry screen will be displayed. This will allow entry of numbers,
letters and a range of punctuation characters including “ ! ? / ( ; etc. by
multiple presses of keys.
Basic operation
E.g. To enter the name cola(74) press:
the d key 3 times c

the h key 3 times o
the g key 3 times l
the d key 1 time a
the c key 11 times (
the i key 5 times 7
the f key 4 times 4
the c key 12 times )
Once a key is pressed, the available characters that can be selected using
that key are shown at the top right of the screen (see the table below).
If a key is not re-pressed within one second, the displayed character will be
accepted.
Key Available characters

1 - ? ! , . : ; “ ‘ ( ) 1
2 a b c 2
3 d e f 3
4 g h i 4
5 j k l 5
6 m n o 6
7 p q r s 7
8 t u v 8
9 w x y z 9
0 + $ % / # < = > _ 0

Keying in numerical values
Numerical values, such as a 33.60° rotation or a polynomial constant
0.0123456, can entered in either fixed decimal point format or in scientific
notation. E.g.:
Fixed decimal point Scientific

1.2345 1.2345E0
or
-123.45 -1.2345E2
0.00012345 1.2345E-4
One of the softkeys (second from left) gives access to the minus (-), decimal
point (.) and exponent (E) symbols that will be required to enter both
numerical formats. As the user enters the number, the instrument responds
to the key strokes by changing the softkey function.
Basic operation
If an error is made while entering the number, press the CLEAR softkey to
erase the entry.
The ENTER softkey is available throughout the process and may be pressed
at any time to accept the entry.
Note that if the number being entered is negative, then press the minus soft-
key before entering the number. Otherwise, if the number is less than 1,
press 0 first to show the decimal point softkey.

Display screen information
Current time
Stability
Progress bar
Reading Result
Measurement
Settings
Softkey
titles
Basic operation

Taking a reading
Fill the polarimeter tube with your sample. Gently rock the tube from end to
end to ensure all air bubbles are released through the centre filling tube. Lift
open the chamber cover and place the tube on the two rails.
The instrument will now start taking readings continually. You should notice
that the reading fluctuates as it settles. Note that the progress bar will slowly
fill, also as an indication that the reading has yet to stabilise, the reading
result is displayed in grey.
Basic operation
When finally stabilised the progress bar will appear full and the reading will
be displayed in black.
Blocked light path

If an article has been left in the chamber which totally blocks the light path,
the display will show all dashes as below:
Grey result display

If the sample is too optically dense to enable an accurate reading to be
calculated, i.e. its optical density (OD) is greater than 3, the background of
the reading will appear grey as shown below.

Zeroing the reading
The instrument should be zeroed often to ensure accurate readings. It is a
quick and simple procedure so can easily be carried out before every
measurement. There must be no sample present and so it can be done
with an empty chamber or, if preferred, with the polarimeter tube that will
be used to measure the sample. However, if a tube is used, it must be
empty, perfectly clean and dry.
Take a clean empty sample tube and place in the chamber. Wait for the
instrument to stabilise, using the reading progress bar as a guide. When
stable press ZERO. The displayed reading will now change to 0.00.
Below the instrument is showing 0.02 °a with an empty tube in the chamber.
Basic operation
Pressing zero will cause the instrument to display all dashes briefly to identify
that the zero has been carried out.
When the dashes disappear the instrument shows 0.00. Also note that the
OD value is also zeroed. The tubes glass end plates were causing a 0.1 OD
loss in light. With the instrument zeroed the OD measurement will take
account for the 0.1 OD loss, and therefore show 0.0 OD.
More advanced use of the polarimeter might require that the instrument is
zeroed with a sample (blank solvent) in the chamber.

Optical density
The optical density is a measure of the light and the sample optical density
(OD)
where:
OD = - Log10 ( % light transmission / 100 )
Basic operation
OD 0.0 = 100% light transmission, no absorption in the sample

OD 1.0 = 10% light transmission, 90% absorption in the sample
OD 2.0 = 1% light transmission, 99% absorption in the sample
OD 3.0 = 0.1% light transmission, 99.9% absorption in the sample
If the optical density of the sample is greater than 3, the background of the
reading area will appear grey, show below (see page 2-10).
Temperature sensor
The ADP440+ has a in-built temperature sensor. The measured
temperature will automatically be updated and displayed in degrees Celsius.
The probe is found inside the measurement chamber.
If the probe is left in its cradle at the rear of the chamber, it will provide a
measure of the general chamber temperature. Alternatively, it can be placed
in the filling arm of a centre filling tube when it will measure the temperature
of the sample itself.

Printing the readings
If the fourth (right hand) softkey is set to ‘Print’ or ‘Prt+Save’, the last
displayed reading can be sent to a printer via the selected port. The print
layout can be either with the reading data listed sequentially, suitable for
narrow printers with 24 columns, or with the data in CSV (comma separated
values) suitable for connection to a LIMS. (See ‘Set the printer mode’ and
‘Available print formats’ in Section 3)
24 column print format

Basic operation
At the start of the printout is a header. This contains general information

about the instrument, such as when the last span was carried out, and
measurement settings.
Each measurement has a number of parameters. On the left is the
parameter name, and on the right is the parameters value.
The stability field has 3 possible values, below shows the stability value and
the associated on screen display.
Printout Screen Printout Screen Printout Screen
Ok Un No
Reading stable Not yet stable Light path blocked
Use interconnecting cable 54-03 to connect the instrument to a parallel

printer. (These cables are available from Bellingham + Stanley. Some devices
may require alternatives.)
Printer options
Optionally the reading can be sent to the RS232 serial port for connection to
either a printer or computer terminal program.

The instrument logs
The ADP440+ polarimeter has two separate logs for storing data. This data
will be held in the instrument whether or not the power is on or off. The
logs can either be downloaded to a computer using the ADP Log Acquisition
Program or viewed directly from the instrument.
The System log

The System log maintains a record of all changes and adjustments made to
the instrument by the operators. This will include span calibration, changes
to the setup, configuration and methods.
If the PIN feature is activated within the instrument, the user who carries
Instrument Logs
out the change will be also logged.
The system log can be viewed by

selecting ‘System Log’ from the Tools
Menu. Pressing ‘0’ will display viewing
options, and arrow keys will show
additional log entry details.
The Reading log

If the fourth (right hand) softkey is set to ‘Save’ or ‘Prt+Save’ then pressing it
will save the last displayed reading into the Reading log. Up to 606 readings
can be stored in the log. When the log is full no further results will be able
to be stored, a warning message will be displayed on the screen. The
current status of the Reading log can be viewed by selecting the ‘Saved
results’ menu option with in the Tools Menu.
The reading log and current status can

be viewed by selecting the ‘Saved results’
menu option within the Tools Menu.
Press the ‘Review’ softkey to display the
contents of the log. When displayed,
pressing the arrow keys will show
additional reading parameters.
ADP Log Acquisition Program

The ADP Log Acquisition Program (B+S code no. 37-301) enables the data
from both of the above logs to be transferred to a PC at which time the logs
will be deleted in the instrument. The data can then be sorted, easily
viewed and also saved in csv format files, which can then be opened in a
spreadsheet. This program can be downloaded free from the Bellingham +
Stanley website…
www.bellinghamandstanley.com

Measurement settings
The measurement settings are accessed in the Mode menu, which is
available from the Measurement Display.
Mode menu
The mode menu will be familiar to users of the ADP220 polarimeter and
many other Bellingham + Stanley instruments.
The measurement settings are changed from the Mode menu, which is
accessed from the Measurement Display.
Reading Mode
Press Quit to return back to the Measurement Display.
The following pages describe each of the measurement settings.

