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    Title: Process Validation Report of Stress Relieving: 1. Abstract

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    Corrosion Factory
    The document is a process validation report for stress relieving at Mythri Metallising Pvt Ltd. It details the installation, operational, and performance qualification tests conducted. The tests verified that the stress relieving process meets specifications of heating to 600°C ± 20°C for 2.5 to 3 hours and then cooling to 200°C at a rate of 50-80°C/hour. All qualification tests were reviewed and their results approved, validating the stress relieving process.

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    Title: Process Validation Report of Stress Relieving: 1. Abstract

    Uploaded by

    Corrosion Factory
    353 views3 pages
    The document is a process validation report for stress relieving at Mythri Metallising Pvt Ltd. It details the installation, operational, and performance qualification tests conducted. The tests verified that the stress relieving process meets specifications of heating to 600°C ± 20°C for 2.5 to 3 hours and then cooling to 200°C at a rate of 50-80°C/hour. All qualification tests were reviewed and their results approved, validating the stress relieving process.

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    PV @ MMPL

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    The document is a process validation report for stress relieving at Mythri Metallising Pvt Ltd. It details the installation, operational, and performance qualification tests conducted. The tests verified that the stress relieving process meets specifications of heating to 600°C ± 20°C for 2.5 to 3 hours and then cooling to 200°C at a rate of 50-80°C/hour. All qualification tests were reviewed and their results approved, validating the stress relieving process.

    Copyright:

    © All Rights Reserved
    Download as DOC, PDF, TXT or read online from Scribd
    Download as doc, pdf, or txt
    353 views3 pages

    Title: Process Validation Report of Stress Relieving: 1. Abstract

    Uploaded by

    Corrosion Factory
    The document is a process validation report for stress relieving at Mythri Metallising Pvt Ltd. It details the installation, operational, and performance qualification tests conducted. The tests verified that the stress relieving process meets specifications of heating to 600°C ± 20°C for 2.5 to 3 hours and then cooling to 200°C at a rate of 50-80°C/hour. All qualification tests were reviewed and their results approved, validating the stress relieving process.

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    © All Rights Reserved
    Download as DOC, PDF, TXT or read online from Scribd
    Download as doc, pdf, or txt
    of 3

    TITLE: PROCESS VALIDATION REPORT OF STRESS RELIEVING

    1. ABSTRACT
    This report contains the test results for qualifying the STRESS RELIEVING processed at MYTHRI
    METALLISING PVT LTD

    2. TEST OBJECTIVE
    To qualify the STRESS RELIEVING process carried out at MYTHRI METALLISING PVT LTD

    Substrate Material: SG 600/3

    3. REFERENCES
    General process validation guidelines 9001:2015.

    4. INSTALLATION QUALIFICATION (IQ):


    During installation of the equipment following parameters were checked.

    Sl. No Equipment/Resources Specification Requirement Records

    Heat treatment 5000mm*3000mm*2500mm Calibration


    1 Calibration
    furnace (LxWxH) report

    ID No.: MMPL_Furnace_01

    Maintenance
    2 Low density oil tank 1000 litres tank Oil to be upto checklist
    minimum level

    Range: Max 800°C Calibration


    3 Thermocouple Calibration
    report
    ID No.: MMPL_TC_02

    1
    4.1 Calibration requirements:

    Details of all the Equipments/Instruments used during the process,

    Sl. No. Equipment/Instrument Identification Calibration due date

    1 Heat treatment furnace MMPL_Furnace-01 25 Nov 2021

    2 Thermocouple MMPL_TC_02 25 Nov 2021

    3 2 Channel Data Loggers DAS/MDL/01 30 Dec 2021

    4.2 Training Needs:

    PROCESSES

    Loading on Temperature Burner feed LDO level Furnace Graph extraction


    Sl no Operator Name
    trolley reading control checking Maintenance

    1 Raghavendra      

    2 Danbahadur      

    3 Bijay Roy      

    5.0 OPERATIONAL QUALIFICATION (OQ):

    Sl. No. Operation Characteristics Specification Observation Results

    50°C to 80°C per hour 50°C to 80°C per


    1 Heating Temperature Verified & found ok
    till 600°C is reached hour

    Temperature 600°C ± 20°C 600°C ± 20°C Verified & found ok


    2 Soaking
    Time 2 ½ hours to 3 hours 3 hours Verified & found ok

    Furnace 50°C to 80°C per hour


    3 Temperature 200°C Verified & found ok
    Cooling till 200°C is reached

    2
    5.1 Following are the parameters which is followed during the process,

    Sl. No. Method Specification

    1 Heating 50°C to 80°C per hour till 600°C is reached

    2 Soaking 620°C ± 20°C for 2 ½ hours to 3 hours

    3 Furnace Cooling 50°C to 80°C per hour till 200°C is reached

    5.2 Work Instruction / Standard Operating Procedure (SOP)

    Sl no Process Work Instruction No. \ Sop No.

    1 Stress Relieving Cycle WI/SRC/ACE


    6.0 PERFORMANCE QUALIFICATION (PQ):

    Sl no. Requirements Evidence Result Remarks

    1 Stress Relieve Cycle Stress Relieving cycle report Acceptable Verified & found ok

    Following test details have been attached,


    1. Stress Relieving Cycle Report

    IQ / OQ / PQ REVIEW:

    Description Yes No
    All tests meet the pre-determined acceptance criteria YES -
    All IQ test report sheets have been reviewed and approved YES -
    All OQ test report sheets have been reviewed and approved YES -
    All PQ test report sheets have been reviewed and approved YES -

    Title: Validation protocol for Stress Relieving of Ferrous materials.


    Revision no: R0
    Part list are available in attached annexure.
    Written by Signature Date Effective Date

    Raghavendra 11 Apr 2021

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