Cleanliness, Particle Counting (Fuel Systems) Rev 13
Cleanliness, Particle Counting (Fuel Systems) Rev 13
Standards
Engineering Standard Number
Name CLEANLINESS,PARTICLE COUNTING (FUEL SYSTEMS)
Abstract
This specification covers requirements for the cleanliness level of fuel systems components and
test methods.
Table of Contents
Abstract .....................................................................................................................................1
Table of Contents ......................................................................................................................2
1. Scope....................................................................................................................................4
2. Applicable Documents.........................................................................................................4
3. Definitions............................................................................................................................4
Figure 1: Fiber .....................................................................................................................6
4. Specifications.......................................................................................................................8
4.1. Significance and Use ...................................................................................................8
4.2. General Rules for Cleanliness Testing.........................................................................9
Table 1: Size Classes for Particle Counting (Test Methods IV, V, VI Only) ...................10
Table 2: Definition of Contamination Level.....................................................................11
4.3. Acceptance Criteria by Test Method .........................................................................12
Table 3: Acceptance Criteria for Gravimetric Analysis (Test Methods II, III) .................13
Table 4: Cleanliness Class Level Defined by Contamination Level/Size Range ..............14
4.4. Properties of Hard Particles .......................................................................................14
5. Additional Requirements ...................................................................................................16
5.1. Residual Magnetism ..................................................................................................16
5.2. Laboratory Approval..................................................................................................16
5.3. Preproduction Parts....................................................................................................16
5.4. Preservation Requirements ........................................................................................16
6. Reference Readings ...........................................................................................................16
Appendix A: Guidelines for Determination of Cleanliness Class /Test Method.....................17
A1. Cleanliness Class ................................................................................................17
Table A1: Guidelines for Cleanliness Class and Test Method Application ......................18
Table A2: Guidelines for Application of Test Methods ....................................................20
Table A3: Suggested Drawing Notes by Example/Situation.............................................22
A2. Suggested/Template Drawing Notes ..................................................................21
Appendix B: General Requirements Test Environment/Equipment/Reagents........................24
Table B1: Equipment, Apparatus, and Reagent Requirements by Test Method ...............25
Appendix C: Test Method I (Visual Examination)..................................................................27
C1. Sampling ....................................................................................................................27
C2. Test Method ...............................................................................................................27
Appendix D: Test Method II (Flush and Brush with Gravimetric Analysis) ..........................28
D1. Contaminant Extraction .............................................................................................28
Appendix E: Test Method III (Ultrasonic with Gravimetric Analysis) ...................................29
E1. Contaminant Extraction .............................................................................................29
Table of Contents
1. Scope
This specification is primarily intended for, but not limited to fuel system components. This
specification covers requirements for the cleanliness level of components and assemblies
processed for, processed by, or supplied to Cummins Inc., Cummins Inc. suppliers or Cummins Inc.
partners. This standard is normally used in conjuction with manufacturing practices found in
CES 18316: Cleanliness Workmanship.
2. Applicable Documents
Applicable documents listed below may be obtained from the respective organizations listed in
CES 10054, Standards Organizations Addresses.
3. Definitions
Terms used in this standard that have a general definition for usage in Cummins Engineering
Standards are defined in CES 10056, Glossary.
As received from supplier refers to components in the condition or state of arrival from an
external supplier.
3.2. Assembly
Assembly refers to a part that contains two or more components which have been fitted together to
form an intermediate of final part number.
A bought out finished part is a part received from a supplier which requires no further machining
or other alteration. These parts are typically washed after receiving and prior to assembly.
The cleanliness class level is an alphabetic code which is typically called out on a Cummins part
drawing. Typical designations can be: AAA, AA, A, B, or V. The cleanliness class level is
comprised of a contamination level number in each particle size category.
Cognizant engineering organization refers to the engineering organization within Cummins that
has design authority over the parts being processed.
Cognizant quality organization refers to the quality assurance organization within Cummins Inc.
that is allied with the cognizant engineering organization and has audit, review and approval
authority over the process and quality control plant for the parts being produced.
The collection system typically consists of the following components: pumps, filters, solvent
reservoir, spray gun able to spray clean rinsing fluid at a known and controlled flow rate.