Measurement settings in detail
The ADP440+ has a number of measurement settings…
Scale (the scale units that the readings is displayed in)
Temp. Comp. (whether temperature compensation is used)
Limits (tests to check if the reading parameters are within set
limits)
Multiplication (a factor the reading in multiplied by)
Range (determines which 180 °C range to display the reading)
Scale
The instrument has a number of scales that measurement can be displayed
in. By default the available scales are…
Scale Name Scale ID
angular (°a) °a
iss (°z) °z
Reading Mode
Temp. Comp. (temperature compensation)

The instrument has a number of temperature compensation modes
available. By default the available temperature compensation modes are…
TC Name TC ID
none nc
sugar sc
quartz qc
Limits
The instrument is able to have limits set on a number of parameters. If the
measured sample fails to meet these limits a line will be drawn through the
result.
This feature is explained in more detail on page 3-12.
Multiplication
This factor will be multiplied with the measurement reading to create the
displayed reading.
Example
If you are using a 100mm length sample tube but want to display the
equivalent reading result for a 200mm length tube, then enter a
multiplication factor of 2.
If the multiplication factor has been set to any value than
1, the scale identification field will show “Scale: °a x 2.0”
on the measurement display.
See " Keying in numerical values ", page 2-8, for details of
how to enter numbers.

Range
The Range setting is only available when the angular degree scale (°a) is
selected. The default range for the °a scale is -89° to +89° (std). The “(std)”
has been added to this one range title to allow easy identification of the
standard range.
Possible ranges are:-
-359° to -181°
-269° to -91°
-179° to -1°
-89° to +89° (std)
+1° to +179°
+91° to +269°
+181° to +359°
All polarimeters measure the amount of rotation of a plane of polarised light
and so it is only possible for the instrument to detect the position of the
rotated light beam over a 180° span. As shown in the diagrams below, the
plane of light leaving a sample with a rotation of +110° is exactly the same as
Reading Mode
that from a sample with a rotation of -70°.

Therefore, a sample with a rotation of +110° will display -70° on the default
range.
0° Rotation 110° Rotation -70° Rotation

If the user is aware that the sample to be measured should have a rotation
greater than +89° then the correct value can be calculated from
180 + Displayed Rotation
Alternatively, if the +1° to +179° (or the +91° to + 269°) scale is selected,
then the correct rotation will be displayed.
If, in the above example, the user is unsure whether the correct rotation is -
70° or +110°, then an additional measurement should be taken with a
different length of tube (e.g. half the length of the first tube). If the original
true rotation was -70° then the second reading will be -35°. Otherwise, if the
original rotation was +110°, then the second reading will be +55°.
If any range other than -89° to +89° is selected, then a
“+ r” will be displayed immediately after the °a scale
identifier code, i.e. “°a + r”. If a Multiplication factor
other than 1 has also been selected (see page 2-16), then
the scale code will be shown as “(°a+r) x 2.0”.
With an empty sample tube and, therefore, no rotation, the reading will be
displayed as approximately
0, 180 or -180
depending on which range has been selected. After the ZERO key has been
pressed, the display will temporarily show "0.00" and then revert to one of
the displays shown above.

Remote operation
Operation of the ADP440+ can be controlled remotely from a computer via
the RS232 Serial port. The 54-07 interconnecting cable optionally available
from Bellingham+Stanley will connect to the COM port of a typical PC. Use
a proprietary terminal program or custom software to send commands and
receive data.
The instrument default RS232 configuration is:

9600 Baud, 8 bits, no parity
Remote operation
Action Key ASCII Typical output data format
code
Each output data string is terminated by
CR+LF (ASCII 13+10)
Request the current reading ‘Return’ 13 96.75 Ok 'z nc 0.1od 25.6'C
Request the current reading in CSV R 82 96.75,Ok,’z,nc,0.1,25.6
format
Request software type & version, ‘Crtl’+R 18
instrument model and serial number 2 50 37-631-01 ADP440 No.PX05000
Only available when Mode menu is accessible (Methods not in use, see page 3-8)
Set scale to °a S 83 Scale(1..2)=?
1 49 Scale: 'a
Set scale to °z S 83 Scale(1..2)=?
2 50 Scale: 'z
Set TC to none T 84 TC(1..3)=?
1 49 TC: nc
Set TC to sugar T 84 TC(1..3)=?
2 50 TC: sc
Set TC to quartz T 84 TC(1..3)=?
3 51 TC: qc
Set Zero calibration C 67 Calibrate(Z/S)=?
Z 90 Zeroed
Set Span calibration C 67 Calibrate(Z/S)=?
S 83 Span Aim=?
<span value> <cr> Spanned
Start a drift run D 68 Driftrun, interval (secs)=?
<no of secs> <cr> Reading, Status, Scale, TC,
OD, Temp
97.06,Ok,'a,qc,0.1,25.3
97.06,Ok,'a,qc,0.1,25.3
97.06,Ok,'a,qc,0.1,25.3
97.06,Ok,'a,qc,0.1,25.3
97.06,Ok,'a,qc,0.1,25.3
97.06,Ok,'a,qc,0.1,25.3
End the drift run Any key Drift run finished
Help H 72 Serial Command Help
. . . . .
. . . . .
When the instrument receives a serial

command, the display will show:
When the action has been completed and the data sent, the instrument will
revert to the normal reading display.

RS232 serial port
The RS232 serial ports can be accessed via the 9 pin “D type” connectors on
the rear of the instrument. The interconnecting cable socket can be secured
with the 2 screws but these must be finger-tightened only – DO NOT OVER-
TIGHTEN..
9 Pin “D type” plug connections
Pin No. Function Data direction

Remote operation
2 Received data in
3 Transmitted data out
4 DTR In
5 Signal Ground
6 DSR Out

Sampling techniques
In order to achieve the maximum performance from the ADP440+ Series
polarimeter, it is essential that extreme care is taken with cleanliness of the
instrument and the polarimeter tubes. Allow the instrument to stabilise for at
Sampling techniques least 30 minutes after switching on before taking accurate readings.
Cleaning
Always empty and clean the polarimeter tube immediately after taking
readings. Remove the cover glasses and thoroughly wash and dry both the
tube and the glasses using an appropriate solvent (normally water with water
based samples).
It is essential that the tube and glasses are scrupulously clean and there are
no finger prints or marks on the glasses.
Wiping the tube and glasses occasionally with ethyl alcohol will remove any
residue of oils left from the samples. NEVER use acetone, white spirit, or
other aggressive solvents or any abrasive fluids on any painted surface or,
particularly, the membrane keypad panel.
Filling the tube

The cover glasses must be directly in contact with the ends of the tube
without any gasket material between them. The rubber washer must be
placed between the end cap and the cover glass. The end caps should be
lightly finger-tightened just enough to prevent leaking. Over tightening will
stress the glass which will cause optical rotation and measurement errors.
DO NOT OVER-TIGHTEN.
Centre bulb tube

Fit a cover glass to one end of the tube. Hold the tube vertically and
completely fill the tube to its end. Slide the second glass onto the tube end
and secure with the end cap. Hold the tube horizontally and rock to allow
any bubbles to enter the bulb so that it is not in the light path.
Centre filling tube and Centre filling tube with cup-shaped filler
Fit both cover glasses and, holding the tube horizontally, slowly fill the tube
through the centre filler. Gently rock the tube to allow any bubbles to
escape via the centre filler.
Funnel tube and Flow-through tube

These tubes are suitable when measuring a large number of similar samples.
The current sample is flushed through and replaced by the new sample. The
amount of sample required for this will depend on the type of sample and its
viscosity and can be determined by experimentation. If there is to be an
extended period before the next sample, the tube should be emptied,
cleaned and dried.

Cover glass stress
As stated above, excessive tightening of an end cap can cause stresses in the
cover glass which will cause optical rotation in the glass itself and so give a
measurement error. The reading displayed will be a combination of the
Sampling techniques rotation of the sample and the rotation in the glass. Careful assembly of the
tube should not cause a problem, however, any resultant rotation can be
eliminated by first setting Zero on the assembled, empty tube. This can be
done on all tube variants except for the ‘Centre bulb’ type.
The tube components must be thoroughly cleaned, dried and assembled.

