Dangote CPP
Dangote CPP
Dangote CPP
A545-02-42-SOI-1680
FOR CAPTIVE POWER PLANT –
Rev A
BALANCE OF PLANT, DANGOTE,
DORC-LEKKI,NIGERIA Page 1 of 161
OPERATING MANUAL
FOR
CAPTIVE POWER PLANT - BALANCE OF
PLANT
UNIT NO. 680
FOR
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FOREWORD
This operating manual for Captive Power Plant – Balance of Plant facilities of M/s
DORC has been prepared by M/s Engineers India Limited.
Operating procedures & conditions given in this manual are indicative. These should
be treated as general guide only for routine start-up and operation of the unit. The
actual operating parameters and procedures may require minor
modifications/changes from those contained in this manual as more experience is
gained in operation of the Plant.
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Contents
FOREWORD ........................................................................................................................ 2
1 INTRODUCTION ...................................................................................................... 10
1.1 Refinery Overview................................................................................................. 10
1.2 Process Objective ................................................................................................. 11
1.3 Process Chemistry ................................................................................................ 11
2 PLANT DESCRIPTION ............................................................................................ 13
2.1 Capacity of the Plant ............................................................................................. 13
2.2 On Stream Factor ................................................................................................. 13
2.3 Turn Down Ratio ................................................................................................... 13
2.4 Feed Specifications............................................................................................... 13
2.5 Product Specifications .......................................................................................... 20
2.6 Material Balance / Stream Data ............................................................................ 20
2.7 Equipment List of the Unit ..................................................................................... 20
2.8 Battery Limit Summary Including Utilities .............................................................. 21
2.9 Effluent Summary ................................................................................................. 22
2.10 Flare Load Summary ............................................................................................ 22
3 PROCESS FLOW DESCRIPTION ........................................................................... 24
3.1 VHP Steam Generation & Consumption/ Distribution ............................................ 24
3.2 HP/ MP/ LP Steam Generation & Consumption/ Distribution ................................. 27
3.3 Power Generation ................................................................................................. 29
3.4 Pressure Reduction and De-super heaters ........................................................... 31
3.5 DM Water/ Condensate Storage & Transfer .......................................................... 34
3.6 Deaerators ............................................................................................................ 35
3.7 VHP BFW Transfer & Distribution ......................................................................... 37
3.8 HP BFW Transfer & Distribution............................................................................ 37
3.9 MP BFW Transfer & Distribution ........................................................................... 38
3.10 HSD Storage & Distribution................................................................................... 38
3.11 LCO/ IFO-2 Storage & Distribution ........................................................................ 39
3.12 CLO/ IFO-1 Storage & Distribution ........................................................................ 40
3.13 Natural Gas/ Fuel Gas Handling & Distribution ..................................................... 41
3.14 Propane Handling & Distribution ........................................................................... 42
3.15 UB SCAPH and BFW Pre Heater Condensate Handling ....................................... 43
3.16 Atmospheric / LP Condensate Handling................................................................ 44
3.17 Cooling Water Distribution .................................................................................... 44
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SECTION-1
INTRODUCTION
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1 INTRODUCTION
1.1 Refinery Overview
Dangote Oil Refining Company Ltd (DORC) is setting up a state-of-the-art refinery complex
in the Lekki Free Zone (LFZ), Nigeria. The refinery plans to produce gasoline, diesel,
kerosene, LPG, polypropylene and sulfur for the local market and export the surplus, if any.
The complex shall comprise of 650,000 BPSD crude oil refinery processing unit, product and
crude oil transfer facilities, tank farm for crude oil and intermediate / product storage, and an
associated effluent treatment facilities.
The proposed Dangote Refinery Plant Complex includes plant site area, pipeline system,
harbor area and access road. The processing facilities will comprise of following process
units:
CRUDE BLOCK
o Crude Distillation Unit (Unit No. 101)
o Sat. Gas Conc. Unit (Unit No. 102)
o Sat. LPG Merox Unit (Unit No. 103)
o Kerosene Merox Unit (Unit No. 104)
RFCC BLOCK
o Reactor - Regenerator Section (Unit No. 111)
o Main Column Section (Unit No. 112)
o UOP Gas Concentration Unit (Unit No. 113)
o Propylene Recovery Unit (Unit No. 114)
o Power Recovery System (Unit No. 115)
o Unsaturated LPG Merox Unit (Unit No. 116)
o C5 Extraction Merox Unit (Unit No. 132)
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MS BLOCK
o Naphtha Hydrotreating Unit (Unit No. 151)
o CCR Platforming Unit (Unit No. 152)
o CCR – Regen Section (Unit No. 153)
o Penex Process Unit (Unit No. 155)
HYDROGEN PLANT
o Hydrogen Generation Unit Train-I & II (Unit No. 161 & 162)
POLYMER BLOCK
o Poly Propylene Unit Train – I & II (Unit No. 171 & 172)
SULPHUR BLOCK
o Non-Phenolic Sour Water Stripper (Unit No. 181)
o Phenolic Sour Water Stripper (Unit No. 182)
o Amine Regeneration Unit (Unsaturated) (Unit No. 183)
o Amine Regeneration Unit (Saturated) (Unit No. 184)
o Sulphur Recovery Unit – I & II (Unit No. 185 & 186)
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SECTION-2
PLANT DESCRIPTION
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2 PLANT DESCRIPTION
2.1 Capacity of the Plant
The major components of captive power plant and their design capacities are as follows:
8 + 0 Frame-6 equivalent GTGs of 35.5 MW each. (Net Power Export at site)
8 + 0 HRSGs each of 110 TPH of VHP steam generation capacity
3 + 1 STGs each of 31 MW extraction (HP & MP) cum condensing. Each STG
extraction shall be VHP to HP (90 TPH max) + MP (180 TPH max) and condensing
(47 TPH max)
3 + 1 utility boilers, each of 400 TPH of VHP steam generation capacity
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DM Water Specifications:
1. pH 6.5 - 7.0
2. Conductivity at 20 oC µmho/cm < 0.2
3. Total hardness ppm Nil
4. Total Suspended Solids ppm Nil
5. Total (reactive) Silica as SiO2 ppm 0.02 (Max)
6. Turbidity NTU Nil
7. Total Iron as Fe ppm 0.03 (Max)
8. KMnO4 value at 100deg C ppm 1 (Max)
9. Total Copper as Cu ppm 0.003 (Max)
10. Sodium as Na ppm 0.01 (Max)
11. Oil ppm Nil
12. Total dissolved solids ppm 0.1
1. pH - 6.5-7.0
2. Turbidity, NTU (5 min settled) NTU NIL
3. Total suspended solids mg/l NIL
4. Total dissolved solids mg/l 0.1
5. Conductivity@20 DEG C µmho/cm <0.2
6. Total Hardness as CaCO3 mg/l Nil
7. Total reactive Silica as SiO2 mg/l <0.02
8. Total Colloidal Silica as SiO2 mg/l <0.005
9. Sodium as Na mg/l 0.01 max.
10. Total Iron mg/l <0.005
11. Chlorides as Cl mg/ l <0.005
12. Total Copper, mg/l 0.003 max.
13. KMnO4 value at 100 DEG C, mg/l 1 max
14. Total Organic Carbon (TOC) mg/ l Nil
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Propane
S. No. Parameter
Volume %
1. Hydrogen
2. Nitrogen
3. CO2
4. CO
5. O2
6. H2O 0.01
7. Methane
8. Ethane 0.88
9. Ethylene
10. Propane 93.33
11. Propene 3.83
12. i-Butane 1.15
13. n-Butane 0.05
14. i-Butene 0.01
15. 1-Butene 0.75
16. tr2-Butene
17. cis2-Butene
18. i-Pentane
19. 2M-1-Butene
20. 2M-2 Butene
21. Pentane and higher hydrocarbon
22. C6 (+) Product
23. H2S
24. Total Sulphur including H2S
25. Molecular Weight 44.06
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CPP also produce Boiler Feed Water (BFW) at Very High Pressure (VHP), High Pressure
(HP) and Medium Pressure (MP) levels. VHP BFW is utilised internally within CPP whereas
HP BFW and MP BFW are exported outside battery limit for refinery complex use. The BFW
quality shall adhere to following specifications:
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Notes:
1. Battery limit conditions for following vendor packages shall be as per Annexure 18.26
Gas Turbine Generator
Utility Boiler
Heat Recovery Steam Generator
Steam Turbine Generator
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SECTION-3
PROCESS FLOW DESCRIPTION
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Eight numbers of HRSG‟s are provided in the captive power plant. Each HRSG is designed
to generate 110 TPH of VHP steam at 107 kg/cm2g pressure and 520 deg C at battery limit.
HRSG‟s are designed to achieve the same at 65% of base load of GTG to 35.5 MW net
power from GTG at all ambient temperatures and for all fuels. HRSG turndown during GTG
load of 35.5 MW net power shall be 80 TPH or below meeting VHP steam parameters for all
fuels (package vendor‟s manual shall be referred).
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designed to generate 400 TPH of VHP steam at 107 kg/cm2g pressure and 520 deg C at
battery limit. Utility Boiler turndown is 30% of Maximum Continuous Rating (MCR) on super
heater temperature control and automatic combustion control mode of operation for gaseous
fuels, whereas for liquid fuel, it is 40% of MCR on super heater temperature control mode
and 30% of MCR on automatic combustion control mode of operation.
Detailed process description of steam generation and components of Utility Boiler shall be
provided by UB supplier in UB‟s operating manual (to be prepared by M/s Thermax).
Emergency steam
During total power failure, to facilitate safe shutdown / quick re-start of refinery and supply
emergency steam to critical consumers, single utility boiler will be designed to continue to
operate even during power failure.
For this operation all corresponding utility required for boiler operation must be ready even in
total power failure. Cooling water for the bearing cooling of devices operating during a power
failure is provided through a separate emergency cooling water header. This header is
served by cooling water pumps operated with steam turbines. This cooling water header
remains operational even during a power failure. Instrument air shall be provided through
separate header to CPP which shall also meet the emergency requirement during power
failure.
The emergency operating provisions are provided in all four boilers; however, during
emergency only one boiler shall be operating. However, as the steam network is common for
all consumers, to prioritize the steam to emergency consumers steam shedding in non-
emergency consumers shall be considered.
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In addition to the above, VHP steam is also consumed in RFCC unit as motive fluid for
turbine drives.
VHP Steam is distributed to Pressure Reducing & De-superheating system (PRDS). Three
numbers of PRDS are provided for converting VHP steam to HP Steam and three numbers
for converting VHP steam to MP Steam. VHP steam is distributed to OBSL (to RFCC unit)
through a 36” header.
Steam generation processes often have multiple boilers that feed a common steam header.
When steam is needed anywhere in the plant, the load is drawn from this common header.
With so many uses, steam load can vary significantly and unpredictably with time in a plant.
The individual boilers must generate and feed steam to the common header at a rate that
matches these load draws. Controlling the main steam header to a constant pressure
provides an important stabilizing influence to plant-wide operation.
Detailed process description of power generation and components of STG shall be provided
by STG supplier in STG‟s operating manual (to be prepared by M/s HTC).
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In addition to the above, HP steam is also consumed in various process units of DRP
complex as motive fluid for turbine drives as well as heating medium in heat exchangers.
HP Steam is also distributed to Pressure Reducing & De-superheating system (PRDS). One
number of PRDS is provided for converting HP steam to MP Steam. HP steam is distributed
to OBSL through a 30” header.
MP Steam Generation:
MP steam is also generated within CPP through Steam Turbine Generators (STG) and MP
steam demand can also be met through three numbers of VHP to MP PRDS and one
number of HP to MP PRDS in the scenario when STG‟s are not available.
In addition to the above, MP steam is also consumed in various process units of DRP
complex as motive fluid for turbine drives, heating medium in heat exchangers as well as
decoking steam. MP Steam is also distributed to Pressure Reducing & De-superheating
system (PRDS). Three numbers of PRDS are provided for converting MP steam to LP
Steam. MP steam is distributed to OBSL through a 40” header.
LP Steam Generation:
LP steam is generated within CPP from HP to LP drives of BFW pumps and IFO-1 / CLO
forwarding pumps. LP steam is also generated from HP-LP drive of FD fans of each utility
boiler and flashed steam from continuous blow down drum of each UB and HRSG. Further
LP steam shall also be generated within CPP through three numbers of MP to LP PRDS in
the scenario when other sources of generation are not available.
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LP steam is also generated as well as consumed in various process units of DRP complex.
In case of any net excess LP steam generation from DRP complex, provision to utilise the
same within CPP is available. Further if there is a net LP steam demand to OSBL LP
network, PRDS provided within CPP shall cater to the same.
Eight numbers of Industrial heavy Duty type GTG‟s are provided in the captive power plant.
Each GTG is designed to generate 34.5 MW net exportable power (after deduction of all
internal consumption and losses). GTG‟s are designed to operate at a turndown of 30% to
100% on each fuel. GTG exhaust gases are routed to Heat Recovery Steam Generator
(HRSG) for production of VHP steam. GTG is provided with bypass stack with diverter
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Each GTG shall also have black start facility. All facilities and associated auxiliaries as
required for one GTG start-up at a time and loading up to its rated capacity are provided.
Diesel generator set complete with all auxiliaries as required are provided for black start of
GTG. Detailed process description of power generation and components of GTG including
black start facilities shall be provided by GTG supplier in GTG‟s operating manual (to be
prepared by M/s GE).
Detailed process description of power generation and components of STG shall be provided
by STG supplier in STG‟s operating manual (to be prepared by M/s HTC).
Emergency Power
Emergency power is required for safe shutdown of various process units in the refinery
complex during general power failure and also to sustain at least one utility boiler continuous
operation during general power failure for quick restart of refinery.
During general power failure, for safe shut down of refinery there are few consumers that
have been provided with emergency power backup to supply power during power failure.
Accordingly Emergency DG set of suitable capacity is being provided.
CPP emergency DG set: During general power failure to sustain one boiler continuous
operation, a DG set dedicated to Boiler power requirements, BFW/Cooling water LO pumps,
Fuel forwarding pumps to Boiler is provided.
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Refinery emergency DG set: During general power failure for safe shutdown of refinery, a
dedicated DG set is provided.
Black start DG: For black start of one GTG, a dedicated black start DG set is considered.
During general power failure, first CPP emergency DG set shall start and provide the power
to CPP emergency power requirements. In case this DG set fails to start, a backup provision
from refinery DG set is made available. The emergency power demand of CPP, i.e., for
sustaining one UB operation is around 200 KW. 750 KVA capacity CPP emergency DG set
is provided to meet the same.
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VHP-HP PRDS
Normally HP steam requirement shall be met through HP steam extraction through STG and
through process steam generators in RFCC, CCR platforming, HGU, SRU, etc. VHP – HP
PRDS is provided to supply HP steam to refinery when any one of the major HP steam
generator is down.
One number of 80 TPH and two numbers of 240 TPH VHP-HP PRDS are provided to cater
to various HP steam shortfall scenarios of the complex. The 80 TPH PRDS (680-YS-1001)
will be in line once the HP steam header pressure falls to 42.5 kg/cm 2g and the 240 TPH
PRDS (680-YS-1002 A) will be in line once the HP steam header pressure falls to 42.0,
whereas the second 240 TPH PRDS (680-YS-1002 B) will be in line when the pressure falls
to 41.5 kg/cm2g. High pressure BFW is provided at the inlet of each PRDS to take care of
de-superheating requirement. Further PRDS downstream is also provided with safety valves
to take care of control valve full open scenario which can result in over pressurisation of HP
steam header due to VHP steam.
VHP-MP PRDS
Normally, MP steam requirement shall be met through MP steam extraction through STG
and other process drives in RFCC, CCR platforming etc. It is to be noted that HP steam
requirement in refinery is lower than MP seam requirement; hence PRDS of VHP to MP is
considered instead of HP to MP extraction, to reduce capacity of VHP to HP PRDS as well
as HP header.