Contamination level is a number ranging from 00-24 that represents a high and low limit of particle
counts for a given size category of particles. A higher contamination level indicates more particles
are present in that particular size category.
3.10. Fiber
A fiber is an irregular shaped non-metallic soft particle (natural or synthetic) with a large length/
diameter ratio for example > 30:1. Debris which is defined as a fiber shall be an individual fiber
which is straight and not tangled with itself or other material. Fibers which are tangled will be
considered particles. Fibers may intersect with other fibers.
Figure 1: Fiber
Patch saturation is a calculated ratio of particle surface area to overall filter surface area. Analyzing
filter patches by optical microscope becomes difficult and will produce more measurement
variability when the % patch saturation exceeds 1.5% for foamed membranes and 3% for uniform
mesh type membranes.
Hard particle/debris is defined as particle/debris, but with the added qualities of having high
hardness as opposed to organic or fibrous debris. Examples of hard particles/debris include, but not
limited to metal chips, abrasive grit, sand, or stiff plastics.
The membrane filter is used to collect debris for the various test methods defined by this
specification. For the purposes of this specification, the membrane is 47 mm in diameter, TMTP,
SVLP, or SMWP filter type (these are filter code designations available through Millipore Corp.)
and has a mean pore size of 5 microns or less.
a. The TMTP filter code designates 5.0 micron pore size patch made of
polycarbonate material
b. The SVLP filter code designates a 5.0 micron pore size patch made of PVDF material
c. The SMWP filter code designates a 5.0 micron pore size patch made of mixed cellulose
ester material
Particle counting system is setup to size and count the collected particles on the membrane filters
using a microscope. Setup usually consists of a microscope system with motorized stage, a digital
camera, and image analysis software.
3.15. Particle/Debris
Particle/debris are removable with specified conditions and possessing mechanical cohesion to a
part or substrate.
The rinsing liquid is defined by the terms of this specification to be a fluid filtered through a
1.0 micrometer or finer filter. A test liquid of low viscosity (≤ 5 mm2/s) and having the capability
of removing (or dissolving) oil and grease is recommended. Fluid is required to meet the
background cleanliness requirements described in ISO 16232-3:2007, Section 6.3.3: Blank Value
prior to use for cleanliness testing.
4. Specifications
4.1. Significance and Use
4.1.1. This specification covers requirements for the cleanliness of components, test methods,
and acceptance limits.
4.1.2. This specification shall not be used unless the engineering drawing or in-process
documentation contains requirements for the following:
4.1.3. Guidelines for cleanliness class and test method are in Appendix A: Guidelines for
Determination of Cleanliness Class /Test Method on page 17.
4.1.4. Test environment, equipment, and reagents shall be in accordance with Appendix B:
General Requirements Test Environment/Equipment/Reagents on page 24.
4.1.5. The frequency for auditing part(s) according to this specification shall be determined
by quality control plan documentation issued by the cognizant quality organization of part in
question or upon request from Fuel Systems Business Unit Materials Engineering Organization.
4.1.6. Components which contain internal filters should be flushed both in the direction of
flow and the reverse direction of flow during the cleanliness evaluation. An example component
would be a high pressure connector with an internal edge filter.
a. Properly drying a membrane filter to prepare for particle extraction (for Test Methods II
and III only)
b. Extracting particles from the test part(s) or fluid sample onto a sample membrane filter
c. Properly drying the membrane filter for analysis
d. Counting, measuring the sizes, and/or weighing of particles on the filter membrane
e. Examination of filter membrane for hard particle (class AA Cleanliness Class Level only)
f. Evaluation of the test results
g. Accepting or rejecting the part(s)
h. Documenting and distributing results
4.2.2.1. Parts shall be free from dirt, manufacturing debris, paint, grease, scale, grit, corrosion,
smut, soot, and any other foreign substance. Particle counts on test parts shall not exceed the
requirements of 4.2.3. Class Cleanliness Requirements on page 10. Heat temper film, corrosion
inhibitors, coatings and marking/identification substances are permitted if documented in a plan
approved by the cognizant quality organization of the purchasing plant. Components with
corrosion inhibitors and coatings applied shall meet the applicable cleanliness class, particle count,
and particle size requirements.
