Mixing& Blending: Hetrogenius To Homogenius
Mixing& Blending: Hetrogenius To Homogenius
Mixing& Blending: Hetrogenius To Homogenius
OBJECTIVE-(Hetrogenius to Homogenius)
Mixing& Blending
AGITATION:- Agitation (action), putting fluid into motion by shaking or stirring,
often to achieve mixing.
An agitator is a device or mechanism to put something into motion by shaking or
stirring.
Purpose of agitation:
Intensification(An intensification is an increase in strength or magnitude (or
intensity) of transport processes in agitated batch(heat and mass transfer)
Preparation of materials of required properties(suspension, emulsion)
Mixing: Mixing may be defined as a unit operation that aims to treat two or more
components, initially in an unmixed or partially mixed state, so that each unit
(particle, molecule etc.) of the components lies as nearly as possible in contact
with a unit of each of the other components
BLENDING :means to mix smoothly and inseparably together during which a
minimum energy is imparted. The terms MIXING and BLENDING are commonly
used interchangeable in the pharmaceutical industry.
Bafle-A device used to restrain the flow of a fluid, gas, etc. Tank baffles are small
vertical paddles(short pole) added to the sides of mixing tanks to improve mixing
Baffles are always used in turbulent flow systems (low viscosity fluids)
e.g. coal ash and cement are blended in a specified ratio to produce Pozzocrete
cement. In other cases, a chemically homogenous material may be mixed to
produce a uniform lot of a desired weight/volume with consistent particle size
distribution, color, texture, and other required attributes(Ice cream,paint &dyes)
Mixing and Blending are the most demanding unit operations in the
chemical process industries. Industries such as pharmaceutical and
foods also rely heavily on mixing and blending technology. Some
common examples are as follows.
Types of mixtures
. Positive mixtures - Positive mixtures are formed from materials such as gases or
miscible liquids which mix spontaneously and irreversibly by diffusion, and tend
to approach a perfect mix.
• Negative mixtures- With negative mixtures the components will tend to separate
out. If this occurs quickly, then energy must be continuously input to keep the
components adequately dispersed, e.g. with a suspension formulation, such as
calamine lotion.
Mixing& Blending
Importance of Mixing Technology
Mixing is a critical process because the quality of the final product and its
attributes are derived from the quality of the mix.
The wide variety and ever increasing complexity of mixing processes encountered
in industrial applications requires careful selection, design, and scale up to
ensure effective and efficient mixing. Improved mixing efficiency leads to shorter
batch cycle times and operational costs.
MODERN MIXERS:-
A mixer is no longer a generic production tool, but a critical and decisive business
tool. This is because profitability and competitive advantage are dependent upon
subtle improvements in Product Quality through gains in mixing performance and
efficiency.
Considering the large industrial operations requiring the blending of bulk solids,
there is a wide range of blender technologies available. Depending on the
principle, mechanism of mixing, blenders is classified as follows:
IMPELLERS
Impellers are THE COMPONENT OF THE MIXER WHICH IMPARTS FLOW.
Their purpose is to transfer the energy driven by the motor to the
contents of a tank as quickly and efficiently as possible. ... Selecting an
impeller based on the unique needs of the application is vital in ensuring
the production of an equal mixture,
The impeller is the component of a mixer that does the actual
mixing and produces the results. That's because when it rotates, it
creates fluid flow and shear
This can be used to combine materials in the form of solids, liquids and
gas .
Mixing& Blending
The impellers are classified into two types, axial and radial, depending on the
angle that the impeller (also known as agitator) blade makes with the plane of
impeller rotation.
Axial Flow Impellers: The impeller blade makes an angle of less than
90° with the plane of impeller rotation. As a result the locus of flow
occurs along the axis of the impeller (parallel to the impeller shaft)
AXIAL FLOW PATTERNS
Axial flow impellers have an up and down flow pattern, ideal for
applications where solids suspension or stratification is a challenge.
