IS 5513 : 1996

Indian Standard VICAT APPARATUS - SPECIFICATION (Second Revision)

ICS 91.100.10

8 BIS 1996

BUREAU
MANAK

OF

INDIAN
9 BAHADUR

STANDARDS
SHAH ZAFAR MARG

BHAVAN,

NEW DELHI 110002 May 1996

Price Group 3

Cement and Concrete Sectional Committee,CED 2

FOREWORD This Indian Standard ( Second Revision ) was adopted by the Bureau of Indian Standards, after the draft finalized by the Cement and Concrete Sectional Committeehad been approved by the Civil Engineering Division Council. A series of standards have been formulated on different types of cement and methods of tests of cement. As it is recognized that reliable and reproducible test results could be obtained only with standard types of testing equipment which are capable of giving the desired level of accuracy, a series of specifications covering the requirements of testing equipment have been brought out to encourage the development and manufacture of standard testing equipment for cement testing in the country. This standard was first brought out in 1969 and subsequently revised in 1976. The present revision has been taken up to incorporate the moditkations found necessary in order to align this standard with EN 196-3 : 1987 Methods of testing cement : Determination of setting time and soundness. The major changes include modifications in the dimensions of the mould and permitting the use of additional materials for making the vicat mould, including stainless steel, hard rubber and plastic, which have high strength and rigidity and are non-corroding and non-absorbent. In this revision the use of square needle for determining initial setting time of cement has been deleted. This revision also makes reference to the latest version of referred standard. The composition of the Committee responsible for the formulation of this standard is given at Annex A. For the purpose of deciding whether a particular reuirement of this standard is complied with, the final value, observed or calculated, expressing the result of test or analysis shall be rounded off in accordance with IS 2 : 1960 Rules for rounding off numerical values ( revised). The number of significant places retained in the rounded off value should be the same as that of the specified value in this standard.

IS 5513: 1996

Indian Standard VICAT APPARATUS SPECIFICATION (Second Revision)

1 SCOPE This standard covers the requirements of the Vicat apparatus used for determination of consistency of standard cement paste and initial and final setting times of cement. 2 REFERENCES 2.1 The following Indian Standards are necessary adjuncts to this standard: IS No. 210 : 1978 292 : 1983 4170 : 1967 6911: 1972 9962 : 1981 3 MATERIALS The materials of construction of different component parts of Vicat apparatus shall be as given in co1 2 of Table 1. Recommended Indian Standards for different materials, where available, are given in co1 5 of Table 1. 4 DIMENSIONS Dimensions of different component parts of Vicat apparatus shall be as detailed in Fig. 1 and 2 (see pages 3 and 4). Where tolerances are not specifically mentioned in the relevantclauses, dimensions shall be considered nominal. 5 CONSTRUCTION 5.1 General The Vicat apparatus shall consist of a frame D having a movable rod B with a platform A at one end and the following which can be attached at the other end: .
Title

of clamping screw as indicated in Fig. 1. Their movement shall be truely vertical and without appreciable friction, and their axis shall coincide with that of the needle or plunger. 5.2 Needles The needles C and F shall be of hardened and tempered steel. Their hilts (fitting ends) shall be of brass. 5.2.1 There shall be about 6 mm clearance between the bottom end of the needle, when it is raised, and the top edge of the ring mould, to enable the mould to be located in position without damage to the needle. 5.2.2 Dimensions of Needles
Needle C shall be round of diameter 1.13 f 0.05 mm. The

Gray iron casting ( third revision ) Leaded brass ingots and castings ( second revision ) Brass rods for general engineering purposes Stainless steel plate, sheet and strip Steel wires for needles