One number of 45 TPH and two numbers of 140 TPH VHP-MP PRDS are provided to cater
to various MP steam shortfall scenarios of the complex. The 45 TPH PRDS (680-YS-1003)
will be in line once the MP steam header pressure falls to 15.5 kg/cm2g and the 140 TPH
PRDS (680-YS-1004 A) will be in line once the MP steam header pressure falls to 15.0,
whereas the second 140 TPH PRDS (680-YS-1004 B) will be in line when the pressure falls
to 14.5 kg/cm2g. High pressure BFW is provided at the inlet of each PRDS to take care of
de-superheating requirement. Further PRDS downstream is also provided with safety valves
to take care of control valve full open scenario which can result in over pressurisation of MP
steam header due to VHP steam.
HP-MP PRDS
Normally MP steam requirement shall be met through MP steam extraction through STG and
other process drives in RFCC, CCR platforming etc. However, this HP-MP PRDS (680-YS-
1007) of 50 TPH is provided within CPP for a case specific scenario. In one of the refinery
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operating case, there is net excess of HP steam generated from the complex and net LP
steam demand in the complex. To avoid venting HP steam, it is envisaged to convert this HP
steam to MP steam and further to LP steam through a HP-MP PRDS (680-YS-1007) and
MP-LP PRDS (680-YS-1008). This HP-MP PRDS will be in line once upstream HP header
pressure rises to 43.5 kg/cm2g.
High pressure BFW is provided at the inlet of each PRDS to take care of de-superheating
requirement. Further PRDS downstream is also provided with safety valves to take care of
control valve full open scenario which can result in over pressurisation of MP steam header
due to HP steam.
MP-LP PRDS
Normally LP steam requirement shall be met through LP steam extraction through various
drives in the complex. Further during the commissioning of various units, LP steam will be
required for steam blowing of various lines. In order to cater to the same, MP-LP PRDS is
provided.
One number of 30 TPH and one number of 90 TPH MP-LP PRDS are provided to cater to
various LP steam shortfall scenarios and commissioning LP steam requirement of the
complex. The 30 TPH PRDS (680-YS-1005) will be in line once the LP steam header
pressure falls to 5.0 kg/cm2g and the 90 TPH PRDS (680-YS-1006) will be in line once the
LP steam header pressure falls to 4.5.
In addition to above one more MP-LP PRDS (680-YS-1008) of 50 TPH is also provided
within CPP. This is provided for a case specific scenario. In one of the refinery operating
case, there is net excess of HP steam generated from the complex and net LP steam
demand in the complex. To avoid venting HP steam, it is envisaged to convert this HP steam
to MP steam and further to LP steam through a HP-MP PRDS and MP-LP PRDS (680-YS-
1008). This MP-LP PRDS (680-YS-1008) will be in line once upstream MP header pressure
rises to 16.5 kg/cm2g, which will occur due to increase in HP steam header pressure to 43.5
kg/cm2g.
High pressure BFW is provided at the inlet of each PRDS to take care of de-superheating
requirement. Further PRDS downstream is also provided with safety valves to take care of
control valve full open scenario which can result in over pressurisation of LP steam header
due to MP steam.
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As per condensate handling philosophy in the complex, the surface and suspect condensate
are collected and routed to Condensate Polishing Unit (CPU) located in RO DM plant battery
limit area via surface and suspect condensate header respectively and pure condensate is
collected and routed back directly to CPP.
The makeup DM water required in CPP is routed from RO DM Plant battery limit. A part of
DM water is also routed to CDU block & RFCC block for cooling process fluids thereby
preheating a part of DM Water. The preheated DM water is routed back to CPP.
In each STG battery limit, there is provision to route the condensate to DM water /
condensate storage tanks within CPP or to Condensate Polishing Unit (CPU) in OSBL RO
DM Plant battery limit through surface condensate header. This routing is based on
conductivity analyser feedback provided in CEP discharge header. The DM water /
condensate storage tanks are provided with nitrogen blanketing to avoid air ingress. PVRV is
also provided for the tank safety. Further, Morpholine dosing provision is kept for adjusting
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MUH feed pumps are provided to route the DM water / condensate stream from storage tank
within CPP to MUH in each HRSG‟s and further to Deaerator. Each MUH is designed to
preheat 115 TPH of DM water / condensate to a temperature of up to 100 ºC. The
Deaerator feed pumps are provided to route the balance DM water / condensate required
directly to Deaerator. From MUH feed pumps discharge header, there is also a provision for
condenser initial filling / CEP sealing in each STG area.
3.6 Deaerators
DM water/ condensate used as boiler feed water for steam generation/ de-superheating shall
be free of dissolved gases so that corrosion as result of dissolved gases shall be avoided in
downstream steam generators, turbines and piping at high temperatures. Thermal
deaerators are provided for the same, two deaerators are provided and each deaerator is
designed to produce BFW of 1650 TPH. They generally consist of two sections, Deaeration
section and Storage Section.
Deaeration Section
Thermal deaerators are direct contact heaters and the water to be deaerated is heated to a
temperature just above the saturation temperature for the corresponding pressure, when the
partial pressure of the dissolved gases becomes zero and dissolved gases are consequently
expelled from liquid.
In order to achieve this, steam is passed counter current to water flow, which is first
dispersed into small droplets and then passed over a tray stack. In some design steam is
passed co-currently. The tray stack brings steam into intimate contact with water dropping
down and ensures a number of reversals exposing fresh water surfaces. The top spraying
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system and the first part of the assembly are so designed that the inlet water gets heated to
nearly the saturation temperature desired. The lower portion of the tray stack acts as a
scrubber removing all the dissolved gases. The rising steam gets condensed when it comes
into contact with inlet spray and only a small amount of steam (max 2 %) is vented to
atmosphere along with the non-condensable gases.
The spray area condenses almost 100% of the steam used thus preventing excess steam
losses. All the steam used flows back over the trays to the storage tank. Water admitted at
the top of the deaerator and sprayed on to the tray stack by spray nozzles flows counter
current to the rising steam and steam is allowed to enter from the bottom of the tray stack.
Storage Section
The storage vessel of a deaerator provides the required residence time for the deaerated
water. In order to provide the required NPSH for the Boiler Feed Water pump, the deaerators
are always located at a higher elevation above the ground. Detailed process description of
Deaerator and its components shall be provided by equipment supplier in Deaerator‟s
operating manual (to be prepared by M/s Sterling Deaerator Company).
Pure condensate (directly from CPP battery limit) and DM water/ polished condensate
(through MUH feed pumps and Deaerator feed pumps) are routed to each deaerator at the
top of spray tower. There is also a provision made to route cold DM water from CPP battery
limit to each deaerator. This connection is kept for initial start-up of the plant as well as for
total power failure scenario. During total power failure scenario, the deaerator shall be able
to generate BFW to run one utility boiler continuously. Since the DM water transfer pumps
(622-PA-101 A/B/C/D/E/F/G/H) are provided with emergency power backup, during power
failure the DM water supply to CPP will continue to remain uninterrupted except a short
interval required for emergency DG set to take over.
In addition to these streams, condensates generated within CPP from steam traps and from
UB condensate (BFW pre heater condensate and Steam Coil Air pre heater condensate) are
also routed to each Deaerator top. The MUH preheated DM water/ condensate and pure
condensate streams are controlled through a HV whereas the DM water/ condensate from
Deaerator feed pumps is under level control with deaerator storage vessel level. LP steam is
introduced at the bottom of spray tower and is regulated by deaerator storage tank pressure
control.
The deaerated water enters the storage vessel through down comers which connects the
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two. In order to ensure dissolved gas free BFW supply, an oxygen scavenger chemical is
also added in the down comer. The dose rate of the oxygen scavenger is based on
maintaining a residual chemical content in the deaerated water. Both the deaerator storage
vessels are interconnected at their liquid and vapour spaces for balancing level and pressure
between both deaerators. Further the balancing drum leak off connections from MP BFW
pumps and Auto Recirculation (ARC) line header of all BFW pumps are also routed to
deaerator storage vessel. The deaerator storage tank is also provided with LP steam
connection for initial heating.
VHP BFW is consumed only within CPP for generation of VHP steam in UB‟s and HRSG‟s.
Four working and two standby VHP BFW pumps (680-PA-1005 A/B/C/D/E/F) are provided
for transferring VHP BFW from deaerator to each UB/ HRSG. Two of the working pumps are
turbine (HP to LP) driven whereas the rest are electrical motor driven. These turbine driven
VHP BFW pumps ensure continuous supply of BFW to one UB during power failure. Each
VHP BFW pump has a rated capacity of 595 m3/ hr. The ARC valve outlet from each VHP
BFW pump is routed to each deaerator storage vessel.
Each VHP BFW pump also has an intermediate bleed to produce HP BFW at 58 kg/cm2g for
consumption within CPP. This HP BFW is utilised within CPP for following purpose:
CLO Transfer Pump turbine drive exhaust steam de-superheating
VHP BFW pump turbine drive exhaust steam de-superheating
FD fan turbine drive exhaust steam de-superheating in each Utility Boiler
Extraction steam de-superheating in each STG
De-superheating in each PRDS
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HSD from storage tank is routed to each GTG by two sets of pumps. HSD to GTG pumps,
680-PA-1002 A/B/C (2 Working + 1 Standby) of rated capacity 26 m3/hr for supplying HSD to
four GTG‟s (I to IV) and 680-PA-1002 D/E/F (2 Working + 1 Standby) of rated capacity of 26
m3/hr for supplying HSD to four GTG‟s (V to VIII) operating at their rated capacity. Each set
of pumps are designed to cater to the needs of four GTG operation. Each GTG is also
provided with HSD return lines which will return a part of HSD during start-up of GTG. Once
GTG ramps to its rated capacity, these HSD return lines will have no flow. These HSD return
lines from each GTG are collected in a common header and routed back to HSD storage
tank.
Further, from the discharge header of both set of HSD to GTG pumps, a connection to
supply HSD to emergency DG set and to Black-start DG set is also provided.
HSD Centrifuge
Two numbers (1 working + 1 standby) of 50 m3/ hr capacity HSD centrifuge is provided near
HSD tank area within CPP for HSD purification. Since the purity of HSD w. r. t its water and
sediment content is critical for GTG operation, HSD centrifuge is provided. HSD from
storage tank is routed to centrifuge through feed pump and the treated HSD is routed back
to HSD storage tank. Centrifuging operation is batch process and is carried out before using
the HSD for GTG start-up. HSD centrifuge is designed to achieve 500 ppmv free water and
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100 % removal of 10µ and above sized particles. The quality of HSD in HSD storage tank
shall be analysed periodically in lab viz., once in an hour or once in two hours, through
manual sampling and depending on the same the centrifuging operation shall be continued
or stopped.
The sludge from centrifuge shall be collected in a sludge tank and pumped to centrifuge skid
battery limit for disposal in nearby OWS connection. Detailed process description of
centrifuge and its components shall be provided by equipment supplier in centrifuge vendor‟s
operating manual (to be prepared by M/s Alfa Laval).
LCO/ IFO-2 is routed to CPP battery limit from OSBL from offsite facility. These LCO lines
from offsite shall also be used to supply diesel to CPP during refinery start-up. The LCO/
IFO-2 received at battery limit is routed to two numbers of LCO storage tank (680-TT-1002
A/B) of nominal capacity 2500 m3. The LCO storage tanks shall also receive the false start
drain tank contents from each GTG. The LCO storage tank is provided with nitrogen
blanketing to avoid air ingress. PVRV is also provided for the tank safety.
Each GTG is also provided with LCO/ IFO-2 return lines which will return a part of LCO/ IFO-
2 during start-up of GTG. After GTG ramps up to its rated capacity, the return flow will stop
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from each GTG. These LCO/ IFO-2 return lines from each GTG are collected in a common
header and routed back to LCO storage tanks.
LCO/ IFO-2 centrifuge is designed to achieve 500 ppmv free water and 100 % removal of
10µ and above sized particles. The quality of LCO/ IFO-2 in LCO storage tank (which was in
receiving/ centrifuging mode) shall be analysed periodically in lab viz., once in an hour or
once in two hours, through manual sampling and depending on the same the centrifuging
operation shall be continued or stopped.
The sludge from centrifuge shall be collected in a sludge tank and pumped to centrifuge skid
battery limit for disposal in nearby OWS connection. Detailed process description of
centrifuge and its components shall be provided by equipment supplier in centrifuge vendor‟s
operating manual (to be prepared by M/s Alfa Laval).
CLO/ IFO-1 is routed to CPP battery limit from OSBL from offsite facility. The CLO/ IFO-1
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received at battery limit is routed to one number of CLO storage tank (680-TT-1003) of
nominal capacity 2500 m3. The CLO/ IFO-1 storage tank is provided with nitrogen blanketing
to avoid air ingress. PVRV is also provided for the tank safety. Since CLO is a viscous fluid,
LP steam heating coil arrangement is provided in the tank to minimise its viscosity to
acceptable limits for UBs. The LP steam heating will maintain the tank content to a minimum
temperature of 80 deg C.
CLO/ IFO-1 from storage tank is routed to UBs through common pumps, CLO supply pumps
to UBs, 680-PA-1008 A/B/C/D (3 Working + 1 Standby) of rated capacity 50 m3/hr. These
pumps are designed to cater to the needs of three UBs operating at its rated capacity. One
of the working pump is turbine (HP to LP) driven whereas the rest are electrical motor driven.
These turbine driven CLO supply pumps ensure continuous supply of fuel to one UB during
power failure.
The discharge from the CLO pumps are routed to a CLO trim heater (680-EE-1001 A/B) for
maintaining the temperature of the fuel considering the heat losses (after insulation) that will
be incurred in the piping from CLO pump area to farther most UB. LP steam is used as
heating medium and is provided to each CLO trim heater under CLO/ IFO-1 outlet
temperature control.
The CLO/ IFO-1 fuel is then routed to a two numbers (1 working + 1 standby) of CLO filter
(680-GN-1003 A/B), which is a basket type filter to remove particle of size 250µ and above
in the fuel to avoid choking of burners in UBs. The filters are designed with a particle
removal efficiency of 99%. The fuel from downstream of the filter is routed further to each UB
battery limit. Since this being a congealing fluid, a return line is provided from each UB so as
to avoid congealing of fluid in piping dead zones. The return from each UB is routed back to
CLO storage tank. The CLO lines within CPP are heat traced and insulated.
One stream is routed to GTG‟s through NG forwarding skid. Two NG forwarding skids are
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provided, each to cater to requirements of four GTG‟s. Each NG forwarding skid comprise of
NG heater, pressure control system and scrubber to meet the GTG fuel specifications.
These skids are supplied by GTG vendor. Detailed process description of NG forwarding
skid and its components shall be provided by equipment supplier in GTG vendor‟s operating
manual (to be prepared by M/s GE). The outlet from these NG skids is routed to each GTG
battery limit. To ensure meeting NG specification for GTG‟s the natural gas from each
forwarding skid is also routed to a chromatograph skid for detailed analysis of the fuel.
The other stream is routed to UB‟s and HRSG‟s. Since the pressure requirement of NG in
UB/ HRSG is very less compared to incoming NG stream at battery limit, the NG stream for
UB/ HRSG is split from NG KOD downstream. This NG stream is first routed to a NG heater
(680-EE-1002 A/B) to take care of temperature drop that would result in downstream
pressure reduction. The outlet from NG heater is routed to pressure control valve assembly
before being routed to each UB / HRSG battery limit. LP steam is used as heating medium in
NG heater and is provided to each NG trim heater under outlet temperature control.
Fuel Gas
Fuel gas is also made available at CPP battery limit. Normally, Fuel gas generated in the
refinery complex is being used in heaters of different process units. In case if the
consumption in process units is less, then the excess fuel gas is envisaged to be used in
CPP. Fuel gas is envisaged to be used as an alternate fuel for UB‟s and HRSG‟s. Fuel gas
within CPP battery limit is first routed to FG KOD (680-VV-1002) for removal of any
condensates in the incoming stream. The NG stream after pressure control valve assembly
mixed with the fuel gas stream at the outlet of FG KOD. The condensate from FG KOD will
be drained manually to CBD after flaring the contents in FG KOD by LP steam purging.