4.2.2.2. For Test Methods II, III, IV, V, and VI, all particles/fibers which are captured on the
prepared test membrane filters shall be counted and reported. However, upon written agreement
between cognizant engineering and quality organizations of supplier and purchaser membrane
filters containing single fibers which do not intersect each other may be excluded from the total
particle counts of the membrane filter. The purchaser and supplier shall also agree on the definition
of a fiber as well, but typically a fiber can be defined as non-metallic and having a high length to
width ratio. When particle counting the standard patch as specified in Appendix B: General
Requirements Test Environment/Equipment/Reagents on page 24 item g., if the patch exceeds
60,000 total particles, it is recommended that the patch should be discarded and another test should
be performed using a smaller sample size for better particle counting accuracy.
4.2.2.3. The following tables are taken from ISO 16232-10 and are accurate as of the 2007
edition. If a dispute emerges between supplier and purchaser of the accuracy of Table 1: Size
Classes for Particle Counting (Test Methods IV, V, VI Only) on page 10 and Table 2: Definition
of Contamination Level on page 11 what is stated in the current revision of ISO 16232 takes
precedence over Table 1: Size Classes for Particle Counting (Test Methods IV, V, VI Only) on
page 10 and Table 2: Definition of Contamination Level on page 11 of this engineering standard.
Table 1: Size Classes for Particle Counting (Test Methods IV, V, VI Only)
B 5 X < 15
C 15 X < 25
D 25 X < 50
E 50 X < 100
F 100 X < 150
G 150 X < 200
H 200 X < 400
I 400 X < 600
J 600 X < 1000
K 1000 X
Taken from ISO 16232-10 (2007 Edition)
Up to and Contamination
More Than
Including Level
0 0 00
0 1 0
1 2 1
2 4 2
4 8 3
8 16 4
16 32 5
32 64 6
64 130 7
130 250 8
250 500 9
500 1 x 103 10
1 x 103 2 x 103 11
2 x 103 4 x 103 12
4 x 103 8 x 103 13
8 x 103 16 x 103 14
Up to and Contamination
More Than
Including Level
16 x 103 32 x 103 15
32 x 103 64 x 103 16
1 x 106 2 x 106 21
2 x 106 4 x 106 22
4 x 106 8 x 106 23
8 x 106 16 x 106 24
Particles larger than 0.5 mm shall not exceed 4 particles within 2000 mm2/20 cm2. In addition,
particles larger than 1.0 mm shall not exceed 1 particle within 2000 mm2/20 cm2. No particles shall
exceed 2 mm in any dimension.
4.3.2. Test Methods II, III-Flush and Brush and Ultrasonic Method
(Appendix D: Test Method II (Flush and Brush with Gravimetric Analysis) on page 28,
Appendix E: Test Method III (Ultrasonic with Gravimetric Analysis) on page 29)
Table 3: Acceptance Criteria for Gravimetric Analysis (Test Methods II, III)
Size >=
6 *µm- 15 µm- 25 µm- 50 µm- 100 µm- 150 µm- 200 µm- 400 µm- 600 µm-
1000
Range 15 µm 25 µm 50 µm 100 µm 150 µm 200 µm 400 µm 600 µm 1000 µm
µm
Size Class B C D E F G H I J K
Class B 20 19 18 16 14 12 10 9 8 3
Class A 17 16 15 13 11 9 8 6 5 0
Class AA 16 14 13 11 8 7 5 2 0 00
total
particles
Class 12 11 10 9 7 6 2 0 00 00
AAA
Test Methods IV, V, VI
Notes:
*Size Class B (6 µm-15 µm) is specified as (5 µm-15 µm) in ISO 16232.
**Hard particles see Section 4.4. Properties of Hard Particles on page 14.
As stated in Section 3. Definitions on page 4 hard debris can be metal, sand, stiff plastic or the like.