Place the tube on the rails in the sample chamber and wait for stabilisation.
Press the Zero key. Fill the tube as described above without touching the end
caps. The displayed rotation will then be strictly related to the sample itself.
Temperature compensation
The optical rotation of any sample will vary with change in its temperature.
The amount of this change for a certain temperature variation will depend
on the sample type and nominal rotation. Typically:
• a sugar solution with a rotation of 100°Z at 20°C will decrease to
approximately 99.5°Z at 30°C
• a quartz control plate with a rotation of 100°Z at 20°C will increase
to approximately 100.14°Z at 30°C
Therefore, it is necessary to maintain the sample at a constant temperature

(usually 20°C) by using a water-jacketed tube or monitor the temperature of
the sample and correct for the change.
Temperature compensation can be selected to suit either sugar solutions

(sc) or quartz control plates (qc) which will correct the reading from the
temperature of the temperature probe to 20°C. That is, it allows the
polarimeter to run at ambient temperature but produces readings as if the
system was running at 20ºC.
Temperature compensation will only be valid if the detected sample

temperature is stable and the probe is at the same temperature as the
sample and so sufficient time should be allowed for the sample to stabilise
within the chamber. This will be simplified when using a centre filling tube by
removing the temperature probe from its holder in the chamber and placing
it in the tube centre arm so that it contacts the sample.
When using a B+S Quartz

Control Plate, the
temperature probe can be
placed in a Thermal Block
Assembly (code 34-241)
which is then clipped to the
body of the QCP.
Mechanically compatible ADP410 model shown

Flow-through and water-jacketed tubes
When using optional water-jacketed polarimeter tubes, the standard upper lid
should be replaced with a slotted type, see ‘Section 5, Accessories’.
Sampling techniques
The upper lid can be easily removed by unscrewing the hinge block retaining
screws using a standard 4mm Allen key.
The slots will allow the circulation hoses to exit the chamber and also ensure
that funnel tubes are held in an upright position. It is important that any
hoses connected to the tube must be sufficiently flexible not to pull the tube
off of the rails. It is essential that both tube support sleeves are firmly in contact
with the rails whilst a measurement is taken.

section 3
Setting up the system
Menu flow chart.......................................................... 3-1
Shortcut keys ............................................................. 3-3
Calibration.................................................................. 3-5
Calibration Standard values ................................ 3-5
Span calibration .................................................. 3-5
Cancel the last calibration ................................... 3-6
Calibration report................................................. 3-6
Calibration warning frequency............................. 3-7
Measurement settings................................................ 3-8
Which to use, the Mode menu or Methods?........ 3-8
To enable the use of Methods............................. 3-8
To disable the use of Methods (if using the Mode
menu) ................................................................. 3-8
Methods ..................................................................... 3-9
Adding a new method ......................................... 3-9
Editing an existing method .................................. 3-10
Hiding the preset methods .................................. 3-10
Method selection type ......................................... 3-11
Print a list of methods.......................................... 3-11
Reading limits...................................................... 3-12
Adding a limit test condition................................. 3-12
Editing or deleting a limit test condition ............... 3-12
User accessibility ....................................................... 3-13
User status .......................................................... 3-14
ID tags................................................................. 3-15
Security features ................................................. 3-16
Preset protection level......................................... 3-17
Setting the protection level .................................. 3-18
Adding a user ...................................................... 3-18
Editing an existing user ....................................... 3-18
21 CFR Part 11 .......................................................... 3-19
System settings.......................................................... 3-20
Setting the date format ........................................ 3-20
Adjust clock for summer (daylight saving) time ... 3-20
Set the clock time................................................ 3-20
Set the print mode............................................... 3-21
Available print formats......................................... 3-21
Select use of ports (serial 1 and parallel) ............ 3-21
Set the serial port configuration........................... 3-21
Using statistics print mode .................................. 3-22
Customising the instrument........................................ 3-23
Change the display layout ................................... 3-23
Change the reading response ............................. 3-23
Change the reading resolution ............................ 3-23
Adjust the display backlight and polarity ............. 3-24
Section 3 37-278’01 Rev. A January 2010 Setting up the system

Measurement traceability ........................................... 3-25
Batch codes ........................................................ 3-25
Using barcodes as batch codes .......................... 3-26
User codes .......................................................... 3-26
Adding extra scales.................................................... 3-27
Adding a standard scale...................................... 3-27
Adding a custom designed scale......................... 3-27
Adding a custom designed temp. compensation. 3-28
Special library scales ................................................. 3-29
Activating special library scales........................... 3-29
Specific rotation................................................... 3-30
Concentration...................................................... 3-32
Purity ................................................................... 3-34
% Inversion of sucrose solution........................... 3-36
% Change of product over a period of time ......... 3-38
Setting the default values........................................... 3-40
Displaying the software / hardware details................. 3-40
Section 3 37-278’01 Rev. A January 2010 Setting up the system

Menu flow chart
1. Span (Top
Menu Calibration) 1. Saved Results
2. Undo 2. System Log
3. Report 3. Setup Wizard…
4. Warning
Frequency 1. Use Methods
2. Hide Preset
1. Calibration 3. Selection Type
2. Tools 4. Print List…
3. Setup
4. Information 1. normal
5. Help 2. span
3. Add new…
4. Settings…
1. administrat. - 000
2. calibrator - 355
3. operator - 123
If methods are in use 4. Add new…
If methods are not in use

1. low
1. Methods 1. Manage Users… 2. medium
2. Users 2. Protection 3. high
3. Display
4. custom
4. Reading
5. System
1. Header
2. Temperature 1. no
3. OD 2. yes
4. Configuration
1. fast (2 sec)
2. medium (20 sec)
1. Response 3. slow (40 sec)
2. Resolution
3. Scales 1. low
4. Temp. Comps 2. medium
3. high
1. Add new…
1. english
2. french 1. Add new…
3. spanish
4. german
1. dd.mm.yy
2. mm.dd.yy
1. Date Format
2. Summer Time 1. no
3. Set Clock… 2. yes
1. none
2. printer
3. save
4. prt + save
1. Language 5. statistics
2. Time / Date
1. Printer 1. Mode
3. Communications
2. Serial Ports 2. Serial 1 1. none
4. Traceability
3. Parallel 2. 24 column
3. csv (lims)
1. 4800
1. Baud Rate 2. 9600
2. Word Length 3. 19200
4. 38400
1. off 1. 7 bit EP
2. number 2. 8 bit NP
3. text
4. dateinc 1. off
1. Batch Codes 5. barcode 2. number
2. Auto Increment 3. text
3. Log Users 4. login
1. off
2. on
Setting up the system 37-278’01 Rev. A January 2010 Section 3-1

Page 3-2 37-278’01 Rev. A January 2010 Setting up the system
Shortcut keys
Shortcut key functions can be activated when the Measurement Display is

shown. Press and hold down the key until the next screen is displayed.
Press and hold to:

Shortcut Keys
switch to
standby
Press and hold to:

adjust the backlight and
display polarity.

Calibration
The ADP440+ calibration can be set at two points:
Zero As described in section 2, the zero sets the low end of the
measurement range, to correct for the day-to-day minor
variations. This should be carried out simply with an empty
tube and, as such, can be performed at regular intervals;
even before every new sample measurement.
Span Sets the high end of the measurement range, using a Quartz
Control Plate, an accurately prepared sugar solution or
other sample of known value.
Calibration standard values

The span aim value must be entered in the scale units, as selected in the
measurement settings.
If the instrument’s measurement settings are being set using Methods then
the span method will automatically be selected when a span is being carried
out.
Span calibration
Calibration
press the Menu softkey

select 1. Calibration
select 1. Span (Top Calibration)
When requested, enter the Span sample value aim value. See ‘Calibration
Standard Values’ above.
In the bottom left of the aim point screen a note displays the current
measurement settings, so that the aim point units can be checked.
Place the sample into the sample chamber and close the lid.
Press ‘Enter’ to start the calibration.
Continuous readings will be taken until stable and then the calibration will be
corrected to the new value.

Cancel the last calibration
If the span calibration was carried out in error, e.g. an incorrect sample was
applied or the wrong value was entered, it can be cancelled.

select 2. Undo
press Yes
Calibration report
Display a report of the last Zero & Span calibrations.

select 3. Report
Calibration
press Print to optionally send the report to a printer.