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Liquid propane is made available at CPP battery limit. Propane forwarding pumps (680-PA-
1027 A/B) of 72 m3/ hr capacity is provided to boost the pressure of liquid propane and also
to further route the same to Propane forwarding skid. Propane forwarding skid (1 number)
comprise of vaporisers, super heaters, vane pack separator and scrubbers to meet GTG fuel
specifications. A slip stream is taken at downstream of vaporiser to meet UB/ HRSG
requirements. These skids are supplied by GTG vendor. Detailed process description of
propane forwarding skid and its components shall be provided by equipment supplier in GTG
vendor‟s operating manual (to be prepared by M/s GE). The outlet from the propane skid is
routed to each GTG battery limit. To ensure meeting fuel specification for GTG‟s the
vaporised propane from forwarding skid is also routed to a chromatograph skid for detailed
analysis of the fuel.
The vaporised propane piping is provided with dual LP steam tracing to avoid condensation
in piping. The propane gas from downstream of vaporiser (in propane forwarding skid) is
further routed to a pressure control valve to meet pressure requirements of UB & HRSG.
The air used for combustion in UB‟s is also required to be preheated and thus a LP steam
based Steam Coil Air Pre Heater (SCAPH) is provided in each UB. The condensate
generated from BFW pre heater and SCAPH is also envisaged to be reused within CPP
since both these streams are pure and is not required to be routed to Condensate Polishing
Unit (CPU). However, these streams required deaeration to eliminate presence of any
dissolved gases.
The BFW pre heater condensate is provided with two separate routings, either it can be
routed directly to Deaerator top or through a flash vessel and pumping system. In case if MP
steam is used in BFW pre heater, the first option of routing it directly to deaerator top shall
be utilised. In case if LP steam is used, then the condensate pressure won‟t be sufficient
enough to route it to deaerator top and hence it is routed first to a flash vessel and then
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pumped to deaerator top. The condensate from SCAPH is routed to flash vessel and then
pumped along with BFW pre-heater condensate to deaerator top.
Condensate generated from these sources are routed to a dedicated Atmospheric flash
drum (680-VV-1012) and further pumped to CPP battery limit through Atmospheric
Condensate pumps (680-PA-1023 A/B) each of 10 m3/ hr. From CPP battery limit the
condensate joins the suspect condensate header is OSBL for further polishing in
Condensate Polishing Unit (CPU). The steam generated in flash drum is routed to a vent
condenser (680-EE-1006) (water cooled) and routed back to flash drum for recovery of
flashed steam.
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A 56” supply header is provided at CPP battery limit from cooling tower-1 for CPP use.
Further since once UB is required to operate during total power failure scenario and also for
GTG emergency operation, a dedicated 20” cooling water supply header is provided at CPP
battery limit for use in each UB and GTG. This emergency cooling water header is fed from
emergency cooling water pumps located in cooling tower-1 area.
18” supply header is provided at CPP battery limit from OSBL for CPP use.
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Plant air is mainly used for oil atomization in Utility Boilers and HRSGs and also in hose
stations within CPP. 6” plant air supply header is provided at CPP battery limit from OSBL
for CPP use.
A separate plant air header, designated as breathing air is also provided within CPP battery
limit. In order to provide clean breathing air to operators who are likely to be exposed to
contaminated air during operation, a breathing air hose connection is also provided in
various locations within CPP. Operating personnel shall come with portable breathing air
stations which can be connected with these breathing air hose connections using hose
stations. This flexible hose with detachable coupling will be incompatible with outlets for non-
respirable plant air or other hose stations. 3” designated breathing air supply header is
provided at CPP battery limit from OSBL for CPP use.
Further, the fuel oil drains from each GTG battery limit is routed to liquid drain tank within
each GTG which also collects false start drain from GTG‟s. From these liquid drain tanks,
the contents are pumped to a separate header within CPP for transferring it to the LCO
storage tank for reuse.
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Morpholine is used for pH correction in deaerator feed streams and as well as in boiler feed
water. Carbohydrazide is used as oxygen scavenger in deaerator and is dosed in the down
comers of each deaerator. Each dosing skid comprise of a solution preparation drum,
solution metering drum and dosing pumps.
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SECTION-4
OPERATING VARIABLE & PROCESS
CONTROL
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A detailed analysis of the system reveals the various operating variables within CPP as
listed in this section. Each will be discussed as an independent with all others held constant.
Further these variables are best studied considering the different sections of the CPP and
accordingly they have been sub-classified as below:
Steam system
o VHP steam header pressure/ Flow
o VHP steam temperature
o HP steam header pressure/ Flow
o HP steam temperature
o MP steam header pressure/ Flow
o MP steam temperature
o LP steam header pressure/ flow
DM water/ Condensate system
o DM water/ condensate storage tank level
o Atmospheric condensate flash drum level
o LP condensate collection drum level
o UB atmospheric condensate flash drum level
Deaerator system
o Deaerator storage tank level
o Deaerator pressure control
Fuel handling system
o Fuel flow/ availability
o CLO heater outlet temperature & CLO heater condensate pot level
o NG heater outlet temperature & NG heater condensate pot level
o NG header pressure/ flow to UB/ HRSG
o Vaporised propane pressure/ flow to UB/ HRSG
o LCO header pressure to GTG‟s
o LCO heater outlet temperature
o HSD header pressure to GTG‟s
Nitrogen Blanketing system
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The individual controllers are mounted on the respective Utility Boilers and HRSGs with
Manual / Auto Selector switch to either control individual steam header pressure or to control
common steam header pressure. The auto controller facility is provided with biasing (+/-)
values by which Boiler/HRSG can be operated in different load sharing. If all the individual
controllers are in automatic, any change in Master Output signal shall pass through and
create an associated change in the firing demand for the UBs and HRSGs as per biasing.
OPTION-I:
All HRSGs shall be base loaded (i.e. firing of each HRSG shall be controlled by respective
individual upstream pressure controllers). Therefore any variation in the main steam header
pressure doesn‟t directly affect the firing demand of HRSGs and it only for the variation in
firing demand of UBs, i.e. UBs firing demand signal shall swing as per biasing input from the
Master signal varies. So, based on the above stated philosophy various scenarios can occur
and are listed below:
Scenario 1:
When all the three boilers (i.e. UB1, UB2 & UB3) are operated below their rated
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capacity, but each operating at same load(as sensed by FT-1202A for UB1, FT-2202A
for UB2 and FT-3202A for UB3), then the Master signal (PIC-1101) shall pass (through
SS-1203, SS-2203 & SS-3203 for UB1, UB2 & UB3 respectively) and create an equal
and associated change in the firing demand (i.e. equal biasing) for the UBs.
Scenario 2:
When all the three boilers (i.e. UB1, UB2 & UB3) are operated below their rated
capacity, and each operating at different load (as sensed by FT-1202A for UB1, FT-
2202A for UB2 and FT-3202A for UB3), then the Master signal (PIC-1101) shall pass
(through SS-1203, SS-2203 & SS-3203 for UB1, UB2 & UB-3 respectively) and create
a change proportional (based on biasing input given) to operating demand.
If, suppose a boiler reached 90% of MCR then the ramping up of that particular boiler
shall stop and the remaining boilers shall ramped up proportionally until they reach
90% of MCR. When all the boilers attain 90% MCR, then biasing shall be equally
distributed.
For decreasing demand, suppose a boiler reached 40% of MCR, then the ramping
down of that particular boiler shall stop and the remaining boilers shall ramped down
proportionally until they reach 40% of MCR. When all the boilers attain 40% MCR, then
biasing shall be equally distributed.
Scenario 3:
When one boiler is operated at MCR (suppose UB1, as sensed by FT-1202A) and
other two boilers (suppose UB2 & UB3) are operated below their rated capacity (as
sensed by FT-2202A for UB2 and FT-3202A for UB3). Then the boiler at MCR (i.e. UB
1) shall be base loaded and UB2 & UB3 shall swing with the Master Controller (PIC-
1101) in accordance with the scheme defined in scenario 1 and scenario 2.
OPTION-II:
All UBs and HRSGs shall swing with the master pressure controller. Therefore any variation
in the main steam header pressure affect the firing demand of both UBs and HRSGs so,
based on the above stated philosophy various scenarios can occur and are listed below:
Scenario 1:
When all the seven HRSGs and all three UBs (i.e. HRSG1, HRSG2, HRSG3, HRSG4,
HRSG5, HRSG6, HRSG7, UB1, UB2 & UB3) are operated below their capacity, but
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each operating at same capacity (as sensed by FT-1102 for HRSG1, FT-2102 for
HRSG2 , FT-3102 for HRSG3, FT-4102 for HRSG4, FT-5102 for HRSG5, FT-6102 for
HRSG6, FT-7102 for HRSG7, FT-1202A for UB1, FT-2202A for UB2 and FT-3202A),
then the Master signal (PIC-1101) shall pass (through HS-1102, HS-2102, HS-3102,
HS-4102, HS-5102, HS-6102, HS-7102, SS-1203, SS-2203 & SS-3203 for HRSG1,
HRSG2, HRSG3, HRSG4, HRSG5, HRSG6, HRSG7, UB1, UB2 & UB3 respectively)
and create a change proportional to total demand with biasing.
Scenario 2:
When all the seven HRSGs and all three UBs (i.e. HRSG1, HRSG2, HRSG3, HRSG4,
HRSG5, HRSG6, HRSG7, UB1, UB2 & UB3) are operated below their capacity, and
each operating at different capacity (as sensed by FT-1102 for HRSG1, FT-2102 for
HRSG2 , FT-3102 for HRSG3, FT-4102 for HRSG4, FT-5102 for HRSG5, FT-6102 for
HRSG6, FT-7102 for HRSG7, FT-1202A for UB1, FT-2202A for UB2 and FT-3202A),
then the Master signal (PIC-1101) shall pass (through HS-1102, HS-2102, HS-3102,
HS-4102, HS-5102, HS-6102, HS-7102, SS-1203, SS-2203 & SS-3203 for HRSG1,
HRSG2, HRSG3, HRSG4, HRSG5, HRSG6, HRSG7, UB1, UB2 & UB3 respectively)
and create a change proportional to total demand with biasing.
If, suppose a boiler reached 90% of MCR then the ramping up of that particular boiler
shall stop and the remaining boilers shall ramped up proportionally until they reached
90% of MCR. When all the boilers attain 90% MCR, then biasing shall be equally
distributed. However, for HRSG‟s the ramping up shall be up to 100% of its rated
capacity.
For decreasing demand, suppose a boiler reached 40% of MCR, then the ramping
down of that particular boiler shall stop and the remaining boilers shall ramped down
proportionally until they reach 40% of MCR. When all the boilers attain 40% MCR, then
biasing shall be equally distributed. For HRSG‟s, ramping down shall be limited to
turndown of HRSG based on GT load. The same shall be confirmed with HRSG
vendor.
The above cases were made considering, UB4 and HRSG8 shall be at standby mode. In
case UB4 and HRSG8 are operating, then their respective tag nos. shall be replaced by their
corresponding standby UB and HRSG.
Further, biasing shall be either automatic or manual. In automatic biasing, the ramp up/ ramp
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down of individual boiler/ HRSG shall be automatically decided based on the operating
capacity of respective boiler/ HRSG, whereas in manual biasing mode, the ramp up/ ramp
down of individual boiler / HRSG shall be manually set and accordingly the respective
equipment shall take part in load sharing operation. Accordingly manual biasing provision
same shall be implemented.
Further the combustion control system provided in each UB and HRSH also ensure that the
VHP steam temperature is maintained as desired. Detailed control description of VHP steam
temperature control shall be provided by equipment supplier in UB & HRSG vendor‟s
operating manual (to be prepared by M/s Thermax).
VHP- HP PRDS
STG extraction control has a maximum limitation of 90 TPH of HP steam in each STG.
However, there could arise a certain case where the net HP steam demand may go higher
than maximum extraction demands from all working STG‟s or if any one of the operating
STG trips, then there could be drop in HP steam header pressure which cannot be taken
care by STG extraction control. During such a scenario, VHP-HP PRDS will come in to
operation. The three VHP-HP PRDS-I/II and III are provided with set points at 42.5, 42.0 and
41.5 kg/cm2g respectively. When this set point reaches as sensed by PT/PIC-
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1402/1404/1406, the respective PRDS converts VHP steam to HP steam thereby stabilising
the HP steam header pressure.
HP- MP PRDS
STG extraction pressure control also takes care of high HP steam header pressure scenario.
However, there could be a certain case where the HP steam header pressure may rise
beyond the controlling limit of STG‟s. In such an eventuality, the HP-MP PRDS will come in
to operation to relieve excess HP steam header pressure. The HP-MP PRDS is provided
with set points at 43.5 kg/cm2g. When this set point reaches as sensed by PT/PIC-4802, the
PRDS converts HP steam to MP steam thereby stabilising the HP steam header pressure.
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VHP- MP PRDS
STG extraction control has a maximum limitation of 180 TPH of MP steam in each STG.
However, there could be a certain case where the net MP steam demand may go higher
than maximum extraction demands from all STG‟s or if any one of the operating STG trips,
then there could be drop in MP steam header pressure which cannot be taken care by STG
extraction control. During such a scenario, VHP-MP PRDS will come in to operation. The
three VHP-MP PRDS-I/II and III are provided with set points at 15.5, 15.0 and 14.5 kg/cm2g
respectively. When this set point reaches as sensed by PT/PIC-1602/1604/1606, the
respective PRDS converts VHP steam to MP steam thereby stabilising the MP steam header
pressure.
MP- LP PRDS-III
STG extraction pressure control also takes care of high MP steam header pressure
scenario. However, there could be a certain case where the MP steam header pressure may
rise beyond the controlling limit of STG‟s. In such an eventuality, the MP-LP PRDS will come
in to operation to relieve excess MP steam header pressure. The MP-LP PRDS-III is
provided with set point at 16.5 kg/cm2g. When this set point reaches as sensed by PT/PIC-
4804, the PRDS converts MP steam to LP steam thereby stabilising the MP steam header
pressure.
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As elaborated above, the same is applicable for the other tank, 680-TT-1004 B as well. The
valves LV-3103 B & C and LV-3103 A will be in operation. Level controllers LIC-3102 and
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LIC-3103 are provided for operation of the split range control for the tanks 680-TT-1004 A &
B respectively.
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condensate distribution to each deaerator, FT/FI-3401 shall be referred. Similarly, for MUH
outlet flow to each deaerator, FT/FI-3302/3303 shall be referred.
The deaerator feed pump discharge only supplies the remaining water to deaerator (in
addition to pure condensate and MUH outlet) required for BFW generation. Thus, this stream
is under level control of deaerator storage tank. The valves LV-3401 and LV-3501 will be in
operation under level control through LIC-3401 and LIC-3501 for the deaerator storage tank
A & B respectively. The LIC-3401 and LIC -3501 takes signal from LT-3401 A & B and LT-
3501 A & B respectively.
The solubility of gas in liquid is directly proportional to the partial pressure & inversely
proportional to temperature of liquid. Thus by adding steam in deaerator, the partial pressure
of dissolved gases are decreased thereby effecting the removal of the same. LP steam flow
to each deaerator is controlled through Deaerator pressure. Pressure control valve PV-3401
& PV-3501 operated through controllers PIC-3401 & PIC-3501 for Deaerator-A & B
respectively is provided to take care of the same. PIC-3401 & PIC-3501 takes input from
PT/PI-3401 A/B & PT/PI-3501 A/B (high selecting) for Deaerator-A & B respectively.
HRSG
Main fuel : Natural gas / Propane
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UTILITY BOILERS
Main fuel : CLO, (CLO+ Diesel) blend (IFO-1)
Alternate fuel : Natural gas, LCO/IFO-2, Fuel gas, Propane
Start-up fuel for pilot : Natural gas/Propane/LPG cylinder
(Boilers shall be designed for combination fuel firing, with any one of liquid and any
one of gaseous fuel in various proportions)
In view of the availability of fuels, natural gas and LCO system within CPP is designed to
cater to supply all eight GTGs/ HRSGs and three utility boilers to operate at 100% load
simultaneously. CLO system, being only utilised in utility boilers, is designed to cater to
supply three utility boilers operating at MCR continuously. Similarly, HSD system, being only
utilised in GTGs, is designed to cater to supply all eight GTGs operating at 100% load
continuously. Propane and fuel gas fuels are used only if the same is available for CPP
operation.