Examination of hard particles should be done visually on a routine basis and shall be done with
incidental (top down) lighting under a microscope. The referee method in case of dispute will be
Scanning Electron Microscope (SEM)/Energy Dispersive Spectrometer (EDS) analysis which will
determine the exact chemical signature of the debris particle. Examples of hard debris include but
are not limited to metallic pieces, sand/abrasive media, or other. Some visual qualities of hard
particles are as follows.
a. Shiny/reflective appearance
b. Sharp edges
c. Solid
d. May be magnetic
e. May be gray or silver in color
f. Chemical signature: predominantly iron or aluminum based alloys or others
g. Not easily breakable upon handling with tweezers under microscope
4.4.3. Others
a. May be spalled hard coatings (Diamond Like Carbon, TiN, Nitrided white layer or the like)
b. Glass-filled polymers
c. Not easily breakable upon handling with tweezers under microscope
5. Additional Requirements
5.1. Residual Magnetism
All components shall meet the acceptance requirements for residual magnetism in accordance with
the engineering drawing, prior to cleanliness testing. A maximum of 5 gauss is required for
cleanliness testing.
The supplier’s laboratory shall be reviewed and approved by Cummins Supplier Quality
Improvement (SQI) Organization. Image analysis equipment and particle counting method shall be
qualified through the Production Part Approval Process (PPAP).
Unless otherwise approved by the Cognizant Engineering Organization, preproduction parts (parts
prior to PPAP and parts for PPAP approval) shall be supplied in the cleanliness condition specified
for the finished part (at time of assembly) on the drawing and with a test report of cleanliness
testing results.
Parts shall be preserved from corrosion before and after cleanliness testing. Parts shall be dried and
preserved with an accepted preservation method after cleanliness evaluation.
6. Reference Readings
The following references were used in the preparation of this standard.
Table A1: Guidelines for Cleanliness Class and Test Method Application
Applicable
Class Class Application
Test Method
Table A1: Guidelines for Cleanliness Class and Test Method Application (Continued)
Applicable
Class Class Application
Test Method
Class B This classification should be used on debris sensitive II, III, IV, V,
“Functionally components and fluid contacting components in the unfiltered VI
Clean” upstream of the fuel circuit. This classification should also be
used on components in the oil circuit. Typical components
include tappets, tappet springs, and tappet spring retainers.
Class V This cleanliness level applies to parts that are not in the fluid I
“Visually path of debris sensitive parts. Typical components include
Clean” fasteners or external parts of the fuel system.
III May be used for in-process control for BOF components. For
(Appendix E:) measurement of cleanliness on all surfaces of the component.
“Ultrasonic Component
Cleanliness”
IV Pressurized spray inspection method used for surfaces that are in the
(Appendix F:) “line of sight” or easily accessible. This method is also applicable to
any parts which contain internal passages for which cleanliness is to
“Pressurized Spraying” be measured. Typical parts where this test method shall be called out
on the print include: fuel filter, spin-on/cartridge fuel filters, fuel
lines, fuel rail, fuel pump, etc. This method is the preferred method
of evaluation for most critical fuel wetted Fuel Systems parts.
a. Testing requires an environment that would be satisfactory for operating high precision
balances and microscope.
b. Components that are intended for testing shall be handled with forceps or lint-free gloves.
c. Cleanliness class level of parts for test shall be maintained prior to test and cross
contamination of groups of parts shall be avoided with plastic polyethylene bags of
adequate size.
d. No paper products such as bags, box, towels, etc. shall be used in test lab environment.
e. Room Environment shall conform to at least class 8 level of cleanliness of airborne
particles per ISO 14644.
f. Calibration of all measuring equipment should be performed on a periodic basis as per
quality control plan.
