SAE 121-1999 去氫脆
SAE 121-1999 去氫脆
SAE 121-1999 去氫脆
Foreword—The changes to this document were made to comply with the new SAE Technical Standards Board
format. They include making Definitions Section 3. AH other section numbers have changed. Also Figure 2,
measurement was changed from 0.0006 in to 0.005 in. This is the correct measurement.
1. Scope—This SAE Recommended Practice covers methods for measuring, classifying, and specifying
decarburization in the threaded section of hardened and tempered steel bolts, screws, studs, and similar
parts. It is not intended to cover products which are specifically carburized to achieve special properties.
2. References
2.1 Applicable Publications—The following publications form a part of this specification to the extent specified
herein. Unless otherwise indicated, the latest issue of SAE publications shall apply.
2.1.1 SAE PUBLICATION—Available from SAE, 400 Commonwealth Drive, Warrendale, PA 15096-0001.
3. Definitions—According to SAE J419, "decarburization" is the loss of carbon at the surface of commercial
ferrous materiais which have been heated to facilitate fabrication or heated to modify mechanical properties.
SAE J419 defines also "complete decarburization," "partial decarburization," and "effective decarburization,"
as related to unhardened steels. This document extends these definitions, as follows, to cover more
specifically hardened and tempered steel bolts, screws, studs, and similar products.
3.1 Partial Decarburization—Decarburization with loss of carbon sufficient to cause a lighter shade of tempered
martensite than that of the immediately adjacent base metal, when examined metallographically by the
method outlined in 5.1, but insufficient carbon loss to show clearly defined ferrite grains. (The hardness
traverse method, outlined in 5.2, is the referee method for determining that partial decarburization is not
present at a point below that shown in Figure 1 for each classification.
3.2 Gross Decarburization—Decarburization with sufficient carbon loss to show only clearly-defined ferrite
grains under metallographic examination by the method outlined in 5.1. This is sometimes called "Complete
Decarburization."
SAE Technical Standards Board Rules provide that: "This report is published by SAE to advance the state of technical and engineering sciences. The use of this report is entirely
voluntary, and its applicability and suitability for any particular use, including any patent infringement arising therefrom, is the sole responsibility of the user."
SAE reviews each technical report at least every five years at which time it may be reaffirmed, revised, or cancelled. SAE invites your written comments and suggestions.
- GROSS DECARBURIZATION
(Sometimes Called Complete
Decarburization)
PARTIAL DECARBURIZATION
Decarburization Decarburization
Class C Class B
(1/2 H) 2 (2/3 H) 2
N N G4
Threads Thread
Per Height
in H1 min m in max
3.3 Carbon Restoration—A process of restoring surface-carbon loss by heat-treating in an atmosphere furnace
of properly controlled carbon potential. (This process is permitted but not recommended for threaded
fasteners unless furnace atmosphere is adequately controlled.)
3.4 Carburization—A darker shade of tempered martensite than that of the immediately adjacent base metal,
when examined metallographically by the method outlined in 5.1, and harder by at least 30 points (Knoop or
Vickers DPH) than the hardness at root diameter when checked by the method outlined in 5.2. (The limits
established by this document exclude this condition.)
3.5 Base-Metal Hardness—For purposes of this document, hardness at root diameter on a line bisecting the
included angle of the thread (Position 1 in Figure 2) is considered "base-metal hardness."
0.005 in
N*
ROOT DIAMETER
2
*See Figure 1
NOTE—This document recognizes that the surface may vary in carbon content from the base-metal carbon
content, and stipulates that this variation shall be either "paltal decarburization" or "gross
decarburization" or a "carbon-restored surface" to the extent allowed in Figure 1 for the different
classes. "Carburization" is not permitted in the surface zone.
5. Methods for Measuring Decarburization—Two methods for measuring decarburization are provided. The
microscopic method is intended primarily for routine inspection purposes. The hardness method is intended
primarily for referee purposes. In the case of gross decarburization, however, only the microscopic method is
applicable.
5.1.1 SPECIMENS—Use longitudinal sections taken through the thread axis of the bolt, screw, or stud, after all heat-
treating operations have been performed on the product. If specimens are prepared from surface-coated
fasteners, care should be used when interpreting the substrate-coating interface.
5.1.2 PREPARATION
a. Mount specimen for grinding and polishing. Protection from rounding the surface to be examined is
essential. The specimen should be mounted in a clamp or in a plastic mount, the latter being the
preferred method.
b. After mounting, grind and polish the surface in accordance with good metallographic practice.
c. Etching in a 3% nital (concentrated nitric acid) or picral (saturated picric acid) is usually suitable for
showing changes in microstructure caused by decarburization.
5.1.3 MEASUREMENT—Unless otherwise agreed on between purchaser and producer, examine at 100X
magnification. Compare with Figure 1 and definitions in 3.1, 3.2, and 3.3.
If the microscope is of a type with a ground glass screen, the extent of decarburization can be measured
directly with a scale. If an eye-piece is used for measurement, it should be an appropriate type containing a
cross hair or a scale.
5.2.2 Determine hardness at three positions, as shown in Figure 2, using a Knoop indenter with a 500 g load or
Vickers DPH with 300 g load.
a. A decrease of more than 30 hardness points from Position 1 to Position 2 indicates that the part does
not conform to the classification specified.
b. An increase of more than 30 points between Position 1 and Position 3 is regarded as "carburization,"
and indicates that part does not conform to the classification specified.
6. Notes
6.1 Marginal Indicia—The change bar (I) located in the left margin is for the conveniente of the user in locating
areas where technical revisions have been made to the previous issue of the report. An (R) symbol to the left
of the document title indicates a complete revision of the report.
Rationale—Figure 2 was changed to read 0.005 in instead of 0.0006 in. Also the Definition Section was
changed to Section 3 to comply with the new SAE Technical Standards Board format. All other section
numbers have changed.
Relationship of SAE Standard to ISO Standard—SAE Standard is similar, but not identical to 150 898-
1:1988.
Application—This SAE Recommended Practice covers methods of measuring, classifying, and specifying
decarburization in the threaded section of hardened and tempered steel bolts, screws, studs, and similar
parts. It is not intended to cover products which are specifically carburized to achieve special properties.
Reference Section