4.4.2 CLO Heater Outlet Temperature & CLO Heater Condensate Pot Level
The CLO stream is heated in CLO trim heater to maintain viscosity of CLO fuel within
acceptable limits for utility boiler burner design. The flow of LP steam, used as heating
medium in CLO trim heater, is controlled based on CLO trim heater‟s exit temperature.
TE/TT/TIC-5801 is provided at the outlet of CLO trim heater to control TV-5801, thereby
controlling the heating medium quantity in trim heater. Further the steam condensed in trim
heater is removed through level control valve LV-5802 acting under LT/LIC-5802 provided in
CLO heater condensate pot.
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Each tank is provided with a sensing line which will give continuous feedback on tank
pressure to individual PCV‟s. Further the tanks are also provided with an interconnection line
on the roof for reducing the overall nitrogen consumption.
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Each tank is provided with a sensing line which will give continuous feedback on tank
pressure to individual PCV‟s. Further the tanks are also provided with an interconnection line
on the roof for reducing the overall nitrogen consumption.
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SECTION-5
UTILITIES & ASSOCIATED FACILITIES
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5.4 Description of Utility Systems OWS, CRWS, CBD, FG, FO, FLO, Flare
KOD & Mist Oil Lubrication Description
5.4.1 Flare System
Flare system is provided within CPP for safe disposal of hydrocarbon gases relieved from
various safety valves provided on equipments/ piping, vents of fuel lines, seal plan vents
from various fuel pumps.
The LP flare relief streams are routed either directly to main LP flare header or through sub-
header depending on the location of the relief valves with respect to main header within
CPP. The main LP flare header is routed to a LP flare KOD (680-VV-1010) for removal of
any condensates before being routed to OSBL main LP flare header. The collected
condensate from the vessel is routed to CBD vessel inside CPP and further to refinery slop
storage.
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5.4.2 OWS
The oily water sewer (OWS) network is mainly to collect water contaminated with
hydrocarbon oil. The OWS stream is a mixture of process/oil and water which
includes process spillages, hydrocarbon drains from equipment, oily condensates, flushing
during routine operation and other drains which have a chance of becoming polluted with oil.
An oily water system safely transfers the collected flows to the treatment facilities through a
combined header. All equipment having CBD connections are normally provided with OWS
connections.
The system consists of drains, funnels, underground piping, clean-outs, catch basins,
manholes, sealed manholes and vent pipes etc.
5.4.3 CRWS
Rainwater collected from process units area is handled by Contaminated Rain Water System
(CRWS). It is expected that first 15 minutes of floor wash of identified equipment area of
process units have oil contamination. The floor wash of contaminated area shall be collected
in a CRWS pit through a network of catch basin and CRWS sewer and shall be sent to ETP
by pumping. Baffle wall shall be provided both for incoming pipe & outgoing discharge to
storm water drain. After 15 minutes, it shall be routed to storm water open drain.
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SECTION-6
PRECOMMISSIONING PROCEDURE
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6 PRECOMMISSIONING PROCEDURE
A "System" is a part of the plant (utility, process, offsites or other) which corresponds to an
independent group of equipment having a specific function or service, and in which the
major part (or the totality) of the Pre-commissioning activities can be performed reasonably
independently to form an individual and functional working area of the whole plant.
Organize the Pre-commissioning activities not at whole plant level, but at functional
systems and sub-systems level, having a total control in respect of the safety and
progress measurement;
Identify the optimum completion sequence, minimizing the time between end of
Construction and Commissioning of the plant, taking advantage of the fact that, while
some subsystems are still under Construction, others can be under Pre-
commissioning and some others can be under Commissioning;
Optimize means and resources with respect to the schedule.
The "system / sub-system" concept will be used during the completion phases to each
the contractual milestones / targets:
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be uploaded in EIL‟s commissioning software PCAMS for the management of all above
activities by systems / sub-systems.
The unit‟s system shall also be checked by respective unit‟s licenser representatives.
Contractor shall be required to liquidate punch list / checklist items of the licenser checklist
also.
Mechanical Completion of systems shall mean that all installation works of the unit have
been completed and hydro tested in accordance with approved construction drawings,
approved specification, applicable code as defined in the bid package, accepted
international good engineering practices and all the activities have been completed in a
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comprehensive manner by the Contractor except for minor mutually agreed leftover works
which may be completed during pre-commissioning phase. All statutory approval shall be
obtained by Contractor as part of mechanical completion.
The Contractor shall issue a certificate of “Ready for Commissioning” of the unit for
acceptance by the Owner / Consultant / Process Licensor in standard format, FORMAT- IV
with all exceptions resolved. After the Unit has been declared as “Ready for
Commissioning”, the Contractor shall not carry out any hot work in the Unit without prior
written permission of the Owner.
PCAMS Software shall be used in pre-commissioning and commissioning. Status of all the
formats shall be through PCAMS.
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The exact order of presentation need not be strictly followed. Depending on the progress of
construction, certain procedures may be required earlier or later than suggested here. A
thorough knowledge of the entire pre commissioning operation will allow the plant personnel
to schedule activities in the most time-saving and labor efficient way. These are the
necessary pre commissioning activities:
1. Vessel Inspection
2. Inspection of other Major Equipment
3. Piping and Instrument Check
4. Hydrostatic Testing
5. Line Flushing
6. Run-in of Pumps and Drivers
7. Servicing and Calibration of Instruments
8. Commissioning of Plant Services
9. Availability Check of Chemicals, Catalysts, and Other Materials
10. Plant Pressure Test
11. Air-Freeing
12. Commissioning of Additional Plant Services
The material in this section gives general guidelines for preparing a unit for startup. Some
sections need to be expanded to give specific instructions, but this can best be done by
personnel on site.
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CAUTION: Before entering a vessel, the refinery's safety precautions should be observed.
These usually include the following:
Sampling the vessel for toxic vapors and oxygen concentration,
Wearing a safety harness, and
Having an attendant outside the vessel.
Centrifugal: NPSH and speed rating, balancing line, warm up lines, seal flush, bearings.
Positive Displacement: discharge relief valve, pulsation dampeners, packing, speed and
stroke rating.
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Vessels that have met hydro testing requirements in the fabricators shop maybe
isolated from the hydro test if desired and if allowed by applicable codes. Before
hydro testing any vessel it should be confirmed that the vessel is designed and
supported such that it can safely be filled with water. If not, the applicable code
should be consulted for testing requirements.
Care should be taken not to exceed the pressure rating of any vessels or equipment
when preparing a hydro test circuit. Internals, such as displacers, level ball floats, or
other instruments not designed for the test pressure must be removed. All relief
valves (PSV's) should be removed, blinded, or gagged during the hydro test. Since
all relief valves must be bench tested and set before final installation, it may be
desirable to perform the testing at this time.
Vents must be provided at all high points of vessels and piping in the hydro test
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All internal valves within a test circuit should be confirmed open. Usually the
hydrostatic pressure test is carried out at 1.5 times the design pressure, but the
proper test pressure must be confirmed for each vessel or piping circuit in question.
Care should be taken that the temperature is not too low, causing the metal to
become brittle. The vessel/piping and water temperature should always be above
15.5°C (60°F) to eliminate the possibility of cold-fracturing the metal.
Note that a water filled system requires venting when being drained in order to avoid
pulling a vacuum and possibly collapsing equipment.
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Upon completion of line flushing of any system, carefully check that all temporary breaks are
re-connected, control valves are replaced, and pump alignments are normal. Also, verify that
all free water has been drained.
As debris collects in the strainers, flow to the pumps will fall off. When this happens to a
centrifugal pump, it will be necessary to throttle the pump discharge by partially closing the
discharge valve. This will prevent the pump from cavitating, which can cause damage to the
pump. However, also avoid restricting the pump discharge to the extent that it causes
internal slippage and excessive heat generation.
In starting a turbine driven centrifugal pump, the rotation should be brought up to speed as
rapidly as possible. Normal operating speeds are usually attained rapidly and automatically
with motor-driven pumps, assuming proper motor starting. The development of discharge
pressure is essential to flush and lubricate the wearing rings. After initially starting the pump,
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close the discharge valve for a short time. Subsequently, it is always advisable, where
practical, to close the pump discharge valve immediately prior to shutting down a centrifugal
pump. However, discharge valves on operating positive displacement pumps should never
be closed. These pumps can over pressure themselves and downstream lines and
equipment. The following items are suggested for checking prior to run-in:
a. The manufacturer's operating instructions for any specific precautions that should
be observed.
b. Completion of overall installation.
c. Alignment of pump and driver for cold operation. No undue strain by the piping on
the pump or driver is allowable.
d. Cooling fluid piping and seal or gland oil piping:
1. Conventionally packed pumps in hot service are generally furnished with gland
oil. Verify that this installation is correct and complete.
2. For pumps with mechanical seals, verify that all of the components of the
flushing system (such as strainers, separators, restriction orifices and coolers)
have been correctly installed and are clean. Loss of flush or dirty flush may
cause the failure of seals.
e. Packing or seals are installed.
f. Bearings and shafts have been cleaned prior to final lubrication.
g. Pump and driver are lubricated according to lubrication instructions.
h. Rotation of electric motor drivers uncoupled from the pump. Run-in uncoupled for a
minimum of four hours, verifying good motor operation.
During run-in, many pumps are delivering a higher density liquid (water) than the normal
process fluid, but the pumps drivers are sized for the normal pumping fluid. Consequently,
there is potential for the overload of many electric motors. To avoid overloading the motor of
a centrifugal pump, the flow must be limited by throttling the pump discharge valve. When
doing so, if possible, check the amperage usage against design. The following procedure is
suggested for pump run-in:
a. Rotate pump and driver by hand, verifying that they roll freely.
b. Check that run-in water circulation is lined up.
c. Open suction valves fully, venting air from piping and pumps, completely filling with
liquid.
d. Establish flow of cooling fluid, where required.
e. Check that lubrication is satisfactory.
f. Make sure electric power is available from the switch gear to the starter of the
electric motor driver.
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i. Final preparation.
Instrument piping should be inspected visually for completeness and condition of welds and
connections, and tested by pressuring with instrument air and brushing joints with soap
solution. During hydrostatic testing of the plant, control valves should be isolated from the
test system and adjacent drain valves should be opened to relieve any pressure. Control
valve assemblies may be included in the hydrostatic test, provided that it is understood by all
personnel that any leaks at control valve stem packings will be corrected by a qualified
instrument technician. It is generally safer to exclude the control valve assemblies from the
hydrostatic test.
Testing and calibration of instruments should include calibration of transmitters (in place, if
possible), control board equipment, and local controllers. Control valves and positioners
should be adjusted. Temperature transmitters should be checked for proper thermocouple
burnout protection. Meter factor tags and valve position indication on controller output
indicators should be installed at this time, and control actions should be set. ("Tuning")
Instrument air signal lines should be checked for leakage, kinked tubing, and for connections
to the proper port of shutdown solenoid valves and controllers. Thermocouple wiring should
be inspected for proper polarity at the thermocouple head. Point by point verification of the
switch identification at the temperature indicator in the control room can be accomplished by
selecting a point to be checked and opening the circuit at the thermocouple head. With
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proper identification, the corresponding temperature indicator will drive upscale or otherwise
indicate an open circuit. Loop checking involves checking inputs and outputs to ensure that
piping and wiring has been properly installed. A signal should be simulated at the
transmitter, and the control board instrument should be watched for response. The controller
output should be adjusted manually, and the control valve watched for response. Proper
response of control valves to air failure should be verified. All safety relief valves should be
bench tested and set, if this was not done previously during the hydrostatic testing.
Final preparation includes checking instrument piping to verify that valves are in the proper
position, making preliminary control mode adjustments, filling seal pots and seal legs, and
making sure that instrument air and electrical power are supplied to all instruments. It may
also be necessary to have the steam tracing operable at this time.
Commissioning of instruments will be carried out as the plant comes on stream. Differential
pressure instrument piping must be drained to eliminate accumulated dirt and water, and the
instrument zero must be adjusted to obtain a correct zero reading on the indicator scale on
the control board. Controllers must be tuned, interface level transmitters must be zero
checked. Scale, weld slag, and trash must be removed from sticking control valves, and
other malfunctions must be corrected.
For ease of operation, the plant's utility systems should be placed into service as soon as
possible. Lines should be flushed and leak tested. Steam lines should be warmed up slowly
to prevent damage from water hammer. All steam traps and control valves are to be placed
into service and tested. The following list of systems should be commissioned:
a. Plant water and treated water systems. These systems should already have been
commissioned prior to the line flushing procedure.
b. All electrical and light systems, including emergency power backups.
c. All plant and instrument air systems.
d. Nitrogen system.
e. Steam and condensate systems, excluding steam tracing for the moment.
f. All drains and effluent systems.
g. All storage tanks must be thoroughly flushed, leak tested, dried, and perhaps air-
freed if the tank is in hydrocarbon service. Those tanks that have been air-freed
should be left under slight positive nitrogen pressure. All lines to and from tankage
must be flushed, blown dry with nitrogen, and pressure tested.
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The steam tracing, plant cooling water, and flare systems will be commissioned after the
plant pressure test has been completed.
The basic procedure consists of pressuring the vessels and lines in the appropriate circuit to
maximum operating pressure or 3.5 kg/cm2 (50 psig), whichever is less, and then conducting
the pressure test. The test pressure should be held for a minimum of one hour, while every
flange and joint in the system is closely examined for leaks. Stubborn flange leaks may often
be stopped by simply unbolting and re bolting the flanges. Screwed connections may require
Teflon tape.
If steam is used, precautions should be taken to avoid the following potential problems or
hazards:
a. Collapse due to Vacuum: Some of the vessels may not be designed for vacuum. This
equipment must not be allowed to stand blocked in with steam since the
condensation of the steam will develop a vacuum. Thus, the vessel must be vented
during steaming and then immediately followed up with an inert fuel gas or nitrogen
purge at the conclusion of the steam out.
b. Flange and Gasket Leaks: Thermal expansion and stress during warm up of
equipment along with dirty flange faces can cause small leaks at flanges and
gasketed joints. These must be corrected at this time.
c. Water Hammering: Care must be taken to prevent “water hammering” when steam
purging the unit. Severe equipment damage can result from water hammering.
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The flare system should be flushed and drained. Also, the flare header must be purged of
oxygen down to an acceptable level, generally less than 1.0%.
The steam tracing system should be flushed with steam to verify free flow of steam. All
steam tracing and condensate return lines should be checked to ensure that the steam and
condensate are free flowing. After commissioning, the tracing should be checked to verify
that it is hot.
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6.3.9 Line flushing, Air Drying, Cardboard Blasting, Steam blowing& Pigging
with necessary Check List.
Considering the type of fluid handled, pipe material and internal wall conditions, pipe
cleaning method shall be selected.
In general following guidelines will be used for selection of flushing medium.
Water flushing:
Process lines up to 8” size except some critical lines
All water lines
Air Blowing:
Air & N2 lines
Flare header
Process lines above 8”size
Critical process lines
Steam Blowing:
Steam line
Condensate lines
Cleaning By Water
As a rule, water flushing shall be done for pipes in liquid service. If cleaning by water is
unsuitable, other methods will be used. Following procedure shall be adopted for water
flushing.
Low point drains and high point vents should be opened.
Low point flanges should be opened during initial flushing, wherever possible.
All instrument connections should be isolated, orifice plates removed, control valves
dropped or isolated and bypassed. In case there is no bypass facility provided,
remove control valves and flush the line. The valve will be installed after clear water
starts coming out and further flushing may be continued. Orifice plate can be installed
only after the total flushing of the loop is over.
If there is any heat exchanger in the line, flushing should be done up to inlet of heat
exchanger and around the exchanger using bypass line. It should be ensured that
dirty water from initial flushing does not get into the exchanger. Wherever by-passes
are not available, the flanged joint at the inlet of heat exchanger should be first
opened (the exchanger nozzle should be covered thereby isolating the exchanger
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internals) and the line flushed till clear water starts coming out. Then reconnect flange
and flush through the exchanger.