Calibration warning frequency
If you require that the instrument is to be spanned every n days, the
instrument can be configured to automatically warn the user that a
calibration is now required.
The Warning Frequency menu item is only accessible to users with Setup
and Calibration rights.

select 4. Warning Frequency
type the number of days, enter 0 to disable
The warning will be displayed after a result is recorded (printed or saved).
Ø
Calibration
After the warning is acknowledged by pressing ‘Quit’ the instrument will

continue to function as normal. However the warning will continue to
appear following recording measurements until the instrument has been re-
spanned.

Measurement settings
The instrument’s measurement settings can be set in one of two ways.
Mode Menu A Mode menu is accessible from the Measurement
display. The mode menu displays the measurement
settings.
Methods Preconfigured Methods are chosen from the
Measurement Display.
Regardless as to how the measurement settings are selected the instrument
has the following measurement settings.
Scale (the scale units that the readings is displayed in)
Temp. Comp. (whether temperature compensation is used)
Limits (tests to check if the reading parameters are within set
limits, see page 3-12)
Multiplication (a factor the reading in multiplied by)
Range (determines which 180° range to display the reading)
Measurement
Which to use, the Mode menu or Methods?

If the complete range of product types that is to be measured on the
polarimeter requires the same measurement settings then ‘Mode Menu’
option would be most suitable. The mode menu is discussed further on
page 2-15.
However, if a number of products with differing settings are to be read, then
a method can be added for each of them. E.g. a range of essential oils could
be regularly measured in the °a scale and the display should show whether
each product reading value is within its set tolerance. The methods can be
given names that are easily identifiable by the operators such as:
Method name Low limit High limit
mint oil 10.9 11.3
lavender oil 9.8 10.5
orange oil 11.0 11.4
By default the measurement settings are changed using the Mode Menu.
To enable the use of Methods

select 3. Setup
select 1. Methods
select 1. Use Methods
select 2. Yes
To disable the use of Methods (if using the Mode menu)

select 3. Setup
select 1. Methods
select 4. Settings (Note: the selection number will change as
methods are added)
select 1. Use Methods
select 1. No

Methods
A method is a set of measurement settings options. This allows the
measurement settings to be changed quickly between frequently used
configurations. Initially, there are two methods set in the instrument:
normal for measuring samples
span the conditions used for a ‘span’ calibration
The span method does not contain the Range settings.
If the complete range of product types that is to be measured on the

polarimeter requires the same measurement settings then the ‘normal’
method can be selected and used for all samples. However, if a number of
products with differing settings are to be checked, then a method can be
added for each of them. E.g. a range of essential oils could be regularly
measured in the °a scale and the display should show whether each product
reading value is within its set tolerance. The methods can be given names
that are easily identifiable by the operators such as:
Method name Low limit High limit

mint oil 10.9 11.3
lavender oil 9.8 10.5
orange oil 11.0 11.4
Adding a new method

select 3. Setup
select 1. Methods
Methods
select 3. Add new… (Note: the selection number will change as

methods are added)
Enter the method name. This could be a common name such as mint oil or
orange oil, a trade name or a product reference code (but not a batch code,
it must identify a generic product type). The name can be a combination of
lower case letters, numbers and other characters.
Set each of the following parameters for the method:

Scale see page 2-16
Temp. Comp. see page 2-16
Limits see page 3-12
Multiplcation see page 2-16
Range see page 2-17
then Quit back to the Measurement Display.

Editing an existing method
select 3. Setup
select 1. Methods
select the method to be edited
To delete a method select option 5. or 6. which is Delete Method.
Hiding the preset methods

The instrument has 2 preset methods; ‘normal’ and ‘span’. If the
polarimeter will always be used with the normal method, i.e. one set of
conditions for all samples, and no other methods have been added, then the
Methods function can be disabled and the second softkey in the
Measurement display will be blank.
Alternatively, if a number of methods are created for a standard range of

products, e.g. mint oil, lavender oil, orange oil, and the normal method will
never be required, then it could be advantageous to hide ‘normal’ and ‘span’
from the Methods list. This will make it easier to select the method of
interest.
To achieve either of these,

select 3. Setup
select 1. Methods
methods are added)
Methods
select 2. Hide Preset

select 2. Yes

Method selection type
Before reading a sample, the relevant method should be selected by pressing
the Method softkey in the Measurement Display. This will show a list of all
available methods and the appropriate one can be selected.
However, if a large number of methods have been created, e.g. greater than
20, then it could be easier to select the required method by its index
number rather than scrolling through the list. To change the method
selection method,

select 3. Setup
select 1. Methods
methods are added)
select 3. Selection Type
select list or number
List selection type Number selection type
Print a list of methods

Methods
To print a list of all available methods with their index numbers,

select 3. Setup
select 1. Methods
methods are added)
select 4. Print List…

Reading limits
Reading Limits allows up to three test conditions to be set. If any of the
reading parameters values fall outside the limits then the reading is identified
as ‘fail’.
The three test conditions can be set to check any, or all, of the available
parameters. These are :
Reading value
Temperature
OD
Adding a limit test condition

Add a new method or select an existing method as detailed above, then
select 3. Limits
limits tests are added)
select the parameter 1. reading, 2. temp, 3. od
enter the Lower Limit
enter the Upper Limit
Example: A method has been configured with the scale set to °a and two
limits tests of:
Reading value; lower limit = 10.5 upper limit = 11.5
OD; lower limit = -0.1 upper limit = 1.2
If the Reading value is lower than 10.5 or higher than 11.5
or
the OD is less than –0.1 or higher than 1.2
Methods
then the reading will be recorded as ‘fail’ and displayed with a line
through it:
Editing or deleting a limit test condition

Select an existing method as detailed above, then
select 3. Limits
select the Limits test to be edited
change the parameter or limits as required
or
select 4. Delete

User accessibility
Access to the instrument functions can be restricted. The sophistication of
the protection can be set to match the operating environment.
The instrument has 3 preset protection levels…
low basic 3 digit PIN code are used
medium user is identified by username and a longer 4 digit PIN
high similar to medium but additional security features are
added which may require maintenance by the
administrator
In addition to the 3 preset options a custom option is available so that the
security features can be customised as required. See page 3-18 on how to
change the protection level.
The high protection level is suitable for use in 21 CFR part 11 compliant
systems.
Access to the ADP440+ functions can be restricted by providing users with
a PIN code (Personal Identification Number) which will allow them specific
rights. Initially, there are three User names with PIN codes preset in the
instrument.
The instrument will be supplied with the protection level set to low.
Accessibility
Rights
User Default
Mode/ Set Set Select Select
Name PIN
Methods Zero Span Tools Setup
administrator 000 Yes Yes Yes Yes Yes
calibrator 355 Yes Yes Yes No No
operator 123 Yes Yes No No No
Note: The length of PIN can be altered (see below), if the PIN length is
not 3 digits the default PIN codes will have the required leading
zeros, for example…
PIN Length PIN Code
3 135
6 000135
8 00000135
The PIN codes for the three preset Users can be changed but their rights
cannot be altered.
Up to 50 additional Users with their PIN codes can be entered. A PIN must
be must be unique, i.e. different to all existing PINs. The rights for the
additional users can be custom selected.
If the administrator PIN is set to all zeros (000), then the PIN system will be
disabled and all users will have unrestricted access.
If the operator PIN is set to all zeros (000), then there will be unrestricted
access to ‘Select Methods’.
CAUTION! Access to all the functions is only possible by the

administrator or user with full rights entering the correct PIN. DO NOT
FORGET IT!
In the event of the PIN being forgotten, contact Bellingham & Stanley Service
Department for assistance.
User status
Once a user has logged in, that user will remain logged until returning to the
Measurement Display. When returned to the Measurement Display the user
is kept logged in for a number of seconds after the last user interaction with
the instrument, for example key presses. The duration that the user is kept
logged in for is specified by the security feature ‘Keep Logged In’, by default
this is set to 30 seconds.
Keeping the user logged in allows for more efficient use of the instrument, as
they are not required to repeatedly log in whilst at the instrument.
There are potential security issues leaving the instrument logged in,
as unauthorised use of the instrument could occur. Therefore please
ensure that the ‘Keep Logged In’ feature is set appropriately for the
instruments working environment.
Accessibility
The current status (whether a user is logged in or not) can be viewed in the
header.
If a user is logged in a complete user If no user is logged in an empty user

icon will be displayed. icon will be displayed.
A user can be logged out by holding the left cursor key from the
Measurement Display.