The flow pattern produced by typical axial flow impeller produces an
excellent top to bottom motion when the agitator is center mounted, and
the vessel is fully baffled (see Fig 1B). If the baffles are removed, the
fluid in the vessel will swirl and vortex resulting in a rather poor mix.
Mixing& Blending
AXIAL FLOW IMPELLERS
Propeller: The propeller is typically used in mixers that are small and portable.
This type of impeller tends to be heavy and quite expensive in larger sizes.
A propeller is a device with a rotating hub and radiating blades that are set at a pitch to
form a helical spiral, that, when rotated, exerts linear thrust upon a working fluid, such as
water or air.
Pitched Blade:( to set up and fix firmly in place) A pitched blade impeller is
used when a balance of flow and shear is required. It is especially useful in
applications where 2 or more liquids are blended, and is well suited for
situations with low bottom clearance or low liquid submergence.
Mixing& Blending
Hydrofoil: The hydrofoil impeller offers the best high flow design. It is known
for its low turbulence, and is excellent for shear sensitive applications.
The hydrofoil is a 3 bladed high efficiency impeller. ... It is known for its
high efficiency because it is able to produce the greatest amount of flow per
horsepower in the spectrum of Mixer Direct's line of mixing blades.
The impeller blade in radial flow impellers is parallel to the axis of the
impeller. As a result, the radial-flow impeller discharges flow along the
impeller radius in distinct patterns.
Axial flow impellers cause the tank fluid to flow parallel to the impeller's axis of
rotation while radial flow impellers cause the tank fluid to flow perpendicular to
the impeller's axis of rotation.
What is radial flow and axial flow?
For high-viscosity materials, the mixing regime changes from one in which
turbulence dominates (as in liquid agitators) to one in which viscous drag forces
dominate. Moreover, some materials exhibit Non-Newtonian behavior. A non-
Newtonian fluid is a fluid whose flow properties are not described by a single
constant value of viscosity. Therefore mixing of such material requires special
heavy duty mixers. These include:
· Double Arm Mixers,· Planetary Mixers&· Dual and Triple Shaft Mixers
Mixing Equipment
Radial-flow impeller
· Radial Flow Impellers: The impeller blade in radial flow impellers is parallel to
the axis of the impeller. As a result, the radial-flow impeller discharges flow along
the impeller radius in distinct patterns.
It is axial flow ,high speed impeller for liquids of low viscosity&effective in large
vessels.
Mixing& Blending
B)Paddles-( a short pole with a broad blade at one end) .
Radial-flow impeller
Fig.Pitched-blade turbine
Mixing& Blending
Solid-solid mixing::
Solid-solid mixing: This is the process in which two or more than two solid
substance are mixed in a mixer by continuous movement of the particle.
Mechanism of mixing in solids: 1- convective mixing (macro mixing) In the case
of convective mixing material in the mixer is transported from one location to
another. This type of mixing process will lead to a less ordered state inside the
mixer, the components which have to be mixed will be distributed over the other
components
Convective mixing is the mixing of solid particles in which groups of particles are
moved from one position to another.
Liquid-liquid mixing::
a – axial-flow pattern, baffled vessel, b – radial-flow pattern, baffled vessel, c – tangential-flow pattern,
unbaffled vessel
VORTEX
a mass of air or water that spins aroundveryfast and pulls objects into its empty
centre &is a dangerous or bad situation in whichparticle become more and
more involved and from which particle cannot escape:
Mixing& Blending
b)able to describe the mechanisms of mixing and their effect on mixing time;
Screw Mixers
Working principle
First step is charging of mixer from the top, manually or vide pneumatic or mechanical conveying.
After the mixer is charged the mixing process starts. The mixing is carried by means of 3 distinct
intermixing actions:
1) The screw agitator, turning on its axis, produces a lifting action as it spirals the materials in
an upward flow.