At each opening of the flanged joint, a thin metallic sheet should be inserted to
prevent dirty water from entering the equipment or piping.
The flow of water should preferably be from top to bottom for flushing of heat
exchangers/coolers. The bottom flange of the equipment should be opened to permit
proper flushing.
Flushing should be carried out with maximum possible flow of water till clear water
starts coming out.
Lines which are long and rather big (say over 100 mm dia.) should preferably be
flushed from top to bottom. This will ensure better flushing. Filling the lines and
releasing from bottom is also helpful. Temporary water connection at suitable points
can be made to carry out flushing operation. The run down lines should be flushed
from the unit to the respective tanks or tanks to unit.
It should be ensured in all flushing operations that design pressure of lines and
equipment are never exceeded. After flushing of lines and equipment, water should
be thoroughly drained from all low points. Lines and equipment containing pockets of
water should not be left idle for a long time; it is preferable to dry these lines and
equipment with air after water flushing. During water flushing wherever applicable for
the equipment having demisters, the demisters are to be removed and shall be
installed only after flushing and subsequent drying with air is completed.
For flushing of stainless steel lines and equipment, DM water shall be used.
In case the piping which is used in gas service is being cleaned by water, temporary
pipe supports may have to be installed. Confirmation from engineering departments
should be obtained regarding weight carrying capability of these lines, prior to
introducing water.
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compressed air to be introduced. Air connection is given with PG. Sheets of card
board are cut according to size of the line and depending on rating of flange holes
are made. A special spacer type flanges are used to hold the card board sheet
.Compressed air introduced slowly. Normally 2 to 3 sheets of cards board blast off at
a pressure of 1.5 to 2.0kg/cm2g. The air injection is stopped once the blast occurred.
The process is repeated till very less dust or material comes out of the pipe. The
cleaned loop is blinded and the second one is taken up for card board blasting.
Precautions:
Barricade the area properly and display „No Entry‟ caution board
Inform commissioning in-charge and other workers nearby
Neighboring plants also may be informed
Maintain Operation standby till completion of the job.
Use ear muffs / ear plugs in addition to PPEs
Wherever possible provide air connection at higher location card board blasting at
lower elevation
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Check pipe supports and expansion loops for free movement during
expansion/contraction of pipe. After steam blowing is over, allow the pipe to cool, with
vent open to prevent vacuum pulling. Open drip leg flanges and ensure that water
drained is clear. Then box up the line. Install the control valves and orifice plates.
Steam blowing of steam lines other than steam turbine line shall be done at least for
four times. Each cycle consisting:
o Heating and blowing of pipe by steam
o Cooling
Safety Precautions
All necessary safety precautions given below are to be followed during flushing activities:
Steam blowing pipe surrounding 3-4 meter area to be cordoned off.
Covering electrical equipment like motors, switch board panel, etc.
Covering instruments like transmitters, diaphragm gauges, control valves,
temperature gauges, flow meters, etc.
Provide tags like „DO NOT OPEN, „BLOWING UNDER PROGRESS‟, „DO NOT
REMOVE BLINDS‟, „DO NOT OPERATE THE PUMP‟ etc.
Cover critical equipment nozzles with tags
PSVs to be handled with care and inlet/outlet to be covered
Wearing safety goggles, ear plugs, hand gloves, dust mask, etc.
Proper communication arrangement to be made.
Box-up Checks
For the safe and smooth startup of the plant, a leak proof plant is must. There are several
incidents known when there were major fires during startup, causing serious damage to the
plant, apart from delay in commissioning and startup. In few of the incidents, there were
fatalities as well. Following are some causes, which lead to leakage from flanged joints:
Damaged gasket-seating surface (burr, dents, grooves, etc.).
Improper cleaning of gasket seating surface.
Improper or no serration on gasket seating surface.
Dirty / soiled gaskets.
Damaged gaskets.
Gasket of wrong size, rating and specification.
Improper positioning of gaskets
Use of stud bolts of wrong size and specification.
Improper tightening of flanges.
Short bolting.
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Box up Procedure:
All the loops are completed in all respect.
Check all provided Spacer/Blind tail is given with mark, one hole for blind and two
holes for spacer.
Check the loops as per the P&ID. Ensure each and every item is made as per the
process requirement.
Check the directions of NRV and globe valve and also the position of globe valves.
Check the directions of all control valves.
Check the direction of the Orifices at the time of installation and instrument shall
check the bore size and keep record.
Ensure all the instruments are fitted and boxed up.
Ensure all the high point vents are blinded with proper gasket. (Hydro test vents to be
seal weld)
Ensure all the Low Point Drains are blinded with proper gasket.
Ensure that all the valves are in operable approach.
Check the freeness of all the valves.
Ensure that all the supports, hanger, spring support etc. have been checked and
certified by Maintenance.
Check all the flanges and the gaskets as per the specified spec. Confirm the color
coding of the gaskets
Check the stud and bolts are the spec. Ensure that there is no short bolting. Check all
studs bolt are as per specification given in ISO.
Mark the flanges with yellow paint after the box up is over.
Check for fine mesh at pumps suction.
Check for filter element in the side steam filter.
Vessel manhole to be boxed up in the presence of operation.
The CPP BOP facilities would require passivation of cooling water circuit. The depiction of
lines which require chemical cleaning are shown in mark-up P&IDs which is annexed as
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Annexure 18.23.
6.3.11 Pumps
Proper installation and operation of pumps and drivers is essential for trouble-free
performance. The pumps and drivers should receive careful handling during initial run-in.
The initial run-in of pumps is generally done by circulating water through the new equipment.
Temporary strainers are installed in the suction line of the pumps, conveniently located for
removal and cleaning. The screens also should be positioned so that dirt particles will not
gravitate to inaccessible places when flow is stopped. During run-in of pumps, the strainers
may cause some restriction of flow.
As debris collects in the strainers, flow to the pumps will fall off. When this happens to a
centrifugal pump, it will be necessary to throttle the pump discharge by partially closing the
discharge valve. This will prevent the pump from cavitating, which can cause damage to the
pump. However, also avoid restricting the pump discharge to the extent that it causes
internal slippage and excessive heat generation.
In starting a turbine driven centrifugal pump, the rotation should be brought up to speed as
rapidly as possible. Normal operating speeds are usually attained rapidly and automatically
with motor-driven pumps, assuming proper motor starting. The development of discharge
pressure is essential to flush and lubricate the wearing rings. After initially starting the pump,
close the discharge valve for a short time. Subsequently, it is always advisable, where
practical, to close the pump discharge valve immediately prior to shutting down a centrifugal
pump. However, discharge valves on operating positive displacement pumps should never
be closed. These pumps can over pressure themselves and downstream lines and
equipment. The following items are suggested for checking prior to run-in:
a. The manufacturer's operating instructions for any specific precautions that should be
observed.
b. Completion of overall installation.
c. Alignment of pump and driver for cold operation. No undue strain by the piping on the
pump or driver is allowable.
d. Cooling fluid piping and seal or gland oil piping:
1) Conventionally packed pumps in hot service are generally furnished with gland oil.
Verify that this installation is correct and complete.
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2) For pumps with mechanical seals, verify that all of the components of the flushing
system (such as strainers, separators, restriction orifices, and coolers) have been
correctly installed and are clean. Loss of flush or dirty flush may cause the failure of
seals.
e. Packing or seals are installed.
f. Bearings and shafts have been cleaned prior to final lubrication.
g. Pump and driver are lubricated according to lubrication instructions.
h. Rotation of electric motor drivers uncoupled from the pump. Run-in uncoupled for a
minimum of four hours, verifying good motor operation.
During run-in, many pumps are delivering a higher density liquid (water) than the normal
process fluid, but the pumps drivers are sized for the normal pumping fluid. Consequently,
there is potential for the overload of many electric motors. To avoid overloading the motor of
a centrifugal pump, the flow must be limited by throttling the pump discharge valve. When
doing so, if possible, check the amperage usage against design. The following procedure is
suggested for pump run-in:
a. Rotate pump and driver by hand, verifying that they roll freely.
b. Check that run-in water circulation is lined up.
c. Open suction valves fully, venting air from piping and pumps, completely filling with
liquid.
d. Establish flow of cooling fluid, where required.
e. Check that lubrication is satisfactory.
f. Make sure electric power is available from the switch gear to the starter of the electric
motor driver.
g. Barely open the discharge valve on the centrifugal pump.
h. Start the pump; if the pressure does not build immediately, stop and resolve problem.
i. When the discharge pressure has increased satisfactorily after starting, gradually
open the discharge valve to obtain the desired flow rate.
j. In the event of unusual noise, vibration, overheating, or other abnormal conditions,
shut the pump down immediately. Correct the cause before resuming use of the
pump. Continue to check for abnormal conditions as these may occur after prolonged
operation.
k. Check shaft sealing; mechanical seals should show no leakage. Conventionally
packed stuffing boxes must always be permitted to leak slightly to provide some
lubrication and to prevent overheating. Stuffing box gland nuts are generally only
finger tight. A leaking mechanical seal will show some leakage on startup. However,
after the pump is started and stopped a few times, the leakage may stop.
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l. Operate the pump, directing flows through all suction and discharge piping circuits.
m. Inspect and clean screens as required.
n. Recheck and realign if required, after any disturbance of piping, such as required for
suction screen inspection if pipe flanges have to be parted for screen removal.
o. When shutting down, close the discharge valve first, maintaining discharge pressure
while the pump rolls to a stop. This will protect against the pump rolling backwards
should the discharge check valve leak, and gives the wearing rings a quick flush.
p. After all lines available to a pump have had suitable flushing, the temporary screen
may be removed, but only after it has shown free of debris on two successive
examinations. The permanent strainers may then be installed where required.
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SECTION-7
COMMISSIONING PROCEDURE
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7 COMMISSIONING PROCEDURE
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All valves stroke checked and actuators of actuated valves taken into operation.
Ensure that all instruments calibrations have been checked, instrument loop checks
have been completed and the instruments have been taken on line and verified. DCS,
PLC, ESD and other control systems (as applicable) are operational.
Ensure that all the utilities like instrument air, power, UPS system, fire water are
available prior to commissioning.
Ensure that safety systems like Fire alarm/protection system, Fire and Gas detection
system are operational. Portable fire extinguishers and breathing apparatus are in
position. Fire tenders are available on all.
Ensure that safety barriers are erected around dispatch & receiving stations and no hot
work or any other construction work is carried out within 100m radius. No other
ignition source is present in the vicinity of the facilities.
Ensure that relevant authorities have been notified and are in attendance if required.
Ensure that all necessary personnel are present and fully briefed regarding their
functions and responsibilities.
No cars/trucks are allowed to be within the region without mufflers.
Ensure that safety officers are in attendance with portable gas detectors at dispatch and
receiving terminals.
A discussion and lists of the major points that must be examined in the inspection of the areas
are listed as following. Check List described in earlier section must also be perused along with it
as the points discussed here may be repetitive or in addition to those mentioned previously.
7.2 Piping
The unit must be constructed in accordance with Piping and Instrumentation Diagrams
(P&ID's), including all details, elevations, dimensions, arrangements, and other notes on the
P&ID's. One must be able to startup, shutdown and conduct normal operations on the unit as
envisioned in the licensor design. Also, piping for special procedures such as dry-out, special
materials preparation, regeneration and/or alternative flow schemes may have been
incorporated into the unit's design, and the unit should be able to operate in all of these modes
with piping as designed and constructed.
If the unit is connected to other process facilities, adequate means must be provided to receive
feed from or send products to these facilities without contamination of these streams, and
minimize as much as possible the effects of upsets of other process units especially where
contamination of feed or product stream might occur. Check all tankage interconnections to
minimize the possibility of stream contamination outside of the battery limits. Check that
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adequate means of measuring flows, pressures, and temperatures, and sampling of all process
streams has been provided.
The following items must be checked to ensure conformity to the design specifications:
Flanges: rating, facing, and metallurgy; type (typically, 2" and smaller are socket weld,
2½" and larger are weld neck flanges).
Gaskets: type; metallurgy (materials of retainer, jackets, winding, filler, etc.); thickness,
ring size, etc.
Fittings, connections and couplings: rating and metallurgy.
Valves: rating and metallurgy (body, trim, seats, etc.); packing; seat inserts; bonnet
gaskets; grease seals; socket-weld or flange type, rating and facing; installed in correct
direction of flow; lubricant provisions; gear operators; extended bonnets; stops; ease of
operation.
Bolting: stud or machine bolts; bolt and nut metallurgy; bolt size.
Pipe: metallurgy, thickness; seamed or seamless; lining.
Tubing: size and thickness; metallurgy; seamed or seamless.
Gauge glasses:
- Through-view types should have rear-mounted lights.
- Design pressure and temperature.
- Special materials of construction.
- Drains to safe location.
- Visible from grade (or platform, if required).
Pressure relief valves:
- Size and style.
- Lever requirement.
- Inlet / outlet flange material, facing and rating.
- Set pressure - must be bench tested.
- Metallurgy of nozzle, disc, spring, etc.
- Type (pilot operated, balanced, etc.).
- Inlet / outlet block valves car-sealed open; valve stems installed in horizontal or
below.
General:
- Utility systems within the battery limit should follow all relevant pipe class
specifications in the same detail required for process lines.
- Package systems (modular units, etc.) shown on the EIL P&ID should follow all
relevant pipe class specifications in the same detail required for other process
lines.
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7.3 Tanks
Following are the general instructions for pre- commissioning and commissioning of cone
roof tanks within CPP, e.g. DM Water/ Condensate Storage Tank, HSD Storage Tank, LCO
Storage Tanks and CLO Storage tank.
Pre-commissioning
Internal Inspection
Open the manhole cover for internal inspection and inspect the tank from inside.
The manhole cover shall be fixed back after completion of inspection with proper
gasket.
Check the tank and connected piping installed as per data sheet & P&ID. Shell,
roof appurtenances and accessories are provided and internals are complete.
Check nozzle orientation/drain elevation, etc.
Ensure drain lines, sump are cleaned.
Ensure tank bottom is properly sloped towards water draw off sump.
Check roof vent is properly working condition.
Check the cleanliness of tank bottom, shell and internals.
Check the condition of internal coating and painting.
Check for installation and functioning of level instruments.
Check alignment of gauge hatch, gauge hatch reference for easy operation & dip pipe
for communication holes at regular intervals, etc. as per drawing.
Ensure removal of blind plates and blind gaskets from nozzles wherever
applicable.
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Check the datum plate arrangement and its position from tank bottom.
Check Steam heating coils are isolated.
External Inspection
Check the moving of ladder/rails/wheels on the roof top for greasing and easy
movement.
Check for provision of fire-foam connections with rupture disc. (Glass)
connections.
Check whether earthing connections and lightening arrestors are provided.
Ensure that calibration is done for all the instruments as well as check their mountings.
Check dyke and drainage system.
Check for breather arrangement and their cleanliness.
Check for fire water spray arrangement.
Check whether hydraulic test and external paining subsequently are over after site
fabrication.
Check the platform for safe operation and maintenance.
Check that the connected pipelines/fittings are erected/ supported as per the
engineering.
Check the foundation bolts for proper size and tight fixing.
Check the accessibility of all the valves connected to the tank nozzles.
Check insulation for the tank is completed.
Commissioning
Once tank-inspection is over fix the cover back with proper gaskets.
Ensure removal of blind plates and blind gaskets from nozzles wherever
applicable and box-up the piping with proper gaskets.
Ensure that fire water is available for emergencies.
Close all drain and vent valves on tank and piping. Close all valves on tank nozzles.
Open drain valve to purge air from the tank. Close the drain valve and check if stable
pressure is maintained.
Now the tank is ready to receive feed (e.g. HSD). Open inlet valve. Line up the HSD
product to the tank inlet. During filling operation look for any leakages from flange joints,
manholes, etc. of the tank. In case of any leakage, stop filling operation and take
corrective action. Care must be observed so as not to fill the tank above its safe filling
height.
When the steam coils are submerged check from the drain points of the
steam/condensate line if there is any oil leakage. Leakage of steam coils is not
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accepted.
Charge heating steam and line up steam traps to maintain proper product
temperature. Steam to be lined up only when steam coils are submerged in liquid.