ID tags
ID tags are used to wirelessly identify a user. ADP440+
instruments are fitted with a RFID (radio frequency
identification) reader at the top of the instrument’s body.
The instrument can read ID tags supplied by Bellingham +
Stanley (see page 5-2).
ID tags are read by placing the tag within 2 cm of the reader. ID tags are paired
to a user setup within the instrument. This enables the user to be identified and
logged in simply and quickly without the need for further authentication (PIN
and or username entry).
As ID tags alone will authenticate a user, please ensure that ID tags are
protected from misuse.
Pairing ID Tags
To pair a ID tag with a user, first select

the user from the User List.
The ‘Pair ID Tag’ value shows whether a

Accessibility
ID Tag has been paired, i.e. ‘none’ or

‘set’.
Select ‘Pair ID Tag’, the instrument will

now request that the relevant ID tag is
placed onto the reader.
If ‘Clear’ is pressed the current ID tag will

be unpaired from the selected user.
Using ID Tags
ID tags can only be read when the instrument is displaying the ‘Measurement
Display’, when a PIN or username is requested, or when specifically prompted
by the instrument.
To log in, read the user’s ID tag, a

message will be displayed briefly.
To log out, read the user’s ID tag a

second time.
Additional uses
When reviewing saved measurements, if a users ID tag is read in, only that users
measurements will be displayed. To view measurements from all users read the
users ID tag a second time.

Security features
The instrument has a range of security features. These are only generally
activated when the high protection level is selected, or they are activated
from the custom security level option.
Feature Settings Description
User pin only When required the user is
Selection identified by entering their PIN.
user and pin When required the user is
identified by entering their
username and PIN. This option is
more secure than ‘pin only’ as two
identifiers have to be entered.
PIN Length 3 to 8 digits The greater the number of digits,
the less the chance or a PIN being
guessed, however the PIN will be
harder to remember.
Max PIN Age 0 (off) to 255 days If set this specifies how often a PIN
must be changed. If the PIN is not
changed within this period the
account will become locked.
Remember 0 (off) to 255 mins This option specifies how long the
Last User instrument will remember the last
Accessibility
users for. If set the instrument will

remember the last entered user, so
the user will not have to re-enter it.
Reset PIN no / yes If selected the administrator will
Only only be able to Reset the PIN
rather than changing it. When a
PIN is reset the next time the user
logs in they will be requested to set
a new PIN.
Prohibit PIN no / yes If selected the instrument will
Recycling check when a new PIN is set that it
has not been used within the last 10
changes. This stops a user from
switching between frequently used
PINs.
User Lockout no / yes If selected the instrument will
automatically lockout the user if
they enter their PIN incorrectly
more than 5 times.
Fast PIN no / yes If selected the user will be able to
Change change their PIN without having
setup rights (which is required to
access the Users menu, where
PINs are usually changed).
Key
Some features are only selectable depending upon what User Selection is set
to. The table of features above is colour coded. The table below explains
this coding.
User Selection pin only
user and pin
either ‘pin only’ or ‘user and pin’

Preset protection level
As mentioned above the instrument has 3 preset protection levels.
low Instrument will request a PIN when entering the main menu.
User Selection ............................... pin
PIN Length ....................................... 3
Maximum PIN Age .........................off
Remember Last User ..................... no
Reset PIN Only............................... no
Prohibit PIN Recycling .................. no
User Lockout .................................. no
Fast PIN Change ............................ no
medium This preset improves security by requiring the user to type

their username and then their PIN. This preset does not have
features enabled that could increase the administration
overheads.
Accessibility
User Selection ..................user and pin

PIN Length ....................................... 4
Maximum PIN Age ......................... off
Remember Last User ............. 10 mins
Reset PIN Only............................... no
Prohibit PIN Recycling .................. no
User Lockout .................................. no
Fast PIN Change ............................ no
high This preset features all the security options set to

recommended levels required when using the instrument in a
21 CFR part 11 compliant environment.
User Selection ..................user and pin
PIN Length ....................................... 4
Maximum PIN Age ................120 days
Remember Last User ............. 10 mins
Reset PIN Only.............................. yes
Prohibit PIN Recycling ................. yes
User Lockout ................................. yes
Fast PIN Change ........................... yes

Setting the protection level
As mentioned above on page 3-17 the instrument has 3 preset protection
levels and a custom setting. To select the protection level…

select 3. Setup
select 2. Users
select 2. Protection
Select the required protection level. If custom is selected a menu will

appear allowing the individual security features to be selected.
Adding a user
The instrument can store up to 50 additional users.

select 3. Setup
select 2. Users
select 1. Manage Users…
users are added)
Accessibility
Enter the User name which can be a combination of lower case letters,
numbers and other characters.
Enter the Actual name which can be a combination of lower and upper case
letters, numbers and other characters.
Then enter the PIN code, see ‘Preset protection levels’ above for PIN
lengths.
If ‘User Selection’ is set to PIN only the PIN must be unique.
Then set the user’s rights.
Editing an existing user

select 3. Setup
select 2. Users
select 1. Manage Users…
select the user to be edited
then edit or delete the user as required.
Note:
If protection level is set to high (for 21 CFR part 11 use) the user will not
have the option to change their PIN from the Manage Users menu, however
the user can have their PIN reset. This will cause the instrument to request
that the user change their PIN when they next log in.

21 CFR Part 11
This instrument complies with the technical aspects of the FDA 21 CFR part
11 regulations. However the instrument is only a small part of the
compliancy. Standard operating procedures are required.
Instrument setup
See page
1. Protection level set to ...................................high 3-16
2. Log User set to.............................................login 3-24
3. Set the print mode ................................... printer 3-19
4. Select use of serial 1 ....................................... csv 3-19
5. Add necessary users 3-16
6. Reset administrators PIN 3-16
7. Log in as the administrator and set a new PIN
21 CFR Part 11
Administration
As the high protection level requires that PINs are changed regularly a SOP
will be required to educate staff, so that they follow your implementation of
21 CFR Part 11.

System settings
Setting the date format
The instrument can display the date in two formats, ‘dd.mm.yy’ (typically
UK) and ‘mm.dd.yy’ (typically US).
select 3. Setup
select 5. System
select 2. Time / Date
select 1. Date Format
Select the required date format from the list.
Adjust clock for summer (daylight saving) time

The instruments clock can easily be adjusted for daylight saving time (adding
one hour to the clock).
select 3. Setup
select 5. System
select 2. Summer Time
Select yes to advance the clock one hour, or no to turn back the clock one
hour.
Set the clock time

select 3. Setup
select 5. System
select 3. Set Clock…
Settings
Enter the time and date digits as shown. The clock will be updated when the
last digit is keyed.

