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    U5 Org q5

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    Mohamed Muhajireen
    (1) A student determines the change in oxidation number of nitrogen when a solution of magnesium nitrate is titrated with titanium(III) chloride. (2) The student prepares a solution of magnesium nitrate and titrates it with a solution of titanium(III) chloride, observing a color change in an indicator from green to yellow at the endpoint. (3) By calculating the moles of titanium(III) chloride used at the endpoint, the student determines that the final oxidation state of nitrogen in the reaction is +5.

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    U5 Org q5

    Uploaded by

    Mohamed Muhajireen
    46 views2 pages
    (1) A student determines the change in oxidation number of nitrogen when a solution of magnesium nitrate is titrated with titanium(III) chloride. (2) The student prepares a solution of magnesium nitrate and titrates it with a solution of titanium(III) chloride, observing a color change in an indicator from green to yellow at the endpoint. (3) By calculating the moles of titanium(III) chloride used at the endpoint, the student determines that the final oxidation state of nitrogen in the reaction is +5.

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    (1) A student determines the change in oxidation number of nitrogen when a solution of magnesium nitrate is titrated with titanium(III) chloride. (2) The student prepares a solution of magnesium nitrate and titrates it with a solution of titanium(III) chloride, observing a color change in an indicator from green to yellow at the endpoint. (3) By calculating the moles of titanium(III) chloride used at the endpoint, the student determines that the final oxidation state of nitrogen in the reaction is +5.

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    © All Rights Reserved
    Download as PDF, TXT or read online from Scribd
    Download as pdf or txt
    46 views2 pages

    U5 Org q5

    Uploaded by

    Mohamed Muhajireen
    (1) A student determines the change in oxidation number of nitrogen when a solution of magnesium nitrate is titrated with titanium(III) chloride. (2) The student prepares a solution of magnesium nitrate and titrates it with a solution of titanium(III) chloride, observing a color change in an indicator from green to yellow at the endpoint. (3) By calculating the moles of titanium(III) chloride used at the endpoint, the student determines that the final oxidation state of nitrogen in the reaction is +5.

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    © All Rights Reserved
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    of 2

    (c)

    A student determines the change in oxidation number of nitrogen when


    a solution of magnesium nitrate, Mg(NO3)2 , is titrated with aqueous
    titanium(III) chloride.
    Procedure
    Step 1 Using a volumetric flask, prepare 100.0 cm3 of an aqueous solution
    containing 0.750 g of solid Mg(NO3)2∙6H2O.
    Step 2 Pipette 10.0  cm3 of the solution from Step 1 into a conical flask and
    add a few drops of alizarin indicator.
    Add 2 cm3 of concentrated hydrochloric acid and heat the mixture.
    Step 3 Fill a burette with 0.0850 mol dm–3 aqueous titanium(III) chloride and
    titrate the contents of the conical flask from Step 2 while continuing to
    heat the mixture.
    During the titration, Ti3+ ions are oxidised to TiO2+ ions

    Ti3+ + H2O → TiO2+ + 2H+ + e–

    Alizarin indicator is green in the presence of aqueous Ti3+ and yellow in the
    presence of aqueous TiO2+.
    The end‑point of the titration is reached on the addition of 20.70 cm3 of aqueous
    titanium(III) chloride.
    (i) State the colour change that would be observed at the end‑point of
    the titration.
    (1)

    From . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ....................................... to ............................................................................................ . .

    20
    *P67131A02032* 

    (ii) Use the results to determine the final oxidation state of nitrogen in
    the titration.
    You must show your working.
    [Mr value: Mg(NO3)2∙6H2O = 256.3]
    (5)

    21
     *P67131A02132* Turn over

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