needle shall have a flat end. The effective length, excluding the hilt shall be 50 f 1 mm (see Fig. 1). 5.2.2.1 Needle F shall be of the same section as needle C but shall be 30 f 1 mm in length, excluding the hilt, and fitted with a brass attachment hollowed out so as to leave a circular cutting edge 5 * 0.1 mm in diameter. The depth hollowed out shall be 0.5 f 0.1 mm. A 0.75 mm diameter vent hole shall be provided as shown. The needle shallproject 0.5 f 0.1 mmbeyond the cutting edge (see Fig. 1). 5.3 Plunger Plunger G shall be of polished brass 10 f 0.05 mm in diameter with a projection at the fitting end for insertion into the movable rod B. The lower edge shall be flat. Its length shall be 50 -+1 mm (see Fig. 1). 5.4 Movable Rod Movable rod B shall carry an indicator which moves over a graduated scale attached to the frame D. A clearance of 0.25 mm around the movable rod is recommended to facilitate free movement. A suitable arrangement shall be provided to secure the movable rod in rest position when the apparatus is not in use ( see Fig. 1). 5.5 Graduated Scale Graduated scale shall be 40 mm in length and the smallest division of the scale shall be 1 mm (see Fig. 1). 5.6 Vicat Mould The Vicat mould shall be of truncated conical form with an internal diameter of 70 f 5 mm at the top, 80 f 5 mm at the bottom and a height 40 f 0.2 mm. The mould shall be adequately rigid and shall have a minimum wall thickness of 4 mm. A non-porous g&S or StainkSS Steel base plate shall be provided. A plate of glass or 1

4 Needle C for determining the initial setting time, b) Needle Ffor determining the final setting time,
and d Plunger G for determining consistency. the standard

5.1.1 The needles C, Fand plunger G-shall be capable of being fixed centrally into the movable rod B by means

IS 5513:

1996

stainless steel of at least 2.5 mm thickness is suitable.

NOTE - Split type Vicat mould may also be used as an alternative to single piece mould. The split type Vmat mould (see Fig. 2) shall consist of a split ring E, having an internal diameter 80.0 + 0.1 mm and a height of 40.0 + 0.2 mm. A non-porous base plate as given in 5.6 shall be provided. The split mould shall also be provided with a suitable clamping ring as shown in Fig. 2. The width and thickness of clamping ring shall be 8 to 10 mm. To ensure interchangeability of the clamping rings, the external diameter at the-base of the split mould shall be 89.0 f 0.1 mm with a taper of 2 on the side from base to top edge. Total taper shall be 4 inwards from base to top. The Inside surface ofthe clamping ring shall similarly be tapered. When assembled, this ring shall be clear above the base of the split mould, by a distance ot 15 to 18 mm.

5.7 Mass The total mass of the moving unit, when in use, complete with all attachments, that is, the cap and rod together with either needle C or needle For plunger G, shall be 300 + 1 g. 5.7.1 Needle C, needle F and plunger G shall each weigh 9 f 0.5 g. 6MARKlNG The following information shall be clearly and indelibly marked on the Vicat apparatus in such a manner that it does not interfere with the performance of the

Table 1 Materials of Construction for Different Parts of VicatApparatus ( Clause 3 )

Sl No. (1) i) ii) iii) iv) Part Material Special Requirement, if any (4) Smooth Smooth surface surface IS 210 IS 4170 IS 292 Recommended Indian Standard, if any (5)

(2) Frame D Cast iron Movable Cap A Needte C ( for initial setting time ) : a) Hilt portion b) Needle portion Brass Hardened rod B

(3) Cast iron Brass Brass

: 1978 : 1967 : 1983

steel

Smooth surface Polished surface

IS 9962

: 1981

v)

Needle F ( for final setting time ) : a) Hilt portion b) Needle portion Brass Hardened Smooth surface Polished surface

steel

IS 9962

: 1981

vi)

Plunger G consistency Non-porous

( for normal ) plate

Brass

Polished

surface

IS 4170

: 1967

vii)

Glass or stainless steel

Smooth

surface

-. IS 6911 1972

viii)

Mould E, Mould E, and clamping ring

High strength, rigid, non-corroding and non-absorbent materials such as brass, stamless steel, hard rubber, plastic, etc. Brass plate

Smooth

internal

fimsh

IS 292 : 1983 ( In case of brass )

ix)

Graduated Indicator movable The Roman

scale attached rod to the

IS 292 IS 292

: 1983 : 1983

x)
NOTl:

Brass

capital

letters succeeding

the names of parts in co1 2 correspond

to those indicated

in Fig. 1 and 2

I I

/-RELEASE

PIN

I
FRONT VIEW

NON-POROUS PLATE

PLUNGER

G
40.0+0-2 I

32.5

) 9 BOt5

SIDE

VIEW

All dimensions

in millimetres.
(

FIG. 1 VICAT APPARATUS

Continued )

IS 5513 : 1996

Enlarged View of Needle F

All dimensions
FIG.

in millimetres.

