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Extraction and Identification of Oleoresin From Siling Labuyo

Siling labuyo (hot chili pepper) was extracted using a reflux method with ethyl alcohol over 30-35 minutes to 1 hour. The solution was filtered and evaporated, leaving a reddish-orange residue of oleoresin. The oleoresin contains capsaicin and other compounds that give siling labuyo its pungency, aroma, and solubility in alcohol and ether. It has uses as an irritant, digestive aid, and seasoning.

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90 views

Extraction and Identification of Oleoresin From Siling Labuyo

Siling labuyo (hot chili pepper) was extracted using a reflux method with ethyl alcohol over 30-35 minutes to 1 hour. The solution was filtered and evaporated, leaving a reddish-orange residue of oleoresin. The oleoresin contains capsaicin and other compounds that give siling labuyo its pungency, aroma, and solubility in alcohol and ether. It has uses as an irritant, digestive aid, and seasoning.

Uploaded by

Avox Everdeen
Copyright
© © All Rights Reserved
We take content rights seriously. If you suspect this is your content, claim it here.
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Download as DOCX, PDF, TXT or read online on Scribd
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Semifinal

EXTRACTION AND IDENTIFICATION OF OLEORESIN FROM SILING


LABUYO

● Siling labuyo (25g)


● Ethyl alcohol (75 mL)
● Reflux - method of extraction (30 to 35 minutes - 1 hour)
● Filter
● Evaporate (syrup consistency) (evaporating dish)
● Weigh (residue)

- Round bottom flask and condenser (REFLUX)


- Erlenmeyer flask and glass tubing → inserted in a cork

(SIMPLE REFLUX)
- nasa water bath
- REDDISH-ORANGE ang color kaya nadidissolve na yung oleoresin sa
ethyl alcohol

Formula:

Capsicum anuum
- Chile pepper, Cayenne pepper
- Fruit contains the active principles: capsaicin, 0.14% and capsicin
- Capsaicin (trans-8-methyl-N-vanillyl-6-nonenamide) is the principal pungent component
in hot peppers, including red chili peppers, jalapeños, and habaneros.
- Cayenne pepper contains fatty oil, 15-20%; some volatile oil; capsaicin, 0.15 - 0.5%;
starch, 0.8-1.4%; pentosans, 8.57%; and pectin, 2.33%
ORGANOLEPTIC EVALUATION
Color: Red orange
Odor: Aromatic
Taste: Residue/ wax-like
SOLUBILITY
Water: Insoluble
Alcohol: Soluble
Ether: Soluble

Capsaicin - oleoresin obtained from siling labuyo Uses:


- Irritant
- Carminative
- Rubefacient
- Stimulant
- Condiment
Natural oleoresin – are mixtures of volatile oil and resins, generally obtained by incising trunks
of trees in which they are found
Prepared oleoresin - are concentrated liquid preparations made by percolating drugs, naturally
containing both volatile oil and resin, with an appropriate solvent, acetone, ether, or alcohol and
concentrating the percolate until the solvent has been dissipated

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