Applies to
Item
Test Method
a. Particle Counting System and software capable of reporting in the optional II
ISO 16232 format. Microscope capable of accurately detecting 6 or and III,
greater µm particles, adjustable lighting, high resolution, high speed IV, V,VI
motor stage, and other features, as needed, to determine/compare the
dimensions of particles with the limits of this specification. The
microscope should conform to the requirements of ISO 16232-7.
b. Analytical laboratory balance that can accurately weigh filter membranes II, III, IV, V,
in the expected range of weights with a percent error of less than or equal VI
to 10%.
c. Mechanical vacuum pump capable of maintaining a vacuum on the filter II, III, IV, V,
apparatus of 85 kPa/25 inches of mercury. VI
d. Drying oven capable of maintaining a temperature of 100 ºC II, III, IV,
(212 °F) minimum V,VI
e. Filter flask, not less than 0.5 L capacity. (Method II and III) II, III, IV,
V,VI
f. Filter holder for 47 mm Millipore filter membranes II, III, IV,
V,VI
g. The filter membrane shall be selected to be compatible with the chosen II, III, IV,
rinsing liquid. Nominal pore size of the filter membrane shall be smaller V,VI
than the smallest particle size to be counted/sized, See Section 3.
Definitions on page 4.
h. Glass slides or specially designed filter membrane holder to capture filter II, III, IV,
membranes for particle counting. V,VI
i. Stainless steel forceps and tweezers suitable for handling filter II, III, IV,
membranes and components. V,VI
j. Bench top ultrasonic cleaning equipment with a frequency of 30-50 kHz III
and a minimum power of 13 W/Liter.
Table B1: Equipment, Apparatus, and Reagent Requirements by Test Method (Continued)
Applies to
Item
Test Method
k. Non-shedding bristle brush. The brush material shall not be detrimental to II
the surface of the part. The diameter of the brush material shall be a
minimum of 10% greater than the hole it is being used to clean.
l. Optical Measurement Equipment: The minimum criteria for I, II, III
measurement equipment is the capability to measure particles at a 10x
magnification. This equipment may be a stereo microscope or other
microscope equipment; this equipment may also be an eye piece capable
of measuring to 10x. In cases of dispute, the referee measurement
equipment shall be a 40x measurement done by the Cognizant
Engineering Organization lab.
m. Rinsing liquid shall be in accordance with the following: II, III, IV,
Does not leave residue V,VI
Maximum of 0.1 mg of contamination per volume used for one test
Rinsing liquid has to be compatible with the component as well as the
extraction and filtration equipment, including all seals and filters used.
Note: Envirosolv 655 or similar solvent is a recommended rinsing liquid
and can be purchased from Fine Organics Corporation. Reclaimed solvent
from vendors shall not be used. Alternatively Neutracare/Neutrapon 5088
can be used as rinsing liquid for Test Method IV, V, VI and can be
purchased from Henkel Technologies.
n. Collection System (Stainless Steel Spray Funnel-Method IV and/or flow IV, V, VI
or functional test stands-Method V, and VI)
o. Clean rinsing media should be at least 2 or better contamination level II, III, IV, V,
numbers cleaner/better than the level indicated for the part/assembly to VI
be tested.
Note: This test method describes the number of particles allowed per a 20 cm2 test area.
C1. Sampling
Sampling for Test Method I shall be in accordance with the following: The minimum number of
parts for each test should be sufficient to provide a total applicable component surface area of
testing greater than or equal to 8000 mm2 (80 cm2) for the test.
This test method is not suggested for final cleanliness evaluation prior to assembly. This test
method may produce variation higher than acceptable and will be difficult to validate as a
cleanliness process.
D1.2. A test filter membrane shall be dried for 1 hour at 66 °C ± 3 °C (151 °F ± 5 °F) and pre-
weighed prior to filtering collected rinsing liquid. The surface as shown on the engineering
drawing or in-process documentation shall be flushed, brushed and rinsed at least twice with
rinsing liquid. Rinsing liquid shall be collected in a clean sampling tray, beaker or similar lab
apparatus. Collected rinsing liquid with debris shall be filtered through the dried filter membrane.
D1.3. Upon extraction of debris, the membrane shall be prepared according to the
requirements in Appendix I: Filter Membrane Preparation on page 34, and analyzed according to
the requirements in Appendix J: Filter Membrane Analysis on page 35.
E1.2. Parts shall be fully immersed in rinsing liquid inside a beaker within bench top ultrasonic
cleaning equipment with a frequency of 30-50 kHz and a power level of 13 W/liter as specified in
Table B1: Equipment, Apparatus, and Reagent Requirements by Test Method on page 25. The
level of the liquid in the ultrasonic equipment shall not be lower than the level of the solvent within
the beaker containing the parts. The following parameters shall be controlled during this process:
E1.3. Upon completion of ultrasonic cleaning, tested parts should additionally be rinsed for a
few seconds with standard laboratory squirt bottle with additional rinsing liquid into the beaker.