When the feed nozzle is almost submerged, increase feeding rate by slowly opening
inlet isolation valve at manifold. Level rise can be checked from LI and LT.
Never fill the tank beyond its safe filling height.
7.4 Pumps
7.4.1 Centrifugal Pumps
Specification Check
The design specifications should be reviewed against the pump curves and data given by
the vendor to confirm agreement on the following:
Head and capacity.
Pressure and temperature rating.
Speed.
NPSH requirement.
Pump type, materials of construction, flange ratings, seals, bearings, number of
stages, lubrication and cooling systems, etc.
Type of driver.
Balancing lines for multistage pumps must have flanged joints (not unions).
Field Inspection
The following items should be checked in the field (as applicable):
Sight flow indicators, inlet/outlet shutoff valves on cooling water lines.
Thermometers/pressure gauges for gland seal and flushing oil manifolds.
Restriction orifices (if required) present in seal flush manifold piping.
Pedestals on pumps operating over 500°F (260°C) should be water cooled.
Cooling water to mechanical seals on pumps operating over 250°F (121°C).
Proper direction of rotation.
During pump trial run with water, it is to be ensured that pump motor is suitable for operation of
increased load due to pumping of water. Also such operation may need approval of pump
vendor/specialist rotary group engineer in certain cases. Pump suction strainer during initial
trial run should be finer (typically 40 mesh). This can be replaced with a coarse strainer
(typically 6 to 8 mesh) or as recommended by pump vendor during normal duty. During trial run
of the pump, seal flushing line can also be charged with pumping fluid, only if approved by
pump and mechanical seal vendor.
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Commissioning
For starting the pumps,
1) Line up sealing system to the seals as per vendor‟s instructions.
2) Settle the source tank as per prevailing operating practices of the COMPANY and drain
accumulated water from the tank drain (as applicable).
3) Identify one of the source tanks. To line up the circuit open tank inlet/outlet body valves,
valve in pump suction line at tank manifold, pump suction/discharge valves, valves
in minimum flow spill back line to the identified source tank. Only one tank outlet valve
should remain open at a time else it may lead to undue transfer of product from one tank to
the other.
4) Valve line up of different products with different tank and pump combinations shall be
followed as per P&ID.
5) Charge the pump‟s suction and discharge lines with the process fluid. Look for any
leakages and correct as required.
6) Open drain/vent, as required to ensure that the all air has been removed from the pump
casing and the piping. Entire piping from tank to pump and pump discharge circuit
(maximum practical and permitted by process) may be charged with the fluid before starting
the pump.
7) Open minimum flow control valve manually to 20-30%. Close the pump discharge valve
and crack open it.
8) Energize the pump motor and kick start to ensure proper direction of rotation.
9) Start the pump motor. Look for any unusual vibration. Check that the pump discharge
pressure gradually builds to a stable value near its normal operating pressure.
Ensure that the shut off pressure is within the specified limit. Open discharge valve
gradually and check the parameters like suction/ discharge pressures, current and flow.
Ensure that the minimum flow protection system is controlling flow properly at the set value.
Look for any leakages and take necessary corrective action.
10) Check for any abnormal sound or excessive vibration. Get the pump vibration checked.
Stop the pump in case of any abnormal scenario and take corrective actions as required.
11) Sometime after pump running, feel bearing, motor to ensure that these are not overheated.
After successful running of one pump, charge the standby pump and run it in the same way.
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BALANCE OF PLANT, DANGOTE,
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Shut Down
1) Close discharge valve fully if pump is single stage. If pump is multi-stage, having high
tension electric motor, follow pump vendors instructions particularly regarding minimum
continuous flow requirements.
2) Stop the pump if pump is going to remain as stand by and has provision for keeping the
pump hot, proceed as follows:
Open the valve in the bypass line across the discharge valve and check valve.
The circulation rate should not be so high as to cause reverse rotation of idle pump
or overloading of the running pump. Reverse rotation of pump may have adverse
effect on thrust bearings as they are not designed for the same.
If pump is to be prepared for maintenance, proceed as follows:
Close suction and discharge valves.
Close valve on check valve by-pass line, if provided.
Close cooling water to bearing, if provided.
Close external flushing liquid to mechanical seals, if provided.
Open pump casing vent.
Slowly open pump bleeder and drain liquid from pump. If the liquid is very hot or
cold, allow sufficient time before draining is started. Ensure that there is no
pressure in the pump. Also drain pump casing.
Blind suction, discharge, check valve by-pass line and pump minimum flow line
Cut off electrical supply to pump motor prior to handing over for maintenance.
Trouble Shooting
1) Pump not developing pressure
Bleed/ vent pump casing.
Check the lining up in the suction side.
Check the suction strainer.
Check the liquid level from where the pump is taking suction (physical verification).
Check pump coupling and rotation
Check the foot valve (in case of vertical lift pumps).
Check the temperature of liquid. If it is higher than for what the pump has been
designed, available NPSH may come down.
Check for any air leakage in the pump suction line or pump casing.
2) This may occur at various joints and packing boxes as the packing ages.
Unusual Noise
Check if coupling guard is touching coupling.
Check for proper fixing of fan and fan cover of the motor.
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BALANCE OF PLANT, DANGOTE,
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BALANCE OF PLANT, DANGOTE,
DORC-LEKKI,NIGERIA Page 101 of 161
Commissioning
1) Check if all mechanical jobs are completed.
2) No load run of the motor to be carried out before coupling with the pump. Start the motor
and check direction of rotation. If wrong correct it. De-energize electrical supply. Couple the
motor with the pump.
3) Flush and renew oil in pump gear box.
4) Check whether suction/discharge blinds are removed.
5) Check whether suction strainer is installed and is clean.
6) Check for proper lining up including the pulsation dampener and pressure safety valve in
the discharge. Open suction valve fully.
7) Check that the motor shaft is reasonably free and coupling secured. Coupling guard should
be in position.
8) Energize motor. Open discharge valve. Start the pump. Never start the pump with
discharge valve closed.
9) Adjust the pump stroke in case of dosing pumps and run the pump at desired settings.
Watch discharge pressure and check the rate of pumping using the flow meter or by taking
suction from the calibration pot. The valve on the recirculation line (provided in case of
gear-pump, screw pump etc.) shall be adjusted to obtain the required discharge pressure.
10) Care should be taken to avoid dry running of pump and back flow of liquid. Bleed if
necessary to expel vapor/air.
11) Check for unusual noise, vibrations, rise of temperature of both motor and pump.
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Shutdown
1) Stop the pump.
2) Close the suction and discharge valves.
3) Drain the liquid if maintenance jobs are to be carried out on the pump. Flush pump casing.
4) De-energize the motor before handing over to maintenance.
Trouble Shooting
1) Insufficient discharge pressure:
Check the line up in suction side.
Check suction pressure.
Check the functioning of the safety valve and pressure control valve on
Discharge to suction.
Check the strainer on the suction side.
Check for insufficient liquid level in the vessel from which pump is taking suction.
Check pumps coupling and rotation.
Get the pump checked by pump technician.
2) High Discharge Pressure
Check the line up on the discharge side.
Check pressure control valve opening.
3) Leaky Gland
Check for normal pump discharge pressure
Tighten the gland nut slowly if possible.
Handover the pump for replacing gland packing.
4) Unusual Vibration
Check the foundation bolts
Check motor fan cover for looseness.
Stop the pump and hand over to maintenance.
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7.5 Instrumentation
All personnel on site should check to ensure that the instrumentation is provided as specified;
that it is functional; and that a minimum of instrumentation problems will occur when the unit is
commissioned. Some of the basic items which must be checked include the following:
Instrument type, range, and size.
Materials of construction and rating of instrument, accessories, and connecting
Piping, flanges, and valves.
Accessibility of instrument for routine checks and maintenance; rigidly mounted.
Installation according to correct drawing details.
Accessories (pulsation dampeners, filter/regulators, diaphragm seals, excess flow
checks, seal pots).
Location of local indicators so they are readable from grade platform or controller
assembly, as required.
Process requirements of flow, temperature, pressure, differential pressure, specific
gravity, etc.
Controller type, number of modes, chart type, range, cascades.
Power requirements of voltage, frequency; emergency power supply and connections.
Calibration of controllers, transmitters, analyzers, special instrumentation.
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Control valve, block and bypass valve sizes for control valve assemblies.
Preparations
Before undertaking any flushing operation, in-line instruments like flow measuring
elements, control valves, static mixers, which may get plugged or damaged due to debris
must be dropped and replaced with temporary spool pieces. If spool piece is not provided,
upstream and downstream pipes may be flushed separately. Strainers should be removed.
All pressure tappings and safety valves should be isolated to ensure that the debris does not
enter in them. All equipment should be disconnected from piping and slip plates should
be provided at the nozzles so that flushed out material does not enter into the tank.
Flushing should be carried out with sufficient flow such that any debris not by picked up
during normal operation. As a normal practice drag force exerted by the flushing fluid should
be more than that of normal process fluid. Drag force is defined by velocity head (density x
square of velocity) of fluid. In larger diameter pipes, required flow shall in general be
prohibitive. Such pipes can be cleaned by pressurizing and depressurizing by bursting disc
of cardboard or gasket material.
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If this method is resorted, it must be ensured that pipe is properly supported and exit end of
the pipe should be provided with temporary fasteners/supports so that the pipe does not
move from its position. Mechanical group must be consulted before deciding on the method
for suitability of this method for the subject piping loop. Cordon off the area so that flying
pieces of solid material do not injure any one. After air blasting, gentle air blowing and
cleaning of drains/vents shall be carried out.
Steam flushing shall be done mainly for steam lines. It is preferable that insulation should be
complete; otherwise when steam is opened lot of condensate formation will take place. Hot
un-insulated pipes may cause injury to personnel. When cleaning by steam is performed
thermal expansion of pipe should be taken into consideration. Following procedure
should be followed.
1) Disconnect equipment to avoid entry of flushed material.
2) If necessary, make temporary arrangement for steam blowing at open end of the
pipe.
3) Open steam trap bypass valves, and isolate steam traps.
4) Slowly allow steam to heat the pipe and then flush thoroughly with a strong flow of
steam. Avoid steam hammering by draining condensate properly. Repeat this
operation after allowing the line to cool for effective flushing.
5) Check pipeline supports and loops for expansion.
6) After blowing is over, allow the pipe to cool, with vent open to prevent vacuum
pulling. Open drip legs flanges and remove accumulated muck. Then box up the line.
Install the control valves and orifice plates.
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1) Ensure that the system that is to be tested is isolated from the rest of the
system.
2) Take the system gradually to a pressure of 1-1.5 kg/cm2g or the operating pressure,
whichever is lower. Check all flanges, joints, manholes etc. for any leakage with
soap solution. Design pressure of the system should never be exceeded.
3) If the operating pressure of the system is more than 1.5 kg/cm2g, slowly raise the
pressure of the system in the stage of 1.0 Kg/cm2g at a time to 3.5-5.0 kg/cm2g.
After each stage check for leaks using soap solution. Attend the leaks if any.
4) Leak testing is complete at 6.0 -7.0 Kg/cm2g. Additional tightness test can be carried
out when the pumps are tested with the process fluid.
7.14 Drying
Systems that have been water flushed or steam flushed may require complete drying before
hydrocarbon can be taken in. If slugs of water are to be removed, the system is initially
blown hard with a strong flow of plant air. Necessary temporary connections for air inlet and
outlet are to be made. Since plant air can give rise to about 7 Kg/cm2g pressure on
blocked out conditions, care should be taken to ensure that line design conditions are
not exceeded.
Ensure that there is no inadvertent closing of valves during air blowing & adequate venting is
available. When major portion of water has been removed, the air drying can be continued
with compressed utility air to make the system completely dry. For pre-specified critical
services, the plant air is to be heated up to 80ºC and blown through the system followed by
instrument air or Nitrogen. Alternatively the line can be blown through by N2 from Nitrogen
cylinders. Portable dew point instrument is to be used to measure the dew point of exit air.
Normal recommended value is - 40 Deg C at Atm pressure.
It is advisable to take up small systems at a time for drying. After drying these are to be
isolated and kept sealed with Nitrogen. While blowing with hot air, precautions are to be
taken to take care of thermal expansion of pipes.
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If the system can operate under vacuum, it is advisable to pull vacuum and refill with N2. In
this case N2 consumption can be reduced to a maximum of 3 times the system volume. HC
is taken while the system is still under slight positive N2 pressure.
7.16.1 Motors
Manufacturer‟s lubrications schedule should be used to ensure that all lubrication points
have been serviced. Each motor should be checked and started on no load. Ensure that it
has the correct direction of rotation. The motor speed should be checked with tachometer to
ensure that RPM is correct. After a short run each bearing should be felt to ensure that it is
free and not over heated.
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7.16.2 Pumps
Generally the pump casing is opened and checked to ensure that it contains no
foreign materials. Pump casings need not be opened up in case the pump had been stored
carefully and the blinds covering suction and discharge nozzles were not removed in
storage or in transit. Cleanliness of suction line and installation of fine mesh strainer should
be ensured. Pumps and motor will be aligned.
As such the system configuration allows for running of all pumps individually without any
dependence to other systems. For example HSD transfer pump may be run on recirculation
back to HSD storage tank without delivering any net flow to downstream system. Therefore,
as such, there is no need to run these pumps on water and the pumps may be run
directly on the designated hydrocarbon fluid. However, if it is decided to carry out trial run of
pumps on water, vendor must be consulted for the required arrangements and precautions.
Temporary connections may have to be made for providing suction to the pump and
collect pumped water.
When running a pump designed for hydrocarbons tested on water, the discharge valve may
have to be throttled, so that the rated current is not exceeded. Ensure that the vents and
drains of the pump are clear. Pressure gauge tapping will be flushed and filled with
sealing fluid wherever necessary.
7.16.3 Instruments
Instruments will be checked, starting from the controller and proceeding logically
through the control loop. Cascade control system will be checked from the impulse point of
primary loop. Operating crew should check proper mounting of control valves. The shutdown
systems of the equipment should be checked by simulating the various conditions in the
control circuits, including the fail safe positions.
Orifice Plates
Before each orifice plate is installed, the orifice taps should be blown clear. The
orifice plate should be callipered to check if the correct size orifice plate is being
installed. The plate should then be installed after checking for the correct direction. Particular
attention should be given to weep holes of orifice, where ever provided.
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Control Valves
Ensure that control valve port is clean. Release control valve hand jack (if provided) is
released. Put on instrument air supply to control valve. Look for any undue leakage of
instrument air. Control valves operation shall be checked with signal from DCS. Typically
stoke should be checked at 0, 25, 50, 75 and 100% opening of the valve, both ways, i.e.
during valve opening and closing. Check valve operation time, any hunting (stability).
Ensure that valve operation is smooth (not jerky).
Alarms
All alarms, auto start and cut off system should be checked by simulating the
conditions.
Start-Up/Shutdown Logic
Check the sequence of startup/shut down interlocks by simulation.
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SECTION-8
NORMAL STARTUP PROCEDURE
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This section covers the normal start up procedure for balance of plant facilities within CPP.
For major package equipment within CPP, refer respective vendor‟s operating manual such
as for GTG, HRSG, Utility Boiler, STG and Deaerator.
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Cooling Water
The utility headers within CPP shall be charged with respective utilities and shall be used for
start-up activities of all equipment within CPP. DM water and polished condensate shall be
stored in DM water/ condensate storage tanks before being pumped for further use within
CPP. Major package equipment within CPP such as GTGs, HRSGs, Utility Boilers, STGs,
Deaerator, NG conditioning skid, etc. shall be commissioned first for startup of CPP. Utility
required for the commissioning of these package units shall be identified and shall be
prioritized and made available for CPP startup.
In addition to above, the drain network (OWS, CRWS & storm sewer – as applicable), closed
blow down system within CPP, CPP Condensate handling system (UB condensate handling,
atmospheric condensate handling and tracer/ trap condensate handling within CPP) shall
also be commissioned and be available before CPP startup.
Since, steam generation source is within CPP, the steam network inside CPP can be only
commissioned after startup of first Utility Boiler/ HRSG. Similarly, for start-up of first GTG for
power generation, emergency DG set provided within CPP shall be utilized for drives
required for first GTG operation.