2) At the same time, orbiting the tank, the screw removes material away from the wall and
deflects it into the centre of the tank.
3) Material lifted by the screw gravitates downward, thoroughly intermixing with material being
spiraled upwards.
The typical speed of the central screw is 70 to 80 Rpm. The Tip speed can fluctuate from 1 to 3 m/s.
The result is most intimate intermingling of all ingredients. The mixing time is depending on product
characteristics, mixing accuracy and batch size.
Applications
Vertical ribbon blenders are generally used in case of applications that require gentle mixing action
and minimal heat generation at the same time these mixers can also be used for applications that
requires high shear mixing this is accomplished using lump breakers, which is driven separately.
Tumble blender-
A tumble blender is available in a variety of geometries, the most common being the V-shaped or double-
cone configurations. The vessel is partially loaded with product and rotated at operating speeds in the
range of 5 to 25 revolutions per minute. Diffusion is the main mechanism for mixing: batch materials
cascade down, distributing particles over a freshly exposed surface as the vessel rotates on a horizontal
axis.
Mixing& Blending
V-shaped blender
In a V-shaped blender, the batch is continuously being split and recombined. In order to take advantage
of this mixing and flow pattern, raw materials are generally loaded to the vessel in layers rather than side
by side. Tumble blending is very low-impact and appropriate for processing abrasive solids. It is also
commonly used in making precise blends containing trace components (<1%) or ingredients that are
vastly dissimilar in size and density.
The geometry of the V-shaped and double-cone vessels allows complete discharge of the blended
material. Both designs however require a large footprint to accommodate the mixer base, as well as
ample overhead space for the vessel to rotate. In certain installations, this type of equipment is operated
from within a dedicated room to ensure safety.
CONSTRUCTION
WORKING PRINCIPLE
APPLICATIONS
Mixing& Blending
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Sigma Mixer
The sigma blade mixer is a commonly used mixer for high viscosity materials. This article details the construction of the sigma
mixer, design and operational features, and its applications. The different variants of the sigma mixer design are discussed.
The sigma mixer is one of the most popular used for mixing and kneading high viscosity materials. It belongs to the
family of double arm kneader mixers.
In mixers handling very viscous materials, it is necessary to promote both lateral and transverse motion of the material. The
geometry and profile of the sigma blade is designed such that the viscous mass of material is pulled, sheared, compressed,
kneaded, and folded by the action of the blades against the walls of the mixer trough. The extent to which this happens depends
on the action of the blades - tangential or overlapping and the ratio of the speed of rotation of the blades.The helix angle of the
blade can be modified depending on the required shearing.
Mixing& Blending
In the tangential design, the blades rotate in the trough meeting tangentially as shown in figure 2. The front blade generally
rotates faster than the rear blade usually in the ratio of 3:2. Tangential blades are generally used for material of higher viscosities
such as adhesives, rubber compounds, flush colors, dyes, and pigments.
In the overlapping design, the blades overlap above the saddle of the container. The overlapping
blade configuration is shown in figure 3. Due to the overlapping action it is necessary that the relative position of the two blades
is unchanged, and as a result, both the blades rotate at the same speed. Materials that flow freely or creep down into the blades are
mixed using the overlapping blade action. This design offers a faster interchange of material from one blade compartment of the
mixer to the other. Overlapping blade action is used for materials of lighter viscosities such as carbon pastes, clay coating,
creams, and ointments. The overlapping blade produces a lower kneading and shearing compared to the tangential blade action.
The tilting discharge arrangement is most common. The tilting arrangement of the container may be designed for manual
operation or may be mechanized using motorized or hydraulic arrangement.
Mixing& Blending
For materials of lower viscosity, the bottom discharge valve may be provided on the mixer trough.
The design profile of the valve should be flush with the mixer trough to avoid any dead or unmixed pockets of material).