E1.4. A test filter membrane shall be dried for 1 hour at 66 °C ± 3 °C (151 °F ± 5 °F) and pre-
weighed prior to filtering collected rinsing liquid. Rinsing liquid shall be collected in a clean
sampling tray, beaker or the like. Collected rinsing liquid with debris shall be filtered through the
dried filter membrane. Upon extraction of debris, the filter membrane shall be prepared according
to the requirements in Appendix I: Filter Membrane Preparation on page 34, and analyzed
according to the requirements in Appendix J: Filter Membrane Analysis on page 35.
Note: The primary use of Test Method IV is to measure the cleanliness of components and the
results are normally expressed in particles per a given surface area.
F1.2. Background cleanliness of the rinsing liquid and collection system shall be determined,
documented, and controlled. Prior to any evaluations, the funnel shall be rinsed at the start of shift
or after 2 hours of idle time. Background contamination should be kept to a level consistent
acceptable level according to what is stated in ISO 16232-3 Section 6.
F1.3. The calculated flow rate from the rinsing nozzle shall be 4L/minute ± 10%. The rinsing
liquid spraying pressure at the 3 millimeter diameter spray gun exit orifice shall be 207 ± 69 kPa
(30 ± 10 psi). The operating conditions of the spray system shall be maintained and monitored
periodically to assure a consistent (i.e., ± 10%) rate of flow from the exit orifice of the spray gun.
The rate of flow (i.e., L/min) from the exit orifice of the spray gun shall be determined,
documented, and monitored. The rate of flow from the exit orifice of the spray gun shall be re-
determined/re-verified prior to use whenever there are changes to the spray system (i.e., new or
replacement hoses, orifice pump, spray gun, filters in the spray system). The minimum spraying
time per part shall be sufficient to deliver a minimum of 0.11 mL/mm2 to the part surfaces. If
multiple parts are required to make the minimum surface area requirement of 8000 mm2 (80 cm2)
the calculated spray time shall be split evenly between all parts used in the test.
F1.4. The filter membrane (refer to Table B1: Equipment, Apparatus, and Reagent
Requirements by Test Method on page 25, item g.) used for the particle/debris collection shall be
documented and controlled.
F1.5. The suction pump below the collection system filter holder should be set to minimize
“ponding” of rinsing liquid above the filter patch on the spray funnel.
F1.6. Parts shall be individually sprayed. However, it is permissible to have all of the parts for
the individual test in the funnel at the same time. After individually spraying the part(s) for the
required individual time(s), completely spray the inside of the funnel (and any internal funnel
fixture) and part(s) for a sufficient amount of time as to wash the liberated debris from the part(s)
down into the collection filter membrane.
F1.7. Upon extraction of debris, the membrane shall be prepared according to the requirements
in Appendix I: Filter Membrane Preparation on page 34, and analyzed according to the
requirements in Appendix J: Filter Membrane Analysis on page 35.
F1.8. In the event that meeting the method IV standard pressure and flow is not possible, an
alternative setup and process may be validated using ISO 16232:2007, Section 6.2 Extraction
Procedure Set-up and Validation.
Note: The primary use of Test Method V is to measure the cleanliness of an assembly that has
internal mechanics that can generate its own fluid pressure/flow i.e., high pressure pumps, low
pressure pumps. This test method shall be used to measure the cleanliness of the fluid which is
expelled from a fuel pump. Alternatively, this test method may also be used to determine fluid
cleanliness within a production process, such as wash fluids or calibration fluids for audit purposes.
G1.2. The fluid sample pulled directly from the test stand or washer tank shall be collected in
a clean sampling tray, beaker or the like. Collected rinsing liquid with debris shall be filtered
through the filter liquid. The filter liquid (refer to Table B1: Equipment, Apparatus, and Reagent
Requirements by Test Method on page 25, item g.) used for the particle/debris collection shall be
documented and controlled.