1 VICATAPPARATUS Concluded (

) MABKING

apparatus: a) Indication of the source of manufacture,

7 BIS CERTIFICATION

The product may also be marked with Standard Mark.

7.1 The use of Standard Mark is governed by the provisions of the Bureau ofIndian StandardsAct, 1986 and the Rules and Regulations made thereunder. The details of conditions under which the licence for the use of Standard Mark may be granted to manufacturers and uroducers may be obtained from the Bureau of Indian Standards.

b) Date of manufacture, c) Serial number/Batch d) Type of mould. number, and

E, CLAMPING RING--CI

p--fI

40.0 -+ 0.2

(WIDTH &THICKNESS 8 TO 13mm) SPLIT MOULD -/

I
*

: I , I /
89.0f O-1 BASE PLATE

All dimensions

in millimetres.

FIG. 2 SPLIT TYPE VICAT MOULD

IS

5513:

1996

ANNEXA (Foreword )
COVE COMPOSlTION Cement and Concrete Sectional Committee, CED 2
Chainnan
DR H. C. VISVESVARYA

Representing In personal capacity ( Universily

of

Roorkee, Roorkee 247 667 )

Members Orissa Cement Limited. New Delhi SHRI H. BHA~ACHARYA B.G. Shirke & Co, Pune SHRIG. R. BHARTIKAR The Associated Cement Companies Ltd. Mumbai DR A. K. CHATTERJEE SHRI S. H. SUBRAMANIAN Alternate ) ( Central Public Works Department, New Delhi CHIEF ENGINEER( DESIGN ) SUPERINTENDING ENGINEER S&S ) ( Alternate ) ( Sardar Sarovar Narmade Nigam Ltd. Gandhinagar CHIEF ENGINEER,NAVACAM DAM SUPERINTENDING ENGINEER, QCC ( Alternate ) Irrigation and Power Research Institute. Amritsar CHIEF ENGINEER,RESEARCH-CUM-DIRECTOR RESEARCHOFFICER,CONCRETETECHNOLOGYAlternate ) ( A, P Engineering Research Laboratories, Hyderabad DIRECTOR JOINT DIRECTOR Alternate ) ( Central Water Commission, New Delhi DIRECTOR (CMDD) ( N&W ) DEPUTY DIRECTOR CMDD ) ( NW&S ) ( Alternate ) ( Hyderabad Industries Ltd, Hyderabad SHRIK. H. GANCWAL SHRJV. PATTABHJ (Alternate ) Structural Engineering Research Centre (CSIR), Ghaziabad SHRIV. K. GHANEKAR SHRJ GOPINATH S. The India Cements Ltd, Madras SHRI R. TAMILAKARAN Alternate ) ( Gannon Dunkerley and Co Ltd. Mumbai SHRIS. K. GUHA THAKURTA SHRI S. P. SANKARANARAYANANAlternate ) ( Central Building Research Institute (CSIR ). Roorkee SHRIN. S. BHAL DR IRSHADMASOOD( Alternate ) Cement Corporation of India, New Delhi SHRIN. C. JAIN Research, Designs and Standards Organization~( Ministry of Railways ), JOINT DIRECTOR STANDARDS B&S ) ( CB-I ) ( Lucknow
JOINTDIRECTOR STANDARDS B&S ) ( CB-II ) ( Alternate ) ( Indian Hume Pipes Co Ltd. Munibai SHRIN. G. JOSHI SHRIP. D. KELKAR Alfemafe ) ( National Test House, Calcutta SHRI D. K. KANUNGO SHRIB. R. MEENA(Alternate ) Larsen and Toubro Limited, Mumbai SHRI P. KRISHNAMIJRTHY SHRI S. CHAKRAVARTHYAlternate ) ( Structural Engineering Research Centre ( CSIR ), Madras DR A. G. MADHAVARAO SHRI K. MANI ( Alternate ) Hospital Services Consultancy Corporation ( India ) Ltd, New Delhi SHRI G. K. MAJUMDAR SHRIJ. SARUP(Alternate ) Ministry of Transport, Department of Surface Transport (Roads Wing), SHRI PRAFULLA KUMAR New Delhi SHRI P. P. NAIR ( Alternate ) Central Board of Irrigation and Power, New Delhi MEMBERSECRETARY DIRECTOR CIVIL ) ( Alternate ) ( Engineer-in-Chiefs Branch, Army Headquarters, New Delhi SHRIS. K. NATHANI,SO I DR A. S. GOEL, EE (Alternate ) Central Road Research Institute ( CSIR ), New Delhi SHRIY. R. PHULL SHRI S. S. SEEHRA (Alternate ) Indian Roads Congress, New Delhi SHRIY. R. PHULL SHRIA. K. SHARMA( Alternate ) National Council for Cement and Building Materials, New Delhi DR C. RAJKUMAR DR S. .C. AHLUWALIA Alfemate ) ( Directorate General of Supplies and Disposals, New Delhi SHRIG. RAMDAS SHRIR. C. SHARMA (Alternate )

