PMI Positive Material Identification
PMI Positive Material Identification
PMI Positive Material Identification
Introduction
Scope
Reference Documents
Equipment
Surface Preparation
Testing Procedure
Traceability
Acceptance Criteria
Reporting
1. Introduction
This procedure specifies the process of carrying out PMI for identification of grade
of alloy steel materials using XRF analyzer.
2. Scope
To carry out Positive material identification using X-ray Fluorescent (XRF)
technology. It is to measure the concentration of elements without causing any
damage to the component being examined.
Equipment used for doing PMI is Delta Professional Analyzer DPO 2000 having
Sr.no.540915
3. Reference documents
User manual of Delta Family: Handheld XRF Analyzer DPO 2000
Reference material part number 100039 standard coin is used to verify the
performance of XRF Analyzer.
4. Equipment
The equipment used is XRF Analyzer DPO 2000 for verification of elements
composition in various types of materials. The instrument is a fully portable
analyzer with an integrated display to view spectra and save data.
This equipment can measure the following elements
5. Surface preparation
The surface shall be free from oil, dirt, paint, scale etc. that affects the result.
Usually a light grinding or power brush is sufficient in probe seating area if not
bare metal.
6. Testing procedure
Instrument Calibration
Prior to analysis, the Instrument shall be calibrated to a known standard
reference and representative to the alloy type to be tested and confirmed.
Various standard reference alloy composition is provided by the equipment
manufacturer.
Instrument Operation Turn
“ON” the instrument
Select Analyze on the Main Menu screen
Input Data
7. Measurements
Place probe on the material / sample to be tested and press the trigger keeping
the probe on the sample / material during the entire measurement.
The measurement on the test / sample will indicate with the time and the elapsed
measurement time on completion of the analyzing of the test item.
The display will indicate the composition on each element in percentage with
deviation and also the common alloy detected, i.e. 316/ 304/ etc. Measurements
will be stored in the Instrument memory. Stored measurement data can be
printed for evaluation and reporting.
8. Traceability
Item tested should be identified and indicated in test report.
9. Acceptance criteria
The minimum elements to be tested for each type of alloy shall be as per material
reference specification.
The element shall meet the requirement of applicable material specification to
determine acceptance.
Deviation allowed: AS per ASME 2011a SECTION I / ASME BPVC I.2015 B-8.2 &
ASME BPVC B-8.4.1
10. Reporting
Standard inspection report format. See attached appendix I.