Set the print mode
The fourth (right hand) softkey function in the Measurement Display can be
set to:
Mode Function Softkey
caption
none None; softkey disabled blank
print Print the last displayed reading to the selected printer Print
port
save Save the last displayed reading to the reading log Save
prt+save Print the last displayed reading to the selected printer Print
port and save it to the reading log
statistics Allows a group of up to 10 measurements to be Print
recorded and printed with a statistical analysis of
the data (see page 3-22)
To select the required mode:

select 3. Setup
select 5. System
select 3. Communications
select 1. Printer
select 1. Mode
Available print formats

This instrument can output data using either the serial port 1 and / or parallel
port. There are 2 formats available.
Format Description
24 column Optimised for use with a 24 column printer.
csv (lims) Designed for easy integration with a LIM system. Each value
is separated using commas.
Settings
Select use of ports (serial 1 and parallel)

If the print mode above is set to ‘printer’ then the instrument can be
programmed to output data via the serial 1 and parallel port.
select 3. Setup
select 5. System
select 1. Printer
select 2. Serial1 or 3. Parallel
select the desired print format
Set the serial port configuration

The serial port baud rate and word length can be set to suit the receiving
device:
select 3. Setup
select 5. System
select 2. Serial Ports

Using statistic print mode
This instrument has an optional statistical printout mode (see page 3-21).
This allows a group of up to 10 results to be temporarily logged together and
a statistical analysis carried out upon the results.
When Print is pressed and no previous results have been logged, the
instrument will request the traceability data (batch and operator details) if
selected. This information will be used to identify all of the measurements in
the group.
The diagram below explains the operation of the statistical printout.
Optional
Settings
Clears the statistics

Customising the instrument
The instrument can be customised to suit individual operating requirements
both in visual aspects, the layout of the screen & the amount of data
displayed, and operational settings.
Change the display layout

select 3. Setup
select 3. Display
The Header, Temperature, OD, and Configuration can be individually

selected to be displayed. If all four options are de-selected then the screen
will show only the reading and the softkey functions.
Change the reading response

The instruments measurement is the result of a running average of a number
Customisation
of measurements. The quantity of measurements the instrument averages

over effects the measurement response, stability, and reading time.
The greater the averaging, the better the stability, the disadvantage is a
slower response to a change in sample, and longer reading time.
The instrument has 3 response settings.
Response Time Description

fast 2 seconds Ideal for low resolution continuous flow
applications
medium 20 seconds A good medium, balancing reading time and
stability
slow 40 seconds Only necessary if displaying results to a high
resolution
To change the response setting…

select 3. Setup
select 4. Reading
select 1. Response
Change the reading resolution

select 3. Setup
select 4. Reading
select 2. Resolution
Medium is the normal resolution for the instrument.
High is one digit higher resolution
Low is one digit lower resolution

Adjust the display backlight and polarity
If the display is difficult to read, especially in either uncommonly bright or
dim ambient lighting conditions, it can be improved by adjusting the backlight
intensity or the display polarity. The instrument must be in the
Measurement Display screen.
Press and hold down the ‘Methods’ or ‘Mode’ softkey for approximately
three seconds. The Configure Display screen will show.
Customisation
Press 1, 2 or 3 for different levels of backlight intensity.

Press 0 to set the display polarity (invert the display).
Press ‘OK’ to use the new settings or ‘Quit’ to revert to the previous
condition.

Measurement traceability
All ‘Printed’ readings are recorded together with the measurement settings
selected and the time & date of the measurement. In addition, an optional
product batch code and a user code can be entered.
Batch codes
If a batch code is required, it can be either a number (in which case the keys
will only enter 0 – 9) or as text (the keys then having full alpha-numeric
capability).
Setting Description
off The instrument will not request a batch code.
number Number from 0 to 32000.
text 14 character alpha-numeric string.
dateinc auto increasing number from 0 to 9999, in the format of
yymmddnnnn
Example
0603117775 (11th March 2006, number 7775)
barcode first 14 character read from a barcode (see the following
page)
Traceability
If number is selected, an Auto Increment option is available which will then

offer a batch code which is one greater than the previous used batch code.

select 3. Setup
select 5. System
select 4. Traceability
select 1. Batch codes
If the Auto Increment option is required then

select 2. Auto Increment only available if Batch Codes is set to
‘number’

Using barcodes as batch codes
If a barcode reader is to be used (55-80 or 55-81) it has be to plugged in to
the instrument’s serial 2 port. With the instrument showing the
Measurement Display, scan in the barcode.
The display will briefly show ‘Result Printed.’ or ‘Result Saved.’ depending
upon printer type configuration.
If the printer type is set to ‘printer’ then the measurement will be printed,
showing the scanned in barcode number.
Traceability
User codes
When the user code option is selected, the user can be recorded in a
number of formats.

select 3. Setup
select 5. System
select 4. Traceability
select 3. Log users
Setting Description
off The instrument will not request a batch code.
number Number from 0 to 99.
text 24 character alpha-numeric string.
login Requires the user to login, as if they were accessing the
Main Menu.

Adding extra scales
As supplied, the ADP440+ can display readings in angle or ISS scales. Other
scales can be added to convert the readings to standard recognised units,
such as specific rotation, or company specific units pertaining to a particular
product.
Adding a standard scale

The following standard scales are held in a library in memory.
1. specif. rotation
2. conc. (g/cm3)
3. purity
4. % inv sucrose
5. % change

select 3. Setup
select 4. Reading
select 3. Scales
select 1. Add new…
select 1. From Library
Select the scale required from the list.
Extra scales
The scale will then be available when adding or editing methods.
Adding a custom designed scale

The readings can be converted to custom units using the following formule:
No. Equation
1 reading = A + Bx + Cx2 + Dx3 + Ex4 + Fx5
2 available later
where: x = rotation - Offset

A,B,C,D,E,F are polynomial constants

select 3. Setup
select 4. Reading
select 3. Scales
scales are added)
select 2. From Data
Enter the new scale name, (16 characters) e.g. mint oil
Enter the scale ID, (2 characters) e.g. mi
Enter the 6 constants A to F. Any constants not required, (e.g. E & F with a
4 term polynomial), should be set to 0.
Enter Offset (this can generally be 0)
Enter the Equation no. (e.g. 1)
Select the Number Format required for displaying and printing the reading.

The scale will then be added to the Scales List and can subsequently be
Altered or Deleted.
The scale will now be available when adding or editing methods.
Adding a custom designed temperature compensation

The readings can be temperature compensated for special temperature
coefficients using the following formule:
No. Equation
1 Corrected reading = Uncorrected reading
1 + ( A × ( x – 20 ) )
2 available later
where: x = sample temperature in °C

A,B,C,D,E,F are equation constants
The Corrected reading is converted to °z or another scale. Therefore, the

correction must also be calculated in rotation.

Extra scales
select 3. Setup
select 4. Reading
select 4. Temp. comps
scales are added)
Enter the new temp. comp name, (16 characters) e.g. mint oil
Enter the temp. comp ID, (2 characters) e.g. mi
Enter the 6 constants A to F. Any constants not required, (e.g. B to F with
equation 1) should be set to 0.
Enter the Equation no. (e.g. 1)
The temp. comp will then be added to the Temp. comps List and can
subsequently be Altered or Deleted.
The temp. comp will now be available when adding or editing methods.

Special library scales
The instrument has 5 special scales. Unlike traditional user defined scales
that use a multi-term polynomial that simply rescales the °a value, these
scales use additional data, and present the result in special measurement
display formats.
Scale Name Scale ID Description

specif. rotation sr Specific rotation, using a known
concentration
conc. (g/cm3) co Concentration, using a known specific
rotation
purity pu Purity, using a known brix value.
% inv sucrose pi % Inversion of sucrose solution
% change pc % Change of product over a period of
time
Activating special library scales

To add one of these scales press
Extra scales
select 3. Setup
select 4. Reading
select 3. Scales
scales are added)
select 1. From Library
select the desired scale from the list.

Specific rotation
The instrument can automatically calculate Specific Rotation. The scale can
be added to the scale list by adding it from the Scale Library menu (see page
3-29). Specific rotation is calculated using the formula shown below.
α D20
[α ] 20
D =
c
×l
100
where:
[α ]20
D is the specific rotation in angular degrees per dm and per g/cm3,
at 20°C and measured using a sodium ’D’ light source
α D20 is the optical rotation in angular degrees at 20°C and measured

using a sodium ’D’ light source
c is the concentration of in g/100cm3
l is the length of the polarimeter tube in dm
The International Commission for Uniform Methods of Sugar Analysis

(ICUMSA) have fixed values that should be used when working to the
International Sugar Scale (ISS).
Extra scales
c = 0.26010 g/cm3 = 26.0160g/100.00 cm3

l = 2.00000 dm = 200.000mm
This scale when added to the scale list defaults to the ICUMSA values.
When the specific rotation scale is activated 2 extra measurement settings
are made available.
When activated the measurement display will change to accommodate the

extra values associated with the specific rotation scale.