G1.3. Upon extraction of debris, the membrane shall be prepared according to the
requirements in Appendix I: Filter Membrane Preparation on page 34, and analyzed according to
the requirements in Appendix J: Filter Membrane Analysis on page 35.
Note: The primary use of Test Method VI is to measure the internal cleanliness of components. The
results are typically expressed as particles per a given internal surface area or volume of the part.
H1.2. The preferred test method is to use in line collection thru membrane holder.
(ISO 16232-4 and 5.1.3 a) This method allows for contaminant collection without having to handle
fluid containers and conduct the filtration process under vacuum.
H1.3. An alternative method (ISO 16232-4 and 5.1.3 b) is to collect the liquid at the outlet of
the filter under test in a clean container and filter it on membrane(s) using a vacuum pump. The
extraction fluid shall be filtered on a filter membrane as specified in Table B1: Equipment,
Apparatus, and Reagent Requirements by Test Method on page 25, item g. using vacuum pump
and vacuum flask. Great care should be taken in that the collection container should be clean prior
sampling the fluid.
H1.4. Sampling for Test Method VI shall be in accordance with the following: The appropriate
fluid volume collected during particle extraction shall be determined by performing an extraction
validation procedure as stated in ISO 16232-3, Section 6.2 Extraction Procedure Setup and
Validation. Once the appropriate parameters have been established, they can be used for future
testing of that part. The flow rate during contaminant extraction should be set at the rated/nominal
flow of the test piece as stated on the individual part print.
H1.5. Upon extraction of debris, the membrane shall be prepared according to the
requirements in Appendix I: Filter Membrane Preparation on page 34, and analyzed according to
the requirements in Appendix J: Filter Membrane Analysis on page 35.
The membrane(s) shall be dried for 1 hour, preferably in an oven, as specified in Table B1:
Equipment, Apparatus, and Reagent Requirements by Test Method on page 25, item d. and
weighed. The filter membrane shall be dried again for at least again 15 minutes and weighed again
until two successive weight readings are within ± 5% of each other. Drying temperature and time
should be documented in the test report.
After filter membrane preparation, if gravimetric analysis of the filter membrane is being
performed as required by methods II and III, record the weight measurement using an analytical
balance as specified in Table B1: Equipment, Apparatus, and Reagent Requirements by Test
Method on page 25. The length and width of the largest hard particle shall be recorded in
micrometers and checked against the appropriate cleanliness class in the table. Acceptance Criteria
for Gravimetric Test Methods in Section 4.3. Acceptance Criteria by Test Method on page 12.
Debris type shall be noted, i.e., metal shavings, metal fines, fibers or plastics.
If particle counting analysis will be performed as required by test methods IV, V, and VI, the filter
membrane will need to be flattened out as much as possible in preparation for microscopic particle
counting analysis. Some common ways to achieve this are to:
a. Sandwich the membrane between two clean glass slides and tape together, or
b. Load membrane onto an appropriately designed filter membrane holder which can be
loaded onto the microscope. Option 1 is the preferred method.
The sizes and numbers of particles on the filter membrane shall be measured and counted using the
particle counting system specified in Table B1: Equipment, Apparatus, and Reagent Requirements
by Test Method on page 25, item a. for every particle size category given in the specified
cleanliness class level requirement.
If the rinsed debris on filter membrane are too numerous such that particles overlay and touch one
another, the overloaded filter membrane shall be discarded and a set of new filter membranes shall
be generated. Alternatively, some particle counting softwares calculate a % patch saturation. The
recommended patch saturation value is < 2%.
Extraction fluid should be filtered using several membranes and counts added together.
After analysis, the filter membranes shall be preserved in a manner that permits recounting for a
period of time approved by the Cummins SQI Organization or manufacturing plant
quality organization.
Reference slides with a documented and/or certified count are required for internal use for periodic
checking of particle count results. Counts shall be within 10% of documented and/or certified value
each time it is checked. The reference slides shall be checked in a frequency consistent with the
quality control plan. The default timeframe is once per week.
All reports shall be saved and archived electronically and/or by hard copy per the time period
specified by facility’s Quality System requirements.