8.4 Start-up of Fuel Oil System within CPP (HSD, CLO and LCO)
Once all the pre-commissioning and commissioning activities are completed, the tank which
is intended to be filled is lined up with the feed piping from CPP B/L. For start-up of first
Utility boiler and GTG/ HRSG, HSD is the preferred fuel. Once the refinery is put in to normal
operation/ when the other fuels are produced from other process units in refinery, the LCO
and CLO fuel handling systems shall be started. For LCO and HSD fuel, CPP is also
provided with respective centrifuge and hence before taking the fuel in HSD/ LCO storage
tanks, the centrifuges shall also be commissioned.
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In addition to HSD storage tank, the LCO storage tanks provided are also designed to
receive and distribute HSD during refinery startup operation. During HSD system startup,
before lining up the tank for transfer, it should be ensured that sufficient time is provided for
centrifuging operation for separation of water and sediments. Once the centrifuging
operation is complete, the tank content is sampled before lining up the tank for further
transfer using transfer pumps to GTG or utility Boiler.
For lining up the tank to transfer pumps, open tank outlet valve. After this, open pump
suction valve and minimum flow recirculation valve. In case of common transfer from two
tanks (case of LCO storage tank) as soon as the suction valve gets opened, close suction
and recirculation valve of other tanks which are floating with the same pump (suction).
In case of two tanks, when one of the tank level reaches near high level, the other tank is to
be prepared for lining up. Before lining up the second tank, note the initial level of the tank.
The second tank is lined up by opening the inlet line valves of the respective tanks and by
closing the inlet line valves of other storage tank after ensuring the tank level of the newly
lined up tank is rising. In case of single tank, the respective tank inlet valve shall be closed
when the level reaches near high level. The HSD shall then be pumped to GTG battery limit
and other users in CPP.
Since all the tanks within CPP are nitrogen blanketed, nitrogen is to be charged from OSBL
header to nitrogen lines within CPP. Before starting the transfer of fuel in to storage tank, the
availability of nitrogen in the respective tanks along with the pressure control valves in
nitrogen blanketing lines shall be ready.
8.5 Start-up of Natural Gas/ Fuel Gas/ Propane System within CPP
Once all the pre-commissioning and commissioning activities are completed, the NG KOD
shall be lined up with natural gas feed piping from CPP B/L. The condensate separated (if
any) from NG KOD shall be collected in NG condensate drain tank and shall be disposed of
manually based on level monitoring in NG condensate drain tank. Then Natural gas shall be
supplied to end users. For routing it to GTG‟s the GTG NG forwarding skid is to be ready.
Similarly, for routing the Natural gas to UB and HRSG, the NG heater and control valves
provided in NG heater downstream shall be commissioned and be ready. Natural Gas (if
available) is the preferred fuel for Utility Boiler Start-up.
Once liquid propane is made available from refinery operation, the same shall be routed
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within CPP. Once it is ensured that the Liquid propane line is charged and Propane
forwarding skid (supplied by GTG vendor) is commissioned and ready for startup, the liquid
propane transfer pumps within CPP shall be started.
8.6 Start-up of DM Water/ Condensate Storage/ Deaerator/ BFW System within CPP
The DM Water/ condensate storage tank which is intended to be filled is lined up with the
feed piping from CPP B/L. For start-up of first Utility boiler and HRSG, the readiness of this
system is essential. As start-up provision, DM water (for Boiler initial filling) from the main
DM water header within CPP shall be routed directly to Utility Boiler B/L. Once the LP steam
is made available within CPP after utility boiler startup, Deaerator/ BFW pumps shall be
started and BFW generated shall then be used for steam generation.
Polished/ Pure Condensate as and when made available at CPP battery limit shall also be
utilized within CPP. As a precaution, regular sampling of DM water, condensate and BFW
stream shall be carried out and to be reported and checked with acceptable limits. If there
arise a deviation in the quality of these streams, package vendor of utility boiler and HRSG
shall be immediately consulted with regarding acceptability of the same.
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All cooling, heating and flush lines must be started and regulated (as applicable)
Start driver (typically electric motor)
After pump is running, adjust the discharge valve slowly until the desired flow is
reached
For pump equipped with mechanical seals, check for seal leakage – there should be
none.
For pumps with shaft packing, observe the leakage from the stuffing boxes and adjust
the sealing liquid valve for proper flow to ensure the lubrication of the packing. If
packing is new, do not tighten up on the gland immediately, but let the packing run in
before reducing the leakage through the stuffing boxes.
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SECTION-9
NORMAL SHUTDOWN
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9 NORMAL SHUTDOWN
For shutdown operation of major package equipment within CPP, refer respective vendor‟s
operating manual such as for GTG, HRSG, Utility Boiler, STG, Deaerator, centrifuge, etc.
CPP is designed for round the clock operation but shutdown of individual equipment may be
carried out depending on the periodic maintenance schedule.
Following are the general guidelines for taking balance of facilities in to shut down for
maintenance activities:
Equipment within CPP handling hydrocarbon is to be emptied following normal refinery
safely practices pertaining to venting, draining, disposing of hydrocarbon, blinding, and
steam out.
Fuel Tanks
- Isolate feed inlet valve and recirculation valve at the manifold.
- Pump out maximum possible liquid – until the transfer pump loses suction.
- A temporary pump requiring lower NPSH may be deployed for further tank
emptying out. Suction of the pump is connected to the drain point of the tank
being decommissioned for maintenance and its discharge is connected to other
similar product tank or to drain network. Pump discharge may be connected to
the available stub in connection or to the drain point at the manifold.
- In case of viscous fluid (for CLO fuel), sometimes flushing oil is mixed before
final emptying out.
- Remaining oil in the tank may be collected in drums / pit through drain line.
Congealing products should not be drained in to OWS. For draining suitable
provision may have to be made by removing drain line spool piece and
connecting it to drums/pit. However, deploying a temporary pump is better
option as the remaining oil quantity will be substantial.
- Put blind in all the available nozzle of the tank towards the tank side to isolate it
from the system.
- In case of tank heating provision, heating source shall be cut off before starting
the decommissioning activities.
- After emptying out, open the manholes (on the shell) and allow the tank to
cool down.
- As flashpoint of the liquids is high (<65°C) natural ventilation is sufficient, but O2
and Hydrocarbon vapor concentration must be checked before man entry.
- Before handing over the tank for maintenance work the residual oil/ sludge/
water are required to be removed.
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For pumps within CPP, the shutdown procedure is just the reverse of startup sequence.
For centrifugal pumps the discharge valve is to be closed slowly, then the driver to be
shut down and finally the suction valve to be closed. For positive displacement pumps
the discharge valve should never be closed when pump is running.
For natural gas/ fuel gas handling facilities, the fuel supply from battery limit is to be cut
off first. Then depressurization of the piping and KOD shall be carried out through vent
lines and the contents to be flared.
To ensure complete removal of fuel gas from the system, the equipment shall be
subjected to steam out operation. Any vessel entry shall only be allowed after ensuring
the O2 and HC vapor content and process blinds are in place.
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SECTION-10
EMERGENCY PROCEDURE
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10 EMERGENCYPROCEDURE
10.1 General
The emergency procedure for shutdown of the CPP Balance of Plant facilities is identical to
those of the normal shutdown procedure.
Emergencies must be recognized and acted upon immediately. The best way to be prepared
for an emergency is to ensure that the proper procedures are in place and that all operators
are fully trained in these procedures. The operators should have an understanding of the
unit and the procedures, which enables them to devise a course of action. Some general
outlines are provided for the following emergency situations.
A. Explosion, Fire, Line Rupture
B. Leaking Valves or Vessels
C. Power Failure
D. Instrument Air Failure
E. Cooling Water Failure
F. Loss of DM Water/ Pure Condensate/ Polished Condensate
G. Loss of Fuel
For above scenarios of various emergencies and their impact on major package equipment
within CPP, refer respective vendor‟s operating manual such as for GTG, HRSG, Utility
Boiler, STG, Deaerator, centrifuge, etc.
Exact procedures cannot be provided for every type of emergency situation. General
procedures for the most common types of emergency situations follow. With an
understanding of these procedures and the various concerns outlined above, the operators
should be able to devise a course of action for the various situations that can arise.
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SECTION-11
GENERAL EQUIPMENT OPERATING
PROCEDURES
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11.1 General
In any unit, the unit has many operating variables, which influence the process parameters,
efficiencies, utility consumption, etc. The process specification for this unit is used only as a
guide as equipment design variations and other factors can and will cause a change in
these process conditions. It is, therefore, up to the unit operators, supervisors, and the
other personnel involved in the startup and subsequent operation of the unit to see that the
unit is being operated at maximum efficiency.
The most useful tool for detecting operational difficulties is the log sheet and listed readings.
The boardman must be careful to list each reading correctly at the appointed time. It is then
important to review all of the readings to determine what and if any changes have occurred.
The cause of any change must be determined; corrective measures can then be taken if
needed.
The outside operator should review the process equipment operation during his routine
duties and report any abnormalities (leak, noise, etc.) to the control room personnel. Proper
coordination between the boardmen and the outside operators is essential for good
operation. The following section will highlight each major piece of equipment and its
operation. This section covers the general procedure for operation and trouble shooting of
commonly used equipment like pumps, heat exchangers and furnace etc. For specific
information and more detail refer to vendor‟s manuals. Further, for major package equipment
within CPP, refer respective vendor‟s operating manual such as for GTG, HRSG, Utility
Boiler, STG and Deaerator for general equipment operating procedures.
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Energies the motor. Start the pump and check the direction of rotation. Rectify the
direction of rotation if it is not right.
Check the discharge pressure. Bleed if necessary to avoid vapour locking.
Open the discharge valve slowly. Keep watch on the current drawn by the motor, if
ammeter is provided. In other cases check at motor control center.
In some pumps a by-pass has been provided across the check valve and discharge valve to
keep the idle pump hot. In such pumps, the by-pass valve should be closed before starting the
pump. It should be ensured that casing of these pumps are heated up sufficiently prior to
starting of the pump to guard against damage of the equipment and associated piping due to
thermal shock.
Shutdown:
Close discharge valve fully.
Stop the pump
If pump is going to remain as standby and has provision for keeping the pump hot, proceed as
follows:
Open the valve in the by-pass line across the discharge valve and check valve.
The circulation rate should not be so high to cause reverse rotation of idle pump and
also overloading of the running pump.
Trouble Shooting:
1. Pump not developing pressure
Bleed to expel vapour/air
Check the lining up in the suction side.
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2. Unusual Noise
Check the coupling guard if it is touching.
Check for proper fixing of fan and fan cover.
Check for pump cavitation.
Get the pump checked by a technician.
4. Hot Gland
Adjust cooling water if facility exists.
Slightly loosen the gland nut, if possible.
Stop the pump and hand over to maintenance.
Arrange external cooling if pump has to be run for some time.
5. Unusual Vibration
Check the foundation bolts.
Check the fan cover for looseness.
Stop the pump and hand over to maintenance.
6. Leaky Gland
Check the pump discharge pressure.
Tighten the gland nut slowly, if possible.
Prepare the pump for gland packing or adjustment/replacement of mechanical seal
as the case may be.
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Shutdown
Stop the pump.
Close the suction and discharge valves.
Drain the liquid if maintenance jobs are to be carried out on the pump.
Trouble Shooting
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3. Leak Gland
Check for normal pump discharge pressure.
Tighten the gland nut slowly if possible.
Handover the pump for replacing gland packing.
4. Unusual Vibrations
Check the foundation bolts.
Check motor fan cover for looseness.
Stop the pump and hand over to maintenance.
The exchangers have been provided with draining and flushing connections. The coolers
and condensers have been provided with TSV‟s on the cooling water side to guard against
possible rise of pressure due to faulty operations with the safety release to atmosphere.
Temperature gauges or thermo wells have been provided at the inlet and outlet of
exchangers. Where water is the cooling medium, no temperature measurement is provided
for water inlet temperature which is the same as cooling water supply header temperature.
Air Coolers
The air coolers/condensers comprise of a fin tube assembly running parallel between the
inlet and outlet headers. These are of the forced draft type. The forced draft fans provided
have auto variable speed rotors in which the fan speeds are adjusted during rotation. This
allows variation in air flow as per the cooling requirements. A high vibration switch is
provided with alarm to indicate any mechanical damage.
Heat Exchangers
Shell and Tube type heat exchangers can be broadly classified into different types. Start-
up/shutdown procedures for each unit shall vary slightly from case to case. However,
general start-up/shutdown procedures are discussed in the following paragraphs:
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Start-up
After the heat exchanger has been pressure tested and all blinds removed, proceed as
follows:-
1. Open cooling medium vent valve to displace non-condensable (air, fuel gas, inert gas
etc.) from the system. Ensure the drain valves are capped. For high pressure system,
drain valves should be flanged. This activity is not required if gas is the medium.
2. Open cooling medium inlet valve. Close vent valve when liquid starts coming out
through it, then open cold medium outlet valve and fully open the inlet valve also.
Where cold medium is also hot, warming up to cold medium side gradually is also
essential.
3. Open hot medium side vent valve to displace non condensable (air, fuel inert gas
etc.). Check that the drain is closed and capped. This activity is not required if gas is
the medium.
4. Check open hot medium inlet valve. When liquid starts coming out from the vent
valve, close it. Open hot medium inlet valve and then open the outlet valve fully. In
case of steam heaters, initially the condensate shall be drained to sewer till pressure
in the system builds up to a level where it can be lined up to the return condensate
header.
5. In case by passes are provided across shells and tube side, gradually close the
bypass on the cold medium side and then the bypass across the hot medium side.
6. Check for normal inlet and outlet temperatures. Check that TSVs are not popping.
7. The operation of inlet and outlet valves should be done carefully ensuring that the
exchangers are not subjected to thermal shock.
8. In case of coolers/condensers, adjust the water flow to maintain the required
temperatures at the outlet.
9. For avoiding fouling, velocity of water should be at least 1 m/sec in a
cooler/condenser.
Shutdown
Shutdown of an exchanger, coolers, and condenser is considered when the equipment is to
be isolated for handling over to maintenance while the main plant is in operation. The
following is the suggested procedure for isolation of the piece of equipment.
1. Isolate the hot medium first. In case both hot and cold medium are from process
streams, exchanger shall remain in service till the hot stream has cooled down
enough.
2. In case of a cooler, adjust cooling water flow to the cooler which is in line so that
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SS-10 66/11.5
SS-09 (ETP) + SS-10 (TTP/RO/DM)
Power to other substation as below shall be distributed at 11KV voltage level taking plant
feeder from nearby substation listed in S.No.6 above.
All the 11KV HT loads in the unit shall be fed from 11KV air insulated switchboard provided
at the substation. The power shall further step down to 415V through in each of the
substation through 11KV/433V distribution transformers catering all the LT loads at 415V
level of all the units/buildings.
Each 11KV switchboards has two separate bus sections (each fed from separate 66KV
feeder & 66/11.5KV transformer) capable of feeding the complete load. Under normal
conditions, each bus section supplies power up to 50% load. However, in case of power
supply failure on one bus section of switchboard, the other bus section feeds to complete
load of the unit.
All 415V switchboards also have similar distribution philosophy, with 2 bus sections and
each bus section capable of feeding the complete load. Overall power distribution is as
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indicated in the Overall Key Single line diagram for the Project (drawing no. A545-999-16-
50-01000).
The above system describes normal power distribution for the plant. Additionally, the
emergency power supply system for the plant shall be designed to feed the following loads
Process loads (i.e. Loads critical for process & plant safety) Electrical loads essential
for the safe shutdown of the plant).
Equipment safety (i.e. Plant communication system, Fire detection & Alarm system,
Firefighting system excluding main fire water pump)
Control system (i.e. UPS systems)
Lighting (AC Emergency & DC critical lighting).