( Continued on page 6 )

IS 5513 : 1996
( Continued ji-om page 5 )

Members SHRI A. REDU S.

REPRESENTATIVE SHRI J.

Representing Gammon India Ltd, Mutiai Builders Association of India, Mumbai Geological Survey of India, Calcutta ) Central Soil and Materials Research Station, New Delhi Alternate ) Public Works Department, Government of Tamil Nadu, Madras (Alternate) Hindustan Prefab Ltd, New Delhi The Institution of Engineers ( India ), Calcutta )
Director General, BIS ( Ex-oficio

S.

SANGANEWA

SHRI L.

N.

AGARWAL (Alternate

SHRI S. B. SURI SHR~N. CHANDRASEKARAN ( SUPERINTENDING ENGINEER( DESIGN ) E~ECU-IWEENGINEER( S. M. R. DWISION )

SHRI K. CHADHA A. SHR~J. R. SIL (Alternate )

DR H. C. VISVESVARAYA SHRI D. C. CHATURVEDI (Alternate SHRI VINOD KUMAR. Director ( Civ Engg )

Member )

.Uernbrr Secretory SHRI J. K. PR-\s.-\D Joint Director (Civ Engg). BIS

Instruments for Cement nnd Concrete Testing Subcommittee, CED 2 : 10

Convener DR A. K. CHA~ERJEE ,Uembers SHRI P. RAY CHAUDHURI SHRI S. S. SEEHRA(.4ltemate SHRI HARIIT SINGH ( DIRECTOR JOW DIRECTOR(

The Associated Cement Companies Ltd. Mumbai

Central Road Research Institute, New Delhi ) A. P. Engineering Research Laboratories, Hyderabad .4ltemote )

Alternate ) Public Works Department, Uttar Pradesh Central Public Works Department, New Delhi All India Instrument Manufacturers and Dealers Association, Mumbai Associated Instruments Manufacturers (I) Pvt L&and Advisory Committee for Standardization of Instruments ( ACSI ), New Delhi ) Hydraulic Engineering Instruments, (Alternate) National Council for Cement and Building Materials, New Delhi National Test House, Calcutta Alternate ) Central Building Research Institute, Roorkee National Physical Laboratory, New Delhi Associated Cement Companies Ltd, Mumbai New Delhi Aitemate ) D ) - V Alternate )

DIRECIUR RESEARCH INS~F DR T. N. CHOJER(

Ex~cu-nv~

ENGINEER (

SHRI H. K. GUHA DEPWY SECRETARY( SHRI S. C. JAIN SHRI S. S. MATHARU (Alternote SHRI JATINDER SINGH SHRI GURBATCHANS~NGH DR ( SHRIMATI) S. LAXMI SHRI K. H. BABU ( SHRI B. ~HRI

Alternate )

R.

MEENA CHHANDA

SHRI B. MANDAL (

J. N.

SHRI S. SHRI B.

P.

TEHRI (Alternate)

DR V. MOHAN

V. B.

PAI

DR D. GHOSH (

Alternate ) Research and Development Organization, Ministry of Defence, Pune

SHaI Y. P.

PATHAK

SHRI M.

V. S.

MURTHY (Alternate)

PROF C. K. RAMESH REPRESENTATIVE SHRI C. SANKARAN PROF S. N. SINHA

Indian Institute of Technology, Mumbai Department of Science and Technology, New Delhi Highways Research Station, Pune Indian Institute of Technology, New Delhi

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Amendments Amend No.

Issued Since Publication Date of Issue Text Affected

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