The concentration value can either be fixed to the value set in the
measurement settings or variable. When set to variable, if a measurement is
recorded (saved or printed) the instrument allows the concentration to be
changed (shown below).
The change whether concentration is fixed or variable press

select 3. Setup
select 4. Reading
select 3. Scales
select 1. specif. rotation (Note: the selection number might be
different, depending upon other scale already
added)
select 2. Alter
select 2. Conc. (g/100cm3)
Extra scales
select either fixed or variable from the list.
By default specific rotation measurements are displayed to the resolution

selected (see page 3-23). For example if medium resolution is selected the
specific rotation measurements will be displayed to 2 decimal places.
If necessary the specific rotation measurements can be displayed to a

different resolution, whilst still displaying all other scales to the selected
resolution.
To change the resolution of specific resolution measurements

select 3. Setup
select 4. Reading
select 3. Scales
select 1. specif. rotation (Note: the selection number might be
added)
select 2. Alter
select 1. Number Format
select the required number format.
The Number Format options are displayed as if the medium resolution has
been selected. Meaning that if low resolution is selected instead, the specific
rotation measurements will be displayed as the Number Format but with
one less decimal place.

Concentration
The concentration scale is selectable from the Scale Library menu (see page
3-29). Concentration is a rearrangement of the specific rotation formula,
however now, the unknown is concentration, below is the formula used.
α D20
c=
[α ]20D × l
where:
c is the concentration in g/cm3
[α ]20
D is the specific rotation in angular degrees per dm and per g/cm3,
at 20°C and measured using a sodium ’D’ light source
α D20 is the optical rotation in angular degrees at 20°C and measured

using a sodium ’D’ light source
When the specific rotation scale is activated 2 extra measurement settings

are made available.
Extra scales


The specific rotation value can either be fixed to the value set in the
recorded (saved or printed) the instrument allows the specific rotation to be

select 3. Setup
select 4. Reading
select 3. Scales
select 1. conc. (g/cm3) (Note: the selection number might be
added)
select 2. Alter
select 2. Specif. Rotation
Extra scales
By default concentration measurements are displayed to the resolution

selected (see page 3-21). For example if medium resolution is selected the
concentration measurements will be displayed to 2 decimal places.
If necessary the concentration measurements can be displayed to a different

resolution, whilst still displaying all other scales to the selected resolution.
To change the resolution of concentration measurements

select 3. Setup
select 4. Reading
select 3. Scales
select 1. conc. (g/cm3) (Note: the selection number might be
added)
select 2. Alter
select 1. Number Format
select the required number format.
The Number Format options are displayed as if the medium resolution has
been selected. Meaning that if low resolution is selected instead, the
concentration measurements will be displayed as the Number Format but
with one less decimal place.

Purity
This instrument has the facility to automatically calculate the purity of sugar
solutions. The value of purity is derived from the angular rotation of the
sample (supplied by the polarimeter), the mass concentration (brix) value
(supplied by a refractometer) and the density (derived from the brix value).
The refractometer reading can be entered into the ADP440+ either
manually by entering the value through the ADP440+ keypad or
automatically if the refractometer is an Bellingham + Stanley RFM
refractometer. As there are different methods used throughout industry for
calculating sugar purity, the ADP440+ has a number of settings which allow
the instrument to be setup using the appropriate calculation.
The general equation used to calculate sugar purity is shown below.
reading × purityconst
purity =
density × brix
where:
reading is the polarimeter reading in degree Z.
purityconst is a user definable purity constant.
density is calculated as a function of brix in accordance with the

Extra scales
ICUMSA Specification and Standard SPS-4 (1994).

brix is the brix value of the sample.
The purity scale is selectable from the Scale Library menu. When selected in
the measurement settings a Brix value, this is the default Brix value.
When the purity scale is selected in the measurement settings the

temperature compensation mode will be disabled, this is because when
purity is selected the instrument automatically uses sugar TC.

Purity Settings
The purity scale has a number of options.
Number Format 0.00 to 0.0000 Determines the format that the

purity value is displayed in.
Constant n Used to customise the purity
equation to match different
measuring methods.
Refractometer manual A default brix value will be available
from the measurement settings.
When a measurement is recorded
(saved or printed) the instrument
will allow this figure to be changed.
rfm The brix value is collected
automatically from a compatible
Bellingham + Stanley RFM
refractometer via the serial port 2.
All these settings are access by

select 3. Setup
select 4. Reading
Extra scales
select 3. Scales
select 1. purity (Note: the selection number might be
different, depending upon other scales
already added)
select 2. Alter
If the brix value is to be returned automatically from an RFM refractometer

please ensure that the instrument is set to read in the brix scale, and that the
serial configuration is 9600 baud, 8 bit even parity.
If using a RFM 300+ or RFM 800 it is necessary to disable the presser. This
stops the instrument from cancelling a measurement when the presser is
raised. To disable the presser, from the refractometers Measurement
Display
select 3. Setup
select 5. System
select 5. Temperature
select 2. Disable Presser

% Inversion of sucrose solution
The instrument can automatically calculate % inversion of sucrose solution.
The scale can be added to the scale list by adding it from the Scale Library
menu (see page 3-29). % inversion of sucrose solution is calculated using
the formula shown below.
%inversion = (rsuc − oA / l / c *158.874) /(rsuc − rinv) *100

where:
rsuc is the rotation in °A of non-inverted 15% Brix sucrose solution in
100mm tube
rinv is the rotation in °A of fully-inverted 15% Brix sucrose solution in
100mm tube
o
A is the rotation in °A of the sucrose solution
c is the concentration of sucrose in g/l
When the % inv sucrose scale is activated 2 extra measurement settings are
made available.
Extra scales



select 3. Setup
select 4. Reading
select 3. Scales
select 1. % inv sucrose (Note: the selection number might be
added)
select 2. Alter
select 1. Conc. (g/l)
Extra scales

% Change of product over a period of time
The instrument can automatically calculate % change of product over a
period of time. The scale can be added to the scale list by adding it from the
Scale Library menu (see page 3-29). % change scale is calculated using the
formula shown below.
%change =( oA * cstart / c − rstart ) /(rstart − rend ) *100

where:
o
A is the rotation in °A of the product sample
rstart is the rotation in °A of product sample in start state (e.g.
non-inverted)
rend is the rotation in °A of product sample in end state (e.g. fully
inverted) * cstart / cend
cstart concentration of product start state sample in g/l
cend concentration of product end state sample in g/l
c is the concentration of product sample in g/l
When the % change scale is activated 4 extra measurement settings are

Extra scales
made available.

extra values associated with the % change scale.


select 3. Setup
select 4. Reading
select 3. Scales
select 1. % change (Note: the selection number might be
added)
select 2. Alter
select 1. Conc. (g/l)
Extra scales

Setting the default values
If the instrument fails to start up correctly after switching on, or it is
functioning unexpectedly, it could be advisable to reset certain settings to
the original factory set (or default) values.
Unplug the instrument. Press, and hold down, the far left softkey (power)
and plug the instrument back in. Do not release the key until LED lights and
then goes out. When the key is released the screen will show…
Default values
Initially the two options will be set to ‘no’ and ‘none’. Select the settings that
you want to return to default values by setting them to show ‘yes’. The
‘Setup…’ option has further options within it. When set correctly press
‘Quit’.
The instrument will ask the user to confirm their choice. Selecting ‘Yes’ will
carry out the default.
Displaying the software / hardware details

If contacting B+S, or a local distributor regarding your instrument it is
advised to have the software and hardware details to hand. This information
can be viewed from the Information Menu.

select 4. Information
select 1. Software or 2. Hardware
Example software details Example hardware details

section 4
Specification
Performance........................................................ 4-1
Polarimeter tube.................................................. 4-1
Temperature........................................................ 4-1
Temperature compensation ................................ 4-1
Light source......................................................... 4-1
RS232 configuration............................................ 4-1
Physical............................................................... 4-1
Power requirements ............................................ 4-1
Specification 37-278’01 Rev. A January 2010 Section 4