In case of complete power failure (i.e. no supply available from CPP), power for the required
emergency loads shall be made available from Emergency generator. The total emergency
load requirements for complete plant (including Process emergency loads, Equipment safety
loads, UPS loads & Lighting loads), following Emergency DG sets have been provided
1 no. 12MW DG located on CPP (for all emergency loads)
1 no. 5MW DG located near SS-19, for energising Trading facilities
1 no. 750KVA DG located in CPP for UB loads
1 no. 1000KVA DG for GTG black start (By GE)
1 no. 750KVA DG located near SS-19, for lighting loads of trading facility areas.
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SECTION-14
INSTRUMENTATION
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12 INSTRUMENTATION
Refer Section 4.0 – Operating Variable and Process Control. For instrumentation and process
control of major package equipment within CPP, refer respective vendor‟s operating manual
such as for GTG, HRSG, Utility Boiler, STG and Deaerator.
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SECTION-15
UNIT SAFEGUARDING SYSTEM
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13.1 General
None.
For Alarms and trip values refer the document annexed in annexure 18.20.
Also the u/s & d/s isolation valves for these PSV / PRV are oriented in such a way that their
stems are in a horizontal plane / position.
The fuel storage tanks and DM water/ condensate storage tanks are provided with PVRV as
safeguarding device.
The flare header valve at the unit B/L is a gear-operated valve installed in such a way that its
spindle is horizontal. The discharge of these PSV / PRV valves is free draining without any
liquid pockets. Also these valves are installed as close to the equipment as possible to protect it
against additional over-pressurization due to back-pressure.
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Isolation valves of the PSV / PRV (which is inline) are kept Locked open to ensure free path for
the relief discharge. The upstream isolation valve of the spare PSV is kept LC to isolate the
spare PSV / PRV, whereas downstream isolation valve is kept LO to ensure that there is no
pressurization in the PSV / PRV downstream line due to the passing upstream isolation valve.
For steam services PSVs / PRVs are not provided with any isolation valve.
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SECTION-16
TROUBLE SHOOTING
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14 TROUBLE SHOOTING
Refer Section 11.0 – General Equipment Operating Procedure for trouble shooting of
equipment. For trouble shooting of major package equipment within CPP, refer respective
vendor‟s operating manual such as for GTG, HRSG, Utility Boiler, STG and Deaerator.
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SECTION-17
CATALYST AND CHEMICALS
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15.1 Catalyst
Not Applicable.
15.2 Chemicals
In CPP BOP facilities, Morpholine and Oxygen Scavenger are used for pH correction and
dissolved oxygen removal respectively.
The information on estimated chemical quantity is annexed as Annexure 18.21. Also refer
MSDS in Annexure 18.4.
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SECTION-18
HEALTH, FIRE AND SAFETY
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16.1 General
Safety instructions for the refinery will also apply to the CPP unit, and general rules for
protection of personnel from moving machinery, electricity, hot equipment and from falling
should be observed.
Pipes and large equipment containing water, liquid hydrocarbon, steam and gas at high
temperature and pressure are installed in the plant. It is important to provide protection of
personnel from burns, where blowing out of such media can occur.
Special hazards pertaining to this plant include the risks of poisoning, fires and explosions
due to the materials handled. The fact that the plant is an open-air installation reduces the
effects of these risks, and any unnecessary housings or casings of the equipment must be
avoided. Use or storage of combustible materials at the site must be avoided.
Vents, drains and other small piping must be placed such that operators do not accidentally
hit, push, kick or slam against them.
In case of fire, water is normally used to keep the surroundings cool until the leak resulting in
the fire can be shut off. If the fire is extinguished before the supply is stopped, there is a risk
that an explosion hazard may be created.
Smoking is forbidden.
All sparks must be avoided where combustible gases may be present. Welding must be
performed with regard to the above.
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Morpholine
Morpholine is utilized in CPP for pH adjustment of DM water, polished condensate, pure
condensate and Boiler Feed Water.
Morpholine is a colorless liquid with fishlike odour. First aid measures on exposure are as
follows:
- After inhalation, remove the victim to fresh air and keep at rest in a position
comfortable for breathing. Immediately call for doctor/ physician.
- After skin contact, remove/ take off immediately all contaminated clothing. Rinse skin
with water/ shower and immediately call for doctor/ physician. Wash contaminated
clothing before reuse.
- After eye contact, rinse cautiously with water for several minutes. Remove contact
lenses, if present and easy to do. Continue rinsing and immediately call for doctor/
physician.
- After ingestion, rinse mouth. Do not induce vomiting. Immediately call for doctor/
physician.
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Persons handling morpholine shall be supplied with gloves, safety glasses and protective
clothing. Respiratory protection not required in normal conditions.
Persons handling oxygen scavenger chemical shall be supplied with gloves, safety glasses
and protective clothing. Respiratory protection not required in normal conditions. However
for nuisance exposures use respirator catridges.
Nitrogen
Nitrogen is non-toxic – 79% of the normal air we breathe is nitrogen. However, in vessels or
areas where there is a high concentration of nitrogen, there is a deficiency of oxygen
for breathing. Breathing an atmosphere deficient in oxygen will rapidly result in dizziness,
unconsciousness or death, depending on the time of exposure. Do not enter or even stick
your head into a vessel containing a high concentration of nitrogen and therefore deficient in
oxygen. Do not stand close to bleeders where nitrogen is being bled out of equipment at a
high rate, which might temporarily cause a deficiency in oxygen close to the bleeder.
Hydrocarbons
The light hydrocarbons that are u s e d i n C P P are only mildly toxic; however, they
present a great safety concern with respect to vapor cloud formation and fire/explosion if
allowed to escape from the process equipment. Avoid breathing the hydrocarbon vapors and
if the clothing becomes wet with hydrocarbons, immediately remove the clothing, wash the
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affected area and put on fresh clothing. Any leaks that are noted should be attended to
without delay including, if necessary, shutdown of the unit to accomplish the repair.
Catalyst
Not Applicable.
F&G network drawing of CPP unit is annexed as Annexure 18.12 for further reference.
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Foam System
For containing large Hydrocarbon fires, foam systems are useful. They have inherent
blanketing ability, heat resistance and security against burn back. Low expansion foam is used
for hydrocarbon oil fire. Foam can be applied over burning oil pool with the help of foam
tenders/foam delivery system.
Fire Signal
Break Glasses have been provided at strategic locations of unit to see fire alarm in fire station.
If a fire is sighted, glass of window should be smashed, causing fire alarm switch to actuate.
This is an emergency call & should be periodically tested for proper functioning.
Steam Smothering
LP Steam hose connections have been provided at every convenient point inside PAD. Steam
lances of standard 15M length can be fitted with these hose stations. Where ever hydrocarbon
leakage is detected which is likely to catch fire, Steam blanketing may be done. Apart from
diluting combustible Hydrocarbons, steam prevents atmospheric oxygen from taking part in
combustion & thus helps in extinguishing fire. However, steam should never be applied on large
pool of hydrocarbon fire. Direct application of steam on burning oil may result in spillage of
burning hydrocarbon & spread of fire. Similarly use of fire water on hot oil surfaces may cause
sputtering & spread of fire.
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Whenever a technical advisor must enter a vessel, a meeting should be arranged between
advisor and the plant personnel who will be involved. The meeting should include review of the
vessel entry procedures, the refiner‟s safety requirements and facilities, preparation of a vessel
entry schedule, assignment of responsibility for the preparation of a blind list, and assignment of
responsibility for the vessel entry permits.
The most common tasks of a technical advisor which could involve a potentially hazardous
vessel entry are:
Unit Checkout Prior to Start-up
Turnaround Inspections
The precautions apply equally to entry into all forms of vessels, including those enclosed areas,
which might not normally be considered vessels.
Examples include:
Knock out drums, Storage tanks, heaters, Sumps
The area around the vessel man ways should also be surveyed for possible sources of
dangerous gases, which might enter the vessel while the person is inside. Examples include
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acetylene cylinders for welding and process vent or drain connections in the same or adjoining
units. Any hazards found in the survey should be isolated or removed.
Vessel Access
Safe access must be provided both to the exterior and interior of the vessel to be entered. The
exterior access should be a solid, permanent ladder and platform or scaffolding strong enough
to support the people and equipment who will be involved in the work to be performed.
Access to the interior should also the strong and solid. Scaffolding is preferred when the vessel
is large enough to permit it to be sued. The scaffolding base should rest firmly on the bottom of
the vessel and be solidly encored. If the scaffolding is tall, the scaffolding should be supported
in several places to prevent sway. The platform boards should be sturdy and capable of
supporting several people and equipment at the same time and also be firmly fastened down.
Rungs should be provided on the scaffolding spaced at a comfortable distance for climbing on
the structure.
If scaffolding will not fit in the vessel a ladder can be used. A rigid ladder is always preferred
over a rope ladder and is essential to avoid fatigue during lengthy periods of work inside a
vessel. The bottom and top of the ladder should be solidly anchored. If additional support is
available, then the ladder should also be anchored at intermediate locations. When possible, a
solid support should pass through the ladder under a rung, thereby providing support for the
entire weight should the bottom support fail. Only one person at a time should be allowed on
the ladder.
When a rope ladder is used, the ropes should be thoroughly inspected prior to each new job.
All rungs should be tested for strength, whether they be made of metal or wood. Each rope
must be individually secured to an immovable support. If possible, a solid support should pass
through the ladder so that a rung can help support the weight and the bottom of the ladder
should be fastened to a support to prevent the ladder from swinging. As with the rigid ladder,
only one person should climb the ladder at a time.
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harness is preferred over a belt because it allows an unconscious person to be lifted from the
shoulders, making it easier to remove him from a tight place such as an internal man way.
A minimum of one harness for each person entering the vessel and at least one spare harness
for the people watching the man way should be provided at the vessel entry.
A communication system should be provided for the man way watch so that they can quickly
call for help in the event that the personnel inside of the vessel encounter difficulty. A radio,
telephone, or public address system is necessary for that purpose.
Fresh air can be circulated through the vessel suing an air mover, a fan, or, for the cases where
moisture is a concern, the vessel can be purged using dry certified instrument air from a hose
or hard piped connection. When an air mover is used, make certain that the gas driver uses
plant air, not nitrogen, and direct the exhaust of the driver out of the vessel to guarantee that
this gas does not enter the vessel. When instrument air is used, the technical adviser must
confirm that a check of the supply header is made to ensure that it is properly lined up and that
there are no connections where nitrogen can enter the system (nitrogen improperly used as a
backup for instrument air by some refiners). The fresh air purge should be continued throughout
the time that people are inside of the vessel. The responsible control room should be informed
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that instrument air is being used for breathing so that if a change to nitrogen is required the
people are removed from the affected vessel.
A minimum of one fresh air mask for each person entering the vessel and at least one spare
mask for the hole-watcher should be provided at the vessel entry. These masks should
completely cover the face, including the eyes, and have a second seal around the mouth and
nose. When use of the mask is required, it must first be donned outside of the vessel where it
is easy to render assistance in order to confirm that the air supply is safe. Each mask must
have a backup air supply that is completely independent of the main supply. It must also be
independent of electrical power. This supply is typically a small, certified cylinder fastened to
the safety harness and connected to the main supply line via a special regulator that activates
when the air pressure to the mask drops below normal. The auxiliary supply should have an
alarm, which alerts the user that he is on backup supply and it should be sufficiently large to
give the user 5 minutes to escape from danger.
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The primary objective of the breathing air system is to supply and distribute “breathing quality”
air which should be as per Grade D described in the ANSI/Compressed Gas Association
Commodity Specification for Air, G-7.1-1989 and adopted by OSHA.
The compressed breathing air shall enable personnel wearing respirators to enter and work in
contaminated or potentially contaminated areas of the unit. Breathing air is also used by
workers wearing respirators when entering enclosed work locations having inadequate
ventilation.
In Dangote Refinery, the breathing air required, is taken from Compressed Air system (Sourced
from common air compressor for Air & N2 system). However, a separate network has been
considered in the whole complex through dedicated prioritized header for supplying breathing
air to various units.
Workers may be exposed to the chemical during solution preparation, routine monitoring in and
around the area or during routine sampling or if leaks or spills occur during routine solution
processing and disposal. Exposure danger occurs principally through the skin and eyes if
protective clothing is not worn. Exposure by inhalation may occur if mist or vapors are
generated. Exposure by ingestion, while possible, is less likely.
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damage on exposure. Repeated exposure to this material can result in absorption through skin
causing significant health hazard. Swallowing a small quantity of this material will result in
serious health hazard.
The American Conference of Governmental Industrial Hygienists (ACGIH) has established the
following exposure limits:
• For Morpholine (TWA): 70 mg/m3 (20 ppm)
First Aid:
Refer section 16.2.
Workers may be exposed to the chemical during solution preparation, routine monitoring in and
around the area or during routine sampling or if leaks or spills occur during routine solution
processing and disposal. Exposure danger occurs principally through the skin and eyes if
protective clothing is not worn. Exposure by inhalation may occur if mist or vapors are
generated. Exposure by ingestion, while possible, is less likely.
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First Aid:
Refer section 16.2.
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SECTION-17
LABORATORY SAMPLING
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17 LABORATORY SAMPLING
17.1 General
The ultimate objective of the CPP is to produce power and steam as well as BFW supply to
various consumers in refinery. Steam & BFW supply to refinery has to be of specific quality/
acceptable limits. In addition, various streams that are received at CPP battery limit such as
fuels, DM water, polished condensate and pure condensate are to be checked and ensured
of their quality. This is required to identify the source of upset of steam quality as well as to
ensure the suitability of material of equipment and piping within CPP. To accomplish this
objective, it becomes necessary to characterize the important physical and chemical
properties of the various refinery streams utilizing specific laboratory analytical testing
procedures. Thus, satisfactory refinery operation depends largely upon proper analytical
procedures for quality control. An analytical quality control program requires five steps as
outlined.
A. Procedure
Sampling
The initial objective must be to obtain a characteristic sample of a particular stream.
Depending upon the properties of a stream in question, sampling technique varies. Various
types of sampling methods are detailed in P&ID of CPP unit. The refinery operation should
be steady and free from fluctuations during sampling. The sample point should be well
purged to eliminate aged material, water, dirt, etc., and to assure withdrawal of a sample
representative of the material flowing in the pipe. The sample container must be adequate
for the analysis to be obtained.
Sample Preservation
Once a proper sample has been obtained, it must, if possible, be preserved intact until it can
be analysed. This requires the prevention of any physical or chemical changes in the
sample. Changes, particularly chemical, can occur as a result of many factors. Some of the
most perplexing changes have later been traced to influences of the sampling equipment
and container. Often a sample may be inherently unstable, requiring immediate analysis.
Others can be stabilized by the addition of a passivating compound or preservative. Some
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Analysis
Follow the analytical method PRECISELY. Each method represents the end result of many
hours of study, testing, and experience. The methods often note appropriate precautions
indicating potential problems to be avoided. Laboratory apparatus and equipment must be
properly calibrated and rechecked frequently.
Error
There are two terms with which one may qualify an analytical result – precision and
accuracy. Precision refers to the dispersion, or spread, of results. One must consider both
repeatability (duplicate results by the same analyst) and reproducibility (duplicate results by
different analysts) of results in order to determine the permissible tolerance in each
specification. A high degree of precision usually requires minimizing the random
experimental error during development of the method. Accuracy refers to the deviation
between a reported analytical result and the true value. It is accuracy that can be the most
damaging since it is normally the result of systematic error. If any of the above procedures
have been compromised, the effect is always seen in the accuracy of the value reported.
Significance
The significance or interpretation of the result obtained is the final step in any analytical
procedure. Misinterpretation of the result would render the whole procedure useless.
Therefore this step is the most important. Often several analyses measuring different
properties may be related to a common characteristic (physical or chemical). Proper
analytical procedure should lead to supporting rather than conflicting conclusions. In
attaching appropriate significance to the analysis, one must consider and relate all of the
previous steps of the analytical procedure to the operation of the process unit. A firm
understanding of the process and its capabilities is essential. From a thorough application of
these five steps, the necessary changes in operation may be implemented in order to reach
the ultimate objective of meeting the necessary product specification.
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For the sampling methods and schedules of steam and water analysis of Utility Boilers and
HRSGs, refer operating manual of respective equipment supplier.
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SECTION-18
LIST OF ANNEXURES
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18 LIST OF ANNEXURES
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