The extruder/screw discharge has an advantage that materials can be directly discharged,
extruded, in the required shape or size for further processing. In addition, the screw design eliminates operator exposure to hot
materials if the mixing processes are carried out at high temperatures and/or with materials that are toxic in nature.
o Adhesives
o Biscuit dough
o Butyl rubber
o Carbon pastes
o Ceramics
o Chemicals
o Chewing gum
o Crayon and pencil lead
o Explosives
o Fiberglass resin doughs
o Food and confectionery products
Mixing& Blending
In the tangential design, the blades rotate in the trough meeting tangentially as shown in figure 2. The front blade generally
rotates faster than the rear blade usually in the ratio of 3:2. Tangential blades are generally used for material of higher viscosities
such as adhesives, rubber compounds, flush colors, dyes, and pigments.
In the overlapping design, the blades overlap above the saddle of the container. The overlapping
blade configuration is shown in figure 3. Due to the overlapping action it is necessary that the relative position of the two blades
is unchanged, and as a result, both the blades rotate at the same speed. Materials that flow freely or creep down into the blades are
mixed using the overlapping blade action. This design offers a faster interchange of material from one blade compartment of the
mixer to the other. Overlapping blade action is used for materials of lighter viscosities such as carbon pastes, clay coating,
creams, and ointments. The overlapping blade produces a lower kneading and shearing compared to the tangential blade action.
The tilting discharge arrangement is most common. The tilting arrangement of the container may be designed for manual
operation or may be mechanized using motorized or hydraulic arrangement.
Mixing& Blending
For materials of lower viscosity, the bottom discharge valve may be provided on the mixer trough.
The design profile of the valve should be flush with the mixer trough to avoid any dead or unmixed pockets of material).
The extruder/screw discharge has an advantage that materials can be directly discharged,
extruded, in the required shape or size for further processing. In addition, the screw design eliminates operator exposure to hot
materials if the mixing processes are carried out at high temperatures and/or with materials that are toxic in nature.
Adhesives
Biscuit dough
Butyl rubber
Carbon pastes
Ceramics
Chemicals
Chewing gum
Crayon and pencil lead
Explosives
Fiberglass resin doughs
Food and confectionery products
Mixing& Blending
In the tangential design, the blades rotate in the trough meeting tangentially as shown in figure 2. The front blade generally
rotates faster than the rear blade usually in the ratio of 3:2. Tangential blades are generally used for material of higher viscosities
such as adhesives, rubber compounds, flush colors, dyes, and pigments.
In the overlapping design, the blades overlap above the saddle of the container. The overlapping
blade configuration is shown in figure 3. Due to the overlapping action it is necessary that the relative position of the two blades
is unchanged, and as a result, both the blades rotate at the same speed. Materials that flow freely or creep down into the blades are
mixed using the overlapping blade action. This design offers a faster interchange of material from one blade compartment of the
mixer to the other. Overlapping blade action is used for materials of lighter viscosities such as carbon pastes, clay coating,
creams, and ointments. The overlapping blade produces a lower kneading and shearing compared to the tangential blade action.
The tilting discharge arrangement is most common. The tilting arrangement of the container may be designed for manual
operation or may be mechanized using motorized or hydraulic arrangement.
Mixing& Blending
For materials of lower viscosity, the bottom discharge valve may be provided on the mixer trough.
The design profile of the valve should be flush with the mixer trough to avoid any dead or unmixed pockets of material).
The extruder/screw discharge has an advantage that materials can be directly discharged,
extruded, in the required shape or size for further processing. In addition, the screw design eliminates operator exposure to hot
materials if the mixing processes are carried out at high temperatures and/or with materials that are toxic in nature.
Adhesives
Biscuit dough
Butyl rubber
Carbon pastes
Ceramics
Chemicals
Chewing gum
Crayon and pencil lead
Explosives
Fiberglass resin doughs
Food and confectionery products
Mixing& Blending