Specification
Performance
Scale ºa - Angular ºz - ISS
-355 to +355 °
Range -225 to +225
selectable
Resolution 0.1 / 0.01 / 0.001
Accuracy (Sucrose solution @
0.01 0.03
20°C) (±)
Maximum OD for accuracy 3
Polarimeter tube
Maximum tube length 220 mm
End cap collar diameter 30 mm
Temperature
Ambient operating range 5 to 40 ºC
Storage -5 to 60 ºC
Specification
Temperature compensation
None -
Sugar 5 to 40 ºC
Quartz 5 to 40 ºC
Light source
Light emitting diode with interference filter 589 nm
Beam diameter, maximum 4 mm
RS232 configuration
Baud rate 9600
Word length 8 bits
Parity None
Physical
Length (polarimeter module only) 640 mm
Width (polarimeter module only) 340 mm
Height (polarimeter module only) 150 mm
Weight (including power supply) 9 Kg
Power requirements
Voltage 110 to 230 V~ ±10%
Frequency 50 to 60 Hz
Maximum current 200 mA
Specification 37-278’01 Rev. A January 2010 Page 4-1

section 5
Spares and accessories
Printers................................................................ 5-1
Barcode readers.................................................. 5-1
Interconnecting cables ........................................ 5-1
Quartz Control Plates .......................................... 5-1
Instruction manuals ............................................. 5-1
Spares................................................................. 5-1
Polarimeter tubes ................................................ 5-2
Upper lids ............................................................ 5-3
Power supplies.................................................... 5-3
Spares and accessories 37-278’01 Rev. A January 2010 Section 5

Spares and accessories
Printers Code
Dot matrix impact printer parallel: Euro version 230V 55-11
Dot matrix impact printer parallel: UK version 230V 55-12
Dot matrix impact printer parallel: US version 110V 55-13
Dot matrix impact printer serial: Euro version 230V 55-14
Dot matrix impact printer serial: UK version 230V 55-15
Dot matrix impact printer serial: US version 110V 55-16
See Spares below for printer spare parts
Barcode readers Code

230V version 55-80
110V version 55-81
Interconnecting cables Code

Printer serial (25way D type) 54-02
Printer parallel (25way D type to Centronics) 54-03
Computer (9way D type) 54-07
Quartz Control Plates Code

Quartz Control Plate nominal 100°Z (34.6°Angular) 34-20
Quartz Control Plate nominal 15°Z (5.2°Angular) 34-21
Accessories
Quartz Control Plate nominal –30°Z (-10.4°Angular) 34-22

QCP UKAS certificate of calibration traceable to PTB 90-803
Thermal Block Assembly 34-241
Instruction manuals Code

English 37-278
French 37-279
Spanish 37-280
German 37-281
Portuguese (Brazilian) 37-282
Spares Code
Paper for dot matrix impact printers Quantity: 20 55-91
Printer ribbon for dot matrix impact printers 55-93
ID tag pack Quantity: 3 22-071
Quantity: 10 22-072
Low strain cover glasses 15.5mm diameter. Quantity: 12 35-60

Rubber washers for use between cover glass and end cap.
Quantity: 12 35-64
End caps, plastic. Quantity: 2 35-68
Low volume tube spares (tubes 35-71 to 35-78 only)
Temperature sensor clip for low volume tubes 35-79
Low volume tube cover glasses Quantity: 6 35-80
Low volume tube sealing washers for use between cover glass and end cap.
Quantity: 10 35-81
Spares for flow-through and water jacketed tubes are available upon
request.
Accessories 37-278’01 Rev. A January 2010 Page 5-1

Polarimeter tubes
Type * Code no. shown Length Slotted Code
(mm) upper lid no.
Standard glass sample 100 Not 35-29 *
tube with bulb to clear 200 required 35-30
bubble from field of
view
Centre filling glass tube 100 Not 35-46
with straight central 200 required 35-47 *
arm for filling from
funnel or flexible tube
Centre filling glass tube 100 Not 35-57
with cup-shaped centre 200 required 35-58 *
filler to reduce risk of
spillage
Low volume 5 37-010 35-74
continuous flow- 10 35-73
through tube 25 35-72
50 35-71 *
Low volume 25 37-012 35-75
continuous flow- 50 35-76 *
through tube with water
jacket for temperature
control
Low volume 25 37-010 35-77
continuous flow- 50 35-78 *
Accessories
through tube for highly

acidic samples
Funnel flow-through 100 37-012 36-57
tube with water jacket 200 37-011 36-58 *
for temperature control
Large Funnel flow- 200 37-011 36-59 *

through tube with water
control
Continuous flow- 100 37-012 36-67

through tube with water 200 37-011 36-68 *
control
Centre-Fill tube with 100 37-010 36-77
water jacket for 200 37-009 36-78 *
temperature control
Page 5-2 37-278’01 Rev. A January 2010 Accessories

Upper lids
Type Code
no.
No slots 37-008
(as supplied)
2 slots 37-009
2 slots 37-010
4 slots 37-011
4 slots 37-012
Accessories
Power supplies Code

Power supply (unsealed) 110-230V 55-105
Mains lead for 55-105 with plug suitable for:
United Kingdom 61-191
Euro (Schuko) 61-193
United States 61-192
Switzerland 61-181
Denmark 61-182
India / South Africa 61-188
Australia 61-189
No plug – open lead 61-190
Power supply (waterproof): 110-230V without mains plug 55-250
Accessories 37-278’01 Rev. A January 2010 Page 5-3

Bellingham Stanley Refractometer Adp 440 Plus Manual 001

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ADP440+

Bellingham + Stanley Ltd. recognise all trademarks

© Copyright Bellingham + Stanley Ltd. 2010

Bellingham + Stanley Ltd. Bellingham + Stanley Inc.

Manufacturer's Name Bellingham & Stanley Limited

Manufacturer's Address Longfield Road,

declares that the product

Product Name ADP440+ Polarimeter

Model Number All

Is designed to conform to the following Product Specifications:

Supplementary The product herewith is designed to comply with the requirements

This symbol is an internationally agreed indicator that the product bearing it

Contents 37-278’01 Rev. A January 2010

Installing the instrument 37-278’01 Rev. A January 2010 Section 1

Mains cord wire colours

Switzerland 230V - - - 61-181

Installing the instrument 37-278’01 Rev. A January 2010 Page 1-1

• dry and indoors

Maximum current 200 mA

Power supply adapter 55-105

Page 1-2 37-278’01 Rev. A January 2010 Installing the instrument

Instrument description 37-278’01 Rev. A January 2010 Section 2

Upper lid: Sample chamber: ID tag reader:

Instrument description 37-278’01 Rev. A January 2010 Page 2-1

RS232 Serial port 1: RS232 Serial port 2:

Page 2-2 37-278’01 Rev. A January 2010 Instrument description

Operation status bar

Soft key functions

Arrow keys Alpha-numeric keys

Instrument description 37-278’01 Rev. A January 2010 Page 2-3

confirmation screen shows (approximately 2 seconds). Press Yes to switch

Note: It is preferable for the instrument to be left on continuously even if a

Switching on for the first time

Initially, it is a requirement to select the language.

Step 1 Setup the standard measurement conditions. These are the

Step 3 Set the printer options. Select whether readings are to be

Step 4 Pair ID tag to administrator. The instrument is supplied with 3

Page 2-4 37-278’01 Rev. A January 2010 Instrument description

The polarimeter is now ready for use.

It is recommended that in order to take accurate readings, allow a further 30

Instrument description 37-278’01 Rev. A January 2010 Page 2-5

pressing the Up/Down softkeys and then pressing Select

Return to the Measurement display by repeatedly pressing Quit to step back

Page 2-6 37-278’01 Rev. A January 2010 Instrument description

E.g. To enter the name cola(74) press:

the d key 3 times c

Key Available characters

Instrument description 37-278’01 Rev. A January 2010 Page 2-7

Fixed decimal point Scientific

Page 2-8 37-278’01 Rev. A January 2010 Instrument description

Instrument description 37-278’01 Rev. A January 2010 Page 2-9

Blocked light path

Grey result display

Page 2-10 37-278’01 Rev. A January 2010 Instrument description

Instrument description 37-278’01 Rev. A January 2010 Page 2-11

OD 0.0 = 100% light transmission, no absorption in the sample

Page 2-12 37-278’01 Rev. A January 2010 Instrument description

24 column print format

At the start of the printout is a header. This contains general information

Reading stable Not yet